CN114522129A - Moisturizing, firming and repairing composition, cosmetic and preparation method - Google Patents
Moisturizing, firming and repairing composition, cosmetic and preparation method Download PDFInfo
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- CN114522129A CN114522129A CN202210197390.0A CN202210197390A CN114522129A CN 114522129 A CN114522129 A CN 114522129A CN 202210197390 A CN202210197390 A CN 202210197390A CN 114522129 A CN114522129 A CN 114522129A
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- extract
- repairing
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a moisturizing, tightening and repairing composition, a cosmetic and a preparation method thereof, and relates to the field of cosmetics. The composition comprises plant extracts such as extract of root of chicory (Cichorium INTYBUS), Caesalpinia spinosa (Caesalpinia spinosa) gum, extract of mycelium of Lentinus EDODES (Lentinus EDODES), extract of seed of Salvia Spanish (SALVIAHISPANICA), fermentation product of lactobacillus, and extract of Chlorella VULGARIS (Chlorella VULGARIS). According to the skin care product, the refreshing oil ester is matched with the vegetable oil ester to effectively moisten the skin, the sticky feeling of the formula is degraded, a refreshing and non-greasy system is achieved, various plant extracts are added, the dry skin is repaired, the dry and itchy skin in winter is solved, the skin elasticity is increased, meanwhile, the skin is converged and relaxed, wrinkles are reduced, and the skin care product has a diversified effect.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a moisturizing, firming and repairing composition, a cosmetic and a preparation method.
Background
The skin, which is the largest organ covering the surface of the human body, is directly in contact with the external environment and is stimulated by various stressful factors such as oxidation, dryness and ultraviolet rays, thereby being damaged. And with the increase of age and the change of climate, skin changes, the problems of dry skin color, uneven skin color, allergy, relaxation, aging and the like can occur, and simultaneously, the phenomena of skin deterioration and aging become more obvious because modern people face more and more working pressure and living pressure.
At present, cosmetics which can solve various skin problems and have obvious effects are not found in the market. Therefore, a formula which is different from the traditional system and skin feel is urgently needed to be developed, the formula can be used for long-acting moisture preservation, can be used for replacing matching of water, milk, cream, essence, facial masks and the like to realize cosmetics with the functions of tightening and resisting wrinkles, and the trouble of overlapping and using various products is solved.
Disclosure of Invention
The invention provides a moisturizing, tightening and repairing composition, a cosmetic and a preparation method thereof, and aims to solve the technical problem that the existing cosmetic is insufficient in effects of combining and solving moisturizing, tightening and repairing.
In order to solve the technical problems, the invention provides a moisturizing, tightening and repairing composition which comprises the following raw materials in parts by weight:
firming composition a: 0.1 to 3 portions;
firming composition B: 0.1 to 5 portions;
moisturizing composition: 1-8 parts;
soothing composition: 0.1 to 8 portions;
repairing composition a: 0.1 to 6 portions;
repairing composition B: 0.1 to 3 portions;
water: 4-90 parts;
wherein said firming composition A comprises hydrolyzed soy protein and acacia senegal (ACACIA SENEGAL) gum; said firming composition B comprises extract of chicory (Cichorium INTYBUS) root and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises an extract of mycelium of Lentinus EDODES (LENTINUS EDODES); the soothing composition comprises stem extract of Dendrobium NOBILE (Dendrobium NOBILE), leaf extract of Aloe BARBADENSIS (Aloe BARBADENSIS), root extract of Sophora FLAVESCENS (Sophora FLAVESCENS), fruit extract of Lycium BARBARUM (Lycium BARBARUM) and Echinacea purpurea (ECHINACEA PURPUREA) extract; the rejuvenating composition a comprises spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises Chlorella VULGARIS (Chlorella VULGARIS) extract.
By adopting the scheme, the salvia in the repairing composition A is commonly called chia, is a natural carbohydrate bracket, can promote wound healing and protect skin and hair from being polluted, and lactobacillus fermentation products are favorable for cell proliferation, wound healing and anti-inflammatory properties, so that ageing traces are prevented from being generated, excellent wound healing, anti-inflammatory, film forming and anti-irritation effects can be provided, the moisture retention is improved, and the skin is helped to resist various environmental stimulation factors; the various extracts in the soothing composition can improve the moisture content of the skin in real time and long term, improve the expression of aquaporins, effectively clear heat and diminish inflammation, effectively inhibit the degradation of hyaluronic acid caused by inflammation, improve the moisturizing and protecting screens of silk fibroin and sluice protein, smooth phosphorus scraps and roughness of the skin caused by dryness, nourish and moisten the skin, enable the skin to feel smooth and smooth, and solve the problem of drying of internal and external sources of the skin; the synergistic effect of the relieving composition and the repairing composition A is better; the chlorella is matched with the chicory tiraparin, so that the skin can be effectively compacted, deep repair is realized, heavy metals in PM2.5 are adsorbed and complexed, and a stratum corneum barrier is repaired; chicory tiramisu has the effects of instant and long-term tightening and lifting, and long-lasting anti-aging effect, and is plump and wrinkle-removing; according to the skin moisturizing cream, the skin is effectively moisturized by matching the refreshing oil ester with the vegetable oil ester, deep moisturizing is achieved by adding the plant moisturizing composition, the sticky feeling of the formula is degraded, a refreshing and non-greasy system is achieved, various plant extracts are added, the dry skin is repaired, the dry and itchy skin in winter is solved, the skin elasticity is increased, the skin is converged and relaxed, wrinkles are reduced, and the skin moisturizing cream has excellent skin feeling and use feeling.
Preferably, the firming composition A further comprises xanthan gum, sodium benzoate and xanthan gum; said firming composition B further comprises glycerin, sodium benzoate, gluconolactone, and calcium gluconate; the moisturizing composition further comprises glycerin and urea; the soothing composition further comprises glycerin, phenoxyethanol, and ethylhexylglycerin; the repairing composition B also comprises glycerol, ethylhexyl glycerol, 1, 2-pentanediol and 1, 2-hexanediol.
Preferably, the active ingredients of the firming composition A comprise water, xanthan gum, sodium benzoate, hydrolyzed soy protein, acacia (ACACIA SENEGAL) gum and xanthan gum in a mass ratio; the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (Cichorium INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract; the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises 98: 2, spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
In order to solve the technical problems, the invention also provides a moisturizing, firming and repairing cosmetic which comprises the following raw materials in parts by weight:
moisturizing repair composition: 41-93 parts;
humectant: 2.6-15 parts;
antioxidant: 0.16 to 1.8 portions;
thickening agent: 0.16 to 0.85 portion;
chelating agent: 0.01 to 0.1 portion;
emulsifier: 1.6-9 parts;
PH blending agent: 0.01 to 0.5 portion;
preservative: 0.2 to 1 portion.
Preferably, the emulsifier comprises the following raw materials in parts by weight: 0.5 to 3 parts of B12/W12 emulsifier, 0.8 to 3 parts of MONTANOV 68 and 0.3 to 3 parts of cetearyl alcohol.
By adopting the scheme, the liquid crystal emulsifier is used, so that the cream is bright and fine in appearance and fast to absorb, the plant humectant is helped to achieve deep moisture retention, the sticky feeling of the formula is degraded, and a refreshing and non-greasy system is achieved.
Preferably, the humectant comprises the following raw materials in parts by weight: 2 to 8 portions of butanediol, 0.5 to 5 portions of polyglycerol-10 and 0.1 to 2 portions of panthenol.
Preferably, the antioxidant comprises the following raw materials in parts by weight: 0.15 to 0.8 portion of p-hydroxyacetophenone and 0.01 to 1 portion of tocopherol; the thickening agent comprises the following raw materials in parts by weight: 0.08 to 0.45 parts of carbomer and 0.08 to 0.4 parts of xanthan gum; the chelating agent is disodium EDTA.
As a preferred scheme, the feed also comprises the following raw materials in parts by weight:
aromatic agent: 0.001 to 0.1 portion;
nicotinamide: 0.5-5 parts;
and (3) an emollient: 2.3-25 parts;
CBSIL-1028: 0.3 to 4 portions.
Preferably, the emollient comprises the following raw materials in parts by weight: 0.5-6 parts of PMX0345 silicone oil, 0.8-5 parts of CBSIL-1020, 0.5-8 parts of canola oil and 0.5-6 parts of shea butter (Butyrospermum PARKII).
In order to solve the above technical problems, the present invention provides a method for preparing a moisturizing, firming and repairing cosmetic, comprising the steps of:
(1) sequentially adding the humectant, part of the antioxidant, the thickener, the chelating agent and the solvent material into an emulsifying device, heating to 82-85 ℃, and uniformly stirring, dispersing and dissolving to obtain a mixed material A;
(2) sequentially adding the emulsifier, the emollient and part of the antioxidant into oil phase equipment, heating to 82-85 ℃, and uniformly stirring and dissolving to obtain a mixture B;
(3) sucking the mixed material B into an emulsifying device, homogenizing at a high speed, keeping the temperature for 20-30 minutes, and cooling;
(4) pre-mixing and dissolving nicotinamide, a pH regulator and CBSIL-1028 into a C mixed material;
(5) stirring and cooling to 45-50 ℃, adding the mixed material C, and homogenizing at low speed;
(6) stirring and cooling to 38-40 deg.C, adding the moisturizing and repairing composition, antiseptic and aromatic, and stirring to obtain moisturizing and firming repairing cosmetic.
Compared with the prior art, the embodiment of the invention has the following beneficial effects:
according to the skin moisturizing cream, the skin is effectively moisturized by matching the refreshing oil ester with the vegetable oil ester, deep moisturizing is achieved by adding the plant moisturizing composition, the sticky feeling of the formula is degraded, a refreshing and non-greasy system is achieved, various plant extracts are added, the dry skin is repaired, the dry and itchy skin in winter is solved, the skin elasticity is increased, the skin is converged and relaxed, wrinkles are reduced, and the skin moisturizing cream has excellent skin feeling and use feeling.
Drawings
FIG. 1 is a photograph showing the eye state of a moisturizing and tightening repair cosmetic according to a third embodiment of the present invention before use;
FIG. 2 is a photograph showing the eye state of a moisturizing and tightening repair cosmetic used for 2 hours according to a third embodiment of the present invention;
FIG. 3 is a 60-day wrinkle resistance test result of a moisturizing, tightening and repairing cosmetic according to an embodiment of the present invention;
FIG. 4 is a 60-day wrinkle resistance test result of a moisturizing, tightening and repairing cosmetic according to a second embodiment of the present invention;
FIG. 5 is a 60-day anti-wrinkle test result of a moisturizing, tightening and repairing cosmetic according to a third embodiment of the present invention;
FIG. 6-is a 60-day anti-wrinkle test result of a moisturizing, tightening and repairing cosmetic according to a fourth embodiment of the present invention;
FIG. 7-is a 60-day wrinkle resistance test result of one of the moisturizing, tightening and repairing cosmetics according to comparative example one of the present invention;
FIG. 8 is a 60-day anti-wrinkle test result of a moisturizing, tightening and repairing cosmetic according to a second comparative example of the present invention;
fig. 9-is a 60-day anti-wrinkle test result of a moisturizing, tightening and repairing cosmetic in the third embodiment of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
TABLE 1 sources and types of raw materials in preparations, examples and comparative examples of the present application
Preparation example 1
The moisturizing, tightening and repairing composition comprises the following raw material components: firming composition a: 0.1 kg; firming composition B: 0.1 kg; moisturizing composition: 1 kg; soothing composition: 0.1 kg; repairing composition a: 0.1 kg; repairing composition B: 0.1 kg; water: 90.36 kg; wherein, the active ingredients of the firming composition A comprise the following components in a mass ratio of 50.6: 2.5: 0.9: 30: 16 of water, xanthan gum, sodium benzoate, hydrolyzed soy protein and acacia (ACACIA SENEGAL) gum; the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (Cichorium INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract; the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises 98: 2, spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
Preparation example two
The moisturizing, tightening and repairing composition comprises the following raw material components: firming composition a: 0.3 kg; firming composition B: 1 kg; moisturizing composition: 5 kg; soothing composition: 3 kg; repairing composition a: 1 kg; repairing composition B: 0.5 kg; water: 71.83 kg; wherein, the active ingredients of the firming composition A comprise the following components in a mass ratio of 50.6: 2.5: 0.9: 30: 16 water, xanthan gum, sodium benzoate, hydrolyzed soy protein and acacia gum (ACACIA SENEGAL); the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (Cichorium INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract; the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises 98: 2, spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
Preparation example three
The moisturizing, tightening and repairing composition comprises the following raw material components: firming composition a: 1.5 kg; firming composition B: 2 kg; moisturizing composition: 6 kg; soothing composition: 5 kg; repairing composition a: 2 kg; repairing composition B: 2 kg; water: 53.08 kg; wherein, the active ingredients of the firming composition A comprise the following components in a mass ratio of 50.6: 2.5: 0.9: 30: 16 of water, xanthan gum, sodium benzoate, hydrolyzed soy protein and acacia (ACACIA SENEGAL) gum; the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (Cichorium INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract; the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises 98: 2 spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
Preparation example four
The moisturizing, tightening and repairing composition comprises the following raw material components: firming composition a: 3 kg; firming composition B: 5 kg; moisturizing composition: 8 kg; the soothing composition comprises: 8 kg; repairing composition a: 6 kg; repairing composition B: 3 kg; water: 4.65 kg; wherein, the active ingredients of the firming composition A comprise the following components in a mass ratio of 50.6: 2.5: 0.9: 30: 16 of water, xanthan gum, sodium benzoate, hydrolyzed soy protein and acacia (ACACIA SENEGAL) gum; the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerol, sodium benzoate, gluconolactone, calcium gluconate, chicory (Cichorium INTYBUS) root extract and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum; the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract; the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA); the repairing composition A comprises 98: 2, spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product; the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
Example one
The moisturizing, tightening and repairing cosmetic comprises the following raw material components: preparation example one moisturizing firming and repairing composition: 92.16 kg; humectant: 2.6 kg; antioxidant: 0.16 kg; thickening agent: 0.16 kg; chelating agent: 0.01 kg; emulsifier: 1.6 kg; PH blending agent: 0.01 kg; preservative: 0.2 kg; aromatic agent: 0.001 kg; nicotinamide: 0.5 kg; and (3) an emollient: 2.3 kg; CBSIL-1028: 0.3 kg; wherein, the humectant comprises the following components in percentage by mass: 5: 1 butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass: 1 of p-hydroxyacetophenone and tocopherol; the thickening agent comprises the following components in a mass ratio of 1: carbomer and xanthan gum of 1; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass: 8: 3B 12/W12 emulsifier, MONTANOV 68 and cetearyl alcohol; the pH regulator is arginine; the emollient comprises 5: 8: 5: 5 PMX0345 silicone oil, CBSIL-1020, canola oil, and shea butter (Butyrospermum PARKII); the preservative comprises 9 mass percent: 1 phenoxyethanol and ethylhexyl glycerol; the preparation method comprises the following preparation steps:
1. accurately weighing each component material in the formula components, and simultaneously cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum and EDTA disodium panthenol into an emulsifying pot, heating to 82 ℃, stirring, dispersing and dissolving uniformly to obtain a mixed material A;
3. sequentially adding B12/W12 emulsifier, MONTANOV 68, cetostearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and shea butter (Butyrospermum PARKII) into oil phase pan, heating to 82 deg.C, stirring for dissolving to obtain B mixture;
4. and (3) sucking the mixed material B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving the heat for 20 minutes, and cooling.
5. Pre-mixing and dissolving arginine, nicotinamide and CBSIL-1028 to prepare a mixed material C;
6. stirring and cooling to 45 ℃, adding the pre-dissolved C mixed material, and homogenizing at low speed (1500 rpm) for 5 minutes;
7. stirring, cooling to 38 deg.C, adding moisturizing and firming repairing composition, antiseptic and rose flower oil (ROSA RUGOSA), stirring, sampling, detecting, and discharging to obtain moisturizing and repairing cosmetic.
Example two
The moisturizing, tightening and repairing cosmetic comprises the following raw material components: preparation two of the moisturizing firming and repairing composition: 82.63 kg; humectant: 6 kg; antioxidant: 0.5 kg; thickening agent: 0.35 kg; chelating agent: 0.01 kg; emulsifier: 3 kg; PH blending agent: 0.01 kg; preservative: 0.2 kg; aromatic agent: 0.001 kg; nicotinamide: 0.5 kg; and (3) an emollient: 6.5 kg; CBSIL-1028: 0.3 kg; wherein, the humectant comprises 8: 3: 1 butanediol, polyglycerol-10 and panthenol; the antioxidant comprises 4: 1 of p-hydroxyacetophenone and tocopherol; the thickening agent comprises the following components in a mass ratio of 3: 4 carbomer and xanthan gum; the chelating agent is EDTA disodium; the emulsifier comprises the following components in a mass ratio of 1: 1: 1B 12/W12 emulsifier, MONTANOV 68 and cetearyl alcohol; the pH regulator is arginine; the emollient comprises the following components in a mass ratio of 2: 3: 6: 2 PMX0345 silicone oil, CBSIL-1020, canola oil, and shea butter (butysospermum PARKII); the preservative comprises 9 mass percent: 1 of phenoxyethanol and ethylhexylglycerin; the preparation method comprises the following preparation steps:
1. accurately weighing each component material in the formula components, and simultaneously cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum and EDTA disodium panthenol into an emulsifying pot, heating to 85 ℃, and stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. sequentially adding B12/W12 emulsifier, MONTANOV 68, cetostearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and shea butter (Butyrospermum PARKII) into oil phase pan, heating to 85 deg.C, stirring for dissolving to obtain B mixture;
4. and (3) sucking the mixed material B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 30 minutes, and cooling.
5. Pre-mixing and dissolving arginine, nicotinamide and CBSIL-1028 to prepare a mixed material C;
6. stirring and cooling to 50 ℃, adding the pre-dissolved C mixed material, and homogenizing at low speed (1500 rpm) for 5 minutes;
7. cooling to 40 deg.C under stirring, adding moisturizing and firming repairing composition, antiseptic and rose flower oil (ROSA RUGOSA), stirring, sampling, detecting, and discharging to obtain moisturizing and repairing cosmetic.
EXAMPLE III
The moisturizing, tightening and repairing cosmetic comprises the following raw material components: preparation three of moisturizing firming and repairing composition: 71.58 kg; humectant: 8 kg; antioxidant: 0.8 kg; thickening agent: 0.6 kg; chelating agent: 0.01 kg; emulsifier: 5 kg; PH blending agent: 0.01 kg; preservative: 0.2 kg; aromatic agent: 0.001 kg; nicotinamide: 0.5 kg; and (3) an emollient: 13 kg; CBSIL-1028: 0.3 kg; wherein, the humectant comprises the following components in percentage by mass: 2: 1 butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in percentage by mass: 3 p-hydroxyacetophenone and tocopherol; the thickening agent comprises the following components in a mass ratio of 1: carbomer and xanthan gum of 1; the chelating agent is EDTA disodium; the emulsifier comprises the following components in a mass ratio of 3: 4: 3B 12/W12 emulsifier, MONTANOV 68 and cetearyl alcohol; the pH regulator is arginine; the emollient comprises the following components in a mass ratio of 3: 2: 5: 3 PMX0345 silicone oil, CBSIL-1020, canola oil and shea butter (Butyrospermum PARKII); the preservative comprises 9 mass percent: 1 of phenoxyethanol and ethylhexylglycerin; the preparation method comprises the following preparation steps:
1. accurately weighing each component material in the formula components, and cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum and EDTA disodium panthenol into an emulsifying pot, heating to 82 ℃, stirring, dispersing and dissolving uniformly to obtain a mixed material A;
3. sequentially adding B12/W12 emulsifier, MONTANOV 68, cetostearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and shea butter (Butyrospermum PARKII) into oil phase pan, heating to 82 deg.C, stirring for dissolving to obtain B mixture;
4. and (3) sucking the mixed material B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving the heat for 20 minutes, and cooling.
5. Pre-mixing and dissolving arginine, nicotinamide and CBSIL-1028 to prepare a mixed material C;
6. stirring and cooling to 45 ℃, adding the pre-dissolved C mixed material, and homogenizing at low speed (1500 rpm) for 5 minutes;
7. stirring, cooling to 38 deg.C, adding moisturizing and firming repairing composition, antiseptic and rose flower oil (ROSA RUGOSA), stirring, sampling, detecting, and discharging to obtain moisturizing and repairing cosmetic.
Example four
The moisturizing, tightening and repairing cosmetic comprises the following raw material components: preparation four moisturizing & firming compositions: 41.65 kg; humectant: 15 kg; antioxidant: 1.8 kg; thickening agent: 0.85 kg; chelating agent: 0.1 kg; emulsifier: 9 kg; PH blending agent: 0.5 kg; preservative: 1 kg; aromatic agent: 0.1 kg; nicotinamide: 5 kg; and (3) an emollient: 25 kg; CBSIL-1028: 4 kg; wherein, the humectant comprises 8: 5: 2 butanediol, polyglycerol-10 and panthenol; the antioxidant comprises the following components in a mass ratio of 0.8: 1 of p-hydroxyacetophenone and tocopherol; the thickening agent comprises the following components in a mass ratio of 4: carbomer and xanthan gum of 1; the chelating agent is EDTA disodium; the emulsifier comprises the following components in percentage by mass of 1: 1: 1B 12/W12 emulsifier, MONTANOV 68 and cetearyl alcohol; the pH regulator is arginine; the emollient comprises the following components in a mass ratio of 6: 5: 8: 6 PMX0345 silicone oil, CBSIL-1020, canola oil, and shea butter (Butyrospermum PARKII); the preservative comprises 9 mass percent: 1 of phenoxyethanol and ethylhexylglycerin; the preparation method comprises the following preparation steps:
1. accurately weighing each component material in the formula components, and simultaneously cleaning production equipment;
2. sequentially adding water, butanediol, polyglycerol-10, p-hydroxyacetophenone, carbomer, xanthan gum and EDTA disodium panthenol into an emulsifying pot, heating to 85 ℃, and stirring, dispersing and dissolving uniformly to obtain a mixture A;
3. sequentially adding B12/W12 emulsifier, MONTANOV 68, cetostearyl alcohol, PMX0345 silicone oil, tocopherol, CBSIL-1020, canola oil and shea butter (Butyrospermum PARKII) into oil phase pan, heating to 85 deg.C, stirring for dissolving to obtain B mixture;
4. and (3) sucking the mixed material B into an emulsifying pot, homogenizing at a high speed (3000 rpm) for 8 minutes, preserving heat for 30 minutes, and cooling.
5. Pre-mixing and dissolving arginine, nicotinamide and CBSIL-1028 to prepare a mixed material C;
6. stirring and cooling to 50 ℃, adding the pre-dissolved C mixed material, and homogenizing at low speed (1500 rpm) for 5 minutes;
7. stirring and cooling to 40 deg.C, adding moisturizing and firming care composition, antiseptic and flos Rosae Rugosae (ROSA RUGOSA) flower oil, stirring, sampling, detecting, and discharging to obtain moisturizing and repairing cosmetic.
Comparative preparation example 1
The moisturizing, tightening and repairing composition has the same steps, reagents and process parameters as those of the preparation example, and is different from the preparation example in that the skin tightening composition B is replaced by water.
Comparative preparation example 2
The moisturizing and firming repairing composition has the same steps, reagents and process parameters as those of the preparation example, and is different from the preparation example in that the repairing composition B is replaced by water.
Comparative preparation example C
The moisturizing and firming repairing composition has the same steps, reagents and process parameters as those of the preparation examples, and is different from the preparation examples in that the addition amount of each component is as follows: firming composition a: 5 kg; firming composition B: 2 kg; moisturizing composition: 0.5 kg; soothing composition: 5 kg; repairing composition a: 8 kg; repairing composition B: 2 kg; water: 49.08 kg;
comparative example 1
A moisturizing and firming repair cosmetic has the same steps and reagents and process parameters as those of the third embodiment, except that the moisturizing and firming repair composition of the third embodiment is replaced by the one of the first embodiment.
Comparative example No. two
A moisturizing and firming repair cosmetic has the same steps and reagents and process parameters as those of the third embodiment, except that the moisturizing and firming repair composition of the third embodiment is replaced by the moisturizing and firming repair composition of the second embodiment.
Comparative example No. three
A moisturizing and firming repair cosmetic has the same steps and reagents and process parameters as those of the third embodiment, except that the moisturizing and firming repair composition of the third embodiment is replaced by the moisturizing and firming repair composition of the third embodiment.
Performance test
1. Moisturizing effect and skin elasticity test:
1) and (3) testing a sample: cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 of the present application;
2) the test method comprises the following steps: the moisturizing and firming repair cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 were test samples, and 140 (28-55 years old) male and female subjects were randomly divided into 6 groups of 20 subjects, each of which was applied to the facial skin twice a day after cleansing each day, the skin moisture content was measured after 24 hours, the skin moisture content and the skin elasticity were measured with a CK Corneometer CM825 skin moisture tester, and the results after 28 days were collectively scored as shown in table 2.
TABLE 2 moisturizing and elasticity test results of examples 1-4 and comparative examples 1-3
2. Immediate tightening anti-wrinkle test:
1) and (3) testing a sample: moisturizing and firming repair cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 of the present application;
2) the test method comprises the following steps: periocular test the moisturizing and firming repair cosmetics prepared in examples 1 to 4 and comparative examples 1 to 3 were test samples, 140 (40 to 55 years old) male and female subjects were randomly divided into 6 groups of 20 subjects, and the skin around the eyes was applied after cleansing, respectively, and the comparison between before use and after use for 2 hours in example 3 shown in fig. 1 to 2 showed significant wrinkle smoothing effect;
3) and (3) anti-wrinkle test: the examiner applies the moisturizing and firming cream to the face 2 times a day, and observes and records the wrinkle length, the wrinkle depth, the wrinkle number and the wrinkle range after 60 days of the experiment, and the results of the test data are shown in fig. 3 to 9.
According to the detection results of the example 3, the comparative examples 1 to 3 and the fig. 5 and 6 to 9 in the table 2, the components and the addition amount of the moisturizing and repairing composition are specifically selected, so that the components are proper, the efficacy is better exerted, and the prepared cosmetic has higher moisturizing and water locking functions, gives higher elasticity to skin, has the effects of tightening and repairing, and can smooth wrinkles and reduce the generation of wrinkles.
The above-mentioned embodiments are provided to further explain the objects, technical solutions and advantages of the present invention in detail, and it should be understood that the above-mentioned embodiments are only examples of the present invention and are not intended to limit the scope of the present invention. It should be understood that any modifications, equivalents, improvements and the like, which come within the spirit and principle of the invention, may occur to those skilled in the art and are intended to be included within the scope of the invention.
Claims (10)
1. The moisturizing, tightening and repairing composition is characterized by comprising the following raw materials in parts by weight:
firming composition a: 0.1 to 3 portions;
firming composition B: 0.1 to 5 portions;
moisturizing composition: 1-8 parts;
soothing composition: 0.1 to 8 portions;
repairing composition a: 0.1 to 6 portions;
repairing composition B: 0.1 to 3 portions;
water: 4-90 parts;
wherein said firming composition A comprises hydrolyzed soy protein and acacia senegal (ACACIA SENEGAL) gum;
said firming composition B comprises extract of chicory (Cichorium INTYBUS) root and Caesalpinia spinosa (CAESALPINIA SPINOSA) gum;
the moisturizing composition comprises an extract of mycelium of Lentinus EDODES (LENTINUS EDODES);
the soothing composition comprises stem extract of Dendrobium NOBILE (Dendrobium NOBILE), leaf extract of Aloe BARBADENSIS (Aloe BARBADENSIS), root extract of Sophora FLAVESCENS (Sophora FLAVESCENS), fruit extract of Lycium BARBARUM (Lycium BARBARUM) and Echinacea purpurea (ECHINACEA PURPUREA) extract;
the rejuvenating composition a comprises spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product;
said rejuvenating composition B comprises Chlorella (Chlorella VULGARIS) extract.
2. The moisturizing, tightening and repairing composition of claim 1, wherein:
the firming composition A also comprises xanthan gum, sodium benzoate and xanthan gum;
said firming composition B further comprises glycerin, sodium benzoate, gluconolactone, and calcium gluconate;
the moisturizing composition further comprises glycerin and urea;
the soothing composition further comprises glycerin, phenoxyethanol, and ethylhexylglycerin;
the repairing composition B also comprises glycerol, ethylhexyl glycerol, 1, 2-pentanediol and 1, 2-hexanediol.
3. The moisturizing, tightening and repairing composition of claim 2, wherein;
the active ingredients of the firming composition A comprise water, xanthan gum, sodium benzoate, hydrolyzed soybean protein, acacia (ACACIA SENEGAL) gum and xanthan gum in a mass ratio;
the firming composition B comprises the following components in a mass ratio of 32.5: 21.5: 0.25: 0.75: 0.01: 44.93: 0.06 parts of water, glycerin, sodium benzoate, gluconolactone, calcium gluconate, chicory (CICHORIUM INTYBUS) root extract, and tara cloud (CAESALPINIA SPINOSA) gum;
the moisturizing composition comprises 69.5: 25: 5: 0.5 of water, glycerin, urea and shiitake (LENTINUS EDODES) mycelium extract;
the soothing composition comprises 69 by mass: 20: 0.63: 0.07: 4: 2: 2: 1.5: 0.8 parts of water, glycerin, phenoxyethanol, ethylhexylglycerin, stem extract of DENDROBIUM NOBILE (DENDROBIUM NOBILE), leaf extract of ALOE BARBADENSIS (ALOE BARBADENSIS), root extract of SOPHORA FLAVESCENS (SOPHORA FLAVESCENS), fruit extract of LYCIUM BARBARUM (LYCIUM BARBARUM) and extract of echinacea purpurea (ECHINACEA PURPUREA);
the repairing composition A comprises the following components in a mass ratio of 98: 2, spanish sage (SALVIA HISPANICA) seed extract and lactobacillus fermentation product;
the repairing composition B comprises 74.15 mass percent: 5: 0.1: 0.25: 0.25: 20 water, glycerol, ethylhexylglycerol, 1, 2-pentanediol, 1, 2-hexanediol, and CHLORELLA (Chlorella VULGARIS) extract.
4. A moisturizing, tightening and repairing cosmetic characterized by adopting the moisturizing, tightening and repairing composition as claimed in any one of claims 1 to 3, which comprises the following raw materials in parts by weight:
moisturizing repair composition: 41-93 parts;
humectant: 2.6-15 parts;
antioxidant: 0.16 to 1.8 portions;
thickening agent: 0.16 to 0.85 portion;
chelating agent: 0.01 to 0.1 portion;
emulsifier: 1.6-9 parts;
PH blending agent: 0.01 to 0.5 portion;
preservative: 0.2 to 1 portion.
5. The moisturizing, tightening and repairing cosmetic as claimed in claim 4, wherein the emulsifier comprises the following raw materials in parts by weight: 0.5 to 3 parts of B12/W12 emulsifier, 0.8 to 3 parts of MONTANOV 68 and 0.3 to 3 parts of cetearyl alcohol.
6. The moisturizing, tightening and repairing cosmetic as claimed in claim 4, wherein the moisturizing agent comprises the following raw materials in parts by weight: 2 to 8 portions of butanediol, 0.5 to 5 portions of polyglycerol-10 and 0.1 to 2 portions of panthenol.
7. The moisturizing, tightening and repairing cosmetic as claimed in claim 4, wherein the antioxidant comprises the following raw materials in parts by weight: 0.15 to 0.8 portion of p-hydroxyacetophenone and 0.01 to 1 portion of tocopherol; the thickening agent comprises the following raw materials in parts by weight: 0.08 to 0.45 parts of carbomer and 0.08 to 0.4 parts of xanthan gum; the chelating agent is disodium EDTA.
8. The moisturizing, tightening and repairing cosmetic as claimed in claim 4, further comprising the following raw materials in parts by weight:
aromatic agent: 0.001 to 0.1 portion;
nicotinamide: 0.5-5 parts;
and (3) an emollient: 2.3-25 parts;
CBSIL-1028: 0.3 to 4 portions.
9. The moisturizing, tightening and repairing cosmetic as claimed in claim 8, wherein the emollient comprises the following raw materials in parts by weight: 0.5-6 parts of PMX0345 silicone oil, 0.8-5 parts of CBSIL-1020, 0.5-8 parts of canola oil and 0.5-6 parts of shea butter (Butyrospermum parkki I) fruit fat.
10. A method for producing a moisturizing and tightening repair cosmetic as claimed in claim 8 or 9, comprising the steps of:
(1) sequentially adding the humectant, part of the antioxidant, the thickener, the chelating agent and the solvent material into an emulsifying device, heating to 82-85 ℃, and uniformly stirring, dispersing and dissolving to obtain a mixed material A;
(2) sequentially adding the emulsifier, the emollient and part of the antioxidant into oil phase equipment, heating to 82-85 ℃, and uniformly stirring and dissolving to obtain a mixture B;
(3) sucking the mixed material B into an emulsifying device, homogenizing at a high speed, keeping the temperature for 20-30 minutes, and cooling;
(4) pre-mixing and dissolving nicotinamide, a pH regulator and CBSIL-1028 into a C mixed material;
(5) stirring and cooling to 45-50 ℃, adding the mixed material C, and homogenizing at low speed;
(6) stirring and cooling to 38-40 deg.C, adding the moisturizing and repairing composition, antiseptic and aromatic, and stirring to obtain moisturizing and firming repairing cosmetic.
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