CN109010173A - A kind of multi-functional skin care is spraying and preparation method thereof - Google Patents
A kind of multi-functional skin care is spraying and preparation method thereof Download PDFInfo
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- CN109010173A CN109010173A CN201811035284.2A CN201811035284A CN109010173A CN 109010173 A CN109010173 A CN 109010173A CN 201811035284 A CN201811035284 A CN 201811035284A CN 109010173 A CN109010173 A CN 109010173A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
Spraying and preparation method thereof the invention discloses a kind of multi-functional skin care, skin care is spraying, Chinese medicine extract, the miscella of 6-12% and the rice wine liquid of surplus for being 22-31% including quality accounting；Raw material of the Chinese medicine extract and including folium cortex eucommiae, the Japanese ardisia, Sophora alopecuroide, Moso Bamboo Leaves, witch hazel, iris, Radix Paeoniae Alba, pomegranate seed, Schisandra chinensis, viola mandshurica, cordate houttuynia and lemongrass；The raw material of the miscella include odd sub- seed oil, perilla herb oil, rice bran oil, grape seed oil and tea oil.The present invention is customized for the skin conditions of man, and has both antibacterial, anti-inflammatory, oil-control, anti-oxidant and sun-proof, meets man to the basic maintenance demand of skin.
Description
Technical field
The present invention relates to filed of daily-use chemical industry, and in particular to a kind of multi-functional skin care is spraying and preparation method thereof.
Background technique
Some researches show that the skin of man and the skin of Ms have following difference:
1, the secretion of male is more vigorous, and pore is coarse, is oiliness mostly, and the secretion of women is few, pore
Exquisiteness, the easy pollutant of skin more than grease, especially fat-soluble organic substance and perhaps multiple-microorganism are put aside, and induce inflammation and
Infection；
2, male's hair is more, and pore is big, and bacterium, fungi, virus etc. can drive straight in, and causes infection, women hair is few, pore
Small, infection chance is accordingly few；
3, male has the habit to shave, is easy to scratch skin, so that the skin of male is easier to infection inflammation.
Above situation show due on skin texture, physiologically, men and women has nothing in common with each other.In skin care, Nan Nvying
When emphasizing particularly on different fields a little.
But present skin care item market main services women, it is rare for the skin care item of man, and effect has a single function,
The daily demand of man cannot be met comprehensively.
Summary of the invention
In view of the above technical problems, spraying and preparation method thereof the present invention provides a kind of multi-functional skin care, it is directed to
The skin conditions of man customize, and have both antibacterial, anti-inflammatory, oil-control, the anti-oxidant and functions such as sun-proof, meet man to the base of skin
This maintenance demand.
The present invention solves technical solution used by the technical problem: a kind of multi-functional skin care is spraying, including quality
Accounting is Chinese medicine extract, the miscella of 6-12% and the rice wine liquid of surplus of 22-31%；
The raw material and its mass fraction of the Chinese medicine extract include 8-13 parts of folium cortex eucommiae, Japanese ardisia 7-11 parts, bitter beans
7-11 parts sub-, 5-10 parts of Moso Bamboo Leaves, 5-10 parts of witch hazel, 4-9 parts of iris, 3-6 parts of Radix Paeoniae Alba, 3-6 parts of pomegranate seed, Schisandra chinensis 3-6
Part, 3-6 parts of viola mandshurica, 1-3 parts of cordate houttuynia and 1-3 parts of lemongrass；
The Chinese medicine extract is prepared by the following method: water steaming is carried out after the raw material of the Chinese medicine extract are crushed
Steam distillation, extraction obtain grease blend, aqueous after centrifugation, the as described Chinese medicine extract；
The raw material and its mass fraction of the miscella include odd sub- 1-3 parts of seed oil, 1-3 parts of perilla herb oil, rice bran oil 1-3
Part, 1-3 parts of grape seed oil and 8-16 parts of tea oil.
Compared with prior art, the present invention has following technical effect that
1, Chinese medicine extract of the invention is rich in antibiotic effective ingredient, anti-inflammatory effective component, oil-control effective component and antioxygen
Change effective component, for the effective component in Chinese medicine extract, or is suitble to deposit in oil or is suitble to deposit in the spy of ethanol solution
Property, the present invention rocks Chinese medicine extract, oil and wine three mixing, used time uniformly again, and it is long-term to store, persistently effectively.Nothing
Preservative need to be in addition added, natural safety.
2, Chinese medicine extract of the invention is compounded by plurality of Chinese raw material, common distillation gained so that antimicrobial component and
Anti-inflammation components are not single, can successfully manage diversified skin infection, really play comprehensively antibacterial anti-inflammatory protecting effect.
3, the preparation method of Chinese medicine extract of the invention refers to the preparation of hydrosol.Hydrosol is also known as crystal's oil
(Hydrolate), refer to essential oil during distillation extraction, the steaming that the one kind 100% separated when refining essential oil is saturated
Stoste is evaporated, is a kind of byproduct of essential oil, composition is naturally pure, and fragrance is light pleasant.Hydrosol is exactly fragrant plant distillation gained
Condensation aqueous solution.Grease can separate during distillation extraction, and because of density difference, essential oil can be swum in above, and moisture then sinks
It forms sediment below, these moisture are just hydrosol.It is also intracorporal containing whole plants in hydrosol other than containing a small amount of derived essential oil
Water-soluble substances.Possess the hydrosol of 100% plant water-soluble substance, contained mineral nutrients (such as tannic acid and flavonoids) are essences
What oil was lacked.Chinese medicine extract of the invention is to obtain after Chinese medicine raw material crush by distillation, distills the oil of acquisition
And moisture, present invention water intaking point while oil contains mass efficient substance, also contain more oil soluble impurities, or even also
The drug molecule of irritating skin, therefore, the present invention take the obtained aqueous solution of distillation, aqueous solution have it is more it is effective at
Point, containing most aqueous soluble active constituent and fraction oil-soluble effective component, and relatively pure oil is more mild, is applicable in
In skin.
4, grape seed oil of the invention contains grape pip glucosidase procyanidins, can protect the oryzanol in rice bran oil, ties up
Raw element E and squalene, and grape pip glucosidase procyanidins itself are also mildly inirritative antioxidant content, and grape seed oil
Itself also vitamin E rich in.Under synergistic effect, grape seed oil and rice bran oil have stronger anti-oxidant and sun-proof function
Effect.
5, miscella main body of the invention is tea oil, good with the compatibility of skin, is easy to skin absorption, is ideal skin care
Solvent is also generally seen on the market.But present invention discover that the tea oil of purity is high is inflammable volatile, and tea oil is in thick, grain
Diameter is big, and medium bad dispersibility influences absorption of human body.Therefore, the present invention is added a variety of with anti-oxidant by the way of miscella
Property it is high, with the good oil product of tea oil harmony, generate compounding effect.Sticky sense is reduced, more clearly, is more suitable for man's use.
Specifically, the rice wine liquid is the black rice wine of 17-22%VOL.The present invention uses black rice wine, on the one hand can dissolve portion
Divide miscella and most Chinese medicine extract, convenient for storage and uses；On the other hand, black rice wine vinosity fragrance glycol, as
Spray can also replace cologne while skin care.Furthermore the present invention takes its natural colorants, and the solution of black, image is special,
It is easy to get the favor of man.
Further, further include 0.5-1% benzophenone-3 and/or 0.5-1% lignocaine oxybenzene formylbenzoate
Own ester.Enhance sun-proof result of the invention, in conjunction with rice bran oil, resists ultraviolet light comprehensively.
In order to solve the above technical problems, The present invention provides another technical solutions: a kind of multi-functional skin care is spraying
Preparation method, its step are as follows:
1) prepare Chinese medicine extract: take raw material include 8-13 parts of folium cortex eucommiae, Japanese ardisia 7-11 parts, 7-11 parts of Sophora alopecuroide,
It is 5-10 parts of Moso Bamboo Leaves, 5-10 parts of witch hazel, 4-9 parts of iris, 3-6 parts of Radix Paeoniae Alba, 3-6 parts of pomegranate seed, 3-6 parts of Schisandra chinensis, pale reddish brown
3-6 parts of fourth, 1-3 parts of cordate houttuynia and 1-3 parts of lemongrass crush, are then placed in steam distillation equipment and carry out steam distillation, mention
Grease blend is obtained, aqueous after centrifugation, the as described Chinese medicine extract, the number is mass fraction；
2) prepare miscella: taking raw material includes odd sub- 1-3 parts of seed oil, 1-3 parts of perilla herb oil, 1-3 parts of rice bran oil, grape pip
Oily 1-3 parts and 8-16 parts of tea oil, it is uniformly mixed to obtain the miscella, the number is mass fraction；
3) prepare shin moisturizer: according to the mass percent meter of the shin moisturizer, take 22-31% the Chinese medicine extract,
The miscella of 6-12% and the rice wine liquid of surplus, mixing, homogeneous obtain the shin moisturizer；
4) by the shin moisturizer packing fill into spray bottle, both the multi-functional skin care be sprayed.
Compared with prior art, the present invention has following technical effect that the spraying preparation of multi-functional skin care of the invention
Method, is disinclined to the psychology of skin care for man, the present invention collect antibacterial, anti-inflammatory, oil-control, anti-aging and after-sun recovery multiple efficacies in
One, so that the simpler convenience of the skin care of man, and presented by the way of spraying, and provide one kind just for man's skin care
Benefit does not need to smear on the whole so that skin care process is equally unsophisticated similar to hair spray, while misty dosage form reduction is sticky
Sense, it is salubrious natural.
Specifically, the odd sub- seed oil is prepared by the following method, and its step are as follows:
S11, the sub- seed of the surprise for being 15% by moisture content are placed in the heating tank of Ohmic heating device and heat, and heating temperature is
90 DEG C, heating time 20min, the sub- seed of the surprise cured；
S12, the sub- seed of the surprise of curing is obtained into odd sub- seed crude oil, 120 DEG C of squeeze pressure 40MPa, pressing temperature by squeezing；
S13, the atlapulgite that its quality 3% is added to odd sub- seed crude oil, in the case where temperature is 105 DEG C, pressure is 2.5kPa
30min is handled, for refining removal of impurities, obtains odd sub- seed oil.
The present invention is heated for the Ohmic heating device in CN 203691647U by odd sub- seed frying one using Authorization Notice No.
Fixed ripe degree destroys odd sub- seed cell, makes the protein water swelling in odd sub- seed cell, and protein sufficiently solidifies denaturation and becomes
Firmly, the small oil droplet coalescence of dispersion is conducive to the extraction separation of grease, and protein denaturation is more thorough, and squeezing oil yield is higher.It mentions
The high recovery rate of odd sub- seed oil, and the odd sub- seed of gained it is oily in Omega-3 content of fatty acid up to 18%.
Specifically, the perilla herb oil is prepared by the following method, and its step are as follows:
S21, purple perilla is dried, controls moisture content 3%；
S22, it the purple perilla benevolence dried is put into -25 DEG C of household freezer freezes 9h, taking-up is placed in -10 DEG C of vacuum environment
8h, then takes out to be placed in 60 DEG C of vacuum environments and is dried 7h；
S23, the purple perilla benevolence obtained after step S22 processing is crushed, is sieved with 40 mesh sieve；
S24, the purple perilla benevolence powder obtained after step S23 processing is passed through into CO2Supercritical extract, fluid extraction pressure are
45MPa, 45 DEG C of extraction temperature, CO2Fluid flow is 1100L/h, and extraction time 100min obtains purple perilla crude oil；
S25, the purple perilla crude oil obtained after step S24 processing is removed into lipoxygenase by hyperfiltration, selects retention
The hyperfiltration film of molecular weight 120kD.
The perilla herb oil that the present invention uses refines for pure physical method, remains the distinctive Flavonoid substances of purple perilla and vitamin
E isoreactivity substance, no solvent residue, pollution-free, safety is good, oil quality is high.Moreover, using Lyophilisation technique for making,
It crushes complete.Furthermore utilize CO2Supercritical extraction technique, so that organic solvent-free remains in product, and vitamin E etc. damages
It loses few.Secondly, this utilizes ultra micro membrane filtration technique, eliminates in perilla herb oil storage process and cause rotten biological factor；Perilla herb oil
In oxygenase, be sprayed in use process in skin care of the invention, will not generate aldehyde ketone etc. makes the smell substance of purple perilla deterioration of oil.
Specifically, the rice bran oil is prepared by the following method, and its step are as follows:
S31, rice bran cross 40 meshes, dry 5 days；
S32, it takes the rice bran after sunning to be packed into extraction kettle, passes through supercritical CO2Extraction equipment extracts Rice bran crude oil stage by stage,
To CO28% wet basis ethyl alcohol is added in fluid as entrainer, setting extraction conditions I is 15MPa, 30 DEG C, extracts 1.0h, separation
Obtain Rice bran crude oil I；Increasing temperature and pressure is 35MPa, 40 DEG C to condition II, continues to extract 4h, isolated Rice bran crude oil II, mixing
Rice bran crude oil I and Rice bran crude oil II, obtains Rice bran crude oil；
S33, it takes Rice bran crude oil in centrifuge tube, is rapidly added the diethanol amine of oily weight 11%, in 55 DEG C of constant temperature oscillation boxes
Middle effect 25min, revolving speed 100rpm are then centrifuged for 30min, and revolving speed 3000rpm separates oily phase, with oily 10% deionized water of weight
Washing oil is mutually secondary, both obtains rice bran oil after dry.
The rice bran oil that the present invention uses is supercritical CO2It, can be by free fatty acid (FFA), wax obtained by stage extraction method
Matter etc. concentrates on low-temp low-pressure area, and the nutriments such as neutral grease, sterol and oryzanol are concentrated on high temperature and pressure area, thus
Make that later period grease coloration is shallow, acid value is low, nutriment is with high purity.Hair oil extracted from rice husks is refined with diethanol amine, depickling can be reached simultaneously
The effect of degumming decoloration, and diethanol amine will not be saponified neutral oil, influence on oryzanol small.
Specifically, the grape seed oil is prepared by the following method, and its step are as follows:
S41, grape pip is crushed to granularity 0.1mm, adjustment moisture to water content 25% heats, and temperature maintains 85-90
DEG C 40min, then add the cellulase of the grape pip weight 3 ‰, 1 ‰ hemicellulase, 0.5 ‰ protease,
0.2 ‰ α-polygalacturonic enzyme and the 0.3 ‰ poly- glucose enzyme of β-digest 2h, and 55 DEG C of hydrolysis temperature；
Grape pip after S42, microwave treatment enzymatic hydrolysis, microwave power 300W are handled 3 times, and then each 20min is heated, temperature
Degree maintains 85-90 DEG C of 40min, dry to water content 6%, squeezes under conditions of temperature≤50 DEG C and grape pip crude oil is made,
S43, alkali refining is carried out to the grape pip crude oil: caustic dosage is the 0.08% of the grape pip crude oil, alkali refining initial temperature
50 DEG C, 80 DEG C of final temperature, mixing speed 70r/min；
S44, aquation is carried out to the grape pip crude oil: aquation amount of water is 15%, and beginning mixing speed is 55r/min,
Oil temperature is 60 DEG C when adding water, and final temperature is controlled at 80-85 DEG C, quiescent setting 6h or so, makes water-oil separating, the grape seed oil after separation
Dehydration；
S45, decolourize to the grape pip crude oil: decolorising agent is carclazyte and active carbon, carclazyte and activated carbon weight ratio
Example is 5: 1, and decolorising agent dosage is the 3% of the quality of the grape pip crude oil, and operating pressure 0.8MPa, temperature is 70 DEG C, is taken off
The color time is 50min；Oil temperature is set to be quickly cooled to 40 DEG C hereinafter, obtaining refining grape seed oil after filtering after the completion of decoloration.
The grape seed oil that the present invention uses is prepared using above method, and oil cut rate is up to 95% or more, procyanidine recovery rate
Up to 60% or more.Below with reference to embodiment, the invention will be further described.
Specific embodiment
Embodiment one
The sub- seed oil of the surprise of embodiment one is prepared by the following method, and its step are as follows:
S11, the sub- seed of the surprise for being 15% by moisture content are placed in the heating tank of Ohmic heating device and heat, and heating temperature is
90 DEG C, heating time 20min, the sub- seed of the surprise cured；
S12, the sub- seed of the surprise of curing is obtained into odd sub- seed crude oil, 120 DEG C of squeeze pressure 40MPa, pressing temperature by squeezing；
S13, the atlapulgite that its quality 3% is added to odd sub- seed crude oil, in the case where temperature is 105 DEG C, pressure is 2.5kPa
30min is handled, for refining removal of impurities, obtains the sub- seed oil of surprise of embodiment one.
Wherein, the Ohmic heating device uses Authorization Notice No. for the Ohmic heating device in CN 203691647U,
It is made of heating device and circuit control system, heating device includes heating tank (being welded by polypropylene board), pole plate (titanium
Plate), thermocouple (temperature-sensitive part applies insulation dipping lacquer, and outer cover teflon sleeve, interface welds with polytetrafluoroethylene (PTFE)), electricity
Path control system (by auto-transformer, circuit control box and temperature controller) forms.
Embodiment two
The perilla herb oil of embodiment two is prepared by the following method, and its step are as follows:
S21, purple perilla is dried, controls moisture content 3%；
S22, it the purple perilla benevolence dried is put into -25 DEG C of household freezer freezes 9h, taking-up is placed in -10 DEG C of vacuum environment
8h, then takes out to be placed in 60 DEG C of vacuum environments and is dried 7h；
S23, the purple perilla benevolence obtained after step S22 processing is crushed, is sieved with 40 mesh sieve；
S24, the purple perilla benevolence powder obtained after step S23 processing is passed through into CO2Supercritical extract, fluid extraction pressure are
45MPa, 45 DEG C of extraction temperature, CO2Fluid flow is 1100L/h, and extraction time 100min obtains purple perilla crude oil；
S25, the purple perilla crude oil obtained after step S24 processing is removed into lipoxygenase by hyperfiltration, selects retention
The hyperfiltration film of molecular weight 120kD obtains the perilla herb oil of embodiment two by collecting after hyperfiltration.
Embodiment three
The rice bran oil of embodiment three is prepared by the following method, and its step are as follows:
S31, rice bran cross 40 meshes, dry 5 days；
S32, it takes the rice bran after sunning to be packed into extraction kettle, passes through supercritical CO2Extraction equipment extracts Rice bran crude oil stage by stage,
To CO28% wet basis ethyl alcohol is added in fluid as entrainer, setting extraction conditions I is 15MPa, 30 DEG C, extracts 1.0h, separation
Obtain Rice bran crude oil I；Increasing temperature and pressure is 35MPa, 40 DEG C to condition II, continues to extract 4h, isolated Rice bran crude oil II, mixing
Rice bran crude oil I and Rice bran crude oil II, obtains Rice bran crude oil；
S33, it takes Rice bran crude oil in centrifuge tube, is rapidly added the diethanol amine of oily weight 11%, in 55 DEG C of constant temperature oscillation boxes
Middle effect 25min, revolving speed 100rpm are then centrifuged for 30min, and revolving speed 3000rpm separates oily phase, with oily 10% deionized water of weight
Washing oil is mutually secondary, and the rice bran oil of embodiment three had both been obtained after dry.
Example IV
The grape seed oil of example IV is prepared by the following method, and its step are as follows:
S41, grape pip is crushed to granularity 0.1mm, adjustment moisture to water content 25% heats, and temperature maintains 85-90
DEG C 40min, then add the cellulase of the grape pip weight 3 ‰, 1 ‰ hemicellulase, 0.5 ‰ protease,
0.2 ‰ α-polygalacturonic enzyme and the 0.3 ‰ poly- glucose enzyme of β-digest 2h, and 55 DEG C of hydrolysis temperature；
Grape pip after S42, microwave treatment enzymatic hydrolysis, microwave power 300W are handled 3 times, and then each 20min is heated, temperature
Degree maintains 85-90 DEG C of 40min, dry to water content 6%, squeezes under conditions of temperature≤50 DEG C and grape pip crude oil is made,
S43, alkali refining is carried out to the grape pip crude oil: caustic dosage is the 0.08% of the grape pip crude oil, alkali refining initial temperature
50 DEG C, 80 DEG C of final temperature, mixing speed 70r/min；
S44, aquation is carried out to the grape pip crude oil: aquation amount of water is 15%, and beginning mixing speed is 55r/min,
Oil temperature is 60 DEG C when adding water, and final temperature is controlled at 80-85 DEG C, quiescent setting 6h or so, makes water-oil separating, the grape seed oil after separation
Dehydration；
S45, decolourize to the grape pip crude oil: decolorising agent is carclazyte and active carbon, carclazyte and activated carbon weight ratio
Example is 5: 1, and decolorising agent dosage is the 3% of the quality of the grape pip crude oil, and operating pressure 0.8MPa, temperature is 70 DEG C, is taken off
The color time is 50min；Oil temperature is set to be quickly cooled to 40 DEG C hereinafter, obtaining the grape pip of example IV after filtering after the completion of decoloration
Oil.
Embodiment five
The spraying preparation method of the multi-functional skin care of embodiment five, its step are as follows:
1) prepare Chinese medicine extract: taking Chinese herb includes folium cortex eucommiae 13g, Japanese ardisia 7g, Sophora alopecuroide 11g, Moso Bamboo Leaves
10g, witch hazel 5g, iris 4g, Radix Paeoniae Alba 3g, pomegranate seed 3g, Schisandra chinensis 6g, viola mandshurica 6g, cordate houttuynia 1g and lemongrass 1g are crushed
To 10 mesh, the distillation water immersion Chinese herb of 350g is added, impregnates 2h, is then put into Chinese herb and distilled water together
It is heated to steam outflow on steam distillation device, distills 3h, collects condensate liquid, upper layer is the essential oil of 9g, and lower layer is the water of 88g
Solution, aqueous are the Chinese medicine extract；
2) prepare miscella: taking oily raw material includes the sub- seed oil 6g of surprise, the perilla herb oil 6g of embodiment two, reality of embodiment one
The rice bran oil 6g of example three, the grape seed oil 6g of example IV and tea oil 24g are applied, the miscella is uniformly mixed to obtain；
3) it prepares shin moisturizer: taking the rice wine liquid of 88g Chinese medicine extract, 48g miscella and 264g, mix, homogeneous, obtain described
Shin moisturizer；
4) shin moisturizer is filled by every part of 50ml packing into spray bottle, both the multi-functional skin care is sprayed.
Wherein, the rice wine liquid purchase that embodiment five uses is produced from Guizhou Province Huishui County good premium brewery, brand is preferably
The black rice wine of premium, Alcohol degree 22%VOL, commodity bar code 6950419300915, production licence number are
QS5227 1505 0054.The 6L dress that the tea oil purchase that embodiment five uses is produced from Hua Yuan green food Co., Ltd of Jiangxi Province
The pure tea-seed oil of Wild camellia seed oil, production licence number are SC10236113010428, and product standard number is GB11765-
2003。
The spraying application method of the multi-functional skin care of embodiment five: will rock spray bottle, keep oil, water and wine therein mixed
Close uniformly, be sprayed at skin, be sprayed into it is just wet be advisable, the case where according to facial-care, each dosage is in 3~10ml
Preferably, once in the morning and once at night.
Embodiment six
The spraying preparation method of the multi-functional skin care of embodiment six, its step are as follows:
1) prepare Chinese medicine extract: taking Chinese herb includes folium cortex eucommiae 8g, Japanese ardisia 11g, Sophora alopecuroide 7g, Moso Bamboo Leaves
5g, witch hazel 10g, iris 9g, Radix Paeoniae Alba 6g, pomegranate seed 6g, Schisandra chinensis 3g, viola mandshurica 3g, cordate houttuynia 3g and lemongrass 3g are crushed
To 20 mesh, the distillation water immersion Chinese herb of 350g is added, impregnates 2h, is then put into Chinese herb and distilled water together
It is heated to steam outflow on steam distillation device, distills 2.5h, collects condensate liquid, upper layer is the essential oil of 7g, and lower layer is 62g's
Aqueous solution, aqueous are the Chinese medicine extract；
2) prepare miscella: taking oily raw material includes the sub- seed oil 1g of surprise, the perilla herb oil 1g of embodiment two, reality of embodiment one
The rice bran oil 1g of example three, the grape seed oil 1g of example IV and tea oil 8g are applied, the miscella is uniformly mixed to obtain；
3) it prepares shin moisturizer: taking 62g Chinese medicine extract, 12g miscella and 126g rice wine liquid, mix, homogeneous obtains the shield
Skin liquid；
4) shin moisturizer is filled by every part of 100ml packing into spray bottle, both the multi-functional skin care is sprayed.
Wherein, the rice wine liquid purchase that embodiment six uses is produced from Huang Shi brewery of Qingzhen County, guizhou Province, china city, brand is Huang Shi's
Black rice wine, Alcohol degree 17%VOL, commodity bar code 6943059512473, production licence number are
SC11552018110106, product standard number are Q/QZHS0001S.The tea that the tea oil and embodiment five that embodiment six uses use
Oil is identical.
The spraying application method of the multi-functional skin care of the embodiment six application method phase spraying with the skin care of embodiment five
Together.
Embodiment seven
The spraying preparation method of the multi-functional skin care of embodiment seven, its step are as follows:
1) prepare Chinese medicine extract: taking Chinese herb includes folium cortex eucommiae 10g, Japanese ardisia 8g, Sophora alopecuroide 8g, Moso Bamboo Leaves
6g, witch hazel 9g, iris 6g, Radix Paeoniae Alba 5g, pomegranate seed 5g, Schisandra chinensis 5g, viola mandshurica 5g, cordate houttuynia 2g and lemongrass 2g are crushed
To 15 mesh, the distillation water immersion Chinese herb of 350g is added, impregnates 2h, is then put into Chinese herb and distilled water together
It is heated to steam outflow on steam distillation device, distills 3h, collects condensate liquid, upper layer is the essential oil of 8g, and lower layer is the water of 84g
Solution, aqueous are the Chinese medicine extract；
2) prepare miscella: take oily raw material include odd sub- seed oil 2g, perilla herb oil 1g, rice bran oil 1g, grape seed oil 1g and
Tea oil 16g is uniformly mixed to obtain the miscella；
3) it prepares shin moisturizer: taking 84g Chinese medicine extract, 21g miscella and 195g rice wine liquid, mix, homogeneous obtains the shield
Skin liquid；
4) shin moisturizer is filled by every part of 30ml packing into spray bottle, both the multi-functional skin care is sprayed.
Wherein, the sub- seed oil of surprise that embodiment seven uses buys the Absolute produced from ECO-FARMS PTY LIMITED
The odd sub- seed oil of Organic, place of production Paraguay.The perilla herb oil purchase that embodiment seven uses is produced from Qingyang Tian Lu grease Co., Ltd
Perilla oil 500ml, production licence number is SC10262100200219, and product standard number is DB21/T 593-2001.It is real
The rice bran oil for applying the use of example seven, which is bought from the 5L that Zhejiang Delekang Food Co., Ltd. produces, obtains happy Kang Tezhi rice bran oil, raw
Producing licensing number is SC10233102401344.The grape seed oil purchase that embodiment seven uses has from Handan morning twilight treasure grease
The grape seed oil of limit company production, production licence number is SC10213043500172.Tea oil, the rice wine of the use of embodiment seven
Tea oil that liquid is used with embodiment five, rice wine liquid phase are same.
The spraying application method of the multi-functional skin care of the embodiment seven application method phase spraying with the skin care of embodiment five
Together.
Embodiment eight
The spraying preparation method of the multi-functional skin care of embodiment eight, its step are as follows:
1) prepare Chinese medicine extract: taking Chinese herb includes folium cortex eucommiae 10g, Japanese ardisia 8g, Sophora alopecuroide 8g, Moso Bamboo Leaves
6g, witch hazel 9g, iris 6g, Radix Paeoniae Alba 5g, pomegranate seed 5g, Schisandra chinensis 5g, viola mandshurica 5g, cordate houttuynia 2g and lemongrass 2g are crushed
To 15 mesh, the distillation water immersion Chinese herb of 350g is added, impregnates 2h, is then put into Chinese herb and distilled water together
It is heated to steam outflow on steam distillation device, distills 3h, collects condensate liquid, upper layer is the essential oil of 8g, and lower layer is the water of 84g
Solution, aqueous are the Chinese medicine extract；
2) prepare miscella: take oily raw material include odd sub- seed oil 2g, perilla herb oil 1g, rice bran oil 1g, grape seed oil 1g and
Tea oil 16g is uniformly mixed to obtain the miscella；
3) it prepares shin moisturizer: taking the diethyl of the Chinese medicine extract of 84g, the miscella of 21g, the benzophenone-3 of 1.5g, 1.5g
The rice wine liquid of the own ester of amino oxybenzene formylbenzoate and 192g, mixing, homogeneous obtain the shin moisturizer；
4) shin moisturizer is filled by every part of 30ml packing into spray bottle, both the multi-functional skin care is sprayed.
Wherein, the sub- seed oil of surprise, perilla herb oil, rice bran oil, grape seed oil, tea oil and the rice wine liquid and implement that embodiment seven uses
Example seven is identical.
The spraying application method of the multi-functional skin care of the embodiment eight application method phase spraying with the skin care of embodiment seven
Together.
The multi-functional skin care of embodiment five-eight respectively refers to the (" area sunscreen cosmetic UVB QB/T 2410-1998 by spraying
The evaluation method ultraviolet absorptivity method of sun-proof result ") it is measured, measure extinction of the product between 280~400nm of wavelength
Degree, and respectively according to the following formula 1 and formula 2 acquire the average value of absorbance A under the area UVB, UVA wavelength, be denoted as A respectivelyUVBAnd AUVA, knot
Fruit is shown in Table 1.
280~320nm of the area UVB:
AUVB=(A280+A290+A300+A310+A320The formula of)/5 (1)
330~400nm of the area UVA:
AUVA=(A330+A340+A350+A360+A370+A380+A390+A400The formula of)/8 (2)
1 sun-proof result comprehensive evaluation form of table
| Absorbance A | Sun-proof result | Use condition |
| 0.5-1.0 | Minimum protects ultraviolet light effect | Winter sunlight, evening in summer sunlight and cloudy day |
| 1.1-1.5 | The medium ultraviolet light effect of protection | The irradiation of moderate strength sunlight |
| 1.6-2.0 | The ultraviolet light effect of high efficient protected | Outwork, the irradiation of summer sunburst |
| 2.1 | Ultraviolet light effect is protected completely | Outwork, the irradiation of summer sunburst |
The multi-functional skin care of 2 embodiment five-eight of table is sprayed the average value of absorbance A
As seen from Table 2, the sun-proof result of embodiment five-eight is up to standard, and the sun-proof result of embodiment eight is excellent.
Evaluation test
One, safety test
For 40 subjects as experimental subjects, the multi-functional skin care in Example five-eight is used as experimental group by spraying
Tested material；The tested material of control group is pure water.Take 0.03ml tested material drop in spot tester with syringe, it will be added with tested material
Spot tester is pasted on the forearm song side of subject with non-stimulated adhesive tape, is gently pressed with palm and is allowed to equably be pasted on skin, held
Continue for 24 hours, experiment position marks, to observe.Remove tested material after 24 hours, after removing patch 0.5h,
For 24 hours, 48h observes dermoreaction, according to dermoreaction grade scale record in " cosmetics health specification " (2007 editions) as a result, mirror
Calibration standard is shown in Table 3, the results are shown in Table 4.
3 standard of perfection of table
| Grade | Standard of perfection |
| 0 | It is non-stimulated, without erythema |
| 1 | Slight erythema |
| 2 | Erythema |
| 3 | Erythema, papule, bubble |
| 4 | Serious edema, bulla |
4 patch test results of table
From table 4, it can be seen that multi-functional skin care of the invention is spraying not to cause any allergy or discomfort to human body, say
Bright multi-functional skin care of the invention is spraying safe, non-stimulated.
Two, anti-inflammatory efficacy is tested
It is spraying with the multi-functional skin care in embodiment five-seven with the black rice wine that is used in embodiment one group as a comparison
As experimental group, compare anti-inflammatory efficacy.Detailed process is as follows:
Kunming male mice 40,40 ± 2g of weight is randomly divided into 5 groups.Each 20 μ L of experimental group, contrast groups is picked with cotton swab
Solution be spread evenly across two sides before and after every mouse right ear, left ear is coated in the same way with physiological saline, then uses cotton
Label pick 20 μ L of about 100% dimethylbenzene and are evenly and rapidly coated on two sides before and after every mouse right ear, record every mouse coating
With the sensitization time, and respectively at cause it is scorching after 0.5,1.5,2.5h repeated drug taking, left ear same amount of normal saline concurrent control.After causing inflammation
4h cuts two ears by animal sacrificed by decapitation, along auricle base line, two ears is laid auricle weighing with 6mm diameter trepan device, and use spiral shell
The thickness of mircrometer gauge measurement bilateral auricle is revolved, the difference of every two auricle weight of mouse is swelling, and the thickness difference of bilateral auricle is
Thickness difference.It is anti-inflammatory to the results are shown in Table 5:
The anti-inflammatory test result of table 5
It can be obtained from table 5, multi-functional skin care of the invention is spraying compared to control group, has good anti-inflammatory effect.
Three, oil-control efficacy test
Experimental principle: using universally acknowledged SEBUMETER method, it is to be based on photometer principle for oil content test, one
After the special delustring adhesive tape absorption grease on human skin of kind of 0.1mm thickness, a kind of translucent adhesive tape just will become, it saturating
Light quantity will change, and the grease of absorption is more, and light transmission capacity will be bigger, can thus measure containing for skin oil and fat
Amount.
Laboratory apparatus: skin oil and fat test probe (Sebumeter, German CK).
Laboratory sample: the black rice wine that experimental group is embodiment five-eight, contrast groups are the use of embodiment five, blank control group
Using pure water.
Experimental method: male subject 60 of selection age 22-35 years old, are oiliness and Combination skin, without any
Skin disease and skin allergy history are divided into 6 groups, and every group of 10 people, every group uses corresponding test sample respectively.Subject's daily morning and evening
Using a test sample, it is used continuously 4 weeks.Follow-up and test are being distinguished once before and after using 4 weeks.When follow-up, ask
Ask and observe whether subject adverse reaction occurs；When test, tester uses skin oil and fat test probe test forehead portion
Position 3 times, is averaged.Experimental result is shown in Table 6.
6 oil-control efficacy outcomes of table
| Group | Before use | After 4 weeks | Grease change rate/% |
| Blank control group | 109.62 | 108.10 | -1.39 |
| Contrast groups | 116.71 | 113.45 | -2.79 |
| Embodiment five | 102.62 | 92.41 | -9.95 |
| Embodiment six | 111.40 | 102.67 | -7.84 |
| Embodiment seven | 105.26 | 94.36 | -10.36 |
| Embodiment eight | 108.79 | 99.48 | -8.56 |
As can be drawn from Table 6, continue that skin oil can be effectively reduced using containing multi-functional skin care of the invention 4 weeks by spraying
Rouge secretion, reaches good oil-control effect.And it is significantly lower than using the oil-control effect containing contrast groups
The product of embodiment five-eight illustrates that the spraying oil-control effect of multi-functional skin care of the invention is good.
Four, in-service evaluation is tested
It will be randomly choosed in Guangzhou street corner and cell according to product made from above-described embodiment five as test sample
100 are ready the male experimenter using this test sample, and experimenter is intended to protect using during this sample without using other together
Skin liquid.
Application method: application method: will rock spray bottle, is uniformly mixed oil, water and wine therein, is sprayed at skin,
Be sprayed into it is just wet be advisable, the case where according to facial-care, each dosage is advisable in 3~10ml, once in the morning and once at night.Make
With investigation statistics using effect after 4 weeks.
Using effect comprehensive value model:
It is fabulous: without allergic conditions, skin moisturizing, smooth elastic, non-greasy, antipruritic effect highly significant；
Preferable: without allergic conditions, skin moisturizing, smooth elastic, non-greasy, antipruritic effect are than more significant；
General: without allergic conditions, skin moisturizing, smooth elastic, non-greasy, antipruritic effect are general；
Poor: the above effect does not embody substantially；
Statistical result is as shown in table 7:
Table 7:
| Overall merit | It is fabulous | Preferably | Generally | It is poor |
| Number | 37 | 54 | 9 | 0 |
As shown in Table 7: have after 91% experimenter's use without allergic conditions, skin moisturizing, smooth elastic, non-greasy,
It is antipruritic, i.e., skin care of the invention be sprayed anti-oxidant, antibacterial anti-inflammatory, oil-control, promoted it is smooth with elastic force, removing free radical, delay to decline
Old effect is than more significant or highly significant.
It is further investigated, 100 experimenters, which think that skin care of the invention is spraying, does not stimulate skin, does not occur secondary work
With.Have 91 experimenters, it is believed that the spraying anti-oxidant, antibacterial anti-inflammatory of skin care of the invention, oil-control, promoted it is smooth with elastic force, it is clear
Except free radical, the significant effect of anti-aging；There are 37 experimenters to think that skin care of the invention spraying anti-oxidant, antibacterial disappear
Inflammation, the significant effect for oil-control, promoting smooth and elastic force, removing free radical, anti-aging；Have 54 experimenters think it is anti-oxidant,
Antibacterial anti-inflammatory, oil-control, promoted it is smooth with elastic force, to remove the effect of free radical, anti-aging significant；It can be seen that the present invention mentions
The multi-functional skin care spray effect supplied is significant, is suitable for promoting and applying.
It should be understood that
The secondary chlorogenic acid of society, alias folium cortex eucommiae caffeotannic acid, the entitled Eucommia ulm odies of foreign language
Chlorogenic acid, a kind of biologically active substance that Chlorogenic Acid from Eucommia ulmoides Leaves system extracts from folium cortex eucommiae leaf.
Chlorogenic acid chemical name is 3-O-caffeoylquinic acid (3-O-caffeoylquinic acid), and relative molecular mass is
354.30, chlorogenic acid is light yellow solid powder.
The Japanese ardisia, scientific name: Ardisia japonica (Thunb) Blume, small green, the short tea of alias, three youth of short foot, external application
Control skin itching.Extract Isosorbide-5-Nitrae-the benzoquinones in the Japanese ardisia, the activity with scavenging activated oxygen can inhibit ultraviolet light irradiation to cause
Wrinkle formed.
Sophora alopecuroide, scientific name Sophora alopecuroides L, different name cloth are sub-.The chemical component of Sophora alopecuroide is mainly egg
White matter, carbohydrate, organic acid, flavonoids, pigment and alkaloid.Alkaloids From Sophora Alopecuroides L belongs to quinolizidine
(Quinolizidine) alkaloid, condensed two piperidine ring formed by trivalent nitrogen atom, also known as double thick piperidines are still fallen within
The derivative of piperidines or pyridine (Piperdine).3 types can be divided by its structure: i.e. lupinine (1upinine), two rings
Type；Sparteine (Cytisine), tricyclic；Sparteine (Spa~eine), four is ring-like.Sophora alopecuroide flavones Stilbene class extract
And its component has good action effect to TYR enzyme, G+ bacterium and G- bacterium within the scope of 1~20mg/L concentrations above；It rises
The material base of effect is clear, and main component is bitter beans ketone L (SA-1), hardship beans ketone C (SA-2), hardship beans ketone K (SA-3), bitter beans ketone
A (SA-4), hardship beans ketone H (SA-5), hardship beans ketone I (SA-6), hardship beans ketone J (SA-7) and hardship beans ketone B (SA-8)；As natural whiting
Antibacterial Constituents are obvious using whitening antibacterial action effect in production cosmetics.
Moso Bamboo Leaves are the blade of moso bamboo.Moso bamboo, scientific name: Phyllostachys heterocycla (Carr.) Mitford
Cv.Pubescens): grass family Phyllostachys, uniaxial scattered type aiphyllium shape bamboo plant.Mainly contain in moso bamboo leaf extract
There are the compounds such as flavonoids abundant and phenolic acid class, such as bamboo-leaves flavones, polysaccharide, lipid and extraordinary amino acid, has excellent
Scavenging capacity oxygen radical and stopping nitrosation reaction ability, have an impact to human endogenous's property Antioxidant Enzymes, can inhibit lactones
The ashamed use and raising immunocompetence of matter peroxidating have the effects of preferable anti-tired anti-aging and intelligent enhancing.
Witch hazel, Hamamelis mollis Oliver, fragrant, ox steps on fruit, Rosales, Hamamelidaceae, gold thread in alias is wooden
Plum category machaka or dungarunga.It is a variety of as Ellagtannin and Hamamlitannin is adjustable that witch hazel includes tannin matter
Sebum secretion, Hydrolyzed Protein and Milk Protein.Promote lymph blood circulation, can specially overcome morning eye bladder and black eye.With town
Cracking, sunburn, acne are had improvement by effect that is quiet, pacifying.The power of regeneration at skin night can effectively be helped.Remove eye
Bag loosens and mitigates and has very excellent effect for the skin of oily skin or allergy.It releives, restrain, antibacterial, resisting
The effect of aging, because there is the significant curative effect of convergence oil-control, sterilization.Hamamelis extract can be substantially reduced in tissue because of intensive ultraviolet
Radiate the malonaldehyde generated strives content, and skin can be prevented by exposure to inflammation caused by ultraviolet light.Mitigate ultraviolet light to shine
Penetrate caused radical damage.Has the function of anti-aging.
Iris, scientific name: Iris tectorum Maxim., also known as: blue butterfly, The purple butterfly, flat bamboo etc. belong to Liliales,
Iridaceae perennial herb, rhizomes can make Chinese medicine, and whole year can adopt, and have antiinflammation.Chinese medicine extract of the invention
The iris mentioned in raw material, refers to the rhizomes for the iris that Chinese medicine defines, rather than petal.
Radix Paeoniae Alba is the dry root of ranunculaceae plant Chinese herbaceous peony Paeonia tacti lora Pall..Summer, the excavation of two season of autumn,
It cleans, removes end to end and radicula, set and boiled again after removing crust or peeling after boiling in boiling water, dried.Mainly contain Paeoniflorin
(Paeoniflorin), hydroxypaeoniflorin, Albiflorin, benzoylpaeoniflorin etc..Radix Paeoniae Alba is sweet in flavor, sour, and cold nature has blood-nourishing
Effect, can treat sallow complexion, facial colour spot, tarnish.
Pomegranate seed also known as seed of pomegranate are the dry seed of Punicaceae plant pomegranate Punica granatum L..Autumn
Pericarp is removed after season fruit maturation, is dried.The main extract of pomegranate seed has strong anti-oxidation, helps to improve joint bullet
Power and skin elasticity strengthen artery, vein and capillary, promote capillary vigor and enhancing capillary wall；Improve skin light
Sliding and elasticity.
Schisandra chinensis is magnoliaceae schisandra Schisandra chinensis (Turcz.) Baill..Schisandra chinensis contains
There are schizandrin (Schisandrin C23H3206) and vitamin C, resin, tannin and a small amount of carbohydrate.Some researches show that the five tastes
The ethanol extract of son is in vitro to bacillus anthracis, staphylococcus aureus, staphylococcus albus, typhoid bacillus, comma bacillus etc.
There is inhibiting effect, Schisandra chinensis has the function of antibacterial anti-inflammatory.
Viola mandshurica, scientific name: Viola philippica, alias open country violet, light valve violet etc..Flavones contained by viola mandshurica
Glucoside and organic acid have gold-coloured staphylococci, pig Pasteurella, Escherichia coli, streptococcus and salmonella stronger antibacterial
Effect.Viola mandshurica is containing organic acid, flavones and its glucoside, phenolic constituent, carbohydrate, amino acid, polypeptide and protein, saponin, plant
10 kinds of effective components such as object sterol, tannin, the microelements such as enriching Cu, iron, manganese, zinc, magnesium.
Cordate houttuynia, source are the dry of saururaceae plant houttuynia cordata (Classification system: Houttuynia cordata Thunb.)
Dry aerial part.The luxuriant flower spike of summer cauline leaf is tapped when more, is removed impurity, is dried.The main extract of cordate houttuynia, to various micro-
Biological (especially saccharomycete and mould) has inhibiting effect, to the streptococcus of hemolytic, staphylococcus aureus, influenza bar
Bacterium, micrococcus catarrhalis, pneumococcus have apparent inhibiting effect.Also there is effect to Escherichia coli, shigella dysenteriae, typhoid bacillus.
Lemongrass, Chinese medicine name.For the herb of gramineae plant lemongrass Cymbopogon citratus (DC.) Stapf.Lemongrass
Main extract component antibacterial, anti-inflammatory, analgesia, mite killing.
Odd Asia seed, is the seed of Lamiaceae plant chia, has been shown to have a variety of health promotion effects.It is " odd
Sub- seed extract Study on Its Antioxidant Activity in Vitro " (being published by " food and fermentation industries ", 2016,42 (6): 197-202) evaluation
The antioxidation activity in vitro of Bai Qiya seed and Hei Qiya seed simultaneously determines its total polyphenols and general flavone content.The result shows that: 2 kinds
Odd Asia seed extract can remove DPPH and ABTS in a manner of concentration dependant+, Bai Qiya seed extract is to DPPH
And ABTS+Scavenging activity be significantly higher than Hei Qiya seed extract；The FeSO of white and the odd sub- seed extract of black4·7H2O
Equivalent is respectively (41.48+2.84) μm ol/g and (29.70 ± 2.43) μm ol/g；Meanwhile 2 kinds of odd sub- seed extracts can be shown
Beta carotene caused by inhibiting linoleic acid free radical is write to bleach.In addition, 2 kinds of odd sub- seed extracts can effectively inhibit freely
The linoleic acid peroxidation of base induction and bovine serum albumin(BSA) oxidative degradation.
Perilla herb oil, correct full name are Purple Perilla Seed Oil, foreign language title are as follows: Perilla Seed Oil.It is with purple perilla seed for original
Expect the edible oil extracted.Purple perilla is the dual purpose plant for the integration of drinking and medicinal herbs that country ratifies in the first batch.Purple Perilla Seed Oil is soluble in ethyl alcohol, indissoluble
In glycerol and propylene glycol.US Experts watababe test discovery, intake Purple Perilla Seed Oil can significantly improve super oxygen in red blood cell
The vigor of object mutase (SOD), to delaying body aging to have obvious effect.In addition, the Alecrim acid that perilla herb oil contains is a kind of
Fragrant acid compound has anticoagulation, antibacterial anti-inflammatory, antiviral isoreactivity, and there is very strong inoxidizability to inhibit allergic reaction.
Rice bran oil, oryzanol rich in, family's chemical combination that oryzanol is made of ten several sterols ferulic acid esters
Object, oryzanol is stronger to ultraviolet radiation absorption in 280-320nm, can protect antitan agent.Also contain rice bran and embryo in rice bran oil
The nutritional ingredients such as a large amount of liposoluble vitamin, sitosterol and other phytosterols in bud.Vitamin E and oryzanol all have anti-
Oxidation.
Grape seed oil, unsaturated fatty acid rich in, mainly oleic acid and linoleic acid, wherein linoleic content is high
Up to 72%~76%.Linoleic acid is essential fatty acid, is easily absorbed by the body.Grape seed oil be rich in vitamin E, have compared with
Strong inoxidizability is rich in grape pip glucosidase procyanidins in grape seed oil, and CAS No is 222838-60-0, and English name is
Grape Seeds Oligomeric Proanthocyanidins。
Tea oil also known as camellia oil, tea oil, tea-seed oil are the oil for refining out as raw material using tea tree seed, of light color
Huang, clear, smell faint scent.Unsaturated fatty acid content is up to 90% or more in tea oil, and wherein oleic acid is about 80~83%,
Linoleic acid is about 7~13%.Contain a certain amount of saponin(e and multivitamin in tea oil, has the function of disinfecting detoxifying, also contain
There is vitamin E abundant, there is anti-aging, anti-oxidation function, there is beauty care, anti-aging.The group of camellia seed oil
It is good with the compatibility of skin at part 70%~80% as human skin, it is easy to skin absorption, Skin Cell can be being maintained just
Normal physiological function and metabolic activity, are used for skin care item, skin can be promoted tender and high resilience, have good moisturizing skin care function
Skin can be made to keep elasticity, the good health status of skin is maintained also to have the function of preventing and treating scabies simultaneously.
Black glutinous rice is carried out de- chaff skin processing, melanoma liquid is extracted from chaff skin by black rice wine, meanwhile, to having taken off chaff skin
The smart fermented brewing process of black rice of white, produce yellow rice wine, suitable melanoma liquid be added in yellow rice wine, just produces black rice wine.
The invention is not limited to above embodiment, if not departing from the present invention to various changes or modifications of the invention
Spirit and scope, if these modification and variations belong within the scope of claim and equivalent technologies of the invention, then this hair
It is bright to be also intended to encompass these modification and variations.
Claims (10)
1. a kind of multi-functional skin care is spraying, it is characterised in that: Chinese medicine extract, the 6- for being 22-31% including quality accounting
12% miscella and the rice wine liquid of surplus；
The raw material and its mass fraction of the Chinese medicine extract include 8-13 parts of folium cortex eucommiae, Japanese ardisia 7-11 parts, Sophora alopecuroide 7-
11 parts, 5-10 parts of Moso Bamboo Leaves, 5-10 parts of witch hazel, 4-9 parts of iris, 3-6 parts of Radix Paeoniae Alba, 3-6 parts of pomegranate seed, 3-6 parts of Schisandra chinensis, purple
Chinese violet 3-6 parts of flower, 1-3 parts of cordate houttuynia and 1-3 parts of lemongrass；The Chinese medicine extract is prepared by the following method: by the Chinese medicine
The raw material of extracting solution carry out steam distillation after crushing, extraction obtains grease blend, and aqueous after centrifugation is as described
Chinese medicine extract；The raw material and its mass fraction of the miscella include odd sub- 1-3 parts of seed oil, 1-3 parts of perilla herb oil, rice bran oil
1-3 parts, 1-3 parts of grape seed oil and 8-16 parts of tea oil.
2. multi-functional skin care as described in claim 1 is spraying, it is characterised in that: the rice wine liquid is the black rice of 17-22%VOL
Wine.
3. multi-functional skin care as described in claim 1 is spraying, it is characterised in that: further include 0.5-1% benzophenone-3 and/or
The Uvinul A Plus of 0.5-1%.
4. a kind of preparation method that multi-functional skin care is spraying, it is characterised in that: its step are as follows:
1) prepare Chinese medicine extract: taking raw material includes 8-13 parts of folium cortex eucommiae, Japanese ardisia 7-11 parts, 7-11 parts of Sophora alopecuroide, moso bamboo
5-10 parts of leaf, 5-10 parts of witch hazel, 4-9 parts of iris, 3-6 parts of Radix Paeoniae Alba, 3-6 parts of pomegranate seed, 3-6 parts of Schisandra chinensis, viola mandshurica 3-6
Part, 1-3 parts of cordate houttuynia and 1-3 parts of lemongrass crush, are then placed in steam distillation equipment and carry out steam distillation, extract
To grease blend, aqueous after centrifugation, the as described Chinese medicine extract, the number is mass fraction；
2) prepare miscella: taking raw material includes odd sub- 1-3 parts of seed oil, 1-3 parts of perilla herb oil, 1-3 parts of rice bran oil, grape seed oil 1-
3 parts and 8-16 parts of tea oil, it is uniformly mixed to obtain the miscella, the number is mass fraction；
3) it prepares shin moisturizer: according to the mass percent meter of the shin moisturizer, taking the Chinese medicine extract, the 6- of 22-31%
12% miscella and the rice wine liquid of surplus, mixing, homogeneous obtain the shin moisturizer；
4) by the shin moisturizer packing fill into spray bottle, both the multi-functional skin care be sprayed.
5. the spraying preparation method of multi-functional skin care as claimed in claim 4, it is characterised in that: the rice wine liquid is 17-
The black rice wine of 22%VOL.
6. the spraying preparation method of multi-functional skin care as claimed in claim 4, it is characterised in that: in step 3), the skin care
Liquid further include 0.5-1% benzophenone-3 mutually and/or 0.5-1% Uvinul A Plus.
7. the spraying preparation method of multi-functional skin care as claimed in claim 4, which is characterized in that the odd sub- seed oil by with
The preparation of lower section method, its step are as follows:
S11, the sub- seed of the surprise for being 15% by moisture content are placed in the heating tank of Ohmic heating device and heat, heating temperature 90
DEG C, heating time 20min, the sub- seed of the surprise cured；
S12, the sub- seed of the surprise of curing is obtained into odd sub- seed crude oil, 120 DEG C of squeeze pressure 40MPa, pressing temperature by squeezing；
S13, the atlapulgite that its quality 3% is added to odd sub- seed crude oil, are handled in the case where temperature is 105 DEG C, pressure is 2.5kPa
30min obtains odd sub- seed oil for refining removal of impurities.
8. the spraying preparation method of multi-functional skin care as claimed in claim 4, which is characterized in that the perilla herb oil passes through following
Method preparation, its step are as follows:
S21, purple perilla is dried, controls moisture content 3%；
S22, it the purple perilla benevolence dried is put into -25 DEG C of household freezer freezing 9h, taking-up is placed in 8h in -10 DEG C of vacuum environment,
It then takes out to be placed in 60 DEG C of vacuum environments and is dried 7h；
S23, the purple perilla benevolence obtained after step S22 processing is crushed, is sieved with 40 mesh sieve；
S24, the purple perilla benevolence powder obtained after step S23 processing is passed through into CO2Supercritical extract, fluid extraction pressure are 45MPa, extraction
Take temperature 45 C, CO2Fluid flow is 1100L/h, and extraction time 100min obtains purple perilla crude oil；
S25, the purple perilla crude oil obtained after step S24 processing is removed into lipoxygenase by hyperfiltration, selects retention molecule
Measure the hyperfiltration film of 120kD.
9. the spraying preparation method of multi-functional skin care as claimed in claim 4, which is characterized in that the rice bran oil passes through following
Method preparation, its step are as follows:
S31, rice bran cross 40 meshes, dry 5 days；
S32, it takes the rice bran after sunning to be packed into extraction kettle, passes through supercritical CO2Extraction equipment extracts Rice bran crude oil stage by stage, to CO2
8% wet basis ethyl alcohol is added in fluid as entrainer, setting extraction conditions I is 15MPa, 30 DEG C, extracts 1.0h, isolated rice
Chaff crude oil I；Increasing temperature and pressure is 35MPa, 40 DEG C to condition II, continues to extract 4h, isolated Rice bran crude oil II, mixing rice bran hair
Oily I and Rice bran crude oil II, obtains Rice bran crude oil；
S33, it takes Rice bran crude oil in centrifuge tube, is rapidly added the diethanol amine of oily weight 11%, make in 55 DEG C of constant temperature oscillation boxes
With 25min, revolving speed 100rpm, it is then centrifuged for 30min, revolving speed 3000rpm separates oily phase, with oily 10% deionized water washing oil of weight
It is mutually secondary, rice bran oil is both obtained after dry.
10. the spraying preparation method of multi-functional skin care as claimed in claim 4, which is characterized in that the grape seed oil passes through
Following methods preparation, its step are as follows:
S41, grape pip is crushed to granularity 0.1mm, adjustment moisture to water content 25% heats, and temperature maintains 85-90 DEG C
Then 40min adds the cellulase, 1 ‰ hemicellulase, 0.5 ‰ protease, 0.2 ‰ of the grape pip weight 3 ‰
α-polygalacturonic enzyme and the 0.3 ‰ poly- glucose enzyme of β-digest 2h, 55 DEG C of hydrolysis temperature；
Grape pip after S42, microwave treatment enzymatic hydrolysis, microwave power 300W are handled 3 times, then each 20min is heated, temperature dimension
It holds to squeeze under conditions of 85-90 DEG C of 40min, drying to water content 6%, temperature≤50 DEG C and grape pip crude oil is made,
S43, to the grape pip crude oil carry out alkali refining: caustic dosage be the grape pip crude oil 0.08%, 50 DEG C of alkali refining initial temperature,
80 DEG C of final temperature, mixing speed 70r/min；
S44, aquation is carried out to the grape pip crude oil: aquation amount of water is 15%, and beginning mixing speed is 55r/min, adds water
When oil temperature be 60 DEG C, final temperature is controlled at 80-85 DEG C, and quiescent setting 6h or so makes water-oil separating, and the grape seed oil after separation is de-
Water；
S45, decolourize to the grape pip crude oil: decolorising agent is carclazyte and active carbon, and carclazyte and activated carbon weight ratio are 5
: 1, decolorising agent dosage is the 3% of the quality of the grape pip crude oil, and operating pressure 0.8MPa, temperature is 70 DEG C, bleaching time
For 50min；Oil temperature is set to be quickly cooled to 40 DEG C hereinafter, obtaining refining grape seed oil after filtering after the completion of decoloration.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112107534A (en) * | 2019-06-19 | 2020-12-22 | 广州市荷花香精香料有限公司 | Rosemary-containing transdermal repair spray |
| CN114392350A (en) * | 2022-01-25 | 2022-04-26 | 浙江瘦金体健康管理集团有限公司 | Hyaluronic acid oral liquid and preparation method thereof |
| CN115040438A (en) * | 2022-06-29 | 2022-09-13 | 广州市科能化妆品科研有限公司 | Skin composition for promoting skin barrier repair function and preparation method and application thereof |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101779705A (en) * | 2010-02-22 | 2010-07-21 | 北京市科威华食品工程技术有限公司 | Production method of grape seed oil |
| CN102226126A (en) * | 2011-04-27 | 2011-10-26 | 王金玲 | Simplified preparation technology of rice oil |
| CN103976906A (en) * | 2014-05-29 | 2014-08-13 | 上海清轩生物科技有限公司 | Plant extract mixture having moisturizing and inflammation-diminishing effects |
| CN104414902A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Citrus-bigarradia-flower skin-moistening spot-removing spray |
| CN104745296A (en) * | 2015-03-30 | 2015-07-01 | 陕西理工学院 | Method for extracting chia seed oil with assistance of ohmic heating |
| CN105154215A (en) * | 2015-08-12 | 2015-12-16 | 查光圣 | Supercritical extraction process for perilla oil |
| CN105963202A (en) * | 2016-06-27 | 2016-09-28 | 青岛艾派克生物科技有限公司 | Anti-acne and anti-inflammation mask |
| CN106389204A (en) * | 2016-10-23 | 2017-02-15 | 广东轻工职业技术学院 | Botanical drug composition with both functions of oil controlling and pox removing and application of botanical drug composition |
| CN107157881A (en) * | 2017-05-26 | 2017-09-15 | 广州鹰远生物科技有限公司 | Composition and cosmetics with acne-removing |
| CN107375082A (en) * | 2017-08-08 | 2017-11-24 | 湖北瑞晟生物有限责任公司 | A kind of moisturizing anti-inflammatory facial mask liquid and preparation method thereof |
| CN107519100A (en) * | 2017-09-30 | 2017-12-29 | 广州环亚化妆品科技有限公司 | A kind of composition and its preparation method and application |
-
2018
- 2018-09-06 CN CN201811035284.2A patent/CN109010173A/en not_active Withdrawn
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101779705A (en) * | 2010-02-22 | 2010-07-21 | 北京市科威华食品工程技术有限公司 | Production method of grape seed oil |
| CN102226126A (en) * | 2011-04-27 | 2011-10-26 | 王金玲 | Simplified preparation technology of rice oil |
| CN104414902A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Citrus-bigarradia-flower skin-moistening spot-removing spray |
| CN103976906A (en) * | 2014-05-29 | 2014-08-13 | 上海清轩生物科技有限公司 | Plant extract mixture having moisturizing and inflammation-diminishing effects |
| CN104745296A (en) * | 2015-03-30 | 2015-07-01 | 陕西理工学院 | Method for extracting chia seed oil with assistance of ohmic heating |
| CN105154215A (en) * | 2015-08-12 | 2015-12-16 | 查光圣 | Supercritical extraction process for perilla oil |
| CN105963202A (en) * | 2016-06-27 | 2016-09-28 | 青岛艾派克生物科技有限公司 | Anti-acne and anti-inflammation mask |
| CN106389204A (en) * | 2016-10-23 | 2017-02-15 | 广东轻工职业技术学院 | Botanical drug composition with both functions of oil controlling and pox removing and application of botanical drug composition |
| CN107157881A (en) * | 2017-05-26 | 2017-09-15 | 广州鹰远生物科技有限公司 | Composition and cosmetics with acne-removing |
| CN107375082A (en) * | 2017-08-08 | 2017-11-24 | 湖北瑞晟生物有限责任公司 | A kind of moisturizing anti-inflammatory facial mask liquid and preparation method thereof |
| CN107519100A (en) * | 2017-09-30 | 2017-12-29 | 广州环亚化妆品科技有限公司 | A kind of composition and its preparation method and application |
Non-Patent Citations (1)
| Title |
|---|
| 王建新: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112107534A (en) * | 2019-06-19 | 2020-12-22 | 广州市荷花香精香料有限公司 | Rosemary-containing transdermal repair spray |
| CN114392350A (en) * | 2022-01-25 | 2022-04-26 | 浙江瘦金体健康管理集团有限公司 | Hyaluronic acid oral liquid and preparation method thereof |
| CN115040438A (en) * | 2022-06-29 | 2022-09-13 | 广州市科能化妆品科研有限公司 | Skin composition for promoting skin barrier repair function and preparation method and application thereof |
| CN115040438B (en) * | 2022-06-29 | 2023-12-15 | 广州市科能化妆品科研有限公司 | Skin composition for promoting skin barrier repair function, preparation method and application thereof |
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