CN113576985B

CN113576985B - High-permeability water-locking composition, and skin-care mask liquid and preparation method thereof

Info

Publication number: CN113576985B
Application number: CN202111056199.6A
Authority: CN
Inventors: 陈炜诗; 陈嘉钰; 周锐; 马飞; 慕德明
Original assignee: Guangdong Xingrui Biotechnology Co ltd
Current assignee: Guangdong Xingrui Biotechnology Co ltd
Priority date: 2021-09-09
Filing date: 2021-09-09
Publication date: 2023-06-20
Anticipated expiration: 2041-09-09
Also published as: CN113576985A

Abstract

The application relates to the field of masks, and particularly discloses a high-permeability water-locking composition, a soothing and moisturizing mask liquid and a preparation method thereof. The high-permeability water-locking composition comprises a composition A, a composition B, a composition C, a soothing agent, a repairing agent and a humectant. The facial mask liquid comprises a high-permeability water-locking composition, glycerol, propylene glycol, trehalose, sodium hyaluronate, a thickener, EDTA disodium, arginine, p-hydroxyacetophenone, 1, 2-hexanediol and water. The preparation method of the mask liquid comprises the following steps: firstly, preparing a high-permeability water-locking composition; mixing and heating glycerol, a part of propylene glycol, trehalose, sodium hyaluronate, a thickening agent, a chelating agent and water, and uniformly stirring to obtain a base solution; cooling, adding arginine and stirring uniformly; mixing, heating and stirring the rest propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, and then adding the mixture into the base solution for stirring; cooling, adding the high-permeability water-locking composition, and stirring to obtain facial mask liquid. The facial mask liquid has the effect of promoting facial skin absorption.

Description

High-permeability water-locking composition, and skin-care mask liquid and preparation method thereof

Technical Field

The invention relates to the field of facial masks, in particular to a high-permeability water-locking composition, a soothing and moisturizing facial mask liquid and a preparation method thereof.

Background

The facial mask is an important category in skin care products, and is a common skin care product for people. The facial mask is quite various in types and different in efficacy in the market at present, and the principle of the facial mask is that various substances in the facial mask liquid permeate into the cuticle of the facial epidermis by covering the face of a user, so that the facial skin is purposefully repaired by moisturizing, relieving, brightening, resisting oxidation and the like, and the skin becomes soft, bright and elastic. In the use process of the facial mask, the facial mask liquid generally needs a certain time to permeate into the cuticle of the facial epidermis to be absorbed and utilized, the effect of the skin on the absorption of the facial mask liquid greatly influences the effect of the facial mask liquid on the facial skin, and the existing facial mask liquid has a great promotion space in the aspect of promoting the absorption.

Disclosure of Invention

In order to improve the absorption effect of facial mask liquid on facial skin, the application provides a high-permeability water-locking composition, a soothing and moisturizing facial mask liquid and a preparation method thereof.

In a first aspect, the present application provides a high-permeability water-locking composition according to the following technical scheme:

the high-permeability water locking composition comprises the following raw materials in percentage by weight:

7.69-23.81% of composition A, 12.82-47.62% of composition B, 7.69-23.81% of composition C, 12.82-47.62% of soothing agent, 5.13-19.05% of repairing agent and 7.69-23.81% of humectant;

the composition A consists of 5-7% wt of alpine leontopodium flower/leaf extract and a solvent;

the composition B consists of 8-12% wt of polygonatum odoratum extract and a solvent;

the composition C consists of 98-99% wt of lactobacillus/rice fermentation product and solvent.

By adopting the technical scheme, the composition A containing the alpine leontopodium herb flower/leaf extract, the composition B containing the fragrant solomonseal rhizome extract and the composition C containing lactobacillus/rice fermentation products form a plurality of high-permeability colloid groups under the combined action of the composition A, the high-permeability colloid groups can quickly permeate into skin deep cells when the high-permeability water-locking composition is contacted with facial skin, a path similar to a high-speed channel is formed on the face, and substances such as a humectant, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition can be wrapped by the colloid groups into the skin deep cells, so that the skin deep cells can be quickly and fully supplemented with water and repaired; the high-permeability colloid group promotes the absorption of the skin to the high-permeability water-locking composition, and can improve the skin care efficiency.

Preferably, the soothing agent comprises a soothing component and a solvent, wherein the soothing component comprises one or more of a herba Cirsii Japonici extract, a fructus Siraitiae Grosvenorii extract, a herba Pileae Scriptae extract, a flos Plumeriae Acutifoliae extract, a flos Nymphaeae extract, and a radix et caulis Opuntiae Dillenii extract.

Preferably, the soothing agent comprises 1.6-1.8% wt of the Cirsium japonicum extract, 1.6-1.8% wt of the Siraitia grosvenorii extract, 1.6-1.8% wt of the Gorgon fruit extract, 1.6-1.8% wt of the Alternaria white extract, 1.6-1.8% wt of the Nymphaea white flower extract, 1.6-1.8% wt of the Cactus fruit extract and a solvent.

By adopting the technical scheme, the phenolic hydroxyl groups of silymarin in the Cirsium japonicum extract have lipid peroxidation resisting activity, so that the collagen structure in skin can be kept unchanged, and the structure of high-permeability colloid groups is stable; the mogrosides, amino acids, flavone, etc. contained in the fructus Siraitiae Grosvenorii extract are beneficial to enhancing the activity of rhizoma Polygonati Odorati extract in composition B; diterpenoid glycoside contained in the herba Pileae Scriptae extract can reduce redness of skin; the white plumeria extract contains sterols, plumeria rubra glycoside, scopoletin and other lipid alcohols, and the white plumeria rubra extract contains various saccharides and alcohols, so that the white plumeria rubra extract and the white plumeria rubra extract act together, thereby being beneficial to enhancing the compatibility of the soothing agent and skin cells; the Opuntia Dillenii extract can promote the generation of skin growth factor, has skin activating effect, and can promote the penetration of colloid group with high permeability by activating skin cells, so as to promote skin absorption.

The plant extracts such as the Cirsium japonicum extract and the Siraitia grosvenorii extract are cooperated in a specific proportion, so that a cooperated compounding effect can be generated, each component substance and high-permeability colloid group in the water supplementing and relieving process can be uniformly dispersed in the process of permeating into skin deep cells, the absorption capacity of the skin is improved, the skin absorption is more balanced, and the balance of the high-permeability water locking composition on the skin repairing effect is also improved.

Preferably, the repairing agent comprises repairing components and a solvent, wherein the repairing components comprise one or more of gentian root extract, honeysuckle flower extract, wild chrysanthemum flower extract, yan Hu Suogen extract, peppermint extract and kuh-seng root extract.

By adopting the technical scheme, the gentian extract has the effect of promoting the secretion of the surface cell cholesterol, and can improve the state of oily rough skin; the honeysuckle extract can change sebum composition, and has effects of regulating skin oiliness and softening skin; the flos Chrysanthemi Indici extract can inhibit 5 a-reductase activity, astringe pores and reduce oil; the gentian root extract, the honeysuckle extract and the wild chrysanthemum extract have synergistic effect, and play a prominent role in conditioning skin oiliness.

The extract of rhizoma corydalis Hu Suogen contains tetrahydropalmatine, tetrahydropalmatine and propylene, and has analgesic and sedative effects; the herba Menthae extract contains volatile oil, flavone, organic acid and amino acid, and has certain inhibiting effect on fungi and viruses; the extract of Yan Hu Suogen and the extract of field mint are helpful for antisepsis and anti-inflammation of skin.

The herba Menthae extract also has effect in promoting collagen production, and radix Sophorae Flavescentis extract also has effect in promoting fibroblast proliferation, and the combination of the two is beneficial to relieving skin damaged cells.

The repairing agent is formed by mixing a plurality of plant extracts such as gentian extract, hu Suogen extract and the like, and realizes the omnibearing repairing of the skin from the aspects of skin grease, antisepsis and anti-inflammation and cell repairing. In addition, the brass, amino acid and other components contained in the substances in the repairing agent are favorable for being blended into the high-permeability colloid groups, so that the stability of the high-permeability colloid groups is enhanced, and the absorption promoting effect of the high-permeability colloid groups on the skin is improved.

Preferably, the humectant is composed of a moisturizing component and a solvent, wherein the moisturizing component comprises one or more of xylitol, centella asiatica extract and tremella extract.

By adopting the technical scheme, the xylitol has long-acting moisturizing and moisturizing effects; the centella asiatica extract mainly contains asiaticoside and madecassoside, which can tighten the connection part of epidermis and dermis, soften skin and help the skin absorb xylitol; the water-soluble polymer polysaccharide in the tremella extract has excellent moisturizing performance and film forming performance, can be fused with xylitol to jointly promote the moisturizing effect, and can also increase the content of colloid in colloid groups with high permeability, so that the stability of the colloid groups is enhanced. The substances in the humectant mutually promote penetration into deep cells of the face to play a remarkable role in moisturizing, and the moisturizing performance of the cells is improved from the deep layers.

In a second aspect, the present application provides a soothing and moisturizing facial mask solution comprising a high permeability water-locking composition, which adopts the following technical scheme:

a soothing and moisturizing mask liquid containing a high-permeability water-locking composition, which comprises the following raw materials in percentage by weight:

phase A: 2-4% of glycerin, 4-6% of propylene glycol, 0.5-1.5% of trehalose, 0.03-0.07% of sodium hyaluronate, 0.2-0.25% of thickener and 0.02-0.04% of EDTA disodium;

and B phase: arginine 0.1-0.15%;

And C phase: 0.9 to 1.0 percent of propylene glycol, 0.45 to 0.5 percent of p-hydroxyacetophenone and 0.45 to 0.5 percent of 1, 2-hexanediol;

and D phase: 2.1-3.9% of high-permeability water-locking composition;

the balance of water.

Preferred thickeners are one or more of ammonium acryloyldimethyl taurate/VP copolymer, carbomer and sclerotium rolfsii.

By adopting the technical scheme, the high-permeability water-locking composition can promote the absorption of facial skin, the high-permeability water-locking composition permeates into skin cuticle and dermal cells to deeply relieve and moisturize facial skin cells, and trehalose, sodium hyaluronate and glycerin are mutually assembled to form a protective film on the surface of the skin, so that the outer layer of the skin is conditioned and water-locked. The high-permeability water-locking composition in the mask liquid acts together with trehalose, sodium hyaluronate and the like to relieve and repair skin from deep layers and double tubes on the surface of the skin respectively, so that the mask liquid has a good absorption effect and a prominent water-locking effect.

Preferably, the arginine is 0.125-0.135% by weight.

By adopting the technical scheme, arginine is basic amino acid which is an amino acid necessary for human body, and the arginine itself can play roles of providing immunity, adjusting acid-base moisture and balancing grease for skin; when the weight percentage of arginine in the mask liquid is 0.125-0.135%, the arginine has better neutralization effect, so that the acid-base balance of the whole mask liquid system is better, the high-permeability water-locking composition is beneficial to being fused with other components in the mask liquid, and a part of arginine can be fused into colloid groups with high permeability, so that the dispersion uniformity of the colloid groups can be better improved, and the uniform absorption of facial skin is promoted; and can promote the colloid groups to penetrate deeply into dermal fibroblasts, thereby improving the skin absorption effect.

Preferably, the thickener comprises one or both of carbomers and sclerotium rolfsii.

By adopting the technical scheme, carbomer molecules are used as carboxyl groups to combine with one or more than two hydroxyl groups to form hydrogen bonds so as to thicken, and the neutralized carbomer is an excellent gel matrix, so that the carbomer can increase the cohesiveness of colloid groups, is beneficial to improving the structural stability of the colloid groups, and is beneficial to improving the cohesiveness between the penetration water-locking composition and other components in mask liquid; the sclerotium rolfsii is a natural polymer of natural capsule-like glucan polysaccharide, is beneficial to controlling the viscosity of the mask liquid, maintains the stability of a mask liquid system, has good cohesiveness with colloid groups, and further improves the cohesiveness between other components in the mask liquid and the colloid groups.

In a third aspect, the present application provides a method for preparing a water-repellent mask liquid containing a high-permeability water-repellent composition, which adopts the following technical scheme:

a method of preparing a soothing and moisturizing facial mask fluid comprising a high permeability water-locking composition comprising the steps of:

step one, preparing a high-permeability water-locking composition: uniformly mixing and stirring the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant to obtain a high-permeability water locking composition for standby;

Mixing glycerol and propylene glycol, adding the rest raw materials of the phase A, heating to 80-85 ℃, and stirring until the rest raw materials are completely dissolved and have no particles to obtain a base solution;

step three, cooling to 60-65 ℃, adding the phase B raw material into the base liquid, and stirring until the phase B raw material is completely dissolved and has no particles;

step four, mixing the C phase raw materials, heating to 50-55 ℃, uniformly stirring, adding into the base liquid, and stirring until the C phase raw materials are completely dissolved and have no particles;

and fifthly, cooling to 40-45 ℃, adding the high-permeability water locking composition prepared in the step one into the base liquid, and uniformly stirring to obtain the soothing and moisturizing mask liquid.

By adopting the technical scheme, the glycerol and the propylene glycol are added into the emulsifying pot, and the glycerol and the propylene glycol are used as solvent base materials of the mask liquid and are used for dissolving other components; trehalose, sodium hyaluronate, a thickening agent and EDTA disodium are added into the solvent base material and are uniformly mixed in the process of heating to 80-85 ℃ to form a mask base solution with the functions of basic relief and moisture preservation; arginine is added after the temperature is reduced to 60-65 ℃, and the arginine has a neutralization and regulation effect on the base solution in the temperature range; mixing and heating p-hydroxyacetophenone, propylene glycol and 1, 2-hexanediol to uniformly mix the three components, adding the mixture of the three components into base liquid, and uniformly dispersing the mixed liquid of the three components in the base liquid so as to improve the overall oxidation resistance and corrosion resistance of the base liquid; and finally, adding the high-permeability water-locking composition into the base liquid after the temperature is reduced to 40-45 ℃, and adding water at a proper temperature for relieving, so that the influence of the temperature on volatile substances in the high-permeability water-locking composition is reduced, the interaction between the high-permeability water-locking composition and the substances in the base liquid is realized, and the optimal improvement of the moisturizing and relieving performances of the facial mask liquid is completed.

In summary, the present application includes at least one of the following beneficial technical effects:

1. the high-permeability water-locking composition comprises a composition A containing a high mountain leontopodium flower/leaf extract, a composition B containing a fragrant solomonseal rhizome extract and a composition C containing lactobacillus/rice fermentation products, wherein a plurality of high-permeability colloid groups can be formed under the synergistic effect of the composition A, the high-permeability colloid groups can quickly permeate into skin horny layers when the high-permeability colloid groups are contacted with facial skin, a path similar to a high-speed channel is formed on the face, and substances such as a humectant, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition are wrapped by colloid groups, so that the substances enter deep cells of the skin quickly, and the deep cells of the skin are repaired and water is supplemented. The high-permeability colloid group improves the absorption capacity of the skin, enhances the absorption capacity of the skin, can absorb sufficient nutrition in a short time, and further improves the skin care efficiency;

2. the mask liquid comprises a basic liquid composed of trehalose, sodium hyaluronate, glycerol and the like and moisturizing and relieving, the high-permeability water-locking composition improves the absorption effect of skin, all components in the high-permeability water-locking composition penetrate deep into deep cells to deeply repair the cells, and the sea trehalose and the like in the basic liquid are used for conditioning the outer layer of the skin, so that the moisturizing and relieving effect of the mask liquid is greatly improved.

Detailed Description

The present application will be described in further detail with reference to examples.

The source information of the raw materials used in the following experimental examples and comparative experimental examples is shown in Table 1.

TABLE 1

Preparation example

Preparation example 1

The preparation example discloses a preparation method of a composition A, which comprises the following steps: 5kg of the extract of flowers/leaves of the alpine leontopodium herb, 70kg of butanediol and 25kg of water are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at the normal temperature and the rotating speed of 30r/min to obtain the composition A.

Preparation example 2

The preparation example discloses a preparation method of a composition A, which comprises the following steps: 7kg of the extract of flowers/leaves of the alpine leontopodium herb, 70kg of butanediol and 23kg of water are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at the normal temperature and the rotating speed of 30r/min to obtain the composition A.

Preparation example 3

The preparation example discloses a preparation method of a composition B, which comprises the following steps: 8kg of polygonatum odoratum extract, 20kg of butanediol, 5kg of 1, 2-hexanediol and 67kg of water are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at the normal temperature and the rotating speed of 35r/min, so as to obtain a composition B.

Preparation example 4

The preparation example discloses a preparation method of a composition B, which comprises the following steps: 12kg of polygonatum extract, 20kg of butanediol, 3kg of 1, 2-hexanediol and 65kg of water are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at the normal temperature and the rotating speed of 35r/min, thus obtaining the composition B.

Preparation example 5

The preparation example discloses a preparation method of a composition C, which comprises the following steps: 98kg of lactobacillus/rice fermentation product, 1kg of 1, 2-pentanediol and 1kg of 1, 2-hexanediol were added into an emulsifying pot and mixed, and stirred at a rotation speed of 35r/min for 5 minutes at normal temperature, to obtain a composition C.

Preparation example 6

The preparation example discloses a preparation method of a composition C, which comprises the following steps: 99kg of lactobacillus/rice fermentation product, 0.5kg of 1, 2-pentanediol and 0.5kg of 1, 2-hexanediol are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at the normal temperature under the condition of the rotating speed of 35r/min, so as to obtain a composition C.

Preparation example 7

The soothing agent in this example is selected from the group consisting of the extract of peach blossom 0.5 wt%, lotus flower 0.5 wt%, hibiscus flower 0.5 wt%, glycerin 37.5 wt%, propylene glycol 3 wt%, 1, 2-glycol 0.5 wt%, caprylic glycol 0.5 wt% and water 57 wt%.

Preparation example 8

The preparation example discloses a preparation method of a soothing agent, which comprises the following steps: 1.6kg of the Cirsium japonicum extract, 18kg of butanediol, 4kg of hexanediol and 76.4kg of water are added into an emulsifying pot and mixed, and stirred for 5 minutes at the normal temperature and the rotating speed of 30r/min, thus obtaining the soothing agent.

Preparation example 9

The preparation example discloses a preparation method of a soothing agent, which comprises the following steps: 1.6kg of Siraitia grosvenorii extract, 1.6kg of gorgon fruit extract, 18kg of butanediol, 4kg of 1, 2-hexanediol and 74.8kg of water are added into an emulsifying pot to be mixed, and stirred for 5 minutes at normal temperature and the rotating speed of 30r/min to obtain the soothing agent.

Preparation example 10

The preparation example discloses a preparation method of a soothing agent, which comprises the following steps: 1.6kg of white plumeria rubra extract, 1.8kg of white water lily flower extract, 1.8kg of cactus fruit extract, 18kg of butanediol, 4kg of 1, 2-hexanediol and 72.8kg of water are added into an emulsifying pot to be mixed, and stirred for 5 minutes at the normal temperature and the rotating speed of 30r/min, thus obtaining the soothing agent.

PREPARATION EXAMPLE 11

The preparation example discloses a preparation method of a soothing agent, which comprises the following steps: adding 1kg of the Cirsium japonicum extract, 1kg of the Siraitia grosvenorii extract, 1kg of the Litsea coreana extract, 1kg of the white plumeria rubra extract, 1kg of the white water lily flower extract, 1kg of the Cactaria sibirica extract, 18kg of butanediol, 4kg of 1, 2-hexanediol and 72kg of water into an emulsifying pot, mixing, and stirring at normal temperature and a rotating speed of 30r/min for 5 minutes to obtain the soothing agent.

Preparation example 12

This preparation differs from preparation 11 in that: the content of the extract of the wild artichoke is 1.6kg, the content of the extract of the fructus momordicae is 1.6kg, the content of the extract of the gorgonian is 1.6kg, the content of the extract of the white plumeria rubra is 1.6kg, the content of the extract of the white water lily is 1.8kg, the content of the extract of the cactus is 1.8kg and the content of water is 68kg.

Preparation example 13

This preparation differs from preparation 11 in that: the content of the extract of the jerusalem artichoke is 1.8kg, the content of the extract of the momordica grosvenori is 1.8kg, the content of the extract of the gorgonian coral is 1.8kg, the content of the extract of the white plumeria rubra is 1.6kg, the content of the extract of the white water lily is 1.6kg, and the content of water is 67.6kg.

PREPARATION EXAMPLE 14

This preparation differs from preparation 11 in that: 1.8kg of the aucubia extract was replaced with 1.8kg of the sarcandra glabra extract; 1.6kg of white water lily flower extract is replaced by 1.6kg of Fucus vesiculosus extract.

Preparation example 15

This preparation differs from preparation 14 in that: 1.8kg of the gorgonian extract was replaced with 1.8kg of the paeonia lactiflora root extract.

PREPARATION EXAMPLE 16

The repairing agent in the preparation example is golden chamomile flower water.

Preparation example 17

The preparation example discloses a preparation method of a repairing agent, which comprises the following steps: 3kg of gentian root extract, 0.5kg of honeysuckle extract, 0.5kg of wild chrysanthemum extract, 0.5kg of Yan Hu Suogen extract, 0.5kg of field mint extract, 0.5kg of kuh-seng root extract, 0.5kg of 1, 2-pentanediol, 0.5kg of octanediol, 17.5kg of propylene glycol and 76kg of water are added into an emulsifying pot to be mixed, and stirred for 5 minutes at the normal temperature and the rotating speed of 35r/min, thus obtaining the repairing agent.

PREPARATION EXAMPLE 18

The humectant in the preparation example is VKFERM201 skin-nourishing lotion produced by KFERM of Biotechnology Co., ltd. Of Guangzhou, and the skin-nourishing lotion comprises lactobacillus/eriodictyo fermentation product extract 33 wt%, hydrolyzed rice extract 32 wt%, rice distilled water 33 wt%, 1, 2-hexanediol 1.5 wt% and 1, 2-pentanediol 0.2 wt%.

Preparation example 19

The preparation example discloses a preparation method of a humectant, which comprises the following specific steps: 7.5kg of xylitol, 35kg of dehydrated xylitol, 15kg of centella asiatica extract, 25kg of tremella extract, 1.5kg of 1, 2-hexanediol and 16kg of water are added into an emulsifying pot to be mixed, and the mixture is stirred for 5 minutes at normal temperature under the condition of 30r/min of rotating speed, thus obtaining the humectant.

Examples

Examples 1 to 5

The high permeability water-locking composition comprises: composition a, composition B, composition C, soothing agent, repairing agent, moisturizing agent and solvent.

The preparation method of the high-permeability water-locking composition comprises the following steps: and (3) adding the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant prepared in the preparation example into an emulsifying pot together, and uniformly dispersing for 5 minutes at normal temperature and under the condition of the rotating speed of 550r/min to obtain the high-permeability water locking composition.

The amounts (in kg) of the raw material components of the high permeability water-blocking compositions of examples 1 to 5 are shown in Table 2 (in Table "\" is regarded as not added).

TABLE 2

Examples 6 to 13

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the soothing agents prepared in preparation examples 8 to 15 were used as soothing agents, respectively.

The soothing agents used in examples 6-13 are detailed in Table 3

TABLE 3 Table 3

Example 14

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the repairing agent prepared in preparation example 17 is selected.

Example 15

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the humectant is the one prepared in preparation example 19.

Examples 16 to 18

The amounts of the raw material components (unit: kg) of the high permeability water-blocking compositions of examples 16 to 18 are shown in Table 3.

TABLE 4 Table 4

Comparative example

Comparative example 1

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the mountain leontopodium flower/leaf extract in composition a was replaced with an equal amount of water.

Comparative example 2

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the rhizoma Polygonati Odorati extract in composition B is replaced with water of equal amount.

Comparative example 3

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the lactobacillus/rice fermentation product in composition C was replaced with an equal amount of water.

Comparative example 4

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the mountain leontopodium flower/leaf extract in the composition A, the polygonatum extract in the composition B and the lactobacillus/rice fermentation product in the composition C are replaced by equal amounts of water.

Comparative example 5

A method for preparing a high permeability water-locking composition, which differs from example 5 in that: the soothing agent is replaced with an equal amount of water.

Experimental example

Experimental example 1

The experimental example discloses a soothing and moisturizing mask liquid containing a high-permeability water-locking composition, which comprises the following raw materials in parts by weight:

phase A: 2kg of glycerin, 4kg of propylene glycol, 0.5kg of trehalose, 0.03kg of sodium hyaluronate, 0.2kg of acrylamide dimethyl taurate/VP copolymer and 0.02kg of EDTA disodium;

and B phase: arginine 0.1kg;

and C phase: 1.0kg of propylene glycol, 0.5kg of p-hydroxyacetophenone and 0.5kg of 1, 2-hexanediol;

And D phase: 2.1kg of high-permeability water-locking composition;

89.05kg of water.

The experimental example also discloses a preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition, which comprises the following steps:

step one, selecting the high-permeability water-locking composition prepared in the embodiment 1 for standby;

adding 2kg of glycerol, 4kg of propylene glycol and 89.05kg of water into an emulsifying pot, adding 0.5kg of trehalose, 0.03kg of sodium hyaluronate, 0.2kg of ammonium acryloyldimethyl taurate/VP copolymer and 0.02kg of disodium EDTA, stirring and heating to 80 ℃, preserving heat for 25 minutes, homogenizing for 3 minutes under the condition of 750r/min to completely dissolve without particles, and obtaining a base solution;

step three, cooling to 60 ℃, adding 0.1kg of arginine into the base liquid, and stirring for 15 minutes under the condition of the rotating speed of 35 r/min; step four, mixing and heating 1.0kg of propylene glycol, 0.5kg of p-hydroxyacetophenone and 0.5kg of 1, 2-hexanediol to 55 ℃, stirring for 3 minutes, adding into an emulsifying pot for mixing, and stirring at the rotating speed of 35r/min until the particles are completely dissolved;

and fifthly, cooling to 40 ℃, adding 2.1kg of the high-permeability water-locking composition in the first step into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Experimental example 2

phase A: 4kg of glycerin, 6kg of propylene glycol, 1.5kg of trehalose, 0.07kg of sodium hyaluronate, 0.25kg of acrylamide dimethyl taurate/VP copolymer and 0.04kg of EDTA disodium;

and B phase: arginine 0.15kg;

and C phase: propylene glycol 0.9kg, p-hydroxyacetophenone 0.45kg, 1, 2-hexanediol 0.45kg;

and D phase: 3.9kg of high-permeability water-locking composition;

82.29kg of water.

adding 4kg of glycerol, 6kg of propylene glycol and 82.29kg of water into an emulsifying pot, adding 1.5kg of trehalose, 0.07kg of sodium hyaluronate, 0.25kg of ammonium acryloyldimethyl taurate/VP copolymer and 0.04kg of disodium EDTA, stirring and heating to 85 ℃, preserving heat for 25 minutes, homogenizing for 3 minutes under the condition of 750r/min to completely dissolve without particles, and obtaining a base solution;

step three, cooling to 65 ℃, adding 0.15kg of arginine into the base liquid, and stirring for 15 minutes under the condition of the rotating speed of 35 r/min;

Step four, mixing and heating 0.9kg of propylene glycol, 0.45kg of p-hydroxyacetophenone and 0.45kg of 1, 2-hexanediol to 50 ℃, stirring for 3 minutes, adding into an emulsifying pot for mixing, and stirring at the rotating speed of 35r/min until the particles are completely dissolved;

and fifthly, cooling to 45 ℃, adding 3.9kg of the high-permeability water-locking composition in the first step into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Experimental examples 3 to 19

A method for preparing a soothing and moisturizing facial mask liquid containing a high-permeability water-locking composition, which is different from experimental example 2 in that: in the first step, the high-permeability water-locking compositions prepared in examples 2 to 18 were used.

Experimental example 20

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: the water content in the second step was 82.315kg, and the arginine content in the third step was 0.125kg.

Experimental example 21

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: the water content in the second step was 82.305kg, and the arginine content in the third step was 0.135kg.

Experimental example 22

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: 0.25kg of the ammonium acryloyldimethyl taurate/VP copolymer in step two was replaced with an equivalent amount of carbomer.

Experimental example 23

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: 0.25kg of the ammonium acryloyldimethyl taurate/VP copolymer in the second step is replaced by an equivalent amount of sclerotium rolfsii.

Experimental example 24

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: 0.25kg of the ammonium acryloyldimethyl taurate/VP copolymer in the second step was replaced with 0.13kg of carbomer and 0.12kg of the sclerotium rolfsii.

Experimental example 25

A method for preparing a soothing and moisturizing facial mask liquid containing a high permeability water-locking composition, which is different from experimental example 18 in that: the water content in the second step is 82.315kg; 0.25kg of the ammonium acryloyldimethyl taurate/VP copolymer in the second step is replaced by 0.13kg of carbomer and 0.12kg of small nuclear fungus gel; the arginine content in step three was 0.125kg.

Experimental example 26

phase A: 3kg of glycerin, 5kg of propylene glycol, 1kg of trehalose, 0.05kg of sodium hyaluronate, 0.13kg of carbomer, 0.1kg of sclerotium rolfsii and 0.03kg of EDTA disodium;

And B phase: arginine 0.13kg;

and D phase: 3.2kg of high-permeability water-locking composition;

85.56kg of water.

adding 3kg of glycerol, 5kg of propylene glycol and 85.56kg of water into an emulsifying pot, adding 1kg of trehalose, 0.05kg of sodium hyaluronate, 0.13kg of carbomer, 0.1kg of sclerotium gum and 0.03kg of disodium EDTA, stirring and heating to 85 ℃, preserving heat for 25 minutes, homogenizing for 3 minutes under the condition of 750r/min to completely dissolve without particles, and obtaining a base solution;

step three, cooling to 65 ℃, adding 0.13kg of arginine into the base liquid, and stirring for 15 minutes under the condition of the rotating speed of 35 r/min;

and fifthly, cooling to 45 ℃, adding 3.2kg of the high-permeability water-locking composition in the first step into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Comparative examples 1 to 5

A method for preparing a soothing and moisturizing facial mask liquid containing a high-permeability water-locking composition, which is different from experimental example 6 in that: in the first step, the high-permeability water-locking compositions prepared in comparative examples 1 to 5 were respectively selected.

Performance test

1. Facial skin absorption rate test: the non-woven fabric mask paper with the absorptivity of 90% and the same regulation is respectively soaked in the mask liquid prepared in the experimental examples 1-26 and the comparative experimental examples 1-5 for 24 hours and then taken out to be used as a test group, a commercial brand of the comfortable and waterproof mask is used as a control group, and the moisture contents of the mask of the test group and the mask of the control group are consistent within an allowable error range (+ -1%). 160 testers with no obvious difference between skin quality and facial skin moisture content were selected: dividing 155 testers into the same test group every 5 testers, testing samples prepared by the same test example in the test group by the same test group, and taking an average value of test results; the remaining 5 testers were used as a control group to test the control group mask, and the test results were averaged. Washing cheeks with warm water for 10 minutes, and measuring the moisture content of the skin horny layer at the forehead of a tester before each test group applies the mask in batches by adopting a Callgari Soft5.5 skin horny layer moisture content tester under the conditions of room temperature and humidity of 75-80 percent, and recording the moisture content as an initial value; and then the test group and the control group respectively use the facial masks of the test group and the control group to apply the face, when the facial masks are used for 5 minutes, the facial masks at the forehead of the tester are lifted, the facial mask liquid at the forehead of the tester is wiped clean by paper towels, and then the moisture content of the skin cuticle at the forehead of the tester is measured by a tester and is recorded as the moisture content of 5 minutes. After the data of the plurality of groups are collected and finished, the increase of the moisture content of the skin cuticle of the face of the trial person (moisture content-initial value of 5 minutes) in 5 minutes of applying the mask to the test group and the control group are analyzed and compared, so that the effect of promoting skin absorption by the mask liquid of the experimental examples 1-23 and the mask liquid of the comparative experimental examples 1-5 is detected, and the greater the increase of the moisture content of the skin cuticle in 5 minutes is, the better the skin absorption effect is proved.

2. Mask moisturizing effect test: on the basis of test 1, after 160 testers apply the mask for 15 minutes, taking down the mask, cleaning the mask liquid remained on the face, and measuring the moisture content of the skin horny layer at the forehead of each test group by adopting a Callgari Soft5.5 skin horny layer moisture content tester in batches, and marking the moisture content as a basic value; the water content of the skin cuticle of the face of the test group and the control group is measured after the test group is subjected to indoor waiting for 30 minutes under the conditions of room temperature and humidity of 75-80 percent, the water content is recorded as 30 minutes, and the 30 minutes loss (the water content of the basic value-30 minutes) is calculated; after 60 minutes of indoor conditioning of the test and control groups, the moisture content of the skin horny layer of the face of the test group and the control group were measured, recorded as 60 minutes moisture content, and the 60 minutes loss (base-60 minutes moisture content) was calculated. Recording data, collecting and finishing multiple groups of data, taking an average value of test results of each group, taking down the mask for 30 minutes and 60 minutes, and showing that the smaller the loss amount of the moisture content of the skin horny layer of the face of the user is, the smaller the water loss of the skin is in the same time of 30 minutes and 60 minutes, and the better the moisturizing effect of the mask is.

3. Evaluating the relaxing effect of the mask: selecting 30 testers with facial redness, wherein the testers have similar facial redness, the testers are 18-45 years old, 10 testers are one group, 3 groups of testers are respectively used for applying the mask for 15 minutes at 10 pm, and the test cases 26, the comparative test cases 5 and the comparative groups are respectively scored according to skin red blood streak reduction conditions and use feelings after one week, wherein the evaluation criteria are as follows:

1 part-after one week of use, the redness degree of the face does not decline, and the effect is basically not achieved;

2 minutes-the redness degree of the face is reduced after one week of use, but the effect of the reduction is not obvious;

3 minutes-the redness degree of the face is reduced after one week of use, and the reduction effect is obvious;

4 minutes-the redness degree of the face is reduced after three days of use, and the reduction effect is obvious;

5 minutes-the redness of the face is reduced in the next day, and the reduction effect is obvious.

The specific test data for runs 1-3 are detailed in tables 5-11.

TABLE 5

According to the detection data of the experimental examples 1-6 and the control group in Table 5, the water content of the skin cuticle of the mask liquid prepared in the experimental examples 1-6 is larger than that of the skin cuticle of the control group after being applied for 5 minutes, and the increase of the water content of the skin cuticle of the experimental examples 1-6 compared with the initial value is larger than that of the control group after being applied for 5 minutes, which shows that the mask liquid prepared in the experimental examples 1-6 has better moisturizing and absorbing effects compared with the commercially available mask.

The moisture content values of the same time after the mask is taken off in the experimental examples 1-6 and the control group are compared, the moisture content of the skin cuticle of the experimental examples 1-6 after the mask is taken off for 30 minutes and 60 minutes is larger than the moisture content of the skin cuticle of the control group after the mask is taken off for 30 minutes and 60 minutes, the moisture loss of the skin cuticle of the experimental examples 1-6 in 30 minutes and 60 minutes is smaller than the moisture loss of the skin cuticle of the control group in 30 minutes and 60 minutes, and the fact that the mask liquid prepared in the experimental examples 1-6 has stronger water locking and moisturizing capacities than the commercially available mask liquid is shown.

TABLE 6

According to the detection data of the experimental examples 6 and the comparative experimental examples 1 to 4 in Table 6, when the experimental examples 1 to 4 were not added with the three substances of the alpine leontopodium flower/leaf extract, the fragrant solomonseal rhizome extract and the lactobacillus/rice fermentation product or one of the three substances was removed, the increase of the moisture content of the skin horny layer after the application of the mask liquid of the comparative experimental examples 1 to 4 by the trial person for 5 minutes was much smaller than the numerical value of the experimental example 6, which indicates that the absorption promoting ability of the mask liquid of the comparative experimental examples 1 to 4 to the skin was weak; the loss amount of the moisture content of the skin cuticle after the mask is taken off in the comparative experiment examples 1-4 for 30 and 60 minutes is larger than that after the mask is taken off in the experiment example 6 for 30 and 60 minutes, which indicates that the effect of the mask liquid prepared in the comparative experiment examples 1-4 on locking and moisturizing is poorer than that in the comparative experiment example 5.

The inventor analyzes that a plurality of high-permeability colloid groups are formed under the synergistic effect of a composition A containing the alpine leontopodium herb flower/leaf extract, a composition B containing the fragrant solomonseal rhizome extract and a composition C containing lactobacillus/rice fermentation products in the high-permeability water-locking composition, when the components of the high-permeability water-locking composition in the mask liquid are contacted with facial skin of a tester, the high-permeability colloid groups can rapidly permeate into deep cells of the skin, and substances such as a humectant, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition are wrapped by the colloid groups and rapidly enter the skin cells together with the colloid groups, so that the absorption of the skin to the high-permeability water-locking composition is promoted, and the absorption capacity of the skin is improved; the humectant, the soothing agent, the repairing agent and the colloid groups in the high-permeability water-locking composition jointly enter deep cells of skin, so that the facial skin can be deeply repaired and moisturized, and nutrition ingredients are not easy to lose, so that the mask liquid has remarkable soothing and moisturizing effects.

In the comparative experiment examples 1-4, one or no three substances are added, the synergistic effect of the three substances is lost, the help of high-permeability colloid groups formed under the synergistic effect of the three substances is lost, and the substances such as the humectant, the soothing agent, the repairing agent and the like in the high-permeability water-locking composition cannot penetrate deep into the skin, so that the absorption capacity of the skin is reduced, the loss of the substances such as the humectant, the soothing agent and the repairing agent floating on the surface is faster, and the water-retaining and water-locking and repairing effects of the mask liquid are reduced.

TABLE 7

According to the detection data of experimental examples 6 and 7-14 in Table 7, the increase of the moisture content of the skin cuticle after the application of the mask for 5 minutes in experimental examples 11-12 is obviously larger than that after the application of the mask for 5 minutes in experimental examples 6 and 7-10, which shows that the effect of moisturizing and promoting skin absorption of the prepared mask liquid is better when the soothing agent in experimental examples 11-12 is prepared by combining the herba Cirsii Japonici extract, the fructus Siraitiae Grosvenorii extract, the herba gorgoniae extract, the flos Plumeriae Acutifoliae extract, the flos Nymphaeae extract and the Opuntiae Dillenii extract in a specific proportion. The value of the increase in the moisture content of the mask liquid in 5 minutes obtained in experimental examples 13 to 14 is similar to the value of the mask liquid in experimental examples 7 to 10 and smaller than the value of the mask liquid in experimental examples 11 to 12, which indicates that the moisturizing and absorption promoting effects of the mask liquid obtained in experimental examples 13 to 14 are weakened after the substances in the soothing agent are replaced by the substances, and the remarkable moisturizing and absorption promoting effects of the mask liquid obtained in experimental examples 11 to 12 on the skin cannot be achieved.

From the test data of comparative example 5 and examples 6 to 14 in Table 7, it was found that the increase in the moisture content of the skin horny layer after 5 minutes of application of the mask of comparative example 5 was significantly smaller than that of the skin horny layer after 5 minutes of application of the mask of examples 6 to 14, indicating that the ability of the mask liquid prepared in comparative example 5 to promote absorption by water was greatly impaired when no soothing agent component was added to comparative example 5.

The inventor analyzes that plant extracts such as the herba Cirsii Japonici extract and the fructus Siraitiae Grosvenorii extract in the soothing agent are cooperated with each other in a specific proportion, so that a cooperated compounding effect can be generated, each component substance in the high-permeability water locking composition and the high-permeability colloid group can be uniformly dispersed in the process of penetrating into deep cells of the skin, and the absorption capacity of the skin is improved. When the above substances are not added or replaced in the formula, the synergistic effect of the above substances in a specific ratio cannot be achieved, so that the water supplementing and absorption promoting effects of the prepared mask liquid cannot be improved.

TABLE 8

According to the detection data of the experimental examples 6 and 15 in table 8, the value of the moisture content increase of the skin cuticle of the mask liquid prepared in the experimental example 15 is improved compared with the value of the experimental example 6 when the mask liquid is applied for 5 minutes, which indicates that the efficacy of the mask liquid prepared in the experimental example 15 in the aspects of supplementing water and promoting absorption is improved when the repairing agent in the mask liquid prepared in the experimental example 15 adopts gentian extract, honeysuckle extract, wild chrysanthemum extract, hu Suogen extract, field mint extract and kuh-seng extract to be mixed with a solvent.

The inventor analyzes that the repairing agent is formed by mixing a plurality of plant extracts such as gentian extract, hu Suogen extract and the like, is beneficial to repairing the skin in all directions, and the components such as brass, amino acid and the like contained in the repairing agent are beneficial to being blended into the high-permeability colloid group, so that the stability of the high-permeability colloid group is enhanced, and the absorption promoting effect of the high-permeability colloid group on the skin is improved.

According to the detection data of the experimental examples 6 and 16 in the table 8, the value of the increase of the moisture content of the skin cuticle when the mask liquid prepared in the experimental example 16 is applied for 5 minutes is larger than that of the experimental example 6, which indicates that the water supplementing and absorption promoting capacity of the mask liquid prepared in the experimental example 16 is improved; experimental example 16 the water loss of the skin cuticle after 30 and 60 minutes of mask removal is smaller than that of experimental example 6, which shows that the mask liquid prepared in experimental example 16 has better water locking and moisturizing capabilities.

The inventor analyzes that all substances in the humectant are mutually promoted to penetrate into deep cells of the face to supplement water for the cells, so that the moisture is not easy to run off, a remarkable moisturizing effect is achieved, and the water locking capacity of the cells is improved from the deep layers of the skin.

The values of the moisture content increase of the skin cuticle of the mask liquid prepared in the experimental examples 17-19 are far larger than those of the mask liquid prepared in the experimental example 6 when the mask liquid is applied for 5 minutes, which shows that the water supplementing and absorption promoting capabilities of the mask liquid prepared in the experimental examples 17-19 are more outstanding; the water retention and moisture retention capacity of the mask liquid prepared in experimental examples 17-19 is improved as the water loss of the skin cuticle after 30 minutes and 60 minutes of mask removal in experimental examples 17-19 is smaller than that in experimental example 6. Experimental examples 17 to 19 adopt the better components in the above examples on the basic formulation of experimental example 6, so that the values of the performance detection data of experimental examples 17 to 19 are greatly improved compared with the values of experimental example 6, and the combination ratio of the components in the moisturizing relieving composition in experimental example 18 is selected as the best combination ratio.

TABLE 9

According to the detection data of the experimental examples 18 and the experimental examples 20-21 in the table 9, the increase of the moisture content of the skin cuticle after the mask liquid prepared in the experimental examples 20-21 is applied for 5 minutes is larger than the data of the experimental example 18, which indicates that the mask liquid has better water supplementing and absorption promoting effects when the mass percentage of arginine in the mask liquid prepared in the experimental examples 20-21 is 0.125-0.135 percent.

According to analysis of the inventor, when the mass percentage of arginine accounts for 0.125-0.135% in the mask liquid, the acid-base regulation effect of the arginine is better, so that the fusion of a colloid group with high permeability and other components in the mask liquid is better, and a part of arginine can be fused into the colloid group with high permeability, so that the dispersion uniformity of the colloid group can be improved, and the uniform absorption of facial skin is promoted; and can promote the colloid groups to penetrate deeply into dermal fibroblasts, thereby improving the skin absorption effect.

Table 10

According to the detection data of experimental examples 18 and 22-24 in Table 10, the increase of the moisture content of the skin cuticle after the mask liquid prepared in experimental examples 22-24 is applied for 5 minutes is obviously higher than that of the mask liquid prepared in experimental example 18, which indicates that the mask liquid prepared in experimental examples 22-24 has better effects of supplementing water, promoting absorption and relieving restoration. The numerical value of the moisture loss amount of the skin cuticle after the mask is taken off for 30 minutes in the experimental examples 22-24 is smaller than that in the experimental example 18, which shows that the mask liquid prepared in the experimental examples 22-24 can achieve a certain moisture-locking and preserving effect in a short time.

According to the analysis of the inventor, carbomer can increase the cohesiveness of the colloid group, is beneficial to improving the structural stability of the colloid group, enhancing the absorption effect of skin, and is beneficial to improving the cohesiveness between the penetration water-locking composition and other components in the mask liquid; the sclerotium rolfsii is beneficial to controlling the viscosity of the mask liquid, maintaining the stability of a mask liquid system, and has good cohesiveness with colloid groups, so that the cohesiveness between other components in the mask liquid and the colloid groups is improved.

The mask liquid prepared in the experimental examples 25-26 adopts the better components in the experimental examples, so that the values of all performance detection data of the experimental examples 25-26 are greatly improved compared with the values of the experimental example 18, the performance data of the mask liquid prepared in the experimental examples 25 and 26 are similar, and the mask liquid prepared in the experimental example 26 is selected as the optimal example of the application.

The redness relieving condition of the face of the testers is classified into a table, and the detail is shown in a table 11.

TABLE 11

According to the scores of 30 testers in table 11 for experiment example 26, comparative experiment example 5 and control group, the composition A prepared in the experiment example 1, the composition B prepared in the preparation example 4, the composition C prepared in the preparation example 5, the soothing agent prepared in the preparation example 13, the repairing agent prepared in the preparation example 16 and the high-permeability water-locking composition prepared in the preparation example 19 are selected, and the overall score of the mask liquid prepared by mixing the high-permeability water-locking composition with carbomer, sclerotium, arginine and other substances is more than 4 minutes, which indicates that the high-permeability water-locking composition in the mask liquid prepared in the experiment example 26 is the optimal proportion and the combined action with other raw material components is optimal, so that the mask liquid has a remarkable effect on the efficacy of relieving and reducing facial redness.

The components of the soothing agent are removed from the mask liquid prepared in the comparative experiment example 5, and when the ingredients of the soothing agent, namely the herba Cirsii Japonici extract, the fructus momordicae extract, the gorgonian coral extract, the white plumeria rubra extract, the white water lily flower extract and the Cactus fruit extract, cannot be combined in a specific proportion to produce a synergistic effect, the components of the mask liquid prepared in the comparative experiment example 5 are all 2-3, which indicates that the effect of other components in the mask liquid prepared in the comparative experiment example 5 on relieving the problem of facial redness after the soothing ingredients are lost is not great, and the obvious soothing effect of the mask liquid prepared in the experiment example 25 cannot be achieved.

The scores of the control groups are all 2-3 points and lower than those of experimental example 26, which shows that the mask liquid prepared according to the optimal component proportion of the application has remarkable effect on relieving compared with the commercially available mask liquid.

The present embodiment is merely illustrative of the present application and is not intended to be limiting, and those skilled in the art, after having read the present specification, may make modifications to the present embodiment without creative contribution as required, but is protected by patent laws within the scope of the claims of the present application.

Claims

1. A soothing and moisturizing mask liquid of a high-permeability water-locking composition is characterized in that: comprises the following raw materials in percentage by weight:

and B phase: arginine 0.125-0.135%;

and D phase: 2.1-3.9% of high-permeability water-locking composition;

the balance being water;

wherein the thickener comprises one or two of carbomer and sclerotium rolfsii;

the high-permeability water-locking composition comprises the following raw materials in percentage by weight:

wherein the composition A consists of 5-7% wt of the alpine leontopodium flower/leaf extract and a solvent;

the composition C consists of 98-99% wt of lactobacillus/rice fermentation product and solvent;

the soothing agent consists of 1.6-1.8% wt of herba Cirsii Japonici extract, 1.6-1.8% wt of fructus Siraitiae Grosvenorii extract, 1.6-1.8% wt of herba Pelargonii Graveolentis extract, 1.6-1.8% wt of white plumeria extract, 1.6-1.8% wt of white water lily flower extract, 1.6-1.8% wt of Opuntia Dillenii extract and solvent;

The repairing agent consists of 3kg of gentian root extract, 0.5kg of honeysuckle flower extract, 0.5kg of wild chrysanthemum flower extract, 0.5kg of Yan Hu Suogen extract, 0.5kg of peppermint extract, 0.5kg of kuh-seng root extract, 0.5kg of 1, 2-pentanediol, 0.5kg of octanediol, 17.5kg of propylene glycol and 76kg of water;

the humectant consists of 7.5kg of xylitol, 35kg of dehydrated xylitol, 15kg of centella asiatica extract, 25kg of tremella extract, 1, 2-hexanediol 1.5kg and 16kg of water.

2. A method for preparing the soothing and moisturizing facial mask liquid according to claim 1, which comprises the following steps: