CN110897987B - Composition for resisting wrinkles and tightening skin and application of composition in cosmetics - Google Patents

Composition for resisting wrinkles and tightening skin and application of composition in cosmetics Download PDF

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CN110897987B
CN110897987B CN201911300094.3A CN201911300094A CN110897987B CN 110897987 B CN110897987 B CN 110897987B CN 201911300094 A CN201911300094 A CN 201911300094A CN 110897987 B CN110897987 B CN 110897987B
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mixture
wrinkle
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CN110897987A (en
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朱昭辉
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Guangzhou Xiran Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a composition for resisting wrinkles and tightening skin and application of the composition in cosmetics. The main effective components comprise the following components: the composition of the glass chicory seed oil, the betaine, the snail secretion, the schizosaccharomyces cerevisiae fermentation product lysate, the hypecoum vulgare extract, the oligopeptide-1, the xanthan gum, the tocopherol acetate, the fullerene, the triethanolamine and the anti-wrinkle and skin-tightening has better anti-wrinkle and skin-tightening effects, has the effects of whitening, anti-aging and moisturizing, is easy to be absorbed by the skin, can be applied to cosmetics, and has a simple and easy preparation method.

Description

Composition for resisting wrinkles and tightening skin and application of composition in cosmetics
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a composition for resisting wrinkles and tightening skin and application of the composition in cosmetics.
Background
With the continuous improvement of mental civilization and material living standards of people, the cosmetic industry for beautifying the life of people is rapidly developed. In particular, cosmetics for moisturizing, anti-aging, whitening and removing freckles are increasingly popular with consumers as the mainstream of a plurality of beauty and skin care products in recent years.
However, while meeting market needs, these cosmetics have increasingly marked negative impact on consumer groups. The process of carrying out moisture exchange on the skin of the moisturizing skin care product only needs a short time, the moisture can volatilize quickly, and the moisture on the surface of the skin volatilizes and can take away the moisture in the skin, so that the skin is drier. In addition, some substances in the skin care product which are not absorbed by the skin can be remained on the surface of the skin after the moisture is volatilized, so that bacteria are easy to breed, and small inflammation of hair follicles is formed. Skin care products for resisting wrinkles, whitening, resisting aging and the like are generally added with some functional components to achieve the purpose, but not all the functional components are suitable for various people to use, the phenomena of acne or allergy caused by overnutrition due to poor absorption can occur when the functional components are selected improperly, and the phenomena of skin injury or poor effect and the like can also occur when the functional components are improperly used. Secondly, most of the existing skin care products have single function, and to achieve better effect, various skin care products need to be bought, so that the consumption cost is increased, and the requirements of consumers cannot be well met.
Chinese patent application CN105147591A discloses an anti-wrinkle cream and a preparation method thereof, the anti-wrinkle cream comprises butylene glycol, ethylhexyl palmitate, caprylic/capric triglyceride, glycerol, polyglycerol-10, ethylhexyl isononanoate, polymethyl methacrylate, polydimethylsiloxane, steareth-21, cetostearyl alcohol, steareth-2, acrylic acid (ester)/acrylamide copolymer, betaine, shea butter, lactobacillus/pomegranate fruit fermentation product extract, chlamydomonas arctica essence, starfish essence, ginseng extract, ganoderma lucidum extract, apple extract, tocopherol acetate, and the like. Has a certain anti-wrinkle effect, but further improvement in whitening is required.
Chinese patent application CN105168065A discloses a multi-effect whitening and freckle-removing essence cream and a preparation method thereof, and the raw materials comprise: 2-3 parts of konjac glucomannan, 1.5-2 parts of laminine, 20-25 parts of isopropyl myristate, 2-2.5 parts of poly dimethyl diallyl ammonium chloride, 1-1.2 parts of ethyl maltol, 10-12 parts of horse oil, 15-18 parts of polydimethylsiloxane, 8-10 parts of walnut oil, 2-2.5 parts of a phyllostachys praecox extract and 1-1.2 parts of a sansevieria trifasciata extract. The multi-effect whitening and freckle-removing essence cream contains multiple nutrient elements, all the nutrient elements are matched, and the cream is prepared by a special process, so that the synergistic effect is remarkable, and the cream has good whitening and freckle-removing effects; especially, the whitening and especially spot removing effects are very remarkable when plant extract components such as the Phyllostachys nigra extract, the sansevieria trifasciata extract and the like are added, but the moisturizing and anti-wrinkle effects of the whitening and especially spot removing effects are to be improved.
Therefore, the research can reduce the complexity of the process on one hand, and on the other hand, the skin care product which has multiple effects on the premise of lower cost and is suitable for various crowds has important significance for consumers.
Disclosure of Invention
In order to overcome the technical problems, the invention provides the anti-wrinkle firming skin composition which has better anti-wrinkle firming effect, simultaneously has the effects of whitening, anti-aging and moisturizing, and is easy to be absorbed by skin; the preparation method of the composition for resisting wrinkles and tightening skin is simple and easy.
In order to achieve the above purpose, the technical scheme provided by the invention is as follows:
a composition for resisting wrinkles and tightening skin comprises the following components:
glass chicory seed oil, betaine, snail secretion, schizosaccharomyces cerevisiae fermentation product lysate, hypecoum vulgare extract, oligopeptide-1, xanthan gum, tocopherol acetate, fullerene and triethanolamine;
preferably, the anti-wrinkle skin-firming composition further comprises: thickening agent, humectant, emollient, emulsifier, preservative, chelating agent, colorant, skin conditioner, water;
preferably, the anti-wrinkle and skin-firming composition comprises the following components in parts by weight: 1-10 parts of glass chicory seed oil, 1-10 parts of betaine, 1-6 parts of snail secretion, 3-10 parts of schizosaccharomyces cerevisiae fermentation product lysate, 2-10 parts of hypecoum vulgare extract, 11-10 parts of oligopeptide, 0.01-0.5 part of xanthan gum, 5-15 parts of thickening agent, 1-10 parts of tocopherol acetate, 1-10 parts of fullerene, 0.1-0.5 part of triethanolamine, 1-10 parts of emollient, 10-25 parts of humectant, 5-15 parts of emulsifier, 0.1-0.5 part of preservative, 0.01-0.05 part of chelating agent, 0.1-1 part of colorant, 5-25 parts of skin conditioner and 60-120 parts of water;
preferably, the anti-wrinkle and skin-firming composition comprises the following components in parts by weight: 1-5 parts of glass chicory seed oil, 1-5 parts of betaine, 3-6 parts of snail secretion, 3-6 parts of schizosaccharomyces cerevisiae fermentation product lysate, 2-8 parts of hypecoum vulgare extract, 11-6 parts of oligopeptide, 0.1-0.5 part of xanthan gum, 5-10 parts of thickening agent, 1-7 parts of tocopherol acetate, 2-6 parts of fullerene, 0.1-0.3 part of triethanolamine, 1-5 parts of emollient, 15-20 parts of humectant, 10-15 parts of emulsifier, 0.1-0.4 part of preservative, 0.01-0.03 part of chelating agent, 0.1-0.5 part of colorant, 5-10 parts of skin conditioner and 60-80 parts of water;
preferably, the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 2-5.
Preferably, the emollient is any one or more of caprylic/capric triglyceride, isononyl isononanoate, hydrogenated polyisobutene, hydrogenated coconut oil glycerides, polydimethylsiloxane;
preferably, the emollient is a mixture of hydrogenated coconut oil glycerides and polydimethylsiloxane in a mass ratio of 2-3: 1;
preferably, the humectant is one or more of propylene glycol, glycerin, hydroxyethyl urea and sodium hyaluronate;
preferably, the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3-7: 1;
preferably, the emulsifier is any one or more of cetearyl olive oleate and sorbitan olive oleate, cetearyl glucoside, cetearyl alcohol;
preferably, the emulsifier is a mixture of cetearyl olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl olive oleate to the sorbitan olive oleate is 1-3: 1;
preferably, the emulsifier is a mixture of cetearyl glucoside and cetearyl alcohol, and the mass ratio of the cetearyl glucoside to the cetearyl alcohol is 1: 2-6;
preferably, the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1-2: 3;
preferably, the chelating agent is EDTA-2 Na;
preferably, the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 1-2: 1;
preferably, the skin conditioning agent is any one or more of collagen, butylene glycol, phytosterol isostearate, acetyl hexapeptide-8, caprylyl glycol, allantoin, dipotassium glycyrrhizinate, ceramide 3, octyldodecanol, hydrogenated lecithin, cholesterol, methyl hydroxybenzoate, propyl hydroxybenzoate, trehalose, ethylhexyl glycerin, disodium hydrogen phosphate, sodium dihydrogen phosphate, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, and p-hydroxyacetophenone.
The invention also aims to provide a preparation method of the anti-wrinkle and skin-firming composition, which comprises the following steps:
(1) mixing tocopheryl acetate and an emollient, adding an emulsifier and the glass chicory seed oil, heating, uniformly stirring, and keeping constant temperature until the mixture is completely dissolved to obtain a phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating, maintaining temperature, and stirring to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing, heating, keeping temperature, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and yeast lysate, adding citric acid to adjust pH, homogenizing, adding antiseptic and colorant, and stirring; discharging and standing to obtain the product.
Preferably, in the step (1), the constant temperature is 80-85 ℃;
preferably, in the step (2), the heating and heat preservation temperature is 80-85 ℃, and the stirring time is 10-20min, preferably 15 min;
preferably, in the step (3), the vacuum homogenization time is 5-10min, preferably 8 min;
preferably, in the step (3), the temperature for heating and heat preservation is 80-85 ℃, and the time is 10-40min, preferably 30 min;
preferably, in the step (4), the cooling is to cool the temperature to 40-50 ℃; preferably 48 deg.c.
Preferably, in the step (4), the discharging is carried out at 30-40 ℃, preferably 38 ℃;
preferably, in the step (4), the standing time is 10-15h, preferably 12 h;
preferably, in the step (4), the concentration of the citric acid is 0.25-1%, and the pH value is 4.2-6.5.
The invention also aims to provide application of the anti-wrinkle and skin-firming composition in cosmetics.
Compared with the prior art, the invention has the technical advantages that:
(1) the composition for resisting wrinkles and tightening skin prepared by the invention has better effects of resisting wrinkles and tightening skin;
(2) the essence prepared by the invention has the effects of resisting wrinkles and tightening, and also has good moisturizing, whitening, anti-aging and other effects, and the anti-wrinkle and tightening skin composition is easy to absorb and can replace various skin care products with single effect after being used;
(3) the snail secretion, the schizosaccharomyces cerevisiae fermentation product lysate and the hypsizygus marmoreus extract have good synergistic effect, and can effectively regulate the skin, so that the skin is smooth and elastic;
(4) the fullerene and the oligopeptide-1 have good synergistic effect, can effectively remove wrinkles and color spots of the skin, promote the formation and metabolism of the skin, stimulate the production of new cells of the skin and ensure that the skin is tender and glossy;
(5) after the citric acid is added, on one hand, the citric acid is beneficial to the absorption of the skin, the effective components of the composition are effectively utilized, the effect of the composition is promoted, and on the other hand, the composition can promote the improvement of the skin and has the effects of beautifying and removing wrinkles.
(6) The lecithin and the xanthan gum have a good thickening effect, and can be used for increasing the stability of a composition system for resisting wrinkles and tightening skin and improving the biological activity of the composition for resisting wrinkles and tightening skin.
Detailed Description
Example 1
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 5 parts of glass chicory seed oil, 5 parts of betaine, 3 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 8 parts of hypsizygus marmoreus extract, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 6 parts of fullerene, 0.3 part of triethanolamine, 5 parts of emollient, 20 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 3;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 2: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 3: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner consists of collagen, allantoin, ceramide 3, hydrogenated lecithin and trehalose in a mass ratio of 3:1:1:2: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping the temperature at 80 ℃ until the mixture is completely dissolved to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 80 deg.C, keeping the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 8min, heating at 80 deg.C and keeping the temperature for 30min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 48 deg.C, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 0.5% citric acid to adjust pH to 5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 38 deg.C, and standing for 12 hr.
Example 2
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 1 part of glass chicory seed oil, 1 part of betaine, 6 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 2 parts of hypecoum extract, 11 parts of oligopeptide, 0.1 part of xanthan gum, 5 parts of thickening agent, 1 part of tocopherol acetate, 2 parts of fullerene, 0.1 part of triethanolamine, 1 part of emollient, 15 parts of humectant, 15 parts of emulsifier, 0.1 part of preservative, 0.01 part of chelating agent, 0.1 part of colorant, 5 parts of skin conditioner and 60 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 2;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 3: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 7: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 1: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 2: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 1: 1;
the skin conditioner is a mixture of hydrogenated lecithin, cholesterol, methyl hydroxybenzoate, trehalose, ethylhexyl glycerin, sodium dihydrogen phosphate and polysorbate-80 in a mass ratio of 1:1:1:2:1:1: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping at 85 deg.C until completely dissolving to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 85 deg.C, maintaining the temperature, and stirring for 10min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 5min, heating at 85 deg.C and keeping the temperature for 10min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 40 deg.C, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 0.25% citric acid to adjust pH to 4.2, homogenizing, adding antiseptic and colorant, and stirring; discharging at 30 deg.C, and standing for 10 hr.
Example 3
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 10 parts of glass chicory seed oil, 10 parts of betaine, 1 part of snail secretion, 10 parts of schizosaccharomyces cerevisiae fermentation product lysate, 10 parts of hypsizygus marmoreus extract, 110 parts of oligopeptide, 0.5 part of xanthan gum, 15 parts of thickening agent, 10 parts of tocopherol acetate, 10 parts of fullerene, 0.5 part of triethanolamine, 10 parts of emollient, 25 parts of humectant, 5 parts of emulsifier, 0.5 part of preservative, 0.05 part of chelating agent, 1 part of colorant, 25 parts of skin conditioner and 120 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 5;
the skin-moistening agent is a mixture of caprylic triglyceride, hydrogenated coconut oil glyceride and polydimethylsiloxane in a mass ratio of 1:1: 1;
the humectant is a mixture of propylene glycol, glycerin, hydroxyethyl urea and sodium hyaluronate, and the mass ratio of the humectant to the humectant is 1:1:1: 1;
the emulsifier is a mixture of cetearyl glucoside and cetearyl alcohol, and the mass ratio of the cetearyl glucoside to the cetearyl alcohol is 1: 6;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 1: 1;
the skin conditioner is a mixture of hydrogenated lecithin, trehalose, ethylhexyl glycerin and polysorbate-80 in a mass ratio of 1:1:1: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping the temperature at 80 ℃ until the mixture is completely dissolved to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 85 deg.C, maintaining the temperature, and stirring for 20min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 10min, heating at 85 deg.C and keeping the temperature for 40min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 50 deg.C, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 1% citric acid to adjust pH to 6.5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 40 deg.C, and standing for 15 hr.
Example 4
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight:
5 parts of glass chicory seed oil, 5 parts of betaine, 3 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 8 parts of hypsizygus marmoreus extract, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 1 part of fullerene, 0.3 part of triethanolamine, 5 parts of emollient, 10 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 3.
The emollient is a mixture of isononyl isononanoate, hydrogenated polyisobutene, hydrogenated coconut oil glyceride and polydimethylsiloxane in a mass ratio of 1:2:1: 1;
the humectant is a mixture of propylene glycol, glycerin, hydroxyethyl urea and sodium hyaluronate, and the mass ratio of the humectant to the humectant is 1:1:1: 1;
the emulsifier is a mixture of cetearyl glucoside and cetearyl alcohol, and the mass ratio of the cetearyl glucoside to the cetearyl alcohol is 1: 2;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 2: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner is a mixture of allantoin, dipotassium glycyrrhizinate, ceramide 3, octyldodecanol and hydrogenated lecithin in a mass ratio of 1:1:1:1: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping at 85 deg.C until completely dissolving to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 85 deg.C, maintaining the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 7min, heating at 80 deg.C and keeping the temperature for 20min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 45 deg.C, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 0.75% citric acid to adjust pH to 6, homogenizing, adding antiseptic and colorant, and stirring; discharging at 35 deg.C, and standing for 10 hr.
Comparative example 1
Compared to example 1, the chicory seed oil was replaced with evening primrose oil with similar properties.
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 5 parts of evening primrose oil, 5 parts of betaine, 3 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 8 parts of hypecoum extract, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 6 parts of fullerene, 0.3 part of triethanolamine, 5 parts of emollient, 20 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 3: 1;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 2: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 3: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner consists of collagen, allantoin, ceramide 3, hydrogenated lecithin and trehalose in a mass ratio of 3:1:1:2: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and evening primrose oil, heating, stirring, and keeping at 80 deg.C until completely dissolving to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 80 deg.C, keeping the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 8min, heating at 80 deg.C and keeping the temperature for 30min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 48 deg.C, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 0.5% citric acid to adjust pH to 5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 38 deg.C, and standing for 12 hr.
Comparative example 2
In comparison with example 1, fullerene was replaced with vitamin C having an antioxidant effect.
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 5 parts of glass chicory seed oil, 5 parts of betaine, 3 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 8 parts of hypsizygus marmoreus extract, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 6 parts of vitamin C, 0.3 part of triethanolamine, 5 parts of emollient, 20 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 3: 1;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 2: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 3: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner consists of collagen, allantoin, ceramide 3, hydrogenated lecithin and trehalose in a mass ratio of 3:1:1:2: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping the temperature at 80 ℃ until the mixture is completely dissolved to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 80 deg.C, keeping the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 8min, heating at 80 deg.C and keeping the temperature for 30min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 48 deg.C, cooling, adding vitamin C, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and yeast lysate, adding 0.5% citric acid to adjust pH to 5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 38 deg.C, and standing for 12 hr.
Comparative example 3
Compared with example 1, the total amount of snail secretion, schizosaccharomyces cerevisiae fermentation product lysate and hypecoum vulgare extract is not changed, hypecoum vulgare extract is not used, and the addition amount of snail secretion and schizosaccharomyces cerevisiae fermentation product lysate is respectively increased.
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 5 parts of glass chicory seed oil, 5 parts of betaine, 7 parts of snail secretion, 7 parts of schizosaccharomyces cerevisiae fermentation product lysate, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 6 parts of fullerene, 0.3 part of triethanolamine, 5 parts of emollient, 20 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
wherein the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 3: 1;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 2: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 3: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner consists of collagen, allantoin, ceramide 3, hydrogenated lecithin and trehalose in a mass ratio of 3:1:1:2: 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping the temperature at 80 ℃ until the mixture is completely dissolved to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 80 deg.C, keeping the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 8min, heating at 80 deg.C and keeping the temperature for 30min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 48 deg.C, cooling, adding fullerene, xanthan gum, snail secretion, oligopeptide-1, and yeast lysate of fission yeast fermentation product, adding 0.5% citric acid to adjust pH to 5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 38 deg.C, and standing for 12 hr.
Comparative example 4
The kind of thickener was different from that of example 1.
The composition for resisting wrinkles and tightening skin comprises the following components in parts by weight: 5 parts of glass chicory seed oil, 5 parts of betaine, 3 parts of snail secretion, 3 parts of schizosaccharomyces cerevisiae fermentation product lysate, 8 parts of hypsizygus marmoreus extract, 16 parts of oligopeptide, 0.1 part of xanthan gum, 10 parts of thickening agent, 7 parts of tocopherol acetate, 6 parts of fullerene, 0.3 part of triethanolamine, 5 parts of emollient, 20 parts of humectant, 10 parts of emulsifier, 0.4 part of preservative, 0.03 part of chelating agent, 0.5 part of colorant, 10 parts of skin conditioner and 80 parts of water;
wherein the thickening agent is a mixture of sodium alginate and carbomer, and the mass ratio of the sodium alginate to the carbomer is 3: 1;
wherein the emollient is a mixture of hydrogenated coconut oil glyceride and polydimethylsiloxane, and the mass ratio of the hydrogenated coconut oil glyceride to the polydimethylsiloxane is 2: 1;
wherein the humectant is a mixture of hydroxyethyl urea and hyaluronic acid, and the mass ratio of the hydroxyethyl urea to the hyaluronic acid is 3: 1;
the emulsifier is a mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, and the mass ratio of the cetearyl alcohol olive oleate to the sorbitan olive oleate is 3: 1;
the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 3;
the chelating agent is EDTA-2 Na;
the colorant is a mixture of CI 19140 and CI 16255; the mass ratio of the two is 2: 1;
the skin conditioner consists of collagen, allantoin, ceramide 3, hydrogenated lecithin and trehalose in a mass ratio of 3:1:1:2: 1.
The preparation method of the anti-wrinkle and skin-firming composition is the same as that of example 1.
Comparative example 5
The preparation method is different compared to example 1.
A composition for anti-wrinkle and skin-firming, which is prepared in the same manner as in example 1.
The preparation method of the anti-wrinkle skin-firming composition comprises the following steps:
(1) mixing tocopheryl acetate and emollient, adding emulsifier and glass chicory seed oil, heating, stirring, and keeping the temperature at 80 ℃ until the mixture is completely dissolved to obtain phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating at 80 deg.C, keeping the temperature, and stirring for 15min to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing for 8min, heating at 80 deg.C and keeping the temperature for 30min, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling to 48 deg.C, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and lysate of yeast fermentation product, adding 0.5% acetic acid to adjust pH to 5, homogenizing, adding antiseptic and colorant, and stirring; discharging at 38 deg.C, and standing for 12 hr.
Examples of effects
1. Skin elasticity probe measurement:
selecting a group of subjects with normal healthy skin and no cosmetic allergy history, wherein the subjects are 20-35 years old and 40 persons in total, dividing the subjects into 8 groups according to examples 1-3 and comparative examples 1-5, cleaning the face of each group of 5 subjects before each application, keeping the same time for cleaning the face each time, applying a corresponding product after the skin is dried, applying the corresponding product to each group of subjects for 2 times each day, 2g each time and 4 weeks continuously, measuring the skin elasticity performance change of 0, 1, 2, 3 and 4 weeks after the product is used by selecting a skin elasticity probe of a PVM600 model produced by German CK company, the measurement result is expressed by an index, the unit is 1, the larger the numerical value is, the stronger the skin elasticity is indicated, and the average value of each group is taken, and the result is shown in Table 1.
TABLE 1 changes in skin elasticity
Test group 0 week 1 week 2 weeks 3 weeks 4 weeks
Example 1 0.511 0.556 0.622 0.653 0.671
Example 2 0.508 0.549 0.617 0.646 0.664
Example 3 0.510 0.547 0.615 0.647 0.668
Comparative example 1 0.512 0.539 0.578 0.601 0.619
Comparative example 2 0.506 0.522 0.553 0.585 0.603
Comparative example 3 0.513 0.535 0.562 0.594 0.612
Comparative example 4 0.508 0.533 0.559 0.586 0.599
Comparative example 5 0.511 0.541 0.590 0.611 0.637
Therefore, the anti-wrinkle and skin-firming composition provided by the invention can well promote the elasticity of skin, thereby playing the roles of anti-wrinkle and skin-firming; and the composition and the preparation method thereof have important influence on the elastic effect.
2. Skin moisture content:
selecting a test population with normal healthy skin and no cosmetic allergy history, wherein the test population is 20-35 years old and 40 people in total, dividing the test population into 8 groups according to examples 1-3 and comparative examples 1-5, cleaning the face of each group of 5 people before smearing, smearing corresponding products after the skin is dried in the air, coating the products for 0h, 1h, 2h, 4h and 6h, selecting a skin moisture test probe CM825 of German CK company, testing the moisture content of the skin at the cheek part under the environment of 20 ℃ and 50% relative humidity, and taking the average value of each group, wherein the result is shown in Table 2.
TABLE 2 variation of skin moisture content
Test group 0h 1h 2h 4h 6h
Example 1 23.03 52.23 49.16 45.32 41.36
Example 2 22.98 51.99 47.68 45.03 40.22
Example 3 23.02 52.08 48.52 44.69 41.64
Comparative example 1 22.99 39.21 34.21 29.63 25.39
Comparative example 2 23.06 36.35 30.55 25.78 20.14
Comparative example 3 22.89 41.26 35.47 30.12 24.46
Comparative example 4 23.02 38.19 32.82 27.96 22.68
Comparative example 5 23.00 46.44 40.66 31.56 25.89
Therefore, the composition provided by the invention has a good moisturizing effect, and has a small water dispersion loss after 2 hours, and a good moisturizing and water locking effect; and the composition and the preparation method thereof have great influence on the moisturizing effect.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.

Claims (7)

1. The composition for resisting wrinkles and tightening skin is characterized by comprising the following components in parts by weight: 1-10 parts of glass chicory seed oil, 1-10 parts of betaine, 1-6 parts of snail secretion, 3-10 parts of schizosaccharomyces cerevisiae fermentation product lysate, 2-10 parts of hypecoum vulgare extract, 11-10 parts of oligopeptide, 0.01-0.5 part of xanthan gum, 5-15 parts of thickening agent, 1-10 parts of tocopherol acetate, 1-10 parts of fullerene, 0.1-0.5 part of triethanolamine, 1-10 parts of emollient, 10-25 parts of humectant, 5-15 parts of emulsifier, 0.1-0.5 part of preservative, 0.01-0.05 part of chelating agent, 0.1-1 part of colorant, 5-25 parts of skin conditioner and 60-120 parts of water;
the thickening agent is a mixture of lecithin and carbomer, and the mass ratio of the lecithin to the carbomer is 1: 2-5.
2. The anti-wrinkle skin-firming composition according to claim 1, wherein said emollient is any one or more of caprylic/capric triglyceride, isononyl isononanoate, hydrogenated polyisobutene, hydrogenated cocoglycerides, dimethicone.
3. The anti-wrinkle and skin-firming composition according to claim 1, wherein the moisturizer is one or more of propylene glycol, glycerin, hydroxyethyl urea, and sodium hyaluronate; the emulsifier is any one or more of cetearyl olive oleate and sorbitan olive oleate, cetearyl glucoside and cetearyl alcohol.
4. The anti-wrinkle and skin-firming composition according to claim 1, wherein the preservative is a mixture of phenoxyethanol and ethylhexylglycerin; the chelating agent is EDTA-2 Na; the colorant is a mixture of CI 19140 and CI 16255.
5. The anti-wrinkle skin-firming composition according to claim 1, wherein the skin conditioning agent is any one or more of collagen, butylene glycol, phytosterol isostearate, acetyl hexapeptide-8, caprylyl glycol, allantoin, dipotassium glycyrrhizinate, ceramide 3, octyldodecanol, hydrogenated lecithin, cholesterol, trehalose, ethylhexylglycerin, and sodium acrylate/sodium acryloyldimethyl taurate copolymer.
6. A method for preparing the anti-wrinkle and skin-firming composition according to any one of claims 1 to 5, comprising the steps of:
(1) mixing tocopheryl acetate and an emollient, adding an emulsifier and the glass chicory seed oil, heating, uniformly stirring, and keeping constant temperature until the mixture is completely dissolved to obtain a phase A;
(2) adding betaine, humectant and thickener into water, adding chelating agent, heating, maintaining temperature, and stirring to obtain phase B;
(3) adding triethanolamine and skin conditioner into phase A, vacuum homogenizing, heating, keeping temperature, stirring, and vacuum defoaming to obtain phase C;
(4) homogenizing phase A, phase B and phase C, stirring, cooling, adding fullerene, xanthan gum, fructus Anisi Stellati extract, snail secretion, oligopeptide-1, and yeast lysate, adding citric acid to adjust pH, homogenizing, adding antiseptic and colorant, and stirring; discharging and standing to obtain the product.
7. Use of the anti-wrinkle and skin-firming composition according to any one of claims 1 to 5 or the composition prepared by the method for preparing the anti-wrinkle and skin-firming composition according to claim 6 in cosmetics.
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