CN111588663B - Fixing gel composition and preparation method thereof - Google Patents
Fixing gel composition and preparation method thereof Download PDFInfo
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- CN111588663B CN111588663B CN202010377973.2A CN202010377973A CN111588663B CN 111588663 B CN111588663 B CN 111588663B CN 202010377973 A CN202010377973 A CN 202010377973A CN 111588663 B CN111588663 B CN 111588663B
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- 239000000203 mixture Substances 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 45
- 230000000694 effects Effects 0.000 claims abstract description 32
- 239000008367 deionised water Substances 0.000 claims abstract description 31
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 31
- 239000000843 powder Substances 0.000 claims abstract description 30
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 239000003086 colorant Substances 0.000 claims abstract description 19
- 239000002562 thickening agent Substances 0.000 claims abstract description 12
- 239000003906 humectant Substances 0.000 claims abstract description 11
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 86
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 54
- 229920001577 copolymer Polymers 0.000 claims description 51
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 40
- 238000003756 stirring Methods 0.000 claims description 28
- 238000005303 weighing Methods 0.000 claims description 28
- 239000003755 preservative agent Substances 0.000 claims description 27
- 239000004408 titanium dioxide Substances 0.000 claims description 27
- 239000000284 extract Substances 0.000 claims description 26
- 230000002335 preservative effect Effects 0.000 claims description 26
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 24
- 244000144730 Amygdalus persica Species 0.000 claims description 22
- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 claims description 22
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 21
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 20
- 239000000377 silicon dioxide Substances 0.000 claims description 20
- 229920006037 cross link polymer Polymers 0.000 claims description 19
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 18
- CCLARULDIPFTCP-BOYHRMMASA-N (2r,3r,4r,5s)-heptane-1,2,3,4,5,6-hexol Chemical compound CC(O)[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO CCLARULDIPFTCP-BOYHRMMASA-N 0.000 claims description 17
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 14
- 238000003860 storage Methods 0.000 claims description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 13
- 239000004480 active ingredient Substances 0.000 claims description 10
- BQMNFPBUAQPINY-UHFFFAOYSA-N azane;2-methyl-2-(prop-2-enoylamino)propane-1-sulfonic acid Chemical compound [NH4+].[O-]S(=O)(=O)CC(C)(C)NC(=O)C=C BQMNFPBUAQPINY-UHFFFAOYSA-N 0.000 claims description 8
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 7
- 229920002261 Corn starch Polymers 0.000 claims description 7
- 239000008120 corn starch Substances 0.000 claims description 7
- 229920002472 Starch Polymers 0.000 claims description 6
- 235000019698 starch Nutrition 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 5
- 240000003183 Manihot esculenta Species 0.000 claims description 5
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 5
- 229920002125 Sokalan® Polymers 0.000 claims description 5
- OWBTYPJTUOEWEK-UHFFFAOYSA-N butane-2,3-diol Chemical compound CC(O)C(C)O OWBTYPJTUOEWEK-UHFFFAOYSA-N 0.000 claims description 5
- 239000002738 chelating agent Substances 0.000 claims description 5
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 5
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 claims description 5
- 239000000600 sorbitol Substances 0.000 claims description 5
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 4
- 229960001631 carbomer Drugs 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 241001112020 Eriocaulon Species 0.000 claims 1
- 239000000834 fixative Substances 0.000 claims 1
- 239000003344 environmental pollutant Substances 0.000 abstract description 7
- 231100000719 pollutant Toxicity 0.000 abstract description 7
- 230000005779 cell damage Effects 0.000 abstract description 3
- 208000037887 cell injury Diseases 0.000 abstract description 3
- 230000008591 skin barrier function Effects 0.000 abstract description 3
- 238000001179 sorption measurement Methods 0.000 abstract description 3
- 239000013543 active substance Substances 0.000 abstract description 2
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000499 gel Substances 0.000 description 28
- 210000003491 skin Anatomy 0.000 description 27
- 229940063556 marrubium vulgare extract Drugs 0.000 description 23
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 17
- 150000002148 esters Chemical class 0.000 description 17
- 230000000052 comparative effect Effects 0.000 description 16
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 14
- 238000012360 testing method Methods 0.000 description 11
- 239000000047 product Substances 0.000 description 9
- FWFUWXVFYKCSQA-UHFFFAOYSA-M sodium;2-methyl-2-(prop-2-enoylamino)propane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(C)(C)NC(=O)C=C FWFUWXVFYKCSQA-UHFFFAOYSA-M 0.000 description 9
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 8
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 8
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 8
- 230000006378 damage Effects 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 210000004243 sweat Anatomy 0.000 description 3
- 240000005809 Prunus persica Species 0.000 description 2
- JMBINOWGIHWPJI-UNSOMVRXSA-N [(2r,3r,4r,5r,6r)-2-[[(2r,3r,4r)-3,4-dihydroxy-4-(hydroxymethyl)oxolan-2-yl]oxymethyl]-6-[2-(3,4-dihydroxyphenyl)ethoxy]-5-hydroxy-4-[(2s,3r,4r,5r,6s)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-3-yl] (e)-3-(3,4-dihydroxyphenyl)prop-2-enoate Chemical group O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC(=O)\C=C\C=2C=C(O)C(O)=CC=2)[C@@H](CO[C@H]2[C@@H]([C@@](O)(CO)CO2)O)O[C@@H](OCCC=2C=C(O)C(O)=CC=2)[C@@H]1O JMBINOWGIHWPJI-UNSOMVRXSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 230000005660 hydrophilic surface Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229940031722 methyl gluceth-20 Drugs 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- YLGYACDQVQQZSW-UHFFFAOYSA-N n,n-dimethylprop-2-enamide Chemical compound CN(C)C(=O)C=C YLGYACDQVQQZSW-UHFFFAOYSA-N 0.000 description 2
- 231100000760 phototoxic Toxicity 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000004381 surface treatment Methods 0.000 description 2
- 230000035900 sweating Effects 0.000 description 2
- 229940104261 taurate Drugs 0.000 description 2
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 2
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 1
- AQTKXCPRNZDOJU-NXRLNHOXSA-N 2-(alpha-D-galactosyl)glycerol Chemical compound OCC(CO)O[C@H]1O[C@H](CO)[C@H](O)[C@H](O)[C@H]1O AQTKXCPRNZDOJU-NXRLNHOXSA-N 0.000 description 1
- AQTKXCPRNZDOJU-UHFFFAOYSA-N 2-O-alpha-D-Galactopyranosylglycerol Natural products OCC(CO)OC1OC(CO)C(O)C(O)C1O AQTKXCPRNZDOJU-UHFFFAOYSA-N 0.000 description 1
- 244000293323 Cosmos caudatus Species 0.000 description 1
- 235000005956 Cosmos caudatus Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 244000137850 Marrubium vulgare Species 0.000 description 1
- 235000005321 Marrubium vulgare Nutrition 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 1
- SOSLMHZOJATCCP-AEIZVZFYSA-N afzelin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1OC1=C(C=2C=CC(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O SOSLMHZOJATCCP-AEIZVZFYSA-N 0.000 description 1
- SOSLMHZOJATCCP-PADPQNGGSA-N afzelin Natural products O([C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@H](C)O1)C1=C(c2ccc(O)cc2)Oc2c(c(O)cc(O)c2)C1=O SOSLMHZOJATCCP-PADPQNGGSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000006315 carbonylation Effects 0.000 description 1
- 238000005810 carbonylation reaction Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- UKYVGQJPUFNXKS-UHFFFAOYSA-N floridoside Natural products CC(=O)OCC(COC(C)=O)OC1OC(COC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O UKYVGQJPUFNXKS-UHFFFAOYSA-N 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000002556 kaempferol derivatives Chemical class 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000003859 lipid peroxidation Effects 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
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- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- -1 pH regulators Substances 0.000 description 1
- JMBINOWGIHWPJI-UHFFFAOYSA-N pedicularoside A Natural products OC1C(O)C(O)C(C)OC1OC1C(OC(=O)C=CC=2C=C(O)C(O)=CC=2)C(COC2C(C(O)(CO)CO2)O)OC(OCCC=2C=C(O)C(O)=CC=2)C1O JMBINOWGIHWPJI-UHFFFAOYSA-N 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 229940104256 sodium taurate Drugs 0.000 description 1
- 210000000434 stratum corneum Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 108700012359 toxins Proteins 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8182—Copolymers of vinyl-pyrrolidones. Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W90/00—Enabling technologies or technologies with a potential or indirect contribution to greenhouse gas [GHG] emissions mitigation
- Y02W90/10—Bio-packaging, e.g. packing containers made from renewable resources or bio-plastics
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a make-up fixing gel composition and a preparation method thereof. The formula comprises the following components in percentage by weight: 0.5 to 5 percent of fixing powder, 0.2 to 3 percent of colorant, 0.35 to 4 percent of film forming agent, 0.2 to 5 percent of active component with anti-pollution effect, 0.05 to 1 percent of thickening agent, 0.5 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water. The invention combines the fixing powder, the colorant and the film forming agent, is convenient to carry and use, does not fly powder, is not sticky to hands, and has good fixing effect and comfortable skin feel. The film forming agent is matched with an anti-pollution active substance, so that physical separation can be formed on the surface of the skin, the adsorption of pollutants on the skin is reduced, cell damage caused by pollution can be resisted, the skin barrier is strengthened, and the tolerance of the skin to the pollutants is increased.
Description
Technical Field
The invention relates to a makeup setting gel composition, belongs to the technical field of daily chemical products, and particularly relates to a makeup setting gel composition and a preparation method thereof.
Background
Beauty is the nature of human, and makeup can adjust the shape and color, mask defects, show spiritual and add charm. With the development of society, makeup is not exclusive for women, and the frequency of makeup for men is gradually increased. In real life, proper makeup is also a behavior that respects others.
Makeup removal due to sweating, oil secretion and the like is an inevitable choice for every person who love makeup. Thus, the makeup-fixing product which can make the makeup more durable has a wide and huge market.
Currently, most of the makeup setting products on the market are makeup setting powder, makeup setting liquid and makeup setting spray. The makeup powder is prepared from pulvis Talci, margarita powder, silica, mica, and plant starch, and has effects of adsorbing excessive facial oil and reducing facial gloss, and can make makeup more durable, fine and smooth. However, such loose powder is easy to spill and fly when in use, inconvenient to use and has inhalation risk. The makeup fixing liquid and the makeup fixing spray usually need to be added with a film forming agent, and have the problems of low film forming speed, hand sticking of the formed protective film and the like.
In recent years, the anti-pollution efficacy of cosmetics has become a new complaint from consumers due to the increase in environmental pollution. Polluted atmosphere contains Polycyclic Aromatic Hydrocarbons (PAHs) and Nitro Polycyclic Aromatic Hydrocarbons (NPAHs) with phototoxic effect, and the phototoxic effect caused by the polycyclic aromatic hydrocarbons can seriously damage skin under ultraviolet irradiation, including accelerating the formation of free radicals and accelerating the aging of the skin.
Therefore, new products of makeup fixing gel compositions capable of improving the disadvantages of makeup fixing powders and makeup fixing liquid products and having an anti-pollution effect are urgently needed.
Disclosure of Invention
In order to overcome the above problems, it is an object of the present invention to provide a make-up fixing gel composition having an anti-contamination effect and a method for preparing the same.
The technical problem to be solved by the present invention is achieved by the following technical means.
The invention provides a make-up fixing gel composition, which comprises the following components in percentage by weight:
0.5 to 5 percent of dressing powder, 0.2 to 3 percent of colorant, 0.35 to 4 percent of film forming agent, 0.2 to 5 percent of active component with anti-pollution effect, 0.05 to 1 percent of thickening agent, 0.5 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water.
Further, the formula of the make-up fixing gel composition comprises the following components in percentage by weight:
0.5 to 4 percent of dressing powder, 0.3 to 2 percent of colorant, 0.5 to 3 percent of film forming agent, 1 to 5 percent of active component with anti-pollution effect, 0.1 to 1 percent of thickening agent, 1 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water.
Further, the dressing powder is selected from one or a mixture of more than two of silica, corn starch and cassava starch.
Further, the coloring agent is selected from titanium dioxide, red iron oxide, black iron oxide and yellow iron oxide, and has hydrophilicity after hydrophilic surface treatment.
Further, the film former is a VP/VA copolymer.
Further, the weight ratio of the total amount of the dressing powder and the colorant to the film forming agent is 0.5 to 2.
Further, the anti-pollution effective active ingredients comprise marrubium vulgare extract and peach blossom extract which are mixed according to the weight ratio of 1.
Further, the thickening agent is selected from one or a mixture of more than two of carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and ammonium acryloyldimethyl taurate/VP copolymer.
Further, the humectant is one or a mixture of more than two of glycerin, propylene glycol, butanediol, methyl propylene glycol, dipropylene glycol, sorbitol, methyl gluceth-20 and glyceryl polyether-26.
Further, the other components are selected from one or more of preservatives, pH regulators, chelating agents.
In addition, the invention also provides a preparation method of the make-up fixing gel composition, which specifically comprises the following process steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding a thickening agent and a chelating agent, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding the dressing powder, the film forming agent, the anti-pollution active ingredient, the coloring agent, the humectant and the preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
By means of the technical scheme, the invention has the following beneficial technical effects:
1) The invention overcomes the problems that the powder for fixing the makeup is inconvenient to use, the film forming speed of the fixing lotion is slow, and the formed protective film is sticky to hands, is convenient to carry and use, can be uniformly smeared after being lightly smeared, does not fly powder, is not sticky to hands, has lasting effect of fixing the makeup and can keep the skin in a dry and comfortable state for a long time.
2) The film-forming agent VP/VA copolymer in the formula of the composition can form physical barrier on the surface of skin, and reduces the adsorption of pollutants on the skin.
3) The active ingredients of the anti-pollution efficacy in the formula of the composition comprise the marrubium vulgare extract and the peach blossom extract, and the two extracts are used together to resist cell damage caused by pollution, strengthen skin barrier and increase the tolerance of skin to pollutants.
Detailed Description
The invention relates to a make-up fixing gel composition, which comprises the following components in percentage by weight:
0.5 to 5 percent of dressing powder, 0.2 to 3 percent of colorant, 0.35 to 4 percent of film forming agent, 0.2 to 5 percent of active component with anti-pollution effect, 0.05 to 1 percent of thickening agent, 0.5 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water.
All the raw material components of the invention are commercially available.
The dressing powder used in the dressing gel composition of the present invention is selected from silica, corn starch, tapioca starch, and is 0.5 to 5%, more preferably 0.5 to 4% of the total amount of the formula. They have a porous structure and can effectively adsorb oil and fat, prevent makeup removal, and give smooth and soft feeling and soft-focus effect to the skin.
The coloring agent used in the make-up fixing gel composition is selected from titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow, and accounts for 0.2-3% of the total amount of the formula, and more preferably 0.3-2%. Wherein the titanium dioxide can be used as a coloring agent and has a sun-screening effect. The titanium dioxide, the iron oxide red, the iron oxide black and the iron oxide yellow are subjected to hydrophilic surface treatment, have hydrophilicity, are easy to disperse in a formula and can be quickly developed. Can be applied to skin for modifying skin color and refining pores.
The film former used in the make-up gel composition of the present invention is a VP/VA copolymer. The VP/VA copolymer, namely the copolymer of the vinyl pyrrolidone and the vinyl acetate, can form a thin protective film on the skin, and shows film flexibility, good adhesiveness and glossiness. 0.35 to 4%, more preferably 0.5 to 3% of the total amount of the formulation.
The fixing powder and the colorant are added into the aqueous formula and are used in combination with the film forming agent, a film containing fine powder is formed on the surface of skin, powder flying during use can be prevented, the phenomenon of powder sticking when the fixing powder is used for drying skin can be prevented, and the sticky feeling of the film forming agent is reduced. The skin feel of the product is more comfortable, the makeup is more natural, and the makeup is more durable.
The anti-pollution effective active ingredients used in the make-up fixing gel composition comprise marrubium vulgare extract and peach blossom extract, and account for 0.2-5% of the total amount of the formula, and the anti-pollution effective active ingredients are more preferably 1-5%. Wherein the marrubium vulgare extract is extracted from the marrubium vulgare, and the main active component is forsythoside B. Can block the migration of contaminants to the nucleus and the production of toxins; prevention of protein carbonylation and lipid peroxidation; help to rebuild a healthy stratum corneum, prevent further damage and dehydration; improve the mitochondrial respiratory chain and thereby replenish energy to the cell.
The marrubium vulgare extract can purify the skin, help the skin keep original fineness, prevent the skin color from becoming dull and dark, and ensure the skin to be smooth and soft. The ingredient is sold under the tradename Citystem TM Supplied by Croda.
Peach blossom extract mainly contains flavonoids such as kaempferol derivatives: floridoside and afzelin. Can obviously reduce the degree of epidermal oxidation caused by pollution, slow down the generation of cell waste and prevent premature senility of cells. The ingredient is named Phytescence TM Peach Flower is supplied by Croda.
The film-forming agent VP/VA copolymer can form physical barrier on the skin surface, and reduces the adsorption of pollutants on the skin. The active ingredients of the anti-pollution efficacy, namely the marrubium vulgare extract and the peach blossom extract, can resist cell damage caused by pollution, strengthen the skin barrier and increase the tolerance of the skin to pollutants. The film forming agent and the anti-pollution effective active ingredient are combined for use, so that the damage of pollutants to the skin can be effectively resisted from inside to outside. The three components have the function of synergy.
The thickener used in the make-up gel composition of the present invention is selected from carbomers, acrylates/C10-30 alkanol acrylate crosspolymer, hydroxyethyl acrylate/sodium acryloyldimethyltaurate copolymer, ammonium acryloyldimethyltaurate/VP copolymer. Can adjust the rheological property of the product and bring better use experience. Is 0.05-1%, preferably 0.1-1%.
The moisturizer used in the make-up remover gel composition of the present invention is selected from the group consisting of glycerin, propylene glycol, butylene glycol, methyl propylene glycol, dipropylene glycol, sorbitol, methyl gluceth-20, glyceryl polyether-26, and the like, which can keep the skin moist and comfortable. Accounting for 0.5 to 10 percent of the total amount of the formula, and more preferably accounting for 1 to 10 percent of the total amount of the formula.
The preparation method of the make-up fixing gel composition specifically comprises the following process steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding a thickening agent and a chelating agent, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding the fixing powder, the film forming agent, the anti-pollution active ingredient, the colorant, the humectant and the preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
The present invention will be described in more detail below with reference to specific preferred embodiments and examples of effects, but the present invention is not limited to the following examples.
Example 1
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
0.5g of silica, 0.2g of titanium dioxide, 0.35g of VP/VA copolymer, 0.1g of marrubium vulgare extract, 0.1g of peach blossom extract, 0.05g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 200.5g of methyl glucitol polyether, 0.05g of disodium EDTA, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating to 75-80 ℃ in a water bath, and keeping the temperature for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the material in the container A is reduced to 45 ℃, adding silica, titanium dioxide, VP/VA copolymer, marrubium vulgare extract, peach blossom extract, methyl glucitol polyether-20 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Example 2
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
1g of corn starch, 2.89g of titanium dioxide, 0.03g of iron oxide red, 0.02g of iron oxide black, 0.06g of iron oxide yellow, 3g of VP/VA copolymer, 1g of marrubium vulgare extract, 1g of peach blossom extract, 0.8g of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 4g of butanediol, 3g of glyceryl polyether-26, 0.05g of disodium EDTA, proper amounts of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding hydroxyethyl acrylate/acryloyl dimethyl sodium taurate copolymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding corn starch, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, marrubium vulgare extract, peach blossom extract, butanediol, glyceryl polyether-26 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Example 3
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
0.5g of cassava starch, 0.2g of titanium dioxide, 1.4g of VP/VA copolymer, 1.5g of marrubium vulgare extract, 1.5g of peach blossom extract, 0.5g of acryloyl dimethyl ammonium taurate/VP copolymer, 2g of glycerol, 3g of propylene glycol, 0.05g of EDTA disodium, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl ammonium taurate/VP copolymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the material in the container A is reduced to 45 ℃, adding the cassava starch, the titanium dioxide, the VP/VA copolymer, the marrubium vulgare extract, the peach blossom extract, the glycerol, the propylene glycol and the preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Example 4
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
3g of silica, 2g of corn starch, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 4g of VP/VA copolymer, 2.5g of marrubium vulgare extract, 2.5g of peach blossom extract, 0.3g of carbomer, 0.7g of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 5g of methyl propylene glycol, 3g of dipropylene glycol, 2g of sorbitol (sugar) alcohol, 0.05g of disodium EDTA, a proper amount of a pH regulator and a proper amount of a preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding carbomer, hydroxyethyl acrylate/acryloyl dimethyl taurate copolymer and EDTA disodium, heating to 75-80 ℃ in a water bath, and keeping the temperature for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, corn starch, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, marrubium vulgare extract, peach blossom extract, methyl propylene glycol, dipropylene glycol, sorbitol and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Example 5
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 2g of VP/VA copolymer, 2g of marrubium vulgare extract, 2g of peach blossom extract, 0.5g of acryloyl dimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, methyl glucitol polyether-201g, 0.05g of EDTA disodium, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, marrubium vulgare extract, peach blossom extract, butanediol, methyl glucitol polyether-20 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Comparative example 1
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of VP/VA copolymer, 2g of marrubium vulgare extract, 2g of peach blossom extract, 0.5g of acryloyl dimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of EDTA disodium, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding the VP/VA copolymer, the marrubium vulgare extract, the peach blossom extract, the butanediol, the methyl glucitol polyether-20 and the preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Comparative example 2
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 2g of marrubium vulgare extract, 2g of peach blossom extract, 0.5g of ammonium acryloyl dimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of disodium EDTA, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, marrubium vulgare extract, peach blossom extract, butanediol, methyl glucitol polyether-20 and preservative, stirring uniformly, then transferring into a closed container for storage and filling.
Comparative example 3
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 2g of VP/VA copolymer, 0.5g of ammonium acryloyldimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of disodium EDTA, a proper amount of a pH regulator and a proper amount of a preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating to 75-80 ℃ in a water bath, and keeping the temperature for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, butanediol, methyl glucitol polyether-20 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Comparative example 4
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 0.5g of ammonium acryloyldimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of disodium EDTA, a proper amount of a pH regulator and a proper amount of a preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, butanediol, methyl glucitol polyether-20 and a preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Comparative example 5
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 2g of VP/VA copolymer, 4g of marrubium vulgare extract, 0.5g of ammonium acryloyl dimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of disodium EDTA, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, marrubium vulgare extract, butanediol, methyl glucitol polyether-20 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
Comparative example 6
A make-up fixing gel composition is prepared from the following components in parts by mass per 100g of the composition:
2g of silica, 0.95g of titanium dioxide, 0.01g of iron oxide red, 0.02g of iron oxide black, 0.02g of iron oxide yellow, 2g of VP/VA copolymer, 4g of peach blossom extract, 0.5g of ammonium acryloyldimethyl taurate/VP copolymer, 0.3g of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 4g of butanediol, 20 g of methyl glucitol polyether-20, 0.05g of disodium EDTA, a proper amount of pH regulator and preservative, and the balance of deionized water.
The preparation process comprises the following steps:
1) Accurately weighing a specified amount of deionized water in the formula into a container A, adding acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and EDTA disodium, heating in a water bath to 75-80 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator in the formula into a container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding silica, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, VP/VA copolymer, peach blossom extract, butanediol, methyl glucitol polyether-20 and preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
The following is a content of the effect application test example section.
Examples of Effect application
1. Efficacy testing
The products of examples 1 to 5 of the present invention and comparative examples 1 to 6 were subjected to efficacy evaluation. 110 volunteers, 20-50 years old, living in cities were selected and randomly divided into 11 groups. After makeup every morning, the makeup setting gels of examples 1 to 5 and comparative examples 1 to 6 were used, and makeup was not applied on the same day for a total of one month.
1) Test of makeup fixation effect
Questionnaires are carried out on volunteers, and the using effect of the product is evaluated from three dimensions of make-up holding capacity, oil control effect and sweat resistance. Wherein the makeup holding capacity standard is as follows:
13-15 hours, 5 minutes, 10-12 hours, 4 minutes, 7-9 hours, 3 minutes, 4-6 hours, 2 minutes and 1 minute for 1-3 hours.
The oil control effect standard is as follows: basically, no oil is discharged for 5 minutes, a small amount of oil is discharged for 4 minutes locally, the oil discharge amount is moderate and can be accepted for 3 minutes, the oil discharge amount is large and 2 minutes, and the oil discharge amount is large and cannot be accepted for 1 minute.
The standard of sweat resistance is as follows: after a large amount of sweating, 5 points of makeup are still removed, 4 points of makeup are slightly removed, 3 points of makeup are partially removed, 2 points of makeup are mostly removed, and 1 point of makeup is completely removed. The test results are shown in table 1 below.
Table 1: average score of makeup fixing effect test for examples 1 to 5 and comparative examples 1 to 6
| Make-up holding ability | Oil control effect | Anti-sweat ability | |
| Example 1 | 4.3 | 4.2 | 4.2 |
| Example 2 | 4.6 | 4.5 | 4.8 |
| Example 3 | 4.5 | 4.4 | 4.4 |
| Example 4 | 4.8 | 4.8 | 4.9 |
| Example 5 | 4.7 | 4.7 | 4.8 |
| Comparative example 1 | 3.9 | 3.3 | 4.5 |
| Comparative example 2 | 3.5 | 4.1 | 3.7 |
| Comparative example 3 | 4.6 | 4.5 | 4.7 |
| Comparative example 4 | 3.4 | 4.2 | 3.8 |
| Comparative example 5 | 4.7 | 4.6 | 4.8 |
| Comparative example 6 | 4.6 | 4.5 | 4.7 |
Through the makeup setting effect test, the result is shown in table 1, and the combination of the makeup setting powder, the coloring agent and the film forming agent obviously improves the makeup holding capacity, the oil control effect and the sweat resistance compared with the single use of each component, which indicates that the combination of the makeup setting powder, the coloring agent and the film forming agent can achieve a better makeup setting effect.
2) Anti-pollution effect test
The air pollutants can damage the skin, so that the skin is sensitive, dry, rough and the like. This test utilizes a VISIA tester to take pictures of volunteers before and after using the product, comparing the data on day 0 and day 30. The skin flatness and the degree of pore condition improvement were observed, and the test results are shown in table 2 below.
Table 2: the anti-contamination effect test of examples 1 to 5 and comparative examples 1 to 6 was equally divided.
As can be seen from Table 2, the anti-pollution effect test shows that the combination of the film-forming agent and the anti-pollution active substance improves the skin flatness and the pore condition by more than 50% compared with the single use of each component. The composition of the marrubium vulgare extract and the peach blossom extract obviously improves the improvement of the skin state compared with the single use of the two extracts. The anti-pollution effect of the invention is realized by the synergistic compounding effect of the raw material components.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (5)
1. A make-up fixative gel composition characterized by: the composition comprises the following components in percentage by weight:
0.5 to 5 percent of fixing powder, 0.2 to 3 percent of colorant, 0.35 to 4 percent of film forming agent, 0.2 to 5 percent of active component with anti-pollution effect, 0.05 to 1 percent of thickening agent, 0.5 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water;
the dressing powder is selected from one or a mixture of more than two of silica, corn starch and cassava starch;
the anti-pollution effective active ingredients comprise an eriocaulon henryi extract and a peach blossom extract, and the two are mixed according to the weight ratio of 1;
the colorant is selected from one or a mixture of more than two of titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow;
the film-forming agent is a VP/VA copolymer;
the other components are selected from one or more of a preservative, a pH regulator and a chelating agent;
the weight ratio of the total amount of the dressing powder and the colorant to the film-forming agent is 0.5 to 2.
2. The make-up setting gel composition of claim 1, wherein: the composition comprises the following components in percentage by weight:
0.5 to 4 percent of dressing powder, 0.3 to 2 percent of colorant, 0.5 to 3 percent of film forming agent, 1 to 5 percent of active component with anti-pollution effect, 0.1 to 1 percent of thickening agent, 1 to 10 percent of humectant, 0.2 to 1 percent of other components and the balance of deionized water.
3. The make-up fixing gel composition according to claim 2, wherein: the surfaces of the titanium dioxide, the iron oxide red, the iron oxide black and the iron oxide yellow are subjected to hydrophilic treatment, so that the titanium dioxide, the iron oxide red, the iron oxide black and the iron oxide yellow have hydrophilicity.
4. The make-up fixing gel composition according to claim 2, wherein:
the thickening agent is selected from one or a mixture of more than two of carbomer, acrylate/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and ammonium acryloyldimethyl taurate/VP copolymer;
the humectant is one or more of glycerol, propylene glycol, butanediol, methyl propylene glycol, dipropylene glycol, sorbitol, methyl glucitol polyether-20, and glyceryl polyether-26.
5. Method for preparing a fixing gel composition according to any one of claims 1 to 4, characterized in that: which comprises the following steps:
1) Accurately weighing a specified amount of deionized water into the container A, adding a thickening agent and a chelating agent, heating in a water bath to 75-70 ℃, and preserving heat for 20 minutes;
2) Accurately weighing a specified amount of pH regulator into the container A, stirring and dissolving uniformly, and then cooling;
3) When the temperature of the materials in the container A is reduced to 45 ℃, adding the dressing powder, the film forming agent, the anti-pollution active ingredient, the coloring agent, the humectant and the preservative, stirring uniformly, and then transferring into a closed container for storage and filling.
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| CN103385839A (en) * | 2012-05-07 | 2013-11-13 | 纪玉杰 | Peach blossom mud for skin care |
| FR3049194B1 (en) * | 2016-03-23 | 2019-10-04 | Sederma | USE OF A COSMETIC INGREDIENT COMPRISING VEGETABLE MATERIAL FROM MARRUBIUM VULGARE FOR COSMETIC TREATMENT |
| JP7121589B2 (en) * | 2018-08-24 | 2022-08-18 | 株式会社コーセー | Water-in-oil cosmetics |
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