CN109199923B - Spray type sleeping mask and preparation method thereof - Google Patents

Spray type sleeping mask and preparation method thereof Download PDF

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CN109199923B
CN109199923B CN201811182192.7A CN201811182192A CN109199923B CN 109199923 B CN109199923 B CN 109199923B CN 201811182192 A CN201811182192 A CN 201811182192A CN 109199923 B CN109199923 B CN 109199923B
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mixture
parts
extract
mask
spray
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CN109199923A (en
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季小洋
董明生
林锦雄
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Guangzhou Aibei Biological Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/046Aerosols; Foams
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/68Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Cosmetics (AREA)

Abstract

The invention discloses a spray-type sleeping mask and a preparation method thereof, belonging to the technical field of cosmetics, wherein an emollient in the mask comprises shea butter, avocado oil, hydrogenated coconut oil, sweet almond oil, isotridecyl and sodium hyaluronate, and has a good moisturizing effect; the active agent in facial mask comprises mixture of wheat ceramide, water/propylene glycol/phytosterol and mixture of hydrogenated polydecene/Dunaliella salina extract, and can improve elasticity of facial skin and supplement water; in addition, the spray type sleeping mask is simple in preparation process, and the prepared mask is good in effect.

Description

Spray type sleeping mask and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a spray type sleep mask and a preparation method thereof.
Background
With the improvement of living standard, people pay more and more attention to the skin care, and especially women pay special attention to facial skin. The cosmetics related to face care in the market comprise a sleep mask and skin lotion, however, the existing sleep mask is mostly in an application type, and the application type mask has some defects: 1) the smearing time is long and the smearing is sticky; 2) it is difficult to quickly enter the facial skin, and the facial skin care effect is limited.
Therefore, there is a need for a new sleeping mask designed to simplify the procedure of using the mask and to improve the maintenance effect of the mask.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide the spray type sleep mask and the preparation method thereof.
In order to achieve the purpose, the invention adopts the technical scheme that: a spray-on sleeping mask comprises emollients including shea butter, avocado oil, hydrogenated coconut oil, sweet almond oil, isotridecane and sodium hyaluronate.
The avocado oil is extracted from avocado fruits by physical squeezing, is rich in omega 9 fatty acid, has the effects of sun screening, moisture retention and skin moistening, and can provide mild moisture and semi-dry skin feeling. The skin moisturizer of the facial mask comprises shea butter, avocado oil, hydrogenated coconut oil, sweet almond oil, isotridecyl and sodium hyaluronate, and the 6 components are compounded in the facial mask to achieve the effect of synergistic skin moisturizing.
As an improvement of the above technical scheme, the spray type sleep mask further comprises an efficacy active agent, wherein the efficacy active agent comprises a mixture of wheat ceramide, water/propylene glycol/phytosterol and a mixture of hydrogenated polydecene/dunaliella salina extract.
Wheat ceramide is a mixture of ceramide and DGDGDG (digalactosyldiglyceride), and is rich in unsaturated fatty acid and natural antioxidant essential for skin; it can fine pores, increase skin moisture retention, strengthen dermis structure, resist oxidation pressure, and provide anti-aging effect. The phytosterols in the water/propylene glycol/phytosterols mixture are extracted from tropical ferns, and can re-compact dermal extracellular matrix, increase epidermal thickness, and rebuild epidermis to make skin plump and smooth. The Dunaliella salina extract in the mixture of hydrogenated polydecene/Dunaliella salina extract is derived from colorless carotenoid of unicellular seaweed, has unique ultraviolet absorption characteristic and hydroxyl free radical capturing characteristic, and has antiaging, antioxidant, free radical capturing, skin whitening and antiinflammatory effects; in addition, the composition can also exert synergistic effect with other active raw materials. The efficacy active agent comprises a mixture of wheat ceramide, water/propylene glycol/phytosterol and a mixture of hydrogenated polydecene/dunaliella salina extract, and the 3 components are compounded in the facial mask to improve the elasticity of facial skin and supplement water.
As an improvement of the technical scheme, the spray type sleeping mask also comprises sodium polystyrene sulfonate. The facial mask disclosed by the invention takes sodium polystyrene sulfonate as a skin firming film forming agent, can form a transparent and elastic film in the facial mask, and shrinks when being dried, so that static electricity is rapidly conducted away; in addition, the film formation has high-temperature stability and can resist the high temperature of more than 300 ℃; it also has a strong anionic nature, helping to reduce surface tension; it has effects in tightening skin and smoothing wrinkles.
As a further improvement of the technical proposal, the spray type sleeping mask also comprises a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer.
The mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer is used as a thickening suspension stabilizer of the mask, and the mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer can obtain high viscosity even under the condition of very low concentration (0.3%); the gel formed by the gel is sensitive to electrolyte, and when the gel is smeared on the skin, the electrolyte on the skin can destroy the network structure of the gel; during this rapid disintegration, the network releases water from the formulation, thereby giving the skin an abnormally fresh, moist feel.
As a further improvement of the above technical scheme, the spray-type sleeping mask further comprises a plant compound anti-allergy agent, wherein the plant compound anti-allergy agent is a mixture of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol.
As a further improvement of the technical scheme, the spray type sleeping mask further comprises bisabolol, tocopherol, an emulsifier, a preservative, a corrosion inhibitor, a pH regulator and purified water.
As a further improvement of the above technical solution, the emulsifier is hydroxylated lecithin, the preservative is a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin, the corrosion inhibitor is a mixture of calcium phosphosilicate/ammonium dihydrogen phosphate, and the pH regulator is triethanolamine.
The preservative in the facial mask is a mild compound preservative which does not contain long-carbon-chain paraben, is lower in addition amount and has broad-spectrum sterilization effect on bacteria, yeasts and molds; it has good gas phase protection effect and is suitable for pH value range up to 8. The corrosion inhibitor for the aerosol can in the mask is a colorless crystal, has small using amount and good effect, and has obvious corrosion inhibition effect.
As a further improvement of the technical scheme, the spray type sleeping mask comprises the following components in parts by weight: 1-10 parts of shea butter, 0.5-3 parts of avocado oil, 1-4 parts of hydrogenated coconut oil, 0.1-0.6 part of bisabolol, 0.1-0.6 part of tocopherol, 1-20 parts of sweet almond oil, 1-20 parts of isotridecane, 1-10 parts of sodium hyaluronate, 1-10 parts of hydroxylated lecithin, 0.1-1 part of wheat ceramide, 0.1-1 part of plant composite anti-allergy agent, 0.1-1.5 parts of a mixture of phenoxyethanol/methyl hydroxybenzoate/ethyl hexyl glycerol, 0.1-1 part of sodium polystyrene sulfonate, 0.2-3 parts of a mixture of water/propylene glycol/phytosterol, 0.3-3 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.1-1 part of a mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate, and 0.1-1 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.1-1 part of triethanolamine and 60-92.1 parts of purified water; the plant composite anti-allergy agent is a mixture of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol.
As a further improvement of the technical scheme, the spray type sleeping mask comprises the following components in parts by weight: 7 parts of shea butter, 1 part of avocado oil, 3 parts of hydrogenated coconut oil, 0.3 part of bisabolol, 0.3 part of tocopherol, 5 parts of sweet almond oil, 5 parts of isotridecyl, 5 parts of sodium hyaluronate, 3 parts of hydroxylated lecithin, 0.2 part of wheat ceramide, 0.3 part of phytocomplex antiallergic agent, 0.5 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.3 part of sodium polystyrene sulfonate, 1 part of a mixture of water/propylene glycol/phytosterol, 1 part of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.4 part of a mixture of calcium sodium phosphosilicate/ammonium dihydrogen phosphate, 0.3 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.3 part of triethanolamine and 66.4 parts of purified water.
In addition, the invention also provides a preparation method of the spray type sleeping mask, which comprises the following steps:
s1) adding shea butter, avocado oil, hydrogenated coconut oil, bisabolol, tocopherol, sweet almond oil, isotridecyl and hydroxylated lecithin into a heating and stirring barrel according to the weight ratio, heating to 70-85 ℃, stirring at the stirring speed of 120 revolutions per minute, and uniformly stirring to obtain an oil phase;
s2) adding a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, sodium polystyrene sulfonate, sodium hyaluronate and purified water into a heating and stirring barrel according to the weight ratio, heating to 80-95 ℃, stirring at the stirring speed of 100 revolutions per minute, and uniformly stirring to obtain a water phase;
s3) adding the oil phase into the water phase, and emulsifying and homogenizing in a homogenizer until emulsification is finished to obtain a mixture I;
s4) adding triethanolamine into the mixture I until the pH value is neutral, and homogenizing for 1-2 minutes; after homogenizing, cooling to 45 ℃, adding a mixture of calcium sodium phosphosilicate and ammonium dihydrogen phosphate, and uniformly stirring to obtain a mixture II;
s5) adding wheat ceramide, a mixture of water/propylene glycol/phytosterol, a mixture of hydrogenated polydecene/Dunaliella salina extract, a mixture of a plant composite anti-allergic agent and a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin into the mixture II, and uniformly stirring; discharging and filling into a spray bottle.
The invention has the beneficial effects that: the invention provides a spray-type sleeping mask and a preparation method thereof, wherein an emollient in the mask comprises shea butter, avocado oil, hydrogenated coconut oil, sweet almond oil, isotridecane and sodium hyaluronate, and has a good moisturizing effect; the active agent in facial mask comprises mixture of wheat ceramide, water/propylene glycol/phytosterol and mixture of hydrogenated polydecene/Dunaliella salina extract, and can improve elasticity of facial skin and supplement water; the plant composite anti-allergy agent contained in the facial mask plays a role in comprehensively repairing and nourishing skin during sleeping; the mask of the invention is of a spray type, and the mask contains a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, so that viscous liquid can be more easily atomized and sprayed; after the face is washed at night, the spray type mask product is used, so that the user can fall asleep, time and labor are saved, and the spray type mask is very suitable for people who want to quickly and conveniently care skin at night; the health care product can be conveniently used by people who often go on a business trip, and the trouble that women take too many health care products when going on a business trip is avoided; in addition, the spray type sleeping mask is simple in preparation process, and the prepared mask is good in effect.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
In the present specification, "mixture of water/propylene glycol/phytosterol" means a mixture of water, propylene glycol and phytosterol, "mixture of hydrogenated polydecene/dunaliella salina extract" means a mixture of hydrogenated polydecene and dunaliella salina extract, "mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer" means a mixture of acrylic acid (ester) and C12-22 alkanol methacrylate copolymer, "mixture of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomilla flower extract/rosemary leaf extract/butylene glycol" means a mixture of centella asiatica extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, and butylene glycol, Mixture of glycyrrhiza glabra root extract, chamomile flower extract, rosemary leaf extract and butylene glycol, "mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin" means mixture of phenoxyethanol, methylparaben, ethylparaben and ethylhexylglycerin, "mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate" means mixture of sodium calcium phosphosilicate and ammonium dihydrogen phosphate.
In the following examples, shea butter is sold under the name Cetiol SB 45, Avocado Oil is sold under the name Avocado Oil, HYDROGENATED COCONUT Oil is sold under the name HYDROGENATED COCONUT OIL, bisabolol is sold under the name Super Sterol Ester, tocopherol is sold under the name FINSOLV TN, and sweet almond Oil is sold under the name Supper Sterol Oil
Figure BDA0001822587670000051
ALM sweet almond oil, isotridecyl oil with the trade name squalane, sodium hyaluronate with the trade name hyaluronic acid, Hydroxylated lecithin with the trade name Hydroxylated lecithin, wheat ceramide with the trade name ceramomOSIDESTMHP, a plant composite ANTI-allergic agent under the trade name ANTI IRRITATION COMPLEX PLUS, and a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin under the trade name ANTI IRRITATION COMPLEX PLUS
Figure BDA0001822587670000052
K350, sodium polystyrene sulfonate tradename
Figure BDA0001822587670000053
II mixture of water/propylene glycol/phytosterols under the trade name
Figure BDA0001822587670000054
(001168), the trade name of the mixture of hydrogenated polydecene/Dunaliella salina extract is IBR-CLC concentrated 0402, the trade name of the mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate is NTD-6A, and the trade name of the mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer is SP-7 thickening suspension stabilizer.
Example 1
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: 7 parts of shea butter, 1 part of avocado oil, 3 parts of hydrogenated coconut oil, 0.3 part of bisabolol, 0.3 part of tocopherol, 5 parts of sweet almond oil, 5 parts of isotridecyl, 5 parts of sodium hyaluronate, 3 parts of hydroxylated lecithin, 0.2 part of wheat ceramide, 0.3 part of phytocomplex antiallergic agent, 0.5 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.3 part of sodium polystyrene sulfonate, 1 part of a mixture of water/propylene glycol/phytosterol, 1 part of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.4 part of a mixture of calcium sodium phosphosilicate/ammonium dihydrogen phosphate, 0.3 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.3 part of triethanolamine and 66.4 parts of purified water.
The embodiment also provides a preparation method of the spray type sleep mask, which comprises the following steps:
s1) adding shea butter, avocado oil, hydrogenated coconut oil, bisabolol, tocopherol, sweet almond oil, isotridecyl and hydroxylated lecithin into a heating and stirring barrel according to the weight ratio, heating to 70-85 ℃, stirring at the stirring speed of 120 revolutions per minute, and uniformly stirring to obtain an oil phase;
s2) adding the mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, sodium polystyrene sulfonate, sodium hyaluronate and purified water into a heating stirring barrel according to the weight ratio, and heating to 80 DEG
Stirring at 95 ℃ to obtain a water phase, wherein the stirring speed is 100 revolutions per minute;
s3) adding the oil phase into the water phase, and emulsifying and homogenizing in a homogenizer until emulsification is finished to obtain a mixture I;
s4) adding triethanolamine into the mixture I until the pH value is neutral, and homogenizing for 1-2 minutes; after homogenizing, cooling to 45 ℃, adding a mixture of calcium sodium phosphosilicate and ammonium dihydrogen phosphate, and uniformly stirring to obtain a mixture II;
s5) adding wheat ceramide, a mixture of water/propylene glycol/phytosterol, a mixture of hydrogenated polydecene/Dunaliella salina extract, a mixture of a plant composite anti-allergic agent and a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin into the mixture II, and uniformly stirring; discharging and filling into a spray bottle.
Example 2
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: 5 parts of shea butter, 0.5 part of avocado oil, 1 part of hydrogenated coconut oil, 0.1 part of bisabolol, 0.1 part of tocopherol, 3 parts of sweet almond oil, 1 part of isotridecyl, 1 part of sodium hyaluronate, 1 part of hydroxylated lecithin, 0.1 part of wheat ceramide, 0.1 part of phytocomplex antiallergic agent, 0.1 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.1 part of sodium polystyrene sulfonate, 0.3 part of a mixture of water/propylene glycol/phytosterols, 0.3 part of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.1 part of a mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate, 0.1 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.1 part of triethanolamine and 86.1 parts of purified water.
This example also provides a method of making the spray sleep mask described above, which is similar to example 1.
Example 3
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: 10 parts of shea butter, 1 part of avocado oil, 3 parts of hydrogenated coconut oil, 0.5 part of bisabolol, 0.5 part of tocopherol, 8 parts of sweet almond oil, 8 parts of isotridecyl, 3 parts of sodium hyaluronate, 4 parts of hydroxylated lecithin, 0.4 part of wheat ceramide, 0.5 part of phytocomplex antiallergic agent, 0.8 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.5 part of sodium polystyrene sulfonate, 2 parts of a mixture of water/propylene glycol/phytosterol, 2 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.5 part of a mixture of calcium phosphosilicate/ammonium dihydrogen phosphate, 0.5 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.5 part of triethanolamine and 0.69.7 part of purified water.
This example also provides a method of making the spray sleep mask described above, which is similar to example 1.
Example 4
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: 5 parts of shea butter, 0.5 part of avocado oil, 2 parts of hydrogenated coconut oil, 0.2 part of bisabolol, 0.2 part of tocopherol, 5 parts of sweet almond oil, 3 parts of isotridecyl, 2 parts of sodium hyaluronate, 1 part of hydroxylated lecithin, 0.1 part of wheat ceramide, 0.2 part of phytocomplex antiallergic agent, 0.5 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.1 part of sodium polystyrene sulfonate, 0.2 part of a mixture of water/propylene glycol/phytosterols, 0.5 part of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.2 part of a mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate, 0.2 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.2 part of triethanolamine and 78.9 parts of purified water.
This example also provides a method of making the spray sleep mask described above, which is similar to example 1.
Example 5
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: 1 part of shea butter, 3 parts of avocado oil, 4 parts of hydrogenated coconut oil, 0.6 part of bisabolol, 0.6 part of tocopherol, 1 part of sweet almond oil, 20 parts of isotridecyl, 5 parts of sodium hyaluronate, 10 parts of hydroxylated lecithin, 1 part of wheat ceramide, 1 part of plant composite anti-allergy agent, 1.1 part of a mixture of phenoxyethanol/methyl hydroxybenzoate/ethylparaben/ethylhexyl glycerol, 0.6 part of sodium polystyrene sulfonate, 2 parts of a mixture of water/propylene glycol/phytosterol, 2 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 1 part of a mixture of calcium phosphosilicate/ammonium dihydrogen phosphate, 1 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.2 part of triethanolamine and 60 parts of purified water.
This example also provides a method of making the spray sleep mask described above, which is similar to example 1.
Example 6
The implementation provides a spray type sleeping mask which is composed of the following components in parts by weight: the composition comprises, by weight, 3 parts of shea butter, 0.6 part of avocado oil, 2.3 parts of hydrogenated coconut oil, 0.4 part of bisabolol, 0.2 part of tocopherol, 20 parts of sweet almond oil, 14 parts of isotridecyl, 10 parts of sodium hyaluronate, 10 parts of hydroxylated lecithin, 0.6 part of wheat ceramide, 0.9 part of phytocomplex antiallergic agent, 1.5 parts of a mixture of phenoxyethanol/methyl hydroxybenzoate/ethylphenyl ethyl ester/ethylhexyl glycerin, 1 part of sodium polystyrene sulfonate, 3 parts of a mixture of water/propylene glycol/phytosterol, 3 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.5 part of a mixture of calcium sodium calcium phosphosilicate/ammonium dihydrogen phosphate, 0.5 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 1 part of triethanolamine and 92.1 parts of purified water.
Effect example 1 bacteriostatic test
Staphylococcus aureus and Escherichia coli are used as test strains, 0.03mol/L phosphate buffer solution is used as a negative control group, and the antibacterial effect test is carried out on the facial mask in the example 1, the market facial mask A (spray type) and the market facial mask B (spread type) according to the QB/T2738-2012 standard; the test results are shown in table 1.
TABLE 1
Figure BDA0001822587670000081
Figure BDA0001822587670000091
As shown in table 1, the mask of example 1 of the present invention has significant inhibitory effects on staphylococcus aureus and escherichia coli, which are similar to the antibacterial effects of the spray-type and spread-type sleep masks in the market.
Effect example 2 moisture and elasticity test
The test method comprises the following steps: 270 female volunteers with mild facial skin aging (dryness, fine lines, elasticity reduction, wrinkles and the like) and no previous skin care cosmetic allergy history are selected, the female volunteers are 28-53 years old, and the female volunteers are randomly divided into 3 groups according to a parallel control principle, and each group comprises 90 persons. Performing a blank test on facial skin of a volunteer 20min after facial cleaning by using a skin moisture tester and a skin elasticity tester at 10 points every night, and determining a blank value; then, using the facial mask for each group of volunteers, carrying out skin moisture and elasticity tests on the volunteers at 5d, 10d, 20d and 40d after the facial mask is used, and calculating the moisture increase rate and the elasticity increase rate; no other skin care products were used during the period; the moisture increase rate and the elasticity increase rate are shown in tables 2 and 3, respectively.
TABLE 2
Figure BDA0001822587670000092
TABLE 3
Figure BDA0001822587670000093
As shown in tables 2 and 3, the mask of example 1 according to the present invention was excellent in increasing the moisture content of the facial skin and improving the elasticity.
Effect example 3 anti-inflammatory and allergy-relieving test
Selecting 150 sensitive skin volunteers (determined by irritation test), wherein the age is 28-53 years, randomly dividing the sensitive skin volunteers into 3 groups, and each group comprises 50 persons; respectively using the mask of the embodiment 1, the market mask A and the market mask B every night; continuously counting the evaluation results after one week; the evaluation results are shown in Table 4. The evaluation criteria for the effects were: and (3) curing: the symptoms of sensitive skin, pruritus, redness, dryness and the like disappear; the method has the following advantages: the symptoms were reduced and the redness of the cheek areas resolved; and (4) invalidation: no obvious change in symptoms.
TABLE 4
Group of Recovery method Is effective Invalidation Effective rate%
Example 1 facial mask 11 33 6 88
Market mask A 8 34 8 84
Market mask B 6 36 8 84
As shown in table 4, the mask of example 1 of the present invention has significant anti-inflammatory and anti-allergy effects, and has a good effect of improving sensitive skin.
The above effect examples only list the test results of embodiment 1 of the present invention, and the facial mask of other embodiments of the present invention can also achieve similar effects. When the spray type mask comprises the following components in parts by weight: 1-10 parts of shea butter, 0.5-3 parts of avocado oil, 1-4 parts of hydrogenated coconut oil, 0.1-0.6 part of bisabolol, 0.1-0.6 part of tocopherol, 1-20 parts of sweet almond oil, 1-20 parts of isotridecane, 1-10 parts of sodium hyaluronate, 1-10 parts of hydroxylated lecithin, 0.1-1 part of wheat ceramide, 0.1-1 part of plant composite anti-allergy agent, 0.1-1.5 parts of a mixture of phenoxyethanol/methyl hydroxybenzoate/ethyl hexyl glycerol, 0.1-1 part of sodium polystyrene sulfonate, 0.2-3 parts of a mixture of water/propylene glycol/phytosterol, 0.3-3 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.1-1 part of a mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate, and 0.1-1 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.1-1 part of triethanolamine and 60-92.1 parts of purified water, wherein the plant composite anti-allergy agent is a mixture of asiatic pennywort herb extract/giant knotweed rhizome extract/baical skullcap root extract/tea extract/glabrous licorice root extract/chamomile flower extract/rosemary leaf extract/butanediol, so that the mask has good skin moistening and repairing effects: increasing skin moisture content, improving skin elasticity, and relieving inflammation and allergy.
Finally, it should be noted that the above embodiments are intended to illustrate the technical solutions of the present invention and not to limit the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications and equivalent substitutions can be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (8)

1. A spray type sleeping mask is characterized by comprising an emollient, an efficacy active agent and sodium polystyrene sulfonate, wherein the emollient comprises shea butter, avocado oil, hydrogenated coconut oil, sweet almond oil, isotridecyl and sodium hyaluronate; the efficacy activator comprises a mixture of wheat ceramide, water/propylene glycol/phytosterols, and a mixture of hydrogenated polydecene/Dunaliella salina extract.
2. The spray sleep mask of claim 1, further comprising a mixture of acrylic/C12-22 alkanol methacrylate copolymers.
3. The spray sleep mask according to claim 1, further comprising a phytocomplex anti-allergic agent which is a mixture of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea leaf extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol.
4. The spray sleep mask according to claim 1, further comprising bisabolol, tocopherol, an emulsifier, a preservative, a corrosion inhibitor, a pH adjuster, and purified water.
5. The spray sleep mask of claim 4, wherein the emulsifier is hydroxylated lecithin, the preservative is a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin, the corrosion inhibitor is a mixture of calcium phosphosilicate/ammonium dihydrogen phosphate, and the pH adjuster is triethanolamine.
6. The spray sleep mask according to claim 1, comprising the following components in parts by weight: 1-10 parts of shea butter, 0.5-3 parts of avocado oil, 1-4 parts of hydrogenated coconut oil, 0.1-0.6 part of bisabolol, 0.1-0.6 part of tocopherol, 1-20 parts of sweet almond oil, 1-20 parts of isotridecane, 1-10 parts of sodium hyaluronate, 1-10 parts of hydroxylated lecithin, 0.1-1 part of wheat ceramide, 0.1-1 part of plant composite anti-allergy agent, 0.1-1.5 parts of a mixture of phenoxyethanol/methyl hydroxybenzoate/ethyl hexyl glycerol, 0.1-1 part of sodium polystyrene sulfonate, 0.2-3 parts of a mixture of water/propylene glycol/phytosterol, 0.3-3 parts of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.1-1 part of a mixture of sodium calcium phosphosilicate/ammonium dihydrogen phosphate, and 0.1-1 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.1-1 part of triethanolamine and 60-92.1 parts of purified water; the plant composite anti-allergy agent is a mixture of centella asiatica extract/polygonum cuspidatum root extract/scutellaria baicalensis root extract/tea extract/glycyrrhiza glabra root extract/chamomile flower extract/rosemary leaf extract/butylene glycol.
7. The spray sleep mask according to claim 6, comprising the following components in parts by weight: 7 parts of shea butter, 1 part of avocado oil, 3 parts of hydrogenated coconut oil, 0.3 part of bisabolol, 0.3 part of tocopherol, 5 parts of sweet almond oil, 5 parts of isotridecyl, 5 parts of sodium hyaluronate, 3 parts of hydroxylated lecithin, 0.2 part of wheat ceramide, 0.3 part of phytocomplex antiallergic agent, 0.5 part of a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexyl glycerol, 0.3 part of sodium polystyrene sulfonate, 1 part of a mixture of water/propylene glycol/phytosterol, 1 part of a mixture of hydrogenated polydecene/dunaliella salina extract, 0.4 part of a mixture of calcium sodium phosphosilicate/ammonium dihydrogen phosphate, 0.3 part of a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, 0.3 part of triethanolamine and 66.4 parts of purified water.
8. The method for preparing a spray type mask pack according to claim 6 or 7, comprising the steps of:
s1) adding shea butter, avocado oil, hydrogenated coconut oil, bisabolol, tocopherol, sweet almond oil, isotridecyl and hydroxylated lecithin into a heating and stirring barrel according to the weight ratio, heating to 70-85 ℃, stirring at the stirring speed of 120 revolutions per minute, and uniformly stirring to obtain an oil phase;
s2) adding a mixture of acrylic acid (ester)/C12-22 alkanol methacrylate copolymer, sodium polystyrene sulfonate, sodium hyaluronate and purified water into a heating and stirring barrel according to a weight ratio, heating to 80-95 ℃, stirring at a stirring speed of 100 revolutions per minute, and uniformly stirring to obtain a water phase;
s3) adding the oil phase into the water phase, and emulsifying and homogenizing in a homogenizer until emulsification is finished to obtain a mixture I;
s4) adding triethanolamine into the mixture I until the pH value is neutral, and homogenizing for 1-2 minutes; after homogenizing, cooling to 45 ℃, adding a mixture of calcium sodium phosphosilicate and ammonium dihydrogen phosphate, and uniformly stirring to obtain a mixture II;
s5) adding wheat ceramide, a mixture of water/propylene glycol/phytosterol, a mixture of hydrogenated polydecene/Dunaliella salina extract, a mixture of a plant composite anti-allergic agent and a mixture of phenoxyethanol/methylparaben/ethylparaben/ethylhexylglycerin into the mixture II, and uniformly stirring; discharging and filling into a spray bottle.
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