CN110974739A - Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof - Google Patents

Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof Download PDF

Info

Publication number
CN110974739A
CN110974739A CN201911101056.5A CN201911101056A CN110974739A CN 110974739 A CN110974739 A CN 110974739A CN 201911101056 A CN201911101056 A CN 201911101056A CN 110974739 A CN110974739 A CN 110974739A
Authority
CN
China
Prior art keywords
extract
whitening
edelweiss
stirring
repairing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911101056.5A
Other languages
Chinese (zh)
Inventor
曾芳芳
王泽智
蒋旭文
王玉琪
林佳明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Llg Biotechnology Co ltd
Original Assignee
Shenzhen Llg Biotechnology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Llg Biotechnology Co ltd filed Critical Shenzhen Llg Biotechnology Co ltd
Priority to CN201911101056.5A priority Critical patent/CN110974739A/en
Publication of CN110974739A publication Critical patent/CN110974739A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a whitening and repairing facial mask containing a leontopodium alpinum extract and a preparation method thereof.

Description

Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a whitening and repairing facial mask containing a leontopodium alpinum extract and a preparation method thereof.
Background
With the development of society and the improvement of living standard of people, the requirements of consumers on daily care products are higher and higher, and the requirements on the efficacy of the product are more and more refined. Because of the skin color problem of yellow people, Asian women generally have the problems of dark skin color, dark yellow color, lack of luster, easy allergy, pigmentation and the like. Because of the traditional beauty concept of "one white shading three ugs", the pursuit of whitening by asian women never stops just like the pursuit of brightness by humans. The skin is intended to be the most attractive white, certainly with some facial masks. The secret formula of getting more white and getting better is that the skin whitening mask is required to be prepared. A whitening facial mask is a facial mask added with components with the effects of promoting melanin metabolism, inhibiting and destroying melanin generation, preventing tyrosinase from activating or reducing melanin intermediates and the like. The whitening component must effectively penetrate into the skin substrate to exert the function, and the product is preferably added with a component for promoting cell metabolism.
Although the whitening masks on the market are various in types, the whitening masks such as face masks, tear-off masks, water-washing masks and sleeping masks are all good, the whitening effect is slow to take effect, the traditional preservative is large in irritation, the product is unstable and easy to discolor, and the like.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide a whitening and repairing facial mask containing a leontopodium alpinum extract and a preparation method thereof.
The purpose of the invention is realized by adopting the following technical scheme:
a whitening and repairing facial mask containing herba Leontopodii Gaoshancei extract is prepared from component A, component B and component C; the component A comprises: 0.5-5 wt% of nicotinamide, 261-5 wt% of glyceryl polyether, 0.2-3 wt% of betaine, 0.05-0.3 wt% of allantoin, 0.01-0.2 wt% of EDTA-disodium, 0.05-0.3 wt% of thickening agent, 0.01-0.1 wt% of a mixture of egg white extract and acrylate copolymer and the balance of water; the component B comprises: 3-10 wt% of polyhydric alcohol and 0.2-1 wt% of preservative; the component C comprises: 1-5 wt% of hydroxyethyl urea, 0.5-3 wt% of PEG/PPG-17/6 copolymer, 0.5-5 wt% of tranexamic acid, 0.3-3 wt% of ellagic acid, 0.1-2 wt% of carnosine, 0-1 wt% of citric acid, 0.2-2 wt% of anti-allergic agent and 0.5-3 wt% of edelweiss/leaf extract; wherein the antiseptic comprises one or more of p-hydroxyacetophenone, zanthoxylum bungeanum maxim fruit extract, grapefruit seed extract, anemone chinensis flower extract, zanthoxylum piperitum fruit plant extract, peony root extract, scutellaria baicalensis root extract and forsythia suspensa extract; the antiallergic agent comprises one or more of oat bran extract, peony root extract, olive leaf extract, Astragalus membranaceus root extract, Atractylodes macrocephala root extract, Saposhnikovia divaricata root extract, Chamomilla flower extract, Albizia julibrissin bark extract and Glycyrrhizae radix extract.
The core components for realizing whitening and repairing of the whitening and repairing mask containing the leontopodium alpinum extract comprise the leontopodium alpinum flower/leaf extract, carnosine and ellagic acid, and the natural plant extract is used as a preservative and an anti-allergy agent, so that the whitening and repairing mask has the effects of relieving, resisting allergy, being safe and free of stimulation.
Alpine leontopodium flower/leaf extract: edelweiss are also known as alpine edelweiss, which are famous alpine flowers in europe, listed as protected plants by many countries, and are more distinguished as national flowers by switzerland. He grows in the alpine mountain over 1700 meters, has a high self-defense ability, and can resist severe weather and other growing environments. The essence components of the skin-care product contain caffeic acid, vanillic acid, protocatechu, chlorogenic acid, luteolin and edetic acid, have strong antioxidation, and can permeate into skin, help to decompose and metabolize impurities, relieve and calm skin, discharge harmful substances in skin, promote cell repair and regeneration, stimulate expression of related genes of strengthening barriers, strengthen skin barriers and other effects. It has good protective effect on skin under the influence of ultraviolet rays, pollution and free radicals, and can resist aging caused by free radicals and inflammation.
Carnosine is a naturally-occurring dipeptide, is present in tissues such as skeletal muscle, brain and the like of vertebrates, consists of β -alanine and L-histidine, can eliminate free radicals, resist oxidation, has excellent anti-glycosylation effect, and has physiological functions of recovering fatigue, delaying senescence, preventing diseases and the like.
Ellagic acid: is a polyphenol component existing in natural berry fruit, which can neutralize copper ion, inhibit tyrosinase activity, effectively block Maillarine pigment generation in melanogenesis cells, and has effects of whitening and speckle reducing. Ellagic acid also has high antioxidant activity, and is effective against free radicals, thereby inhibiting oxidation of melanin of tannin, inhibiting pigment blackening, and reducing color spot. In addition, ellagic acid is strongly absorbed in the whole ultraviolet region, and can be effectively protected from external damage. Ellagic acid has effects of promoting proteasome activity, inhibiting B-galactosidase activity, enhancing cell metabolism activity, and promoting wound healing and repair.
Further, the thickening agent comprises one or more of carbomer, hydroxyethyl cellulose, polyacrylate cross-linked polymer-6 and xanthan gum.
Still further, the polyhydric alcohol comprises one or more of glycerol, butanediol, and propylene glycol.
The preparation method of the whitening and repairing mask containing the edelweiss extract comprises the following steps:
1) mixing the thickening agent with water for later use;
2) adding the preservative into the polyhydric alcohol, stirring and heating, and cooling for later use after complete dissolution;
3) mixing the mixture of the egg white extract and the acrylate copolymer with the glyceryl polyether-26, and stirring uniformly for later use;
4) sequentially adding water, nicotinamide, allantoin, disodium EDTA, betaine, the solution obtained in the step 1) and the mixture obtained in the step 3) into an emulsifying pot, heating, stirring and dissolving to 85-90 ℃, and homogenizing at a high speed;
5) stopping heating, cooling the mixture obtained in the step 4) to 50-55 ℃, adding the solution obtained in the step 2), and uniformly stirring;
6) cooling the mixture obtained in the step 5) to 35-40 ℃, sequentially adding PEG/PPG-17/6 copolymer, ellagic acid, tranexamic acid, carnosine, an anti-allergic agent, citric acid, hydroxyethyl urea and the extract of the flowers/leaves of the alpine edelweiss, and uniformly stirring to obtain the whitening and repairing facial mask containing the extract of the alpine edelweiss.
Further, in the step 2), the heating temperature is 50-80 ℃.
Further, in the step 4), the homogenizing time is 5-10 minutes, and the homogenizing speed is 2500-; stirring for 20-40 minutes at the stirring speed of 60-80 rpm.
Further, in the step 5) and the step 6), the stirring speed is 60-80 rpm; the stirring time of the step 6) is 40-60 minutes.
Further, in the step 6), the added extract of the flowers/leaves of the leontopodium alpinum is diluted by water and butanediol, wherein the weight ratio of the extract of the flowers/leaves of the leontopodium alpinum to the water to the butanediol is 3: 30: 67.
compared with the prior art, the invention has the beneficial effects that:
the whitening and repairing facial mask containing the edelweiss extract disclosed by the invention takes the edelweiss flower/leaf extract, the carnosine and the ellagic acid as core components, has the effects of relieving, repairing, whitening and removing freckles, adopts the plant preservative and the anti-allergic agent, and is safe and non-irritant.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
Example 1
A whitening and repairing mask containing a Hibiscus sabdariffa extract is composed of the following raw materials in parts by weight: the component A comprises:
Figure BDA0002269882780000051
and B component:
3 percent of propylene glycol
0.3 percent of preservative
C component
Figure BDA0002269882780000052
Wherein the thickening agent is carbomer and hydroxyethyl cellulose, and the weight ratio of carbomer to hydroxyethyl cellulose is 2: 1; the preservative is p-hydroxyacetophenone, zanthoxylum bungeanum fruit extract and scutellaria baicalensis root extract, and the weight ratio of the p-hydroxyacetophenone to the zanthoxylum bungeanum fruit extract to the scutellaria baicalensis root extract is 2: 3: 3; the antiallergic agent is a mixture of six plant extracts of oat bran extract, peony root extract, astragalus membranaceus root extract, bighead atractylodes rhizome root extract, divaricate saposhnikovia root extract and chamomile extract, and the weight ratio of each plant extract is the same. Diluting the added edelweiss flower/leaf extract by water and butanediol, wherein the weight ratio of the edelweiss flower/leaf extract to the water to the butanediol is 3: 30: 67.
the preparation method of the whitening and repairing mask containing the edelweiss extract comprises the following steps:
1) mixing the thickening agent with water for later use;
2) adding the preservative into the polyhydric alcohol, stirring and heating to 50 ℃, and cooling for later use after complete dissolution;
3) mixing the mixture of the egg white extract and the acrylate copolymer with the glyceryl polyether-26, and stirring uniformly for later use;
4) sequentially adding water, nicotinamide, allantoin, disodium EDTA, betaine, the solution obtained in the step 1) and the mixture obtained in the step 3) into an emulsifying pot, heating, stirring and dissolving to 85-90 ℃, and homogenizing at a high speed; wherein the homogenizing time is 5 minutes, and the homogenizing speed is 2500 rpm; stirring for 20 minutes at the stirring speed of 60rpm under the heat preservation condition;
5) stopping heating, cooling the mixture obtained in the step 4) to 50 ℃, adding the solution obtained in the step 2), and uniformly stirring; wherein the stirring speed was 60 rpm.
6) Cooling the mixture obtained in the step 5) to 35 ℃, sequentially adding PEG/PPG-17/6 copolymer, ellagic acid, tranexamic acid, carnosine, an anti-allergic agent, citric acid, hydroxyethyl urea and the extract of the flowers/leaves of the alpine edelweiss, and uniformly stirring to obtain the whitening and repairing facial mask containing the extract of the alpine edelweiss. Wherein the stirring speed was 60rpm and the stirring time was 40 minutes.
Example 2
A whitening and repairing mask containing a Hibiscus sabdariffa extract is composed of the following raw materials in parts by weight: the component A comprises:
Figure BDA0002269882780000071
and B component:
propylene glycol 5%
0.5 percent of preservative
C component
Figure BDA0002269882780000072
Wherein the thickening agent is carbomer and hydroxyethyl cellulose, and the weight ratio of carbomer to hydroxyethyl cellulose is 2: 1; the preservative is p-hydroxyacetophenone, zanthoxylum bungeanum fruit extract and scutellaria baicalensis root extract, and the weight ratio of the p-hydroxyacetophenone to the zanthoxylum bungeanum fruit extract to the scutellaria baicalensis root extract is 2: 3: 3; the antiallergic agent is a mixture of six plant extracts of oat bran extract, peony root extract, astragalus membranaceus root extract, bighead atractylodes rhizome root extract, divaricate saposhnikovia root extract and chamomile extract, and the weight ratio of each plant extract is the same. Diluting the added edelweiss flower/leaf extract by water and butanediol, wherein the weight ratio of the edelweiss flower/leaf extract to the water to the butanediol is 3: 30: 67.
the preparation method of the whitening and repairing mask containing the edelweiss extract comprises the following steps:
1) mixing the thickening agent with water for later use;
2) adding the preservative into the polyhydric alcohol, stirring and heating to 65 ℃, and cooling for later use after complete dissolution;
3) mixing the mixture of the egg white extract and the acrylate copolymer with the glyceryl polyether-26, and stirring uniformly for later use;
4) sequentially adding water, nicotinamide, allantoin, disodium EDTA, betaine, the solution obtained in the step 1) and the mixture obtained in the step 3) into an emulsifying pot, heating, stirring and dissolving to 85 ℃, and homogenizing at a high speed; wherein the homogenizing time is 7 minutes, and the homogenizing speed is 2600 rpm; stirring for 30 minutes at the stirring speed of 70rpm under the heat preservation condition;
5) stopping heating, cooling the mixture obtained in the step 4) to 55 ℃, adding the solution obtained in the step 2), and uniformly stirring; wherein the stirring speed was 70 rpm.
6) Cooling the mixture obtained in the step 5) to 37 ℃, sequentially adding PEG/PPG-17/6 copolymer, ellagic acid, tranexamic acid, carnosine, an anti-allergic agent, citric acid, hydroxyethyl urea and the extract of the flowers/leaves of the alpine edelweiss, and uniformly stirring to obtain the whitening and repairing facial mask containing the extract of the alpine edelweiss. Wherein the stirring speed was 70rpm and the stirring time was 50 minutes.
Example 3
A whitening and repairing mask containing a Hibiscus sabdariffa extract is composed of the following raw materials in parts by weight:
the component A comprises:
Figure BDA0002269882780000091
and B component:
propylene glycol 6%
0.6 percent of preservative
C component
Figure BDA0002269882780000092
Wherein the thickening agent is carbomer and hydroxyethyl cellulose, and the weight ratio of carbomer to hydroxyethyl cellulose is 2: 1; the preservative is p-hydroxyacetophenone, zanthoxylum bungeanum fruit extract and scutellaria baicalensis root extract, and the weight ratio of the p-hydroxyacetophenone to the zanthoxylum bungeanum fruit extract to the scutellaria baicalensis root extract is 2: 3: 3; the antiallergic agent is a mixture of six plant extracts of oat bran extract, peony root extract, astragalus membranaceus root extract, bighead atractylodes rhizome root extract, divaricate saposhnikovia root extract and chamomile extract, and the weight ratio of each plant extract is the same. Diluting the added edelweiss flower/leaf extract by water and butanediol, wherein the weight ratio of the edelweiss flower/leaf extract to the water to the butanediol is 3: 30: 67.
the preparation method of the whitening and repairing mask containing the edelweiss extract comprises the following steps:
1) mixing the thickening agent with water for later use;
2) adding the preservative into the polyhydric alcohol, stirring and heating to 80 ℃, and cooling for later use after complete dissolution;
3) mixing the mixture of the egg white extract and the acrylate copolymer with the glyceryl polyether-26, and stirring uniformly for later use;
4) sequentially adding water, nicotinamide, allantoin, disodium EDTA, betaine, the solution obtained in the step 1) and the mixture obtained in the step 3) into an emulsifying pot, heating, stirring and dissolving to 90 ℃, and homogenizing at a high speed; wherein the homogenizing time is 10 minutes, and the homogenizing speed is 2700 rpm; stirring for 40 minutes at the stirring speed of 80rpm under the heat preservation condition;
5) stopping heating, cooling the mixture obtained in the step 4) to 55 ℃, adding the solution obtained in the step 2), and uniformly stirring; here, the stirring speed was 80 rpm.
6) Cooling the mixture obtained in the step 5) to 40 ℃, sequentially adding PEG/PPG-17/6 copolymer, ellagic acid, tranexamic acid, carnosine, an anti-allergic agent, citric acid, hydroxyethyl urea and the extract of the flowers/leaves of the alpine edelweiss, and uniformly stirring to obtain the whitening and repairing facial mask containing the extract of the alpine edelweiss. Wherein the stirring speed was 80rpm and the stirring time was 60 minutes.
Example 4
A whitening and repairing mask containing a Hibiscus sabdariffa extract is composed of the following raw materials in parts by weight:
the component A comprises:
Figure BDA0002269882780000101
Figure BDA0002269882780000111
and B component:
propylene glycol 8%
0.8 percent of preservative
C component
Figure BDA0002269882780000112
Wherein the thickening agent is carbomer and hydroxyethyl cellulose, and the weight ratio of carbomer to hydroxyethyl cellulose is 2: 1; the preservative is p-hydroxyacetophenone, zanthoxylum bungeanum fruit extract and scutellaria baicalensis root extract, and the weight ratio of the p-hydroxyacetophenone to the zanthoxylum bungeanum fruit extract to the scutellaria baicalensis root extract is 2: 3: 3; the antiallergic agent is a mixture of six plant extracts of oat bran extract, peony root extract, astragalus membranaceus root extract, bighead atractylodes rhizome root extract, divaricate saposhnikovia root extract and chamomile extract, and the weight ratio of each plant extract is the same. Diluting the added edelweiss flower/leaf extract by water and butanediol, wherein the weight ratio of the edelweiss flower/leaf extract to the water to the butanediol is 3: 30: 67.
the preparation method of the whitening and repairing mask containing the edelweiss extract is the same as that of example 3.
Example 5
A whitening and repairing mask containing a Hibiscus sabdariffa extract is composed of the following raw materials in parts by weight:
the component A comprises:
Figure BDA0002269882780000121
and B component:
10 percent of propylene glycol
1 percent of preservative
C component
Figure BDA0002269882780000122
Figure BDA0002269882780000131
Wherein the thickening agent is carbomer and hydroxyethyl cellulose, and the weight ratio of carbomer to hydroxyethyl cellulose is 2: 1; the preservative is p-hydroxyacetophenone, zanthoxylum bungeanum fruit extract and scutellaria baicalensis root extract, and the weight ratio of the p-hydroxyacetophenone to the zanthoxylum bungeanum fruit extract to the scutellaria baicalensis root extract is 2: 3: 3; the antiallergic agent is a mixture of six plant extracts of oat bran extract, peony root extract, astragalus membranaceus root extract, bighead atractylodes rhizome root extract, divaricate saposhnikovia root extract and chamomile extract, and the weight ratio of each plant extract is the same. Diluting the added edelweiss flower/leaf extract by water and butanediol, wherein the weight ratio of the edelweiss flower/leaf extract to the water to the butanediol is 3: 30: 67.
the preparation method of the whitening and repairing mask containing the edelweiss extract is the same as that of example 3.
Control group 1
The mask of control 1 was prepared in the same manner as in example 3, except that no extract of flowers/leaves of Hibiscus alpinus was added.
Control group 2
The facial mask of control 2 was prepared in the same manner as in example 3 except that no carnosine was added.
Control group 3
The mask of control 3 was prepared in the same manner as in example 3 except that ellagic acid was not added.
Test evaluation
Test 1 test subjects routine experience test
Volunteers included 80 females and 40 males, aged between 20-50 years, and were divided on average into 8 groups, corresponding to examples 1-5 and control groups 1-3, respectively, each group consisting of 10 females and 5 males, respectively, for a test period of 8 weeks. The facial mask of the corresponding group was applied three times a week for 8 weeks to 8 volunteers.
The test of the use experience and the degree of skin improvement before and after the use of the product was evaluated by the volunteers themselves in the form of table evaluation, and the following table shows the evaluation results of the skin-sticking property, air permeability, freshness, moisture retention, safety, repair effect and whitening effect of the volunteers using the product. The test effects are graded, each item is 10 points in total: scores 9-10 are high, indicating good, scores 8-9 indicating good, scores 8-6 indicating acceptable, scores 3-5 indicating poor, and scores 1-2 not acceptable. The evaluation results are shown in the table (the data in the table are average data).
TABLE 1 volunteers assessment of use and degree of skin improvement of examples 1-5 and control groups 1-3
Item Skin-sticking property Air permeability Degree of freshness Moisture retention Safety feature Repairing effect Whitening effect
Example 1 8.2 7.8 8.0 8.4 8.8 7.8 6.1
Example 2 8.6 8.3 8.2 8.9 9.0 8.5 7.3
Example 3 9.2 9.0 8.8 9.4 9.5 9.2 8.2
Example 4 8.5 8.5 9.0 9.3 9.6 9.3 8.0
Example 5 8.4 8.0 8.8 9.0 9.8 9.4 7.7
Control group 1 9.2 9.0 8.5 8.7 8.8 6.5 8.0
Control group 2 9.2 9.0 8.9 9.4 9.2 8.8 6.9
Control group 3 9.0 9.0 8.8 9.3 9.4 9.1 6.5
As is clear from table 1, in examples 1 to 5, the skin-adhering, air-permeable, moisturizing, repairing, and whitening effects of example 3 were superior to those of the other examples. In examples 1 to 5, the addition amounts of ellagic acid, carnosine, the flower/leaf extract of leontopodium alpinum and nicotinamide are gradually increased, but the efficacy and effect do not show an increasing effect, so that in the formula, the more the whitening components are, the better the whitening components are, the proper proportion of the components is, and the better effect can be achieved through synergistic effect.
Example 3 and controls 1-3 were the same except that no extract of flowers/leaves of Hibiscus alpina, carnosine or ellagic acid was added. However, compared with example 3, the control group 1 has no added extract of flowers/leaves of leontopodium japonicum, and has a large influence on the moisturizing, safety and repairing effects of the product; compared with the embodiment 3, the control group 2 does not add carnosine, and has larger influence on the repairing, anti-aging and whitening effects of the product; in comparison with example 3, the control group 3 had a greater effect on the whitening effect of the product without adding ellagic acid.
Test 2 whitening repair test
The volunteers were tested for melanin and stratum corneum. The test method comprises the following steps: before test 1, the right half face of each group of volunteers was tested for melanin content and stratum corneum thickness using an MC680 skin tester; after 8 weeks in trial 1, the skin melanin content and the stratum corneum thickness were measured at the same site in each group of volunteers, and the reduction in melanin and the increase in stratum corneum were determined in the following table (the data in the table are mean data).
TABLE 2 volunteers decreased amount of melanin and increased amount of the angle layer for examples 1-5 and controls 1-3
Figure BDA0002269882780000151
As can be seen from table 2, after the facial masks of examples 1 to 5 and control groups 1 to 3 were used, the skin melanin was decreased to different degrees, and the thickness of the stratum corneum was increased to different degrees, i.e., the facial masks of examples 1 to 5 and control groups 1 to 3 had the whitening and repairing effects.
Among them, the decrease amount of melanin and the increase amount of the thickness of the horny layer in examples 2 to 5 are superior to those in control groups 1 to 3, so that the whitening and repairing effects of examples 2 to 5 are more remarkable. The control group 1 had a greater reduction in melanin than the control group 2 and the control group 3, indicating that the alpine leontopodium flower/leaf extract enhanced the whitening effect. The control group 2 and the control group 3 showed a larger increase in the stratum corneum than the control group 2, indicating that carnosine and ellagic acid enhanced the repairing effect.
Test 3 Patch test
Test article-whitening mask solution prepared in example 3.
Negative control deionized water
The test persons are 120 persons, 40 persons in men and 80 persons in women, the age is 20-50 years old, and the test persons meet the volunteer selection standard of the test subjects.
The spot sticking method comprises selecting qualified spot tester, dropping 0.020-0.025 mL (semifluid) of the tested object and negative control into the spot tester, applying special adhesive tape (hypoallergenic) on the forearm curve side of the tested object, applying the adhesive tape on the skin by light pressing with palm, removing the tested object after 24 hr, observing skin reaction for 0.5 hr, 24 hr and 48 hr after removal, and recording the result according to skin reaction grading standard in technical Specification for safety of cosmetics (2015 version). The classification criteria are as follows: 0-negative reaction; 1-suspicious reaction, only faint erythema; 2-weak positive reaction (erythema reaction), erythema, infiltration, edema, and possibly pimples; 3-strong positive reaction (herpetic reaction), erythema, infiltration, water, pimples, herpes, which can go beyond the test area; 4-very strong positive reaction (confluent herpes reaction), marked erythema, severe infiltration, edema, confluent herpes, reaction beyond the test area. The number of volunteers with skin reactions of grade 0-4 after 0.5h, 24h and 48h of removal of the test substance was recorded. The test results are shown in Table 3.
TABLE 3 Patch test reaction
Figure BDA0002269882780000161
Figure BDA0002269882780000171
As can be seen from table 3, 120 volunteers all showed negative reactions and no adverse reactions after using the whitening and repairing facial mask containing the leontopodium alpinum extract of example 3, which indicates that the facial mask of the present invention is safe and non-irritant after using the natural plant extract as the antiseptic and the anti-allergic agent.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and those skilled in the art can make any insubstantial changes and substitutions based on the present invention.

Claims (8)

1. A whitening and repairing facial mask containing a Hibiscus sabdariffa extract is characterized by being prepared from a component A, a component B and a component C; the component A comprises: 0.5-5 wt% of nicotinamide, 261-5 wt% of glyceryl polyether, 0.2-3 wt% of betaine, 0.05-0.3 wt% of allantoin, 0.01-0.2 wt% of EDTA-disodium, 0.05-0.3 wt% of thickening agent, 0.01-0.1 wt% of a mixture of egg white extract and acrylate copolymer and the balance of water; the component B comprises: 3-10 wt% of polyhydric alcohol and 0.2-1 wt% of preservative; the component C comprises: 1-5 wt% of hydroxyethyl urea, 0.5-3 wt% of PEG/PPG-17/6 copolymer, 0.5-5 wt% of tranexamic acid, 0.3-3 wt% of ellagic acid, 0.1-2 wt% of carnosine, 0-1 wt% of citric acid, 0.2-2 wt% of anti-allergic agent and 0.5-3 wt% of edelweiss/leaf extract; wherein the antiseptic comprises one or more of p-hydroxyacetophenone, zanthoxylum bungeanum maxim fruit extract, grapefruit seed extract, anemone chinensis flower extract, zanthoxylum piperitum fruit plant extract, peony root extract, scutellaria baicalensis root extract and forsythia suspensa extract; the antiallergic agent comprises one or more of oat bran extract, peony root extract, olive leaf extract, Astragalus membranaceus root extract, Atractylodes macrocephala root extract, Saposhnikovia divaricata root extract, Chamomilla flower extract, Albizia julibrissin bark extract and Glycyrrhizae radix extract.
2. The mask of claim 1, wherein the thickener comprises one or more of carbomer, hydroxyethyl cellulose, polyacrylate crosspolymer-6, xanthan gum.
3. The mask of claim 1, wherein the polyhydric alcohol comprises one or more of glycerin, butylene glycol, and propylene glycol.
4. The method for preparing a whitening and repairing mask containing the edelweiss extract as set forth in any one of claims 1 to 3, comprising the steps of:
1) mixing the thickening agent with water for later use;
2) adding the preservative into the polyhydric alcohol, stirring and heating, and cooling for later use after complete dissolution;
3) mixing the mixture of the egg white extract and the acrylate copolymer with the glyceryl polyether-26, and stirring uniformly for later use;
4) sequentially adding water, nicotinamide, allantoin, disodium EDTA, betaine, the solution obtained in the step 1) and the mixture obtained in the step 3) into an emulsifying pot, heating, stirring and dissolving to 85-90 ℃, and homogenizing at a high speed;
5) stopping heating, cooling the mixture obtained in the step 4) to 50-55 ℃, adding the solution obtained in the step 2), and uniformly stirring;
6) cooling the mixture obtained in the step 5) to 35-40 ℃, sequentially adding PEG/PPG-17/6 copolymer, ellagic acid, tranexamic acid, carnosine, an anti-allergic agent, citric acid, hydroxyethyl urea and the extract of the flowers/leaves of the alpine edelweiss, and uniformly stirring to obtain the whitening and repairing facial mask containing the extract of the alpine edelweiss.
5. The method for preparing a whitening and repairing mask containing the edelweiss extract as claimed in claim 4, wherein the heating temperature in the step 2) is 50-80 ℃.
6. The method for preparing a whitening and repairing mask containing the extract of leontopodium alpinum as claimed in claim 4, wherein in the step 4), the homogenizing time is 5-10 minutes, and the homogenizing speed is 2500-; stirring for 20-40 minutes at the stirring speed of 60-80 rpm.
7. The method for preparing a whitening and repairing mask containing the edelweiss extract as claimed in claim 4, wherein the stirring speed in step 5) and step 6) is 60-80 rpm; the stirring time of the step 6) is 40-60 minutes.
8. The method for preparing a whitening and repairing mask containing the edelweiss extract as claimed in claim 4, wherein in the step 6), the added edelweiss flower/leaf extract is diluted by water and butanediol, and the weight ratio of the edelweiss flower/leaf extract, the water and the butanediol is 3: 30: 67.
CN201911101056.5A 2019-11-12 2019-11-12 Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof Pending CN110974739A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911101056.5A CN110974739A (en) 2019-11-12 2019-11-12 Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911101056.5A CN110974739A (en) 2019-11-12 2019-11-12 Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof

Publications (1)

Publication Number Publication Date
CN110974739A true CN110974739A (en) 2020-04-10

Family

ID=70083919

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911101056.5A Pending CN110974739A (en) 2019-11-12 2019-11-12 Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof

Country Status (1)

Country Link
CN (1) CN110974739A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111603428A (en) * 2020-06-04 2020-09-01 陶兴仲 Whitening and freckle-removing plant type essence, preparation method and use method
CN112516022A (en) * 2020-12-03 2021-03-19 深圳市琉璃光生物科技有限公司 Sun-screening lotion and preparation method thereof
CN113576985A (en) * 2021-09-09 2021-11-02 广东星芮生物科技有限公司 High-permeability water-locking composition, soothing and moisturizing mask liquid and preparation method thereof
CN116196250A (en) * 2023-04-07 2023-06-02 中科未来(无锡)生物技术研究院有限公司 Recombinant collagen freeze-dried mask with repairing effect and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20100056168A (en) * 2008-11-19 2010-05-27 (주)아모레퍼시픽 Skin adhesive cosmetic formulation using papyrus
CN106265330A (en) * 2016-08-29 2017-01-04 杭州千岛湖蓝色天使实业有限公司 The cream that a kind of wrinkle removing is anti-ageing
CN107280998A (en) * 2017-06-16 2017-10-24 湖南御家化妆品制造有限公司 Tyrosinase inhibiting composition and application thereof
CN110075059A (en) * 2019-05-29 2019-08-02 广州睿晞生化科技有限公司 It is a kind of can the antipruritic reparation of antiallergic composition

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20100056168A (en) * 2008-11-19 2010-05-27 (주)아모레퍼시픽 Skin adhesive cosmetic formulation using papyrus
CN106265330A (en) * 2016-08-29 2017-01-04 杭州千岛湖蓝色天使实业有限公司 The cream that a kind of wrinkle removing is anti-ageing
CN107280998A (en) * 2017-06-16 2017-10-24 湖南御家化妆品制造有限公司 Tyrosinase inhibiting composition and application thereof
CN110075059A (en) * 2019-05-29 2019-08-02 广州睿晞生化科技有限公司 It is a kind of can the antipruritic reparation of antiallergic composition

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
国产非特殊用途化妆品备案服务平台: ""赛因诗婷亮肤蚕丝面膜"", 《HTTP://FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=20191023153144KUSO9》 *
国产非特殊用途化妆品备案服务平台: ""阿奇米雅透亮面膜"", 《HTTP://FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=20190820130713ZX83W&NID=20190820130713ZX8》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111603428A (en) * 2020-06-04 2020-09-01 陶兴仲 Whitening and freckle-removing plant type essence, preparation method and use method
CN112516022A (en) * 2020-12-03 2021-03-19 深圳市琉璃光生物科技有限公司 Sun-screening lotion and preparation method thereof
CN112516022B (en) * 2020-12-03 2022-08-12 深圳市琉璃光生物科技有限公司 Sun-screening lotion and preparation method thereof
CN113576985A (en) * 2021-09-09 2021-11-02 广东星芮生物科技有限公司 High-permeability water-locking composition, soothing and moisturizing mask liquid and preparation method thereof
CN116196250A (en) * 2023-04-07 2023-06-02 中科未来(无锡)生物技术研究院有限公司 Recombinant collagen freeze-dried mask with repairing effect and preparation method thereof
CN116196250B (en) * 2023-04-07 2024-04-02 中科未来(无锡)生物技术研究院有限公司 Recombinant collagen freeze-dried mask with repairing effect and preparation method thereof

Similar Documents

Publication Publication Date Title
CN110974739A (en) Whitening and repairing mask containing alpine edelweiss extract and preparation method thereof
CN110200875A (en) A kind of antiallergic whitening mask and preparation method thereof
CN112263493B (en) Sunscreen composition, sunscreen gel containing sunscreen composition and preparation method of sunscreen gel
CN112494406A (en) Whitening and freckle-removing cosmetic and preparation method thereof
CN110623882A (en) Whitening and freckle removing mask and preparation method thereof
CN112641694B (en) Whitening essence milk and preparation method thereof
CN103751057A (en) Skin-whitening moisture-preserving wrinkle-resisting mask liquid and preparation method thereof
CN110917051A (en) Whitening essence and preparation method thereof
CN112587456B (en) Repairing and whitening composition and preparation method thereof
CN110384623A (en) One kind is spraying according to safe and comfortable draft is protected
CN110585048A (en) Composition with anti-saccharification and anti-oxidation functions and application thereof
CN111920730A (en) Repairing moisturizing cream and preparation method thereof
KR102164246B1 (en) Cosmetic Compositions for Anti-oxidation and Protecting Skin from UV Comprising Complex Extracts of Plants
CN108498390B (en) Tibetan herbal extract for treating acne and preparation method and application thereof
CN112043661A (en) Whitening aloe gel and preparation method thereof
CN106214548B (en) A kind of Skin whitening care cosmetics composition and preparation method thereof
CN114344220A (en) Whitening essence and preparation method thereof
CN106727247A (en) A kind of anti acne of traditional Chinese medicine facial mask and preparation method thereof
CN112402308A (en) Multi-effect relieving moisturizing lotion and preparation method thereof
CN114159333B (en) Myobase liquid and preparation method thereof
CN113975211A (en) Composition capable of improving skin color, application thereof and face cream
CN107823111A (en) A kind of Moisturizer containing pot marigold stem cell extract
CN112220724A (en) Plant composition and preparation method and application thereof
CN109199988B (en) Whitening skin care product and preparation method thereof
CN112263525A (en) Natural cosmetic with whitening effect

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20200410