KR101194059B1 - A cleansing composition for preventing loss of hair and promoting growth of hair comprising herbal extracts and the process of preparation thereof - Google Patents

Abstract

The present invention relates to a hair loss preventing and regrowth cleaning composition comprising herbal herbal medicine extract and a method for preparing the same, in the hair loss preventing and regrowth cleaning composition comprising herbal herbal medicine extract, the herbal herbal extract is Thuja orientalis (Thuja orientalis) 0.6 kg, Morus bombysis 0.6-0.8 kg, Bamboo leaf (Seaa borealis) 0.4-0.55 kg, Ginkgo biloba L. 0.6-0.8 kg, Pine needles (Pinus denciflora) 0.6-0.8 kg, Licorice (Glycyrrluizae urealensis) ) 0.3 to 0.4 kg, Ginseng urealensis 0.3 to 0.4 kg, Pulsatilla Radix 0.1 to 0.13 kg, Kochiae Fructus 0.2 to 0.27 kg, Peonia suffruticosa 0.2 to 0.27 kg, Goji (Lycium chinense) ) 0.2 to 0.27 kg, Rehmannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 to 0.4 kg, Glycine max Merr 0.3 to 0.4 kg, Black Don't (Sesanmum indicum) 0.4 to 0.53 kg, Gochu (Capsicum annuum L.) 0.3 to 0.4 kg, Ogapi (Acanthopanx sessiliflorus) 0.4 kg, Talc (Alisima plantago-aquatica) 0.3 kg, Mushroom (Agaricus blazei) 0.5 to 0.67 kg (Taraxacum ohwianum) Herbal herbal medicine powder containing 0.4 to 0.53 kg, 0.5 to 0.67 kg of balsam (Laminariae Folium) and 0.3 to 0.4 kg of white porcelain (Spermary) is extracted using N ₂ or CO ₂ carrier gas (Carrier Gas) And as obtained by concentrating, the herbal herbal extracts for hair loss preventing and regrowth of the present invention, characterized in that the herbal herbal extract in an amount of 5 to 20% by weight based on the total weight of the composition, vitamins, amino acids, etc. Can not only maximize the anti-oxidation effect due to enzyme activity, low oxygen solubility, high viscosity, but also change in physical properties, taste, aroma, color, etc. By having a slowly varying characteristics is the effect of preventing hair loss and hair growth effect is significantly improved is expected to be very useful in the art.

Description

Hair loss prevention and regrowth cleaning composition comprising herbal herbal extracts and a method for producing the same {A CLEANSING COMPOSITION FOR PREVENTING LOSS OF HAIR AND PROMOTING GROWTH OF HAIR COMPRISING HERBAL EXTRACTS AND THE PROCESS OF PREPARATION THEREOF}

The present invention relates to a hair loss preventing and regrowth cleaning composition comprising a herbal herbal medicine extract and a method for preparing the same, and more specifically, white leaf, upper leaf, bamboo leaf, ginkgo leaf, pine leaf, licorice, ginseng, baekduong, branch, velvet, goji berry Extracted and concentrated herbal medicine raw materials consisting of Sukji Hyang, Baekbokyeong, Cornus, Black bean, Black Jim, Gocho, Ogapi, Taxa, Mushroom, Pogongyoung, Bale and White porridge using N ₂ or CO ₂ Carrier Gas It relates to a hair loss preventing and regrowth detergent composition comprising the herbal herbal extracts and chemicals obtained and a method for producing the same.

Generally, there are many causes of hair loss, but there are genetic and acquired factors. Genes directly related to the cause of hair loss in the genetic factors are not known, but several genes have been reported to be involved. The degree of hair loss caused by genetic factors can predict the progress of hair loss to some extent by comprehensively determining the inherent history, the current hair loss state, and the progress of the hair loss. The causes of acquired hair loss include alopecia areata, alopecia areata, feminine alopecia, pediatric alopecia, drug alopecia, traumatic alopecia, skin alopecia and scarring alopecia.

Alopecia areata is a round or oval of various sizes, with a clear border of hair loss, single or multiple hairs, and in severe cases, may spread to the entire area of the hair, and it is difficult to detect hair loss and has high recurrence. Recent studies have shown that alopecia areata is a type of autoimmune disease. In other words, lymphocytes that can damage the follicles are concentrated around the follicle, and the main targets are known as the causes of melanocytes, keratinocytes, dermal papilla and vascular endothelium. .

Androgenetic alopecia, commonly referred to as adult or mild alopecia, is mainly seen in people with genetic causes caused by male hormones, and it is a phenomenon in which the number of hair is naturally reduced after hair loss.

In female alopecia, hair loss progresses as the hair of the crown gets thinner without a specific form, which is caused by male hormones secreted in small amounts by women, and there are other environmental factors, such as mental factors and drug use.

Hair loss caused by drugs caused by side effects such as anticancer drugs, antibiotics, hormones, etc. are mainly caused by chemicals affecting hair growth.

Hair loss due to abnormal endocrine system occurs due to problems of the body's endocrine system, such as diabetes or hypothyroidism, and alopecia caused by dermatosis is caused by infectious diseases or atopic dermatitis.

Recently, hair loss symptoms are frequently caused by environmental factors, mental stress, and excessive use of shampoo or beauty soap. Therefore, hair loss symptoms not only give a lot of stress to the self, but also lose confidence, it will interfere with the relationship is good, it is desirable to treat the hair loss symptoms in the early stages. Especially, when the cause of genetic hair loss and the cause of acquired hair loss are combined, hair loss symptoms are more severe. Therefore, it is important to diagnose and prevent it early.

Currently, there are many products on the market as a hair loss treatment and hair regrowth, but there are many products in which the effect is insignificant or the effects of hair loss and hair growth treatment are not verified. As a conventional method for treating hair loss, herbal medicines are selected and pulverized, pulverized herbal medicines are selected and pulverized, water is added to the herbal medicines, put in a container and boiled for 3 to 5 hours to extract the ingredients contained in the herbal medicines. In addition, the extracted mixture is put into a press equipped with a filtration means and pressed to obtain a primary extract containing about 1300 to 1400 cc of herbal ingredients, and the primary extract is added to a water bath again and then boiled for 20 to 25 hours while stirring. Concentrate to obtain a second herbal extract, that is, a first component, and the first component is mixed with a second component such as an oil component and vegetable glycerin, and a third component which is a soap component, mixed and agitated at a fixed ratio, and solidified. There is a method for producing a hair growth functional shampoo, rinse and soap using.

In the prior art, methods used for separation of herbal medicines include distillation, solvent extraction, membrane separation, crystallization, evaporation, and adsorption methods, and the most widely used distillation method is a method using a difference in volatilities between materials, The solvent extraction method has a separation method using a difference in solubility and a membrane separation using a difference in permeability.

Distillation is used to separate substances with similar or non-volatile vapor pressures and requires a lot of energy. This method is disadvantageous in that pyrolysis and thermally denatured materials such as herbal herbal medicines are difficult to be processed to high temperatures. Solvent extraction method is expensive to extract by using a large amount of highly toxic solvents and post-treatment to obtain desired purity. The membrane separation method has a disadvantage in that it is difficult to obtain a high purity extract due to polarization of concentration.

In the present invention, while solving the above problems by including the herbal medicine extract extracted without destroying the active ingredient contained in the herbal herbal medicine carrier gas (continuous research to develop a cleaning composition having excellent hair loss prevention and hair regrowth effect ( Herbal herbal extracts obtained by concentrating the extracts by using Carrier Gas and concentrating them into high concentration syrup or jelly form do not destroy vitamins, amino acids, etc., and have an antioxidant effect due to enzyme activity, low oxygen solubility, and high viscosity. The present invention has been completed by discovering that not only it can be maximized but also have the property of changing very slowly in the air after extraction without changing the physical properties, taste, aroma, and color, thereby preventing hair loss and improving hair growth.

An object of the present invention is to activate the scalp tissue without destroying the active ingredient contained in the herbal herbal medicine, and to prevent hair loss from falling out of the scalp while using hair for a period of time, hair loss can be generated and grown from the pores of the activated scalp tissue. It is to provide a cleaning composition for preventing and regrowth.

Another object of the present invention is to provide a method for preparing the hair loss preventing and hair growth cleaning composition.

In order to achieve the above object, in the present invention, in the hair loss preventing and regrowth cleaning composition comprising herbal herbal medicine extract, the herbal herbal extract is 0.6 kg of Thuja orientalis, 0.6 to 0.8 kg of upper leaf (Morus bombysis), Bamboo leaf (Seaa borealis) 0.4 to 0.55 kg, Ginkgo biloba L. 0.6 to 0.8 kg, Pine needles (Pinus denciflora) 0.6 to 0.8 kg, Licorice (Glycyrrluizae urealensis) 0.3 to 0.4 kg, Ginseng (Ginseng urealensis) 0.3 to 0.4 kg, Pulsatilla Radix 0.1 to 0.13 kg, Kochiae Fructus 0.2 to 0.27 kg, Peyonia suffruticosa 0.2 to 0.27 kg, Lycium chinense 0.2 to 0.27 kg, Rejimannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 to 0.4 kg, Glycine max Merr 0.3 to 0.4 kg, Black injima (Sesanmum indicum) 0.4 to 0.53 kg, Capsicum annuum L.) 0.3 to 0.4 kg, 0.4 kg of Acanthopanx sessiliflorus, 0.3 kg of Alisima plantago-aquatica, 0.5 to 0.67 kg of mushroom (Agaricus blazei), 0.4 to 0.53 kg of Taraxacum ohwianum, 0.5 to 0.67 kg of balsam (Laminariae Folium) ) The herbal herbal powder containing 0.3 to 0.4 kg was extracted and concentrated by using N ₂ or CO ₂ carrier gas, and the herbal herbal extracts were added in an amount of 5 to 20 weight based on the total weight of the composition. It provides a cleaning composition for preventing hair loss and hair growth, characterized in that the amount of%.

In order to achieve the above another object, in the present invention, in the method for preparing a hair loss preventing and hair regrowth detergent composition comprising herbal herbal medicine extract,

0.6 kg of Thuja orientalis, 0.6 to 0.8 kg of upper leaf (Morus bombysis), 0.4 to 0.55 kg of Seaa borealis, 0.6 to 0.8 kg of Ginkgo biloba L., 0.6 to 0.8 kg of Pinus denciflora , Glycyrrluizae urealensis 0.3 to 0.4 kg, Ginseng urealensis 0.3 to 0.4 kg, Pulsatilla Radix 0.1 to 0.13 kg, Kochiae Fructus 0.2 to 0.27 kg, Peonia suffruticosa 0.2 to 0.27 kg , Lycium chinense 0.2 to 0.27 kg, Rehmannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 to 0.4 kg, Glycine max Merr 0.3 To 0.4 kg, black injima (Sesanmum indicum) 0.4 to 0.53 kg, Kosi (Capsicum annuum L.) 0.3 to 0.4 kg, Ogapi (Acanthopanx sessiliflorus) 0.4 kg, Talc (Alisima plantago-aquatica) 0.3 kg, Mushroom (Agaricus blazei) 0.5 to 0.67 kg, Taxacum ohwianum 0.4 to 0.53 kg, Laminariae Folium 0.5 to 0.67 kg and Spermary 0.3 to 0.4 kg are mixed, extracted and concentrated using N ₂ or CO ₂ carrier gas, and then the herbal herbal extracts are added in an amount of 5 to 20 wt% based on the total weight of the composition. It provides a method for producing a hair loss preventing and hair refining cleaning composition comprising an amount.

The detergent composition containing the herbal herbal medicine extract of the present invention does not destroy any vitamins, amino acids, etc. of the herbal herbal medicines, and can maximize the anti-oxidation effect due to high viscosity and enzymatic activity, low oxygen solubility, as well as physical properties, taste, It is expected that the hair loss prevention effect and the hair regrowth effect will be greatly improved by having a property that does not denature well in the air after extraction without changing the fragrance and chromaticity.

Figure 1 schematically shows the manufacturing process of the soap, shampoo and rinse using the hair loss prevention and hair removal cleaning composition of the present invention.
2 schematically shows the function of the carrier gas concentrator used in the present invention.
Figure 3 shows a schematic diagram of the extracting concentrator used in the present invention.
Figure 4 shows the expected analysis data of the extraction concentration temperature when using a carrier gas concentrator.
Figure 5 shows the comparative experiment data of the separation of the carrier gas condenser and the conventional vacuum condenser.
6 shows a state diagram of the temperature and mole fraction of the carrier gas concentrator.
7 shows the temperature change process inside the carrier gas concentrator.

Unless otherwise defined in the technical terms and scientific terms used in the present invention, it can be interpreted to mean that those of ordinary skill in the art to which the present invention belongs.

Hair loss preventing and regrowth cleaning composition of the present invention is 0.6 kg of Thuja orientalis, 0.6 to 0.8 kg of upper leaves (Morus bombysis), 0.4 to 0.55 kg of bamboo leaves (Seaa borealis), 0.6 to 0.8 Ginkgo biloba L. Kg, Pineus denciflora 0.6-0.8kg, Glycyrrluizae urealensis 0.3-0.4kg, Ginseng urealensis 0.3-0.4kg, Pulsatilla Radix 0.1-0.13kg, Kochiae Fructus 0.2-0.27 Kg, Paeonia suffruticosa 0.2 to 0.27 kg, Lycium chinense 0.2 to 0.27 kg, Rehmannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 To 0.4 kg, Glycine max Merr 0.3 to 0.4 kg, Black tide (Sesanmum indicum) 0.4 to 0.53 kg, Kosi (Capsicum annuum L.) 0.3 to 0.4 kg, Ogapi (Acanthopanx sessiliflorus) 0.4 kg, Alixa plantago -aquatica) 0.3 kg, mushrooms (Agaricus blazei) 0.5 to 0.67 kg, pogongyoung (T Herbal herbal medicines powder containing araxacum ohwianum 0.4 to 0.53 kg, 0.5 to 0.67 kg of balsam (Laminariae Folium) and 0.3 to 0.4 kg of white porcelain is extracted and extracted using N ₂ or CO ₂ carrier gas. It can be prepared by adding the herbal herbal extract obtained by concentration in an amount of 5 to 20% by weight.

Hair loss prevention and hair removal cleaning composition of the present invention is a herbal herbal extract 5 to 20% by weight, as a second component 4 to 6% by weight of the oil component, 1 to 2% by weight of the chemical material and the fourth component The component includes 83 to 89% by weight of the cleaning component.

Hair loss preventing and regrowth cleaning composition of the present invention may be a soap, shampoo or rinse composition. Figure 1 schematically shows the manufacturing process of the soap, shampoo and rinse using the hair loss prevention and hair removal cleaning composition of the present invention.

Herbal herbal medicine which is the raw material of the herbal herbal medicine extract as the first component in the hair loss preventing and regrowth cleaning composition of the present invention is baekbaek leaves, upper leaves, bamboo leaves, ginkgo leaves, pine needles, licorice, ginseng, Baekduong, branch branch, bark skin, gojija, sukjihyang, Baekbokryeong, Cornus, Black Bean, Black Jim, Gocho, Ogapi, Taxa, Mushroom, Pogongyoung, Packing, and White Porcelain, and when the active ingredients of these extracts are absorbed into the scalp tissue, it promotes blood circulation of the scalp, It not only enhances cell activity, but also makes hair root healthy and promotes hair growth.

As a result of analyzing the herbal herbal extracts included in the hair loss preventing and regrowth cleaning composition of the present invention, it appears to have an active ingredient (% by weight) as shown in Table 1 below.

Ogapi (eleutheroside A, B, B1, C, E (2%))
2. Licorice (Glycyrrhizin (2-7%), glabric acid, Liguiritin, formononetin (3%))
3.Ginseng (Alkaloid: (+ matrine, oxymatrine, sophoranol, anagyrine, baptifolinr) 1-2%)
4. Wolfberry (zeaxanthin, physalien, vitamin A, B1, B2, C, scopoletin (2-4%))
5. Antlers (Collagen, ertrone, uridine, creatinine, ganglioside (3-4%))
6. Angelica (decursin, pyranocoumarin umbelliferon (0.5%))
7. Macmundong (Ophiopogonin A, B, C, D, C ', D', Homoisoflavonoid (1%))
8. Mint (menthone, camphene, piperitone, pulegone (1-2%))
9. Ginseng (ginsenoside (Ro, a, b, c, d, e, f, g1, g2, h) 4%, panacene, spinacine 1%)
10. Earl (Paeoniflorin, gallotannin, albiflorin (3-4%))
11. Baekbongryeong (pachyman, triterpenoid, ergostero (1%))
12. aloe (aloin (aloinoside A, B) (3%), anthraquinone (trace))
13. Sookjiwang (catalpol (2.8%), cerebroside, rehmannioside A, B, C, amino acid (16 species))
14. Ligustilide (falgustinolone, apiod 2-3%)
15. Sewage (chrysophanol, Emodin, rhein, physion, stilben (2%))
16. Biota orientalis Endlicher (2%)
17. Morus alba Linne (1%)
18. Bamboo Leaf (竹葉, Sasa borealis var. Gracilis (1%))
19. Buttercup (傘形 科 Apiaceae (2%))
20. Ginkgo biloba (銀杏, ginkgo (2%))
21.Others ((2%))

A brief description of their efficacy is as follows.

Ogapi uses the root and bark of the medicine as a medicine, the weakness is warm, the taste is spicy and bitter, it is not poisonous, physical strength and anti-stress action, taking a long time to lighten the body and delay the aging effect.

Licorice normalizes menstruation, communicates all blood vessels, and detoxifies all drugs.

Ginseng is a perennial herb of the dicotyledonous plant Rosaceae, whose roots are dried and called ginseng.It is known for its taste and efficacy of ginseng.It is effective in tonic and neurodermatitis, which may cause scalp when used in the scalp. It is effective in preventing various skin diseases.

Goji is a fruit of goji berry, which contains protein, fat, calcium, iron, phosphorus, vitamins, etc., so it is fast absorbed and used as a tonic and antipyretic agent.It has no side effects and is mixed with perilla oil to prevent baldness. It is known that this is.

Deer antler is a dry horn cut deer's soft horns and can be called a typical herbal medicine. The taste is sweet and salty and warm in nature, acting on the liver and kidneys to protect the tablets and blood and strengthen the muscles.

Angelica is a perennial or perennial herb belonging to the Araaceae family, and has a peculiar smell. It is one of the many medicines that use root as a medicinal herb and helps to circulate blood and keeps the body warm and elastic and keeps it clear and clean. It is known to have a function to make skin tissue and hair roots healthy.

Macmundong is a perennial herbaceous herbaceous herb, which extracts the lumps of roots in early spring or late autumn, cleans them, and then dries them. It is effective in nourishing tonic, restoring weakness, coughing and phlegm.

Peppermint is a perennial herb with water grass, and it is effective in improving angina, heart pain, and blood circulation.

Ginseng promotes protein synthesis in vivo, promotes metabolism, defends against various stresses, facilitates blood circulation, and is effective in fatigue recovery.

Baek Pak is a perennial herb that is attached to the peony family and distributed throughout Korea. It is known to have stems and leaves and dried it in the shade. It is known to have specific skin diseases, scalp health, and scalp bleeding to prevent hair loss. .

Baekbongryeong is a parasitic mushroom rooted in pine roots to strengthen the spleen and stomach to excrete the stagnant foreign body in the body to ease the mind and body.

Aloe is an evergreen perennial herb, which is effective for wound healing and angiogenesis, induction of cell regeneration and proliferation, and prevention of aging of skin and body. It helps to prevent hair loss by being healthy, and is known to be particularly effective in skin diseases such as dandruff and scalp inflammation.

Sukjihwang is a perennial plant belonging to Hyunsamaceae. Its roots are harvested and dried in the shade, and raw raw sulfur and raw sulfur are steamed for 24 hours to become black succinate sulfur, which is not only blackheaded but also improves blood circulation. It helps energy, and when used on the scalp, it helps the growth of the scalp and hair and prevents hair loss.

Cheonggung is an medicinal herb that belongs to the morphology family. It is a highly economical medicinal crop that uses roots with irregular lumps as a medicinal herb.It communicates, releases ulcers, removes customs, promotes blood circulation, and has analgesic effects. It is known to restore the energy of the scalp when used in the scalp to promote blood circulation of the scalp.

Pine needles are the leaves of pine, and Donggibogam writes that the effect of pine needles is effective in preventing adult diseases such as gastrointestinal disease, high blood pressure, stroke, neuralgia, asthma, and arteriosclerosis. In addition, pine needles are used as a treatment or tonic of each disease and indigestion, it promotes blood circulation of the scalp and prevents hair loss.

Ha-Soo is a perennial herb of Park Ju-Ki, which is a root of Park Ju-Ki, which expands blood vessels and relieves spasms, supplying sufficient blood to skin cells, brain cells, and scalp. It is known to be glossy, whiten and effective against severe alopecia.

Side white leaves (側栢葉) to cool the blood while hemostasis and lack of blood is used to thin the hair early and whitening, has the effect of hair growth.

Sangbaekpi (桑白皮) is the heat of the lungs to lower the heat of the lungs to give up the lungs to treat the symptoms of cough, asthma, etc. caused by lung fever. Epidermis has diuretic effect, so it can be used for early acute nephritis, fragile edema, epidemic hepatitis. In addition to the blood pressure strengthening effect, there is an effect to prevent hair loss.

Bamboo leaves are very bitter and cold and have the effect of reducing body heat. The bitter cold nature of bamboo leaves lowers the heat in the heart and lungs, and the spicy temper distracts the wind and heat of the vinegar and prevents hair loss caused by the stress of the body.

Buttercup leaves are effective for pneumonia and jaundice and stabilize the scalp temperature and reduce stress to prevent hair loss.

Ginkgo biloba leaves contain various compounds, especially butyric acid, which is known to act as an insect repellent. Flavonoid-based substances help human blood circulation and promote the blood circulation of the scalp, thereby promoting the role of hair growth. have.

Peppermint is used for a wide range of treatments such as sweating, fever, pain, health, detoxification and early colds, headaches, sore throats and skin diseases. The leaves contain about 1.5% essential oils and about 10% tannins. In addition, in Europe, the leaves of spearmint are used for the treatment of gastric cramps, hyperacidity, dyspepsia, diarrhea, etc. as edema, old wind, pain relief, and soothing agents. Commonly used in dentistry (口中 水) is to drink the peppermint in the water, the smell of the mouth in the direction (芳香), as well as using the topical paralysis, disinfection and antiseptic action of menthol. It is effective in maintaining a healthy scalp.

Walnuts contain large amounts of fat and protein, and are high in vitamin B1 (0.5 mg%). It contains about 60% fat and is a light yellow transparent oil with a very good quality without bad smell or taste. The protein is about 23%, and it is a good protein because it has more tryptophan than other vegetable proteins. There are also many calcium (100 mg%) and phosphorus (300 mg%). It is effective in maintaining healthy scalp by supplying calcium and phosphorus to the scalp. In addition, the fruit of the walnut tree, a deciduous arbor of the sputum family, is known for its high protein and nutritional value, making it shiny on the hair and preventing aging and strengthening kidney function.

Extraction and concentration technology using N ₂ or CO ₂ carrier gas used to extract herbal medicines from the hair loss preventing and regrowth cleaning composition of the present invention is one of the most important processes in the production process of the product as a chemical process It is used in a variety of methods in the laboratory, the carrier gas concentrator system is a heat-sensitive material or a mixture of high evaporation point can be effectively separated using a carrier.

In the present invention, the extraction and concentration system circulates the carrier gas (CO ₂ or N ₂ ) in place of the vacuum pump to reduce the vapor pressure of the solvent to prevent denaturation of thermally unstable compounds, the carrier gas is a closed circuit of the system By circulating in the product can be prepared with a unique herbal ingredients, aromas, flavors of herbal herbal extracts that are easy to volatilize even at low temperatures, and the concentration of the extract can be adjusted according to the application conditions. Figure 2 shows the function of the carrier gas concentrator used in the present invention is shown schematically, Figure 3 shows a schematic diagram of the extraction condenser used in the present invention. As shown in FIG. 2, when the inert CO ₂ or N ₂ is circulated through the pump in the confined space of the system, the vapor pressure of the concentrate (green) portion is lowered, and the carrier containing the solvent moves to the cooler portion, and the solvent condenses. Are collected in a container (red). After condensation, the dried N ₂ is recycled through a pump. Extractive thickeners used in the present invention have the following characteristics:

Extraction Concentrator Capacity: 10-100ℓ

Solvent collector: 10-30ℓ

Circulation pump: up to 2-5㎥ / min, 5HP

Heat exchanger: 2-4㎾ / h

Pressure regulator: Atmospheric pressure

Refrigerant Circulation System: 1-2㎾ / h

N ₂ circulation rate is adjustable (dropping effect of water boiling point 40-41 ℃)

Separation function of herbal herbal extracts (separation efficiency about 80-88%)

Bubble Inhibition and Bumping Inhibitory Effect of Extract Concentrate

Dropping effect of extraction concentration temperature: Figure 4 shows the expected analysis data of the extraction concentration temperature. As shown in FIG. 4, when 200 ml of water is used as a carrier gas, the boiling point has a lowering effect. It was observed that the boiling point was at 56 ° C. when the gas volume was 15 m 3 / h. As a result, it was confirmed that water can be distilled under optimum conditions when the heating temperature is 60 ° C. and the gas volume is 15 m 3 / h.

Separation effect: Figure 5 shows the comparative data of the separation performance of the carrier gas concentrator of the present invention and the conventional vacuum condenser. As shown in FIG. 5, while the reduced pressure concentration is efficient at a gas volume of 8 m 3 / h, the resolution is 20% higher than the reduced pressure distillation when the gas volume is 10 m 3 / h. The optimum condition increased the resolution up to 80% at 15 m 3 / h (gas volume). However, when the maximum gas volume (20㎥ / h), the common material is mixed in the condensate, rather the separation efficiency is lowered.

6 shows a state diagram of temperature and mole fraction. Concentration is an operation that separates solutes and solvents with high boiling point differences and can be compared to stripping of distillation. Distillation is an operation to purify and remove multi-component solution having small boiling point with low boiling point and high boiling point material. For this purpose, when comparing the evaporation concentration and distillation operation using a phase TXY equilibrium diagram, the X value of the phase represents the liquid phase fraction of the low boiling point material and the Y value represents the gas phase fraction of the low boiling point material. The solvent fraction X0 and temperature T0 to be separated are heated by the solvent fraction Y2 and the temperature T2 steam to become the temperature T1, and the ratio (X0-X1) / (Y1-X1) becomes vapor according to the Reverse Bar Scale equation and the rest is evaporated. Is gas-liquid equilibrium in the liquid phase. At this time, the solvent fraction in the liquid phase becomes X1, the solute is concentrated, and the solvent fraction in the gas phase becomes Y1, and the solvent is purified. In this way, the distillation column contacts the low temperature liquid phase and the high temperature gas phase in the reverse direction, repeats evaporative condensation, and concentrates (removes) the boiling point material and purifies the low boiling point material.

Extractive concentrator used in the present invention is a herbal herbal medicine as a main raw material to put a solvent (ethanol, water) and is heated to a constant temperature and pressure, the soluble liquid extracted is called an extract. In addition, the extracted liquid is kept at a constant pressure or reduced pressure to increase the concentration as necessary, and the water (or ethanol) evaporated is introduced into a cooling device, recovered or evaporated, and recycled. The remaining residue (extract or extraction) Concentrated liquid).

In the present invention, herbal herbal medicines are extracted with CO ₂ or N ₂ under low temperature and vacuum, and the extracts are concentrated and concentrated in the form of syrup or jelly in high concentration, without destroying any vitamins, amino acids, etc. Anti-oxidation effect due to viscosity can be maximized, and the physical properties, tastes, aromas and colors generally do not change at all, and change very slowly in the air after extraction. The characteristics of the general extraction and concentration process are as follows.

Antimicrobial and enzymatic effects are more effective than Open Pan evaporators.

50 ~ 60% of the extracted concentrate is monosaccharide and acid with very high osmotic pressure, and the product containing the amount of sugar with low osmotic pressure can be extracted and concentrated to 65-70% of solid content.

In the case of high sugar content such as licorice, it can be heated to evaporation temperature in order to make jam and syrup form.

Pine needles, etc. are usually extracted and concentrated to a concentration of 16-28%, and a suitable mixture may be added or further treatment such as autoclaving.

Ginseng can be concentrated like Open Pan or vacuum concentrator.

Quality changes such as the Maillard reaction by heating are possible.

This extraction concentration evaporation process is carried out under reduced pressure at 60 ℃.

Extract and concentrate without considering the physical properties of herbal medicines, considering the minimum pressure and the maximum temperature for extract concentration.

In the concentration process, the concentration and viscosity are gradually increased, so it is difficult to cool the reaction heat, so that stirring is performed, and extraction concentration is performed.

The carrier gas concentrator used in the present invention is a reactor, the concentrate inlet of the upper part is made of tempered glass, the inside of the concentrator can be observed with the naked eye, and the lid is sealed with a silicone ring to prevent leakage of circulating gas. Use materials that can inhibit the reactivity of the concentrate. The upper part of the reactor is equipped with a stirrer, heat exchanger, control box, heater, operation key, agitator, cooler, and gas circulation pump controller so that all processes are automated and can be easily operated by non-experts. The separator is a device for recovering the solvent of the concentrate, and the glass tube is installed at the side of the separator so that the solvent level can be easily measured. The water tank is a place to store the refrigerant of the heat exchanger, the temperature of the refrigerant can be adjusted to 8-15 ℃, and to increase the concentration efficiency by increasing the solvent exchange rate of the refrigerant circulation device.

Performance test using this carrier gas concentrator (Aerosol Test) To check the azeotropic point of the concentrator to operate with the maximum amount of circulating gas, 10 l of distilled water was added and 0.1 g fluorescein was added to give a light green color. . After operating for 2 hours at a temperature of 50 ° C., a stirrer rotational speed of 60 rpm, a cooler temperature of 15 ° C., and a gas circulation pump of 15 m ³ / h, the separator solution was collected and judged as color by spectrophotometer. No color appeared in the collected solution in this experiment, and it was found that there was no transition of particles at the maximum gas volume.

In addition, the ginseng concentrated in experiments using ginseng juice ground in a crusher, and then extract the experiment the stock solution was placed in a 5ℓ filter concentrator concentrator temperature 60 ℃, N ₂ circulation 10㎥ / h, the coolant temperature heat exchanger 15 ℃ Was performed. Figure 7 shows the temperature change in the interior (concentrate) of the extraction concentrator, the temperature of the concentrate was kept constant after 20 minutes after operation, showing a solvent evaporation amount of 2ℓ / h, the state of the concentrate almost after 2 hours It turned into syrup form and the temperature began to rise slightly. When concentrated under reduced pressure under the same conditions, it was no longer possible to reduce the pressure due to boiling of the concentrate at 400 mbar, and the solvent evaporation amount was 1.2 L / h, indicating that the carrier gas concentrator was 60% efficient in terms of evaporation amount. In the case of reduced pressure concentration, the concentrate of the final syrup form was yellowish brown, and the color of the final concentrate of the extract concentration system of the present invention was yellow, which was the color of the undiluted solution.

As described above, the herbal herbal extract of the present invention extracted from the carrier gas extractor is included in an amount of 5 to 20% by weight based on the total weight of the total composition. When the mixing ratio of the herbal herbal extract is increased, the effect of hair loss prevention and hair growth function is increased. However, it is not directly proportional to the ratio of increasing the content of the herbal herbal medicine extract, containing 8% by weight based on the total weight of the composition has the highest effect of preventing hair loss and hair growth function. When it is contained in an amount of less than 5% by weight there was a problem in that the effect of hair loss prevention and hair loss is inferior.

Hair loss preventing and regrowth cleaning composition of the present invention as a second component of lavender essential oil, peppermint essential oil, tea tree essential oil, vitamin e essential oil and vegetable glycerin of 4 to 6% by weight based on the total weight of the total composition By containing it in an amount, it prevents hair loss and improves hair growth, and also promotes the role of skin neutralization and relieving function.

The hair loss preventing and regrowth cleaning composition of the present invention includes polymycin B sulfate, carfostine C, palmitoyl-DL-carnitine hydrochloric acid, protein kinase C-proanthocyanidin, dichloromethane, perrolic acid, 1.3-butylene recall , A third component consisting of risphosphosphatinic acid and N-ylamino acid ester is added in an amount of 1 to 2% by weight, based on the total weight of the total composition.

In addition, the hair loss preventing and regrowth cleaning composition of the present invention is 2.4-diamino-6-piperadinopi radiamine-3 oxide, sodium sulfate, glacial acetic acid, hydroxyl, alkylsulfonyl, alkyl to promote the cleanliness and health of the scalp 83 to 89% by weight of the cleaning component, the fourth component including sulfinyl, N-pentadecyl, nicotinate, N-oxide, sodium hypochlorite, polymethylene, minoxidil, and propylene glycol, based on the total weight of the total composition It includes.

By using the detergent composition for preventing hair loss and hair regrowth of the present invention, a product such as soap, shampoo, rinse, etc., having anti-hair loss and hair growth function can be prepared by commercialization according to a conventional process. Specifically, for example, each of the first component, the second component, the third component, and the fourth component may be mixed and stirred to solidify, and molded into a required shape to prepare a hair growth functional soap, a shampoo, and a rinse.

Herbal herbal medicines and chemicals that can be added during the production of functional soaps in the hair loss preventing and regrowth cleaning composition of the present invention are shown in Table 2 below.

Addition of Oriental Herbs by Functional Soap Making Additive Chemical Material Malt powder, black sesame seeds, acorns, kelp, seaweed, seaweed, pumpkin seeds, Chinese cabbage seeds, milk, eggs, honey, pollen, juniper, anchovy, ginseng, Astragalus, Angelica, sesame, hodo, bokbunja. Raw yellow hwang, golgoji, pineapple, sweet ginseng, safflower, fermented soybeans, corn oil extract, Chinese cabbage seed oil, letter seed oil, black sesame, goat and fur powder, ox horn powder, silkworm stool and cocoon powder, rice bran oil, raw sesame oil, sun salt , Honey, wheat berry extract, old, soybean, black rice, yeast concentrate, perilla, sesame, walnut, seaweed, mussels, oyster, anchovy, seaweed, kelp, sterilized water, ganoderma lucidum, sugar, pepper seed, bark skin, peppermint, ginseng, Licorice, Yeonmyeongpi, Sewao, Placenta extract, Cordyceps sinensis, Herbal extract, Natural vinegar, Alite powder, onion, castor oil, olive oil, sesame oil, ocher, garlic ginger, mugwort, ginseng, aloe, shiitake bustle , Ogapi, Vitamin Concentrate, Licorice, Rice Bran, Glucose, Lactose, Corn Beard, Straw, Red Ginseng Root, Honey, Black Sesame, Sewage, Sukchangpo, Fresh Green Yellow, Sweet Ginseng, Jindae, Astronomical Bronze, Upper Leaf, Ogapi, Bokbunja, Almond, Raw Garlic Extract, Sugar, snowflake, black rice, apple rock, gardenia, mint, mulberry , Persimmon leaves, wolfberry, peach leaf, ginseng, pine needle, mulberry, ginkgo biloba, raspberry, ganoderma lucidum, walnut, black sesame, jujube, garlic, soybeans, ginger, red pepper, spinach, pumpkin, honey, kelp, seaweed, Buttercup, Bellflower, Leafy, Cordyceps, Soybeans, Yulmu, Buckwheat, Ogapi, Wolfberry, Shou, Ginger, Black Sesame, White Leaf, Vitamin B2 2.4-diamino-6-piperadinopy radiamine-3oxide, sodium sulfate, glacial acetic acid, hydroxyl, alkylsulfonyl, alkylsulfinyl, N-pentadecyl, nicotinate, N-oxide, sodium hypochlorite, poly Methylene, minoxidil, propylene glycol

In addition, herbal organisms and additional chemical materials added during the production of the functional shampoo are as shown in Table 3 below.

Natural material Chemical material Shrimp orchid extract, navel extract, canned extract, crunchy extract, persimmon extract, lemon extract, tangerine extract, aloe extract, ginseng extract, ginseng extract, triticale extract, cypress leaf extract, mangle, cheongung, white paper, lotus leaf, sessin, White porcelain, sandalwood, vinegar, rich man, walnut Polymycin B sulfate, carfostine C,
Palmitoyl-DL-carnitine hydrochloric acid, protein kinase C-proanthocyanidins,
Dichloromethane, perrolic acid, 1.3-butylene recall, risphospatidinic acid, N-ylsilamino acid ester

In addition, herbal organisms and additional chemical materials added during the functional rinse preparation are shown in Table 4 below.

Natural material Chemical material Health, wolfberry, dansam, donkey, caucus, tofu, manza, pasta, half, white porcelain, baekchul, golgoji, bokbunja, cornus, ginger, small fennel, sukjiji, shiho, baekbaekpi, yeojangsil, ogalpi, omija, osuyu, broiler , Breeding, ginseng, red ginseng, cloves, Cheongung, Cheoncho, Shouo, Hyangbuja, safflower, Astragalus Polymycin B sulfate, carfostine C,
Palmitoyl-DL-carnitine hydrochloric acid,
Protein kinase C-proanthocyanidins, dichloromethane, ferrolic acid, 1.3-butylene recalls, risphospatidinic acid, N-ylsilaminoacid esters

The cleaning composition comprising the herbal herbal extract of the present invention can not only prevent hair loss but also obtain the effect of hair growth, and does not destroy vitamins, amino acids, etc., which are the active ingredients of herbal herbal medicines, and has high viscosity with enzymatic activity and low oxygen solubility. The anti-oxidation effect can be maximized and it changes very slowly even in the air after extraction without changing the physical properties, taste, aroma and color.

Herbal herbal medicine contained in shampoo by leaving hair for 5-10 minutes in the state of foaming by shampooing hair twice a day using soap, shampoo and rinse prepared using the hair loss preventing and hair removal cleaning composition of the present invention By allowing the pharmacological components of the extract to be absorbed into the scalp, the active ingredient of each herbal medicine can be absorbed into the scalp, and it is more effective to lightly massage or scrub the scalp of the head with soap bubbles during shampooing. In addition, the use of shampoo is not a problem even if the scalp is used several times a day.

Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the following examples are only for illustrating the present invention, and the scope of the present invention is not limited thereto.

Example 1: Preparation of detergent composition comprising herbal herbal extract

(Step 1)

The herbal herbal powders shown in Table 5 were mixed, extracted and concentrated using N ₂ or CO ₂ carrier gas to obtain herbal herbal extracts.

Herbal Herbs Content (kg) Thuja orientalis 0.6 Morus bombysis 0.6 Bamboo leaf (Seaa borealis) 0.4 Ginkgo biloba L. 0.6 Pine needles (Pinus denciflora) 0.6 Licorice (Glycyrrluizae urealensis) 0.3 Ginseng (Ginseng urealensis) 0.3 Pulsatilla Radix 0.1 Branch (Kochiae Fructus) 0.2 Paeonia suffruticosa 0.2 Wolfberry (Lycium chinense) 0.2 Soojijihyang (Rehmannia hlutinosa Liboschtz) 0.5 Baekbokyeong (Poria cocos) 0.3 Cornus officinalis 0.3 Black bean (Glycine max Merr) 0.3 Black tide (Sesanmum indicum) 0.4 Capsicum annuum L. 0.3 Acanthopanx sessiliflorus 0.4 Taxi (Alisima plantago-aquatica) 0.3 Mushroom (Agaricus blazei) 0.5 Pogongyoung (Taraxacum ohwianum) 0.4 Packing (Laminariae Folium) 0.5 White 0.3

(Step 2)

The herbal herbal extract 5-20% by weight, lavender essential oil, peppermint essential oil, tea tree essential oil, vitamin e essential oil 5-6% by weight of the oil component consisting of vegetable glycerin, polymycin B sulfate, carfostine C, 1-2 wt% of chemicals consisting of palmitoyl-DL-carnitine hydrochloric acid, protein kinase C-proanthocyanidins, dichloromethane, ferrolic acid, 1.3-butylene recall, risphospatidinic acid and N-ylsilamino acid esters and 2.4-diamino-6-piperadinopy radiamine-3oxide, sodium sulfate, glacial acetic acid, hydroxyl, alkylsulfonyl, alkylsulfinyl, N-pentadecyl, nicotinate, N-oxide, sodium hypochlorite, poly 80-85% by weight of the cleaning component consisting of methylene, minoxidil and propylene glycol were mixed, stirred and solidified, and molded into the required shape to prepare functional soaps, shampoos and rinses.

Test Example 1 Hair Loss Prevention and Hair Growth Effect Measurement

50 subjects with hair loss and baldness were selected and shampooed twice a day using the shampoo obtained in Example 1, and left in the shampoo for 5-10 minutes in a state of foaming. The pharmacological components of the herbal herbal extracts were absorbed into the scalp, so that the active ingredients of each herbal biomaterial were absorbed into the scalp. In the shampooing process, a light massage or acupressure was applied to the scalp of the head with soap bubbles.

As a result, after 50 months of continuous baldness, 48 patients had a significant reduction in hair loss. Among them, 36 hairs were found to have fluffy initial hair growth from the hair follicles. After 2 months, hair regrowth gradually thickened, and at the same time, new hair began to develop on the scalp, which had not been regrown in just 1 month, and after 4-5 months, symptoms gradually improved, compared to the beginning of use at 6 months. It was possible to identify the hair growth to be clearly distinguished. From these results, hair loss was reduced from 2 to 3 days, and hair loss was almost stopped after 20 days. Hair loss was stopped after about 1 month. It is believed that new hair growth will occur, as are the subjects of baldness. Among these experiments, there was a difference in the degree of improvement according to the subject's constitution, occupation, and lifestyle, but generally satisfactory effects were obtained.

The detergent composition containing the herbal herbal medicine extract of the present invention does not destroy any vitamins, amino acids, etc. of the herbal herbal medicines, and can maximize the anti-oxidation effect due to high viscosity and enzymatic activity, low oxygen solubility, as well as physical properties, taste, It is expected to be very useful in the art as the hair loss prevention effect and hair growth effect are greatly improved by having a characteristic that changes very slowly in the atmosphere after extraction without changing the fragrance and color.

Claims (7)

In the hair loss preventing and regrowth cleaning composition comprising herbal herbal medicine extract,
0.6 kg of Thuja orientalis, 0.6 to 0.8 kg of upper leaf (Morus bombysis), 0.4 to 0.55 kg of Seaa borealis, 0.6 to 0.8 kg of Ginkgo biloba L., 0.6 to 0.8 kg of Pinus denciflora , Glycyrrluizae urealensis 0.3 to 0.4 kg, Ginseng urealensis 0.3 to 0.4 kg, Pulsatilla Radix 0.1 to 0.13 kg, Kochiae Fructus 0.2 to 0.27 kg, Peonia suffruticosa 0.2 to 0.27 kg , Lycium chinense 0.2 to 0.27 kg, Rehmannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 to 0.4 kg, Glycine max Merr 0.3 To 0.4 kg, Black injima (Sesanmum indicum) 0.4 to 0.53 kg, Gochu (Capsicum annuum L.) 0.3 to 0.4 kg, Ogapi (Acanthopanx sessiliflorus) 0.4 kg, Taxa (Alisima plantago-aquatica) 0.3 kg Mushroom (Agaricus blazei) 0.5 To 0.67 kg, Taxacum ohwianum 0.4 to 0.53 kg, Laminariae Folium 0 Herbal herbal medicine extracts obtained by extracting and concentrating herbal herbal powders containing .5-0.67 kg and 0.3-0.4 kg of white porcelain using N ₂ or CO ₂ Carrier Gas were added to the total weight of the total composition. 5 to 20% by weight,
5 to 6% by weight of an oil component consisting of lavender essential oil, peppermint essential oil, tea tree essential oil, vitamin e essential oil and vegetable glycerin,
Polymycin B Sulfuric Acid, Carfostine C, Palmitoyl-DL-Carnitine Hydrochloric Acid, Protein Kinase C-Proanthocyanidins, Dichloromethane, Perrolic Acid, 1.3-Butylene Recall, Rizophosphatidic Acid and N-Isylamino Acid Ester 1 to 2% by weight based on the total weight of the chemical material and
2.4-diamino-6-piperadinopy radiamine-3oxide, sodium sulfate, glacial acetic acid, hydroxyl, alkylsulfonyl, alkylsulfinyl, N-pentadecyl, nicotinate, N-oxide, sodium hypochlorite, poly A cleaning composition for preventing hair loss and regrowth, comprising a cleaning component consisting of methylene, minoxidil and propylene glycol in an amount of 80 to 85% by weight based on the total weight of the composition. delete The method of claim 1,
Herbal herbal medicine extract for hair loss prevention and regrowth, characterized in that the extract is contained in an amount of 8% by weight. delete delete delete 0.6 kg of Thuja orientalis, 0.6 to 0.8 kg of upper leaf (Morus bombysis), 0.4 to 0.55 kg of Seaa borealis, 0.6 to 0.8 kg of Ginkgo biloba L., 0.6 to 0.8 kg of Pinus denciflora , Glycyrrluizae urealensis 0.3 to 0.4 kg, Ginseng urealensis 0.3 to 0.4 kg, Pulsatilla Radix 0.1 to 0.13 kg, Kochiae Fructus 0.2 to 0.27 kg, Peonia suffruticosa 0.2 to 0.27 kg , Lycium chinense 0.2 to 0.27 kg, Rehmannia hlutinosa Liboschtz 0.5 to 0.67 kg, Poria cocos 0.3 to 0.4 kg, Cornus officinalis 0.3 to 0.4 kg, Glycine max Merr 0.3 To 0.4 kg, Black injima (Sesanmum indicum) 0.4 to 0.53 kg, Gochu (Capsicum annuum L.) 0.3 to 0.4 kg, Ogapi (Acanthopanx sessiliflorus) 0.4 kg, Taxa (Alisima plantago-aquatica) 0.3 kg Mushroom (Agaricus blazei) 0.5 To 0.67 kg, Taxacum ohwianum 0.4 to 0.53 kg, Laminariae Folium 0 .5 to 0.67 kg and 0.3 to 0.4 kg of White are mixed, extracted and concentrated using N ₂ or CO ₂ carrier gas,
5 to 20% by weight of the herbal herbal extracts obtained based on the total weight of the composition,
5 to 6% by weight of an oil component consisting of lavender essential oil, peppermint essential oil, tea tree essential oil, vitamin e essential oil and vegetable glycerin,
Polymycin B Sulfuric Acid, Carfostine C, Palmitoyl-DL-Carnitine Hydrochloric Acid, Protein Kinase C-Proanthocyanidins, Dichloromethane, Perrolic Acid, 1.3-Butylene Recall, Rizophosphatidic Acid and N-Isylamino Acid Ester 1 to 2% by weight based on the total weight of the chemical material and
2.4-diamino-6-piperadinopy radiamine-3oxide, sodium sulfate, glacial acetic acid, hydroxyl, alkylsulfonyl, alkylsulfinyl, N-pentadecyl, nicotinate, N-oxide, sodium hypochlorite, poly A method for producing a cleaning composition for preventing hair loss and regrowth, comprising mixing 80 to 85% by weight of a cleaning component consisting of methylene, minoxidil and propylene glycol with respect to the total weight of the composition.

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