CN114522129B - Moisturizing and tightening repair composition, cosmetic and preparation method - Google Patents
Moisturizing and tightening repair composition, cosmetic and preparation method Download PDFInfo
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- CN114522129B CN114522129B CN202210197390.0A CN202210197390A CN114522129B CN 114522129 B CN114522129 B CN 114522129B CN 202210197390 A CN202210197390 A CN 202210197390A CN 114522129 B CN114522129 B CN 114522129B
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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Abstract
The application discloses a moisturizing and tightening repair composition, a cosmetic and a preparation method, and relates to the field of cosmetics. The composition comprises extracts of Cichorium intybus (CICHORIUM INTYBUS) root, caesalpinia spinosa (CAESALPINIASPINOSA) gum, lentinus Edodes (LENTINUS EDODES) mycelium, sage (SALVIAHISPANICA) seed extract, lactobacillus fermentation product, and Chlorella (CHLORELLA VULGARIS) extract. According to the application, the fresh oil ester is matched with the vegetable oil ester to effectively moisten skin, degrade the sticky feeling of the formula, achieve a fresh and non-greasy system, and add various plant extracts to repair dry skin, solve dry and itchy skin in winter, increase skin elasticity, simultaneously astringe and relax skin, reduce wrinkles, and have a diversified effect.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a moisturizing and tightening repair composition, a cosmetic and a preparation method.
Background
The skin is the organ which is covered on the surface of the human body and has the largest surface, and is damaged due to the direct contact with the external environment and the stimulation of various tension factors such as oxidation, dryness, ultraviolet rays and the like. And the skin has a lot of changes along with the aging and the climate change, and the problems of dryness, uneven skin color, allergy, relaxation, aging and the like of the skin color can occur, and meanwhile, the skin is obviously degraded and aged due to the increasing working pressure and living pressure of modern people.
At present, cosmetics which solve various skin problems in a multi-effect manner and have obvious effects are not found in the market at present. Therefore, a formulation different from the traditional system and skin feel is urgently needed to be developed, which not only can keep moisture for a long time, but also can replace water, milk, cream, essence, facial mask and the like to be matched for use so as to realize the functions of tightening and anti-wrinkle, and solves the trouble of overlapping and using various products.
Disclosure of Invention
The invention provides a moisturizing tightening repair composition, a cosmetic and a preparation method thereof, which are used for solving the technical problem that the existing cosmetic is insufficient in efficacy in the aspects of moisturizing, tightening and repairing.
In order to solve the technical problems, one of the purposes of the invention is to provide a moisturizing and tightening repair composition which comprises the following raw materials in parts by weight:
skin tightening composition a: 0.1-3 parts;
skin tightening composition B: 0.1-5 parts;
moisturizing composition: 1-8 parts;
A soothing composition: 0.1-8 parts;
repairing composition a: 0.1-6 parts;
repairing composition B: 0.1-3 parts;
water: 4-90 parts;
Wherein the skin tightening composition a comprises hydrolyzed soy protein and acacia senegal (ACACIA SENEGAL) gum; the skin tightening composition B comprises chicory (CICHORIUM INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises a shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe barbansis), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (Lycium BARBARUM) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repair composition a comprises spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repair composition B includes chlorella (CHLORELLA VULGARIS) extract.
By adopting the scheme, the sage in the repairing composition A is commonly called chia, is a natural carbohydrate scaffold, can promote wound healing, protect skin and hair from pollution, and the lactobacillus fermentation product is beneficial to cell proliferation, wound healing and anti-inflammatory properties, so that the generation of aging marks is prevented, excellent wound healing, anti-inflammatory, film forming and anti-irritation effects can be provided, the moisturizing performance is improved, and the skin is helped to resist various environmental stimulus factors; various extracts in the soothing composition can immediately and long-term improve the moisture content of skin, improve the expression of aquaporin, effectively clear heat and diminish inflammation, effectively inhibit degradation of hyaluronic acid caused by inflammation, improve the fixation of silk fibroin and sluice protein, protect the screen, smooth and smooth phosphorus scraps and roughness of skin caused by dryness, nourish and moisten the skin, enable the skin feel of the skin to be smooth, and solve the problems of internal and external dryness of the skin; the synergistic effect of the combination of the soothing composition and the repairing composition A is better; the chlorella and the chicory pulling element can effectively tighten the skin, deeply repair, adsorb and complex heavy metals in PM2.5 and repair the stratum corneum barrier; the chicory pulling element has instant and long-term tightening pulling effect and lasting anti-aging effect and has the effects of plumping and removing wrinkles; according to the application, the fresh oil ester is matched with the vegetable oil ester to effectively moisten skin, the plant moisturizing composition is added to achieve deep moisturizing, the sticky and greasy feeling of the formula is degraded, a fresh and non-greasy system is achieved, and the dry skin is repaired by adding various plant extracts, so that the dry and itchy skin in winter is solved, the skin elasticity is increased, the skin is converged and relaxed, the wrinkles are reduced, and the skin care cream has excellent skin feeling and use feeling.
Preferably, the skin tightening composition a further comprises xanthan gum, sodium benzoate and xanthan gum; the skin tightening composition B further comprises glycerin, sodium benzoate, gluconolactone and calcium gluconate; the moisturizing composition further comprises glycerin and urea; the soothing composition further comprises glycerin, phenoxyethanol and ethylhexyl glycerin; the repair composition B further comprises glycerin, ethylhexyl glycerin, 1, 2-pentanediol, and 1, 2-hexanediol.
As a preferred scheme, the active ingredients of the skin tightening composition A comprise water, xanthan gum, sodium benzoate, hydrolyzed soy protein, acacia gum (ACACIA SENEGAL) gum and xanthan gum in a mass ratio; the skin tightening composition B comprises the following components in percentage by mass of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product; the repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
In order to solve the technical problems, the second purpose of the invention is to provide a moisturizing and tightening cosmetic, which comprises the following raw materials in parts by weight:
Moisturizing repair composition: 41-93 parts;
humectant: 2.6-15 parts;
antioxidant: 0.16 to 1.8 parts;
and (3) a thickening agent: 0.16 to 0.85 parts;
chelating agent: 0.01 to 0.1 part;
Emulsifying agent: 1.6-9 parts;
PH harmonizing agent: 0.01 to 0.5 part;
Preservative: 0.2 to 1 part.
As a preferred scheme, the emulsifier comprises the following raw materials in parts by weight: 0.5 to 3 parts of B12/W12 emulsifier, 0.8 to 3 parts MONTANOV to 68 and 0.3 to 3 parts cetostearyl alcohol.
By adopting the scheme, the liquid crystal emulsifier is used, so that the paste is bright and fine in appearance and quick in absorption, the plant humectant is helped to achieve deep moisture retention, the sticky feeling of the formula is degraded, and a fresh and non-greasy system is realized.
Preferably, the humectant comprises the following raw materials in parts by weight: 2 to 8 parts of butanediol, 0.5 to 5 parts of polyglycerol-10 and 0.1 to 2 parts of panthenol.
Preferably, the antioxidant comprises the following raw materials in parts by weight: 0.15-0.8 part of p-hydroxyacetophenone and 0.01-1 part of tocopherol; the thickener comprises the following raw materials in parts by weight: 0.08 to 0.45 parts carbomer and 0.08 to 0.4 parts xanthan gum; the chelating agent is disodium EDTA.
As a preferable scheme, the material also comprises the following raw materials in parts by weight:
fragrance: 0.001 parts to 0.1 parts;
Nicotinamide: 0.5-5 parts;
An emollient: 2.3-25 parts;
CBSIL-1028: 0.3-4 parts.
Preferably, the emollient comprises the following raw materials in parts by weight: 0.5 to 6 parts of PMX0345 silicone oil, 0.8 to 5 parts of CBSIL to 1020, 0.5 to 8 parts of canola oil and 0.5 to 6 parts of butter tree (BUTYROSPERMUM PARKII) fruit fat.
In order to solve the above technical problems, the third object of the present invention is to provide a method for preparing a moisturizing and tightening cosmetic, comprising the steps of:
(1) Sequentially adding a humectant, a part of antioxidant, a thickener, a chelating agent and a solvent material into emulsifying equipment, heating to 82-85 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
(2) Sequentially adding an emulsifying agent, an emollient and a part of antioxidant into oil phase equipment, heating to 82-85 ℃, and stirring and dissolving uniformly to obtain a mixture B;
(3) Sucking the mixture B into emulsifying equipment, homogenizing at high speed, maintaining the temperature for 20-30 min, and cooling;
(4) Pre-mixing nicotinamide, PH regulator and CBSIL-1028 to dissolve into a C mixed material;
(5) Stirring and cooling to 45-50 ℃, adding the C mixed material, and homogenizing at a low speed;
(6) Stirring and cooling to 38-40deg.C, adding moisturizing repair composition, antiseptic and aromatic, and stirring to obtain the final product.
Compared with the prior art, the embodiment of the invention has the following beneficial effects:
According to the application, the fresh oil ester is matched with the vegetable oil ester to effectively moisten skin, the plant moisturizing composition is added to achieve deep moisturizing, the sticky and greasy feeling of the formula is degraded, a fresh and non-greasy system is achieved, and the dry skin is repaired by adding various plant extracts, so that the dry and itchy skin in winter is solved, the skin elasticity is increased, the skin is converged and relaxed, the wrinkles are reduced, and the skin care cream has excellent skin feeling and use feeling.
Drawings
FIG. 1 is a photograph showing the state of eyes of a moisturizing compact repair cosmetic before use according to a third embodiment of the present invention;
FIG. 2 is a photograph showing the state of eyes of a moisturizing compact repair cosmetic according to a third embodiment of the present invention after 2 hours of use;
FIG. 3-is a 60-day anti-wrinkle test result of a moisturizing compact repair cosmetic in accordance with one embodiment of the present invention;
FIG. 4 is a graph showing the results of a 60-day anti-wrinkle test of a moisturizing compact cosmetic in accordance with the second embodiment of the present invention;
FIG. 5 is a graph showing the results of a 60-day anti-wrinkle test of a moisturizing compact cosmetic in accordance with the third embodiment of the present invention;
FIG. 6-is a 60-day anti-wrinkle test result of a moisturizing compact repair cosmetic according to the fourth embodiment of the present disclosure;
FIG. 7-is a 60-day anti-wrinkle test result of a moisturizing compact repair cosmetic in comparative example one of the present invention;
FIG. 8-is a 60-day anti-wrinkle test result of one of the moisturizing compact repair cosmetics of comparative example two of the present invention;
FIG. 9-is a 60-day anti-wrinkle test result of a moisturizing compact repair cosmetic in accordance with the third embodiment of the present invention.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
TABLE 1 sources and types of raw materials in preparation examples, examples and comparative examples of the present application
Preparation example one
The moisturizing and tightening repair composition comprises the following raw material components: skin tightening composition a:0.1kg; skin tightening composition B:0.1kg; moisturizing composition: 1kg; a soothing composition: 0.1kg; repairing composition a:0.1kg; repairing composition B:0.1kg; water: 90.36kg; wherein, the active ingredients of the skin tightening composition A comprise the following components in mass ratio of 50.6:2.5:0.9:30:16, xanthan gum, sodium benzoate, hydrolyzed soy protein, and acacia gum (ACACIA SENEGAL); the skin tightening composition B comprises the following components in mass ratio of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product; the repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
Preparation example two
The moisturizing and tightening repair composition comprises the following raw material components: skin tightening composition a:0.3kg; skin tightening composition B:1kg; moisturizing composition: 5kg; a soothing composition: 3kg; repairing composition a:1kg; repairing composition B:0.5kg; water: 71.83kg; wherein, the active ingredients of the skin tightening composition A comprise the following components in mass ratio of 50.6:2.5:0.9:30:16, xanthan gum, sodium benzoate, hydrolyzed soy protein, and acacia gum (ACACIA SENEGAL); the skin tightening composition B comprises the following components in mass ratio of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product; the repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
Preparation example three
The moisturizing and tightening repair composition comprises the following raw material components: skin tightening composition a:1.5kg; skin tightening composition B:2kg; moisturizing composition: 6kg; a soothing composition: 5kg; repairing composition a:2kg; repairing composition B:2kg; water: 53.08kg; wherein, the active ingredients of the skin tightening composition A comprise the following components in mass ratio of 50.6:2.5:0.9:30:16, xanthan gum, sodium benzoate, hydrolyzed soy protein, and acacia gum (ACACIA SENEGAL); the skin tightening composition B comprises the following components in mass ratio of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product; the repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
Preparation example IV
The moisturizing and tightening repair composition comprises the following raw material components: skin tightening composition a:3kg; skin tightening composition B:5kg; moisturizing composition: 8kg; a soothing composition: 8kg; repairing composition a:6kg; repairing composition B:3kg; water: 4.65kg; wherein, the active ingredients of the skin tightening composition A comprise the following components in mass ratio of 50.6:2.5:0.9:30:16, xanthan gum, sodium benzoate, hydrolyzed soy protein, and acacia gum (ACACIA SENEGAL); the skin tightening composition B comprises the following components in mass ratio of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract; the soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product; the repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
Example 1
A moisturizing and tightening cosmetic comprises the following raw material components: moisturizing and tightening repair composition of preparation example one: 92.16kg; humectant: 2.6kg; antioxidant: 0.16kg; and (3) a thickening agent: 0.16kg; chelating agent: 0.01kg; emulsifying agent: 1.6kg; PH harmonizing agent: 0.01kg; preservative: 0.2kg; fragrance: 0.001kg; nicotinamide: 0.5kg; an emollient: 2.3kg; CBSIL-1028:0.3kg; wherein, the humectant comprises the following components in percentage by mass: 5:1, butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass: 1 p-hydroxyacetophenone and tocopherol; the thickener comprises the following components in percentage by mass: 1 carbomer and xanthan gum; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass: 8:3, B12/W12 emulsifier, MONTANOV, and cetostearyl alcohol; the PH regulator is arginine; the emollient comprises a mass ratio of 5:8:5:5 PMX0345 silicone oil, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat; the preservative comprises the following components in percentage by mass: 1 phenoxyethanol and ethylhexyl glycerol; the preparation method comprises the following preparation steps:
1. Accurately weighing the materials of all components in the formula, and cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum, EDTA disodium box panthenol into an emulsifying pot, heating to 82 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. Sequentially adding a B12/W12 emulsifier, MONTANOV, cetylstearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat into an oil phase pot, heating to 82 ℃, stirring and dissolving uniformly to obtain a B mixed material;
4. And (3) sucking the mixture B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 20 minutes, and cooling.
5. Mixing arginine, nicotinamide and CBSIL-1028 in advance for dissolving to obtain a C mixed material;
6. Stirring and cooling to 45 ℃, adding the pre-dissolved C mixture, and homogenizing at a low speed (1500 rpm) for 5 minutes;
7. Stirring and cooling to 38deg.C, adding moisturizing and tightening composition, antiseptic and flos Rosae Rugosae (Rosa RUGOSA) flower oil, stirring, sampling, detecting, and discharging after passing the test to obtain the moisturizing and tightening cosmetic.
Example two
A moisturizing and tightening cosmetic comprises the following raw material components: moisturizing and tightening repair composition of preparation II: 82.63kg; humectant: 6kg; antioxidant: 0.5kg; and (3) a thickening agent: 0.35kg; chelating agent: 0.01kg; emulsifying agent: 3kg; PH harmonizing agent: 0.01kg; preservative: 0.2kg; fragrance: 0.001kg; nicotinamide: 0.5kg; an emollient: 6.5kg; CBSIL-1028:0.3kg; wherein, the humectant comprises the following components in percentage by mass: 3:1, butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass: 1 p-hydroxyacetophenone and tocopherol; the thickener comprises the following components in mass ratio 3: carbomer and xanthan gum of 4; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass: 1: B12/W12 emulsifier of 1, MONTANOV and cetostearyl alcohol; the PH regulator is arginine; the emollient comprises a mass ratio of 2:3:6:2, PMX0345 silicone oil, CBSIL-1020, canola oil and shea butter (BUTYROSPERMUM PARKII) butter; the preservative comprises the following components in percentage by mass: 1 phenoxyethanol and ethylhexyl glycerol; the preparation method comprises the following preparation steps:
1. Accurately weighing the materials of all components in the formula, and cleaning production equipment;
2. Sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum, EDTA disodium box panthenol into an emulsifying pot, heating to 85 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. sequentially adding a B12/W12 emulsifier, MONTANOV, cetylstearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat into an oil phase pot, heating to 85 ℃, stirring and dissolving uniformly to obtain a B mixed material;
4. And (3) sucking the mixture B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 30 minutes, and cooling.
5. Mixing arginine, nicotinamide and CBSIL-1028 in advance for dissolving to obtain a C mixed material;
6. stirring and cooling to 50 ℃, adding the pre-dissolved C mixture, and homogenizing at a low speed (1500 rpm) for 5 minutes;
7. stirring and cooling to 40 ℃, adding the moisturizing and tightening composition, the preservative and rose (ROSA RUGOSA) flower oil, uniformly stirring, sampling, detecting, discharging after the mixture is qualified, and obtaining the moisturizing and tightening cosmetic.
Example III
A moisturizing and tightening cosmetic comprises the following raw material components: moisturizing and tightening repair composition of preparation III: 71.58kg; humectant: 8kg; antioxidant: 0.8kg; and (3) a thickening agent: 0.6kg; chelating agent: 0.01kg; emulsifying agent: 5kg; PH harmonizing agent: 0.01kg; preservative: 0.2kg; fragrance: 0.001kg; nicotinamide: 0.5kg; an emollient: 13kg; CBSIL-1028:0.3kg; wherein, the humectant comprises the following components in percentage by mass: 2:1, butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass: 3 p-hydroxyacetophenone and tocopherol; the thickener comprises the following components in percentage by mass: 1 carbomer and xanthan gum; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass: 4:3, B12/W12 emulsifier, MONTANOV, and cetostearyl alcohol; the PH regulator is arginine; the emollient comprises 3 mass ratio: 2:5:3, PMX0345 silicone oil, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat; the preservative comprises the following components in percentage by mass: 1 phenoxyethanol and ethylhexyl glycerol; the preparation method comprises the following preparation steps:
1. Accurately weighing the materials of all components in the formula, and cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum, EDTA disodium box panthenol into an emulsifying pot, heating to 82 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. Sequentially adding a B12/W12 emulsifier, MONTANOV, cetylstearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat into an oil phase pot, heating to 82 ℃, stirring and dissolving uniformly to obtain a B mixed material;
4. And (3) sucking the mixture B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 20 minutes, and cooling.
5. Mixing arginine, nicotinamide and CBSIL-1028 in advance for dissolving to obtain a C mixed material;
6. Stirring and cooling to 45 ℃, adding the pre-dissolved C mixture, and homogenizing at a low speed (1500 rpm) for 5 minutes;
7. Stirring and cooling to 38deg.C, adding moisturizing and tightening composition, antiseptic and flos Rosae Rugosae (Rosa RUGOSA) flower oil, stirring, sampling, detecting, and discharging after passing the test to obtain the moisturizing and tightening cosmetic.
Example IV
A moisturizing and tightening cosmetic comprises the following raw material components: moisturizing and tightening repair composition of preparation example four: 41.65kg; humectant: 15kg; antioxidant: 1.8kg; and (3) a thickening agent: 0.85kg; chelating agent: 0.1kg; emulsifying agent: 9kg; PH harmonizing agent: 0.5kg; preservative: 1kg; fragrance: 0.1kg; nicotinamide: 5kg; an emollient: 25kg; CBSIL-1028:4kg; wherein, the humectant comprises the following components in percentage by mass: 5:2, butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass of 0.8:1 p-hydroxyacetophenone and tocopherol; the thickener comprises the following components in percentage by mass: 1 carbomer and xanthan gum; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass: 1: B12/W12 emulsifier of 1, MONTANOV and cetostearyl alcohol; the PH regulator is arginine; the emollient comprises a mass ratio of 6:5:8:6 PMX0345 silicone oil, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat; the preservative comprises the following components in percentage by mass: 1 phenoxyethanol and ethylhexyl glycerol; the preparation method comprises the following preparation steps:
1. Accurately weighing the materials of all components in the formula, and cleaning production equipment;
2. Sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum, EDTA disodium box panthenol into an emulsifying pot, heating to 85 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. sequentially adding a B12/W12 emulsifier, MONTANOV, cetylstearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and butter tree (BUTYROSPERMUM PARKII) fruit fat into an oil phase pot, heating to 85 ℃, stirring and dissolving uniformly to obtain a B mixed material;
4. And (3) sucking the mixture B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 30 minutes, and cooling.
5. Mixing arginine, nicotinamide and CBSIL-1028 in advance for dissolving to obtain a C mixed material;
6. stirring and cooling to 50 ℃, adding the pre-dissolved C mixture, and homogenizing at a low speed (1500 rpm) for 5 minutes;
7. stirring and cooling to 40 ℃, adding the moisturizing and tightening composition, the preservative and rose (ROSA RUGOSA) flower oil, uniformly stirring, sampling, detecting, discharging after the mixture is qualified, and obtaining the moisturizing and tightening cosmetic.
Comparative preparation example one
The moisturizing and tightening composition is characterized in that the tightening composition B is replaced by water, and the agent and the technological parameters used in each step are the same as those in the preparation example.
Comparative preparation II
The moisturizing and tightening repairing composition is different from the preparation example in that the repairing composition B is replaced by water.
Comparative preparation example three
The moisturizing and tightening composition is characterized in that the moisturizing and tightening composition comprises the following components in parts by weight: skin tightening composition a:5kg; skin tightening composition B:2kg; moisturizing composition: 0.5kg; a soothing composition: 5kg; repairing composition a:8kg; repairing composition B:2kg; water: 49.08kg;
Comparative example one
The moisturizing and tightening cosmetic used in each step and the reagents and process parameters used in each step are the same as those in the three embodiments, except that the moisturizing and tightening cosmetic composition of the third embodiment is replaced by that of the first comparative embodiment.
Comparative example two
The moisturizing and tightening cosmetic used in each step and the reagents and process parameters used in each step are the same as those in the three-phase example, except that the moisturizing and tightening cosmetic composition of the third preparation example is replaced by the moisturizing and tightening cosmetic composition of the second preparation example.
Comparative example three
The moisturizing and tightening cosmetic used in each step and the reagents and process parameters used in each step are the same as those in the three-phase example, except that the moisturizing and tightening cosmetic composition of the third preparation example is replaced by the moisturizing and tightening cosmetic composition of the third preparation example.
Performance test
1. Moisturizing effect and skin elasticity test:
1) Sample to be tested: cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 of the present application;
2) The test method comprises the following steps: the moisturizing and tightening cosmetic prepared in examples 1 to 4 and comparative examples 1 to 3 was used as a test sample, 140 men and women (28 to 55 years old) were selected and randomly divided into 6 groups of 20 persons each, and each group was applied to facial skin twice a day after cleansing, skin moisture content and skin elasticity were measured with a CK Corneometer CM skin moisture tester after 24 hours, and the overall score of the results after 28 days was shown in table 2.
TABLE 2 results of moisture retention and elasticity test for examples 1-4 and comparative examples 1-3
2. Immediate tightening wrinkle resistance test:
1) Sample to be tested: moisturizing compact repair cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 of the present application;
2) The test method comprises the following steps: the moisturizing and tightening repair cosmetics prepared in examples 1-4 and comparative examples 1-3 are used as test samples, 140 men and women (40-55 years old) are selected to be randomly divided into 6 groups, 20 persons are respectively coated on the skin around eyes after face cleaning, and the comparison between the use of example 3 and the use of example 2 hours is shown in fig. 1-2, so that the wrinkle smoothing effect is remarkable;
3) Anti-wrinkle test: the tester smears the moisturizing and tightening cream on the face 2 times a day, observes and records the wrinkle length, the wrinkle depth, the wrinkle number and the wrinkle range after 60 days of the test, and the test data results are shown in fig. 3 to 9.
As can be seen from the results of the tests of example 3 and comparative examples 1-3 and FIGS. 5 and 6-9 in Table 2, the present application specifically selects the components and the addition amounts of the moisturizing and repairing composition, so that the components are proper and the effects are better, and the prepared cosmetic has higher moisturizing and water locking functions, gives higher elasticity to the skin, has tightening and repairing effects, and can smooth wrinkles and reduce the occurrence of wrinkles.
The foregoing embodiments have been provided for the purpose of illustrating the general principles of the present invention, and are not to be construed as limiting the scope of the invention. It should be noted that any modifications, equivalent substitutions, improvements, etc. made by those skilled in the art without departing from the spirit and principles of the present invention are intended to be included in the scope of the present invention.
Claims (7)
1. The moisturizing and tightening cosmetic is characterized by comprising the following raw materials in parts by weight:
moisturizing and tightening composition: 41-71.58 parts;
Humectant: 8-15 parts;
antioxidant: 0.8-1.8 parts;
and (3) a thickening agent: 0.6-0.85 parts;
chelating agent: 0.01 to 0.1 part;
Emulsifying agent: 5-9 parts;
PH harmonizing agent: 0.01 to 0.5 part;
preservative: 0.2-1 part;
The moisturizing and tightening repair composition comprises the following raw materials in parts by weight:
skin tightening composition a: 1.5-3 parts;
Skin tightening composition B: 2-5 parts;
moisturizing composition: 6-8 parts;
A soothing composition: 5-8 parts;
Repairing composition a: 2-6 parts;
Repairing composition B: 2-3 parts;
water: 4 parts to 53.08 parts;
wherein, the active ingredients of the skin tightening composition A comprise the following components in mass ratio of 50.6:2.5:0.9:30:16, xanthan gum, sodium benzoate, hydrolyzed soy protein, and acacia gum (ACACIA SENEGAL);
The skin tightening composition B comprises the following components in percentage by mass of 32.5:21.5:0.25:0.75:0.01:44.93:0.06 of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract and tarragon (CAESALPINIA SPINOSA) gum;
The moisturizing composition comprises the following components in percentage by mass of 69.5:25:5:0.5 water, glycerol, urea and shiitake mushroom (LENTINUS EDODES) mycelium extract;
The soothing composition comprises the following components in percentage by mass: 20:0.63:0.07:4:2:2:1.5:0.8 of water, glycerol, phenoxyethanol, ethylhexyl glycerol, stem extract of Dendrobium nobile (DENDROBIUM NOBILE), leaf extract of Aloe vera (Aloe BARBADENSIS), root extract of Sophora flavescens (SOPHORA FLAVESCENS), fruit extract of Lycium BARBARUM (LYCIUM barbarbus) and extract of Echinacea purpurea (ECHINACEA PURPUREA);
the repairing composition A comprises the following components in percentage by mass: 2, a spanish sage (SALVIA HISPANICA) seed extract and a lactobacillus fermentation product;
The repairing composition B comprises the following components in percentage by mass of 74.15:5:0.1:0.25:0.25:20, glycerol, ethylhexyl glycerol, 1, 2-pentanediol, 1, 2-hexanediol, and chlorella (CHLORELLA VULGARIS) extract.
2. The moisturizing and tightening cosmetic as recited in claim 1, wherein the emulsifier comprises the following raw materials in parts by weight: 0.5 to 3 parts of B12/W12 emulsifier, 0.8 to 3 parts MONTANOV to 68 and 0.3 to 3 parts cetostearyl alcohol.
3. The moisturizing and tightening cosmetic as recited in claim 1, wherein the moisturizing agent comprises the following raw materials in parts by weight: 2 to 8 parts of butanediol, 0.5 to 5 parts of polyglycerol-10 and 0.1 to 2 parts of panthenol.
4. The moisturizing and tightening cosmetic as recited in claim 1, wherein the antioxidant comprises the following raw materials in parts by weight: 0.15-0.8 part of p-hydroxyacetophenone and 0.01-1 part of tocopherol; the thickener comprises the following raw materials in parts by weight: 0.08 to 0.45 parts carbomer and 0.08 to 0.4 parts xanthan gum; the chelating agent is disodium EDTA.
5. The moisturizing and tightening cosmetic as recited in claim 1, further comprising the following raw materials in parts by weight:
fragrance: 0.001 parts to 0.1 parts;
Nicotinamide: 0.5-5 parts;
An emollient: 2.3-25 parts;
CBSIL-1028: 0.3-4 parts.
6. The moisturizing compact cosmetic of claim 5, wherein the emollient comprises the following ingredients in parts by weight: 0.5 to 6 parts of PMX0345 silicone oil, 0.8 to 5 parts of CBSIL to 1020, 0.5 to 8 parts of canola oil and 0.5 to 6 parts of butter tree (BUTYROSPERMUM PARKII) fruit fat.
7. A method for preparing the moisturizing and tightening cosmetic according to claim 5 or 6, comprising the steps of:
(1) Sequentially adding a humectant, a part of antioxidant, a thickener, a chelating agent and a solvent material into emulsifying equipment, heating to 82-85 ℃, stirring, dispersing and dissolving uniformly to obtain a mixture A;
(2) Sequentially adding an emulsifying agent, an emollient and a part of antioxidant into oil phase equipment, heating to 82-85 ℃, and stirring and dissolving uniformly to obtain a mixture B;
(3) Sucking the mixture B into emulsifying equipment, homogenizing at high speed, maintaining the temperature for 20-30 min, and cooling;
(4) Pre-mixing nicotinamide, PH regulator and CBSIL-1028 to dissolve into a C mixed material;
(5) Stirring and cooling to 45-50 ℃, adding the C mixed material, and homogenizing at a low speed;
(6) Stirring and cooling to 38-40deg.C, adding moisturizing and tightening composition, antiseptic and aromatic, and stirring to obtain the final product.
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| CN115120551B (en) * | 2022-08-11 | 2024-03-22 | 露乐健康科技股份有限公司 | Chlorella extract and application of lactobacillus fermentation product in nursing products |
| CN115192498A (en) * | 2022-08-31 | 2022-10-18 | 新法丽赛尔(山东)化妆品有限公司 | Formula and preparation process of firming anti-aging skin-nourishing product |
| CN115836990A (en) * | 2022-09-06 | 2023-03-24 | 上海皮宝生物科技发展有限公司 | Multi-effect body repairing composition and skin care preparation and application thereof |
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