CN103976906B - A kind of plant extract liquid mixture with moisturizing antiinflammation - Google Patents
A kind of plant extract liquid mixture with moisturizing antiinflammation Download PDFInfo
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- CN103976906B CN103976906B CN201410235489.0A CN201410235489A CN103976906B CN 103976906 B CN103976906 B CN 103976906B CN 201410235489 A CN201410235489 A CN 201410235489A CN 103976906 B CN103976906 B CN 103976906B
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Abstract
The invention discloses a kind of plant extract liquid mixture with moisturizing antiinflammation; This mixture comprises each component of following weight percent content: Aloe extract 60 ~ 70%, camomile extract 10 ~ 20%, Peony Root extract 5 ~ 10%, peony root extractive 5 ~ 10%, Semen Maydis core extract 5 ~ 10%.The present invention utilize pure natural plant extract prepare to skin easily have problems have comprehensive improvement and conditioning effect, especially have the pure natural compound preparation of moisturizing anti-inflammatory effect concurrently; This compound preparation does not have dense taste of Chinese medicine, and gentle, safety, can be used as functional additive and prepare various skin care item, and then realize the comprehensive and comprehensive of skin care item effect.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, be specifically related to a kind of plant extract liquid mixture with moisturizing antiinflammation.
Background technology
Xerosis cutis, elasticity attenuation not only affect skin appearance, and can cause that consumer is subjective occurs discomfort, and likely cause some dermopathic deterioration.Hydration status in skin and lost degree directly related with the soft and moist of skin and elasticity, keep the moistening degree of skin to strengthen skin elasticity, make skin metabolism normal, reduce the generation of wrinkle and mottle.The cuticular moisture of usual healthy skin remains on 10% ~ 20%.Moisture-keeping efficacy is the most basic function of skin protection cosmetics, and the moisture-keeping efficacy how improving cosmetics is applied all significant to the research and development of cosmetics and clinical medicine.
Wetting agent plays an important role to maintenance moisture of skin and reparation skin barrier function.Existing wetting agent kind is a lot, wherein with glycerol, silicone oil, vaseline, the most common from oil, lanoline, carbamide etc.; The major defect of this kind of wetting agent is that after using, skin often has greasy feeling, and some preparation (as lanoline, carbamide etc.) also has abnormal flavour.Therefore, from plant, find natural moisture preserving agent meet people to the demand coming from natural cosmetics.
In addition, skin, toward the skin problem of contact with other, e.g., is casted off a skin, is itched, eczema, urticaria, comedo, pustule etc., and in actual applications, simple wetting agent is not enough to the skin problem solving these complexity; And a large amount of both effectiveness skin care item occurred on the market, be play effect by adding reactive compound on the basis of moisturizing mostly, not only safety is low for such chemosynthesis composition, and effect is too single; Skin condition cannot be improved by the organizational structure of comprehensive improvement skin comprehensively.Also have in some skin care item and with the addition of Chinese herbal medicine extract, but its majority is folk prescription, is difficult to realize the comprehensive and comprehensive of effect.
Summary of the invention
The object of the invention is to the deficiency overcoming the existence of above-mentioned prior art, a kind of plant extract liquid mixture with moisturizing antiinflammation is provided.The present invention utilize pure natural plant extract prepare to skin easily have problems have comprehensive improvement and conditioning effect, especially have the pure natural compound preparation of moisturizing anti-inflammatory effect concurrently; This compound preparation does not have dense taste of Chinese medicine, and gentle, safety, can be used as functional additive and prepare various skin care item, and then realize the comprehensive and comprehensive of skin care item effect.
The object of the invention is to be achieved through the following technical solutions:
The present invention relates to a kind of plant extract liquid mixture with moisturizing antiinflammation, comprise each component of following weight percent content:
Preferably, the weight sum of described Peony Root extract, peony root extractive, Semen Maydis core extract accounts for the weight percent content of plant extraction liquid mixture total weight is 15 ~ 20%.
Preferably, in described camomile extract, Flos Matricariae chamomillae is the Matricaria recutita of Matricaria.
The invention still further relates to a kind of preparation method of above-mentioned plant extract liquid mixture, described method comprises the steps:
A, respectively Aloe, Flos Matricariae chamomillae dry petal, Peony Root, root of Paeonia suffruticosa Ardr. or Semen Maydis core are pulverized, sieved, add ethanol, 50-100 degree reflux, extract, 4 ~ 8 hours, feed liquid w/v was 1: 5 ~ 50;
B, by extracting liquid filtering, through vacuum concentration to without alcohol taste;
C, concentrated solution obtained for step B is added aqueous dispersion after, upper macroporous resin column or polyamide resin column, be the ethanol water eluting of 30% ~ 45% successively by the water elution of 3 ~ 5 times of column volumes, the volume fraction of 4 ~ 6 times of column volumes, the volume fraction of 3 ~ 5 times of column volumes is the ethanol water eluting of 50% ~ 75%, and the volume fraction of 4 ~ 6 times of column volumes is the ethanol water eluting of 85% ~ 95%;
D, merging eluent, be concentrated into 1/3 ~ 1/6 of original weight amount, obtain each component extract;
E, by each component extract by the mixing of described weight percent content, obtain described plant extract liquid mixture.
Preferably, in steps A, described in sieve into cross 60 ~ 80 mesh sieves.
The invention still further relates to a kind of purposes of above-mentioned plant extract liquid mixture, for the preparation of skin protection cosmetics.
Preferably, described skin protection cosmetics is selected from: preserving moisture and protecting skin cosmetics, have the anti-inflammatory skin protection cosmetics of moisture-keeping efficacy or have the antisenility skin care cosmetics of moisture-keeping efficacy.
Preferably, the dosage form of described skin protection cosmetics is solution, emulsion, suspension, frost, gel, foam or spraying.
Preferably, described plant extract liquid mixture accounts for 20% ~ 40% of skin protection cosmetics gross weight.
In plant extraction liquid design of mixture of the present invention,
Aloe extract: containing Aloe Radix Et Rhizoma Rhei, Saponin, aminoacid and polysaccharide, in cosmetics, primary efficacy is moisturizing lock water, antiinflammatory, promotion wound healing.
Camomile extract: moisturizing, the calm skin restrain pore of releiving; There is refrigerant, to help skin tissue regeneration effect.
Peony Root extract: antiinflammatory, defying age.
Peony root extractive: can produce by T suppression cell free radical, mainly contain the effect such as antiinflammatory, antiallergic.
Semen Maydis core extract: the synthesis promoting ATP, for tired skin injects new energy, resists townie invasion and attack, protection skin, antipollution, anti peroxidation of lipid, antiinflammatory.
Compared with prior art, the present invention has following beneficial effect:
The natural component safety of 1, adding, gentle, effectively, to skin easily occur cast off a skin, itch, the phenomenon such as eczema, comedo, pustule has antiinflammatory opsonic action.
2, by composite use, the antiinflammatory made, moisturizing, Nutrition play comprehensively, also have the auxiliary effects such as foster skin, antiinflammatory, antioxidation, thus play the effect comprehensively improving dry skin problem while skin moistening.
3, not only there is the Symptomatic effect of alleviation, more can play the effect preventing or delay dry skin and occur undesirable condition.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.Following examples will contribute to those skilled in the art and understand the present invention further, but not limit the present invention in any form.It should be pointed out that to those skilled in the art, without departing from the inventive concept of the premise, some distortion and improvement can also be made.These all belong to protection scope of the present invention.
In the present invention, term " Aloe extract " refers to the extract containing effective ingredient extracted from Aloe by any appropriate ways.Term " camomile extract " refers to the extract containing effective ingredient extracted from Flos Matricariae chamomillae by any appropriate ways.Term " Peony Root extract " refers to the extract containing effective ingredient extracted from Peony Root by any appropriate ways.Term " peony root extractive " refers to the extract containing effective ingredient extracted from root of Paeonia suffruticosa Ardr. by any appropriate ways.Term " Semen Maydis core extract " refers to the extract containing effective ingredient extracted from Semen Maydis core by any appropriate ways.
Term " cosmetics " refers to smear, spray or other similar approach, intersperse among any position of human body surface, as: skin, hair, refer to toenail, lips and teeth etc., to reach clean, maintenance, beauty treatment, modify and change outward appearance, or correction human scent, the chemical industrial product for the purpose of maintaining a good state or fine chemical product.According in the preferred embodiment of the present invention, described cosmetics comprise: moisture-keeping cosmetics, have the anti-inflammatory cosmetics of moisture-keeping efficacy or have the anti-aging cosmetics of moisture-keeping efficacy.
embodiment 1
The present embodiment relates to a kind of plant extract liquid mixture with moisturizing antiinflammation, comprises Aloe extract 60%, camomile extract 20%, Peony Root extract 10%, peony root extractive 5%, Semen Maydis core extract 5%.
Its preparation method is specific as follows:
A, respectively the Matricaria recutita dry petal of Aloe, Matricaria, Peony Root, root of Paeonia suffruticosa Ardr. or Semen Maydis core are pulverized, sieved, add ethanol, 80 DEG C of reflux, extract, 6 hours, feed liquid w/v was 1: 30;
B, by extracting liquid filtering, through vacuum concentration to without alcohol taste;
C, concentrated solution obtained for step B is added aqueous dispersion after, upper macroporous resin column or polyamide resin column, be the ethanol water eluting of 40% successively by the water elution of 4 times of column volumes, the volume fraction of 5 times of column volumes, the volume fraction of 4 times of column volumes is the ethanol water eluting of 70%, and the volume fraction of 5 times of column volumes is the ethanol water eluting of 90%;
D, merging eluent, be concentrated into 1/5 of original weight amount, obtain each component extract;
E, by each component extract by the mixing of described weight percent content, obtain described plant extract liquid mixture.
embodiment 2
The present embodiment relates to a kind of plant extract liquid mixture with moisturizing antiinflammation, comprises Aloe extract 65%, camomile extract 15%, Peony Root extract 5%, peony root extractive 5%, Semen Maydis core extract 10%.
Its preparation method is specific as follows:
A, respectively Aloe, Flos Matricariae chamomillae dry petal, Peony Root, root of Paeonia suffruticosa Ardr. or Semen Maydis core are pulverized, sieved, add ethanol, 100 DEG C of reflux, extract, 4 hours, feed liquid w/v was 1: 5;
B, by extracting liquid filtering, through vacuum concentration to without alcohol taste;
C, concentrated solution obtained for step B is added aqueous dispersion after, upper macroporous resin column or polyamide resin column, be the ethanol water eluting of 30% successively by the water elution of 3 times of column volumes, the volume fraction of 6 times of column volumes, the volume fraction of 3 times of column volumes is the ethanol water eluting of 50%, and the volume fraction of 4 times of column volumes is the ethanol water eluting of 85%;
D, merging eluent, be concentrated into 1/6 of original weight amount, obtain each component extract;
E, by each component extract by the mixing of described weight percent content, obtain described plant extract liquid mixture.
embodiment 3
The present embodiment relates to a kind of plant extract liquid mixture with moisturizing antiinflammation, comprises Aloe extract 70%, camomile extract 10%, Peony Root extract 5%, peony root extractive 10%, Semen Maydis core extract 5%.
Its preparation method is specific as follows:
A, respectively Aloe, Anthemis nobilis dry petal, Peony Root, root of Paeonia suffruticosa Ardr. or Semen Maydis core are pulverized, sieved, add ethanol, 50 DEG C of reflux, extract, 8 hours, feed liquid w/v was 1: 50;
B, by extracting liquid filtering, through vacuum concentration to without alcohol taste;
C, concentrated solution obtained for step B is added aqueous dispersion after, upper macroporous resin column or polyamide resin column, be the ethanol water eluting of 45% successively by the water elution of 5 times of column volumes, the volume fraction of 4 times of column volumes, the volume fraction of 5 times of column volumes is the ethanol water eluting of 75%, and the volume fraction of 4 times of column volumes is the ethanol water eluting of 95%;
D, merging eluent, be concentrated into 1/3 of original weight amount, obtain each component extract;
E, by each component extract by the mixing of described weight percent content, obtain described plant extract liquid mixture.
embodiment 4, application
Plant extract liquid mixture of the present invention can be mixed with the skin protection cosmetics of various dosage form with the acceptable adjuvant in skin protection cosmetics field; Wherein, plant extract liquid mixture accounts for 20% ~ 40% of skin protection cosmetics gross weight.The acceptable adjuvant in described skin protection cosmetics field is selected from: solvent, solubilizing agent, antiseptic, antioxidant, pH adjusting agent, penetrating agent, liposome, wetting agent, thickening agent, chelating agen, skinfeel regulator, surfactant, emulsifying agent, propelling/propellant, essence, pigment, and other functional additives.
The present embodiment is for facial cream, and it comprises each component of following weight percent content: the plant extract liquid mixture 40% of embodiment 1, stearic acid 2%, hydrogenated lanolin 2%, octadecanol 6%, squalane 6%, octyl dodecanol 7%, polyoxyethylene hexadecanol ether 2%, lipophile tristerin 1%, glycerol 3%, 1,3 one butanediols 2%, essence, antiseptic, antioxidant are appropriate, and surplus is deionization; Stir discharging, obtained facial cream.
Cutaneous safety assessment is carried out to obtained facial cream:
Participate in the personnel of test by subject enrollment Standard Selection 30,15 male, 15 women, the mean age is 31 years old.Tested material is put into speckle examination device, consumption is about 0.020g ~ 0.025g.Control wells is blank (not placing any material), the speckle being added with tested material is tried device is overlying on experimenter back with non-stimulated tape sticker, gently presses and make it to be covered on skin uniformly, continue 24h with palm.30min after removal speckle examination device, observes dermoreaction, divides untoward reaction grade by skin adverse reaction grade scale table after impression disappears.If result is negative, after patch test, 24h and 48h observes once respectively again.Result is as shown in table 1:
Table 1
| Test substances | Average response degree | Grade |
| Facial cream | 0 | Non-stimulated |
As shown in Table 1, the facial cream that the present embodiment is obtained, does not produce stimulation to skin.Therefore known, the skin protection cosmetics that plant extract liquid mixture of the present invention obtains is safe to skin.
embodiment 5, moisture-keeping efficacy are verified
With Aloe extract obtained in embodiment 1 as a comparison case, using the plant extract liquid mixture in embodiment 1,2,3 as experimental group, compare moisture content value (MMV) before and after the two effect and to scatter and disappear value (TEWL) through transepidermal water.
It is comparatively commonly use and generally acknowledge the moistening effect evaluation methodology that degree is the highest that moisture-keeping efficacy is evaluated in human trial.Therefore, the present embodiment adopts human trial to evaluate moisture-keeping efficacy.Concrete process of the test is as follows:
1) select the left and right inboard arm of experimenter apart from palm base portion 5cm place, define the identical conduct use region, region (4cm × 4cm) of 2 areas at left forearm; The point of right forearm same position is as blank region, and the corresponding region of left and right arm is tested simultaneously.
2) experimenter smears Aloe extract and plant extract liquid mixture respectively at two pilot regions of arm.After smearing 1,2,4,6,8h, moisture of skin measuring instrument CorneometerCM825 (German CourageKhazaka company) is used to test the hydration status of skin, percutaneous moisture loss measuring instrument TewameterTM300 (German CourageKhazaka company) is adopted to test the water loss amount of skin, measure 5 times, average.
Blank group is the meansigma methods of 5 hydration status relative value and the moisture loss value recorded in the 0h moment.Result is as shown in following table 2,3:
Table 2 skin hydration state verification result
Table 3 moisture of skin scatters and disappears test result
From comparing of embodiment in table 2 and comparative example, in plant extract liquid mixture of the present invention each component composite can significantly promote use after skin hydration state, there is obvious moistening effect.From comparing of embodiment in table 3 and comparative example, in plant extract liquid mixture of the present invention each component composite can significantly promote use after skin barrier function, reduce moisture of skin and scatter and disappear, there is excellent lock water effect.
embodiment 6, anti-inflammatory efficacy are verified
With Aloe extract group as a comparison obtained in embodiment 1, using the plant extract liquid mixture in embodiment 1,2,3 as experimental group, compare the anti-inflammatory efficacy of the two.Detailed process is as follows:
Kunming male mice 40, body weight 30 ± 2g, is divided into 5 groups at random.With cotton swab pick drug study group, the medicinal liquid of each 20 μ L of contrast groups is spread evenly across two sides before and after every mouse right ear, left ear normal saline is coated with in the same way, then pick about 100% dimethylbenzene 20 μ L with cotton swab and coat two sides before and after every mouse right ear evenly and rapidly, record every mice coating and sensitization time, and respectively at cause scorching after 0.5,1.5,2.5h repeated drug taking, left ear normal saline concurrent control.Cause scorching rear 4h by animal sacrificed by decapitation, cut two ears along auricle baseline, two ear 6mm diameter trepan devices are laid auricle and weighs, and measure the thickness of bilateral auricle with micrometer caliper, the difference of every Mus two auricle weight is swelling, and the thickness difference of bilateral auricle is that thickness is looked into.
Table 4
From comparing of embodiment in table 4 and contrast groups, in plant extract liquid mixture of the present invention, each component is composite significantly can promote anti-inflammatory efficacy.
Above specific embodiments of the invention are described.It is to be appreciated that the present invention is not limited to above-mentioned particular implementation, those skilled in the art can make various distortion or amendment within the scope of the claims, and this does not affect flesh and blood of the present invention.
Claims (8)
1. there is a plant extract liquid mixture for moisturizing antiinflammation, it is characterized in that, comprise each component of following weight percent content:
The weight percent content that the weight sum of described Peony Root extract, peony root extractive, Semen Maydis core extract accounts for plant extraction liquid mixture total weight is 15 ~ 20%.
2. the plant extract liquid mixture with moisturizing antiinflammation according to claim 1, is characterized in that, in described camomile extract, Flos Matricariae chamomillae is the Matricaria recutita of Matricaria.
3. a preparation method with the plant extract liquid mixture of moisturizing antiinflammation according to claim 1, it is characterized in that, described method comprises the steps:
A, respectively Aloe, Flos Matricariae chamomillae dry petal, Peony Root, root of Paeonia suffruticosa Ardr. and Semen Maydis core are pulverized, sieved, add ethanol, 50 ~ 100 DEG C of reflux, extract, 4 ~ 8 hours, feed liquid w/v was 1:5 ~ 50;
B, by extracting liquid filtering, through vacuum concentration to without alcohol taste;
C, concentrated solution obtained for step B is added aqueous dispersion after, upper macroporous resin column or polyamide resin column, be the ethanol water eluting of 30% ~ 45% successively by the water elution of 3 ~ 5 times of column volumes, the volume fraction of 4 ~ 6 times of column volumes, the volume fraction of 3 ~ 5 times of column volumes is the ethanol water eluting of 50% ~ 75%, and the volume fraction of 4 ~ 6 times of column volumes is the ethanol water eluting of 85% ~ 95%;
D, merging eluent, be concentrated into 1/3 ~ 1/6 of original weight amount, obtain each component extract;
E, by each component extract by the mixing of described weight percent content, obtain described plant extract liquid mixture.
4. the preparation method with the plant extract liquid mixture of moisturizing antiinflammation according to claim 3, is characterized in that, in steps A, described in sieve into cross 60 ~ 80 mesh sieves.
5. a purposes for plant extract liquid mixture according to claim 1, is characterized in that, described plant extract liquid mixture is for the preparation of skin protection cosmetics.
6. purposes according to claim 5, is characterized in that, described skin protection cosmetics is selected from: preserving moisture and protecting skin cosmetics, have the anti-inflammatory skin protection cosmetics of moisture-keeping efficacy or have the antisenility skin care cosmetics of moisture-keeping efficacy.
7. purposes according to claim 5, is characterized in that, the dosage form of described skin protection cosmetics is solution, emulsion, suspension, frost, gel, foam or spraying.
8. purposes according to claim 5, is characterized in that, described plant extract liquid mixture accounts for 20% ~ 40% of skin protection cosmetics gross weight.
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| CN104644500B (en) * | 2015-01-30 | 2018-05-11 | 广州澳医生物科技有限公司 | A kind of plant moisturizing composition and preparation method thereof |
| CN105796462A (en) * | 2016-03-25 | 2016-07-27 | 无锡简玺生物科技有限公司 | Composition used for cleaning skin and preparation method thereof |
| CN106420596B (en) * | 2016-11-30 | 2019-03-29 | 广东芭薇生物科技股份有限公司 | A kind of composition of the extract containing corn kernel and its application |
| CN106667849A (en) * | 2017-01-04 | 2017-05-17 | 广州聚澜健康产业研究院有限公司 | Radiation-proof plant composition |
| CN107137305A (en) * | 2017-05-02 | 2017-09-08 | 韩后化妆品股份有限公司 | Composition and its application with moisturizing and sensitiveness skin therapeutic action |
| CN107550815A (en) * | 2017-09-18 | 2018-01-09 | 上海家化联合股份有限公司 | A kind of maize seed extract and its application in skin preparations for extenal use |
| CN107714589A (en) * | 2017-11-27 | 2018-02-23 | 任超 | A kind of preserving moisture and protecting skin emulsion and preparation method thereof |
| CN110547983A (en) * | 2018-05-31 | 2019-12-10 | 上海黛兰娜实业有限公司 | Composition for deeply cleaning pores and method for deeply cleaning pores |
| CN109010173A (en) * | 2018-09-06 | 2018-12-18 | 王国香 | A kind of multi-functional skin care is spraying and preparation method thereof |
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| CN101297878A (en) * | 2008-06-13 | 2008-11-05 | 宁波立华制药有限公司 | Preparation technique of high-content white peony root effective composition |
| CN102166176B (en) * | 2011-04-08 | 2012-11-21 | 清华大学 | Corn germ oil nano emulsion and preparation method thereof |
| CN102988261B (en) * | 2012-12-14 | 2014-07-09 | 北海黑珍珠海洋生物科技有限公司 | Facial mask solution and preparation method thereof |
| CN103070803B (en) * | 2013-01-25 | 2016-01-27 | 金红叶纸业集团有限公司 | Moisture-keeping composition and apply its napkin |
| CN103230357B (en) * | 2013-05-08 | 2015-04-22 | 苏州谷力生物科技有限公司 | Antiallergic moisturizing composition and external preparation thereof |
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