CN114983909B - Repairing composition and essence lotion and essence emulsion containing same - Google Patents

Repairing composition and essence lotion and essence emulsion containing same Download PDF

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CN114983909B
CN114983909B CN202210841427.9A CN202210841427A CN114983909B CN 114983909 B CN114983909 B CN 114983909B CN 202210841427 A CN202210841427 A CN 202210841427A CN 114983909 B CN114983909 B CN 114983909B
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extract
component
humectant
composition
water
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CN114983909A (en
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高德爱
姜森南
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Guangzhou Shouyang Pharmaceutical Biotechnology Co ltd
Guangzhou Xilisha Biotechnology Co ltd
Weiyimei Biotechnology Guangzhou Co ltd
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Guangzhou Xilisha Biotechnology Co ltd
Weiyimei Biotechnology Guangzhou Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
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    • AHUMAN NECESSITIES
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    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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    • A61P37/08Antiallergic agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The application relates to the field of sensitive skin care products, in particular to a repairing composition, essence water and essence emulsion containing the composition. The repairing composition comprises a component A, a component B, a component C and glucan; the component A comprises Dendrobium officinale stem extract, taxus cuspidata leaf extract, glycyrrhiza glabra root extract, other plant extracts, humectant A and water; the component B comprises extract of Sufang flower, other flower extract, humectant A, thickener A, antibacterial agent and water; the component C comprises radix Ophiopogonis root extract, radix Scutellariae root extract, radix Paeoniae root extract, additional plant extract, humectant A, and water. The repairing composition can be used for preparing essence water and essence emulsion. The composition is suitable for sensitive muscles and can be used for a long time.

Description

Repairing composition and essence lotion and essence emulsion containing same
Technical Field
The application relates to the field of sensitive skin care products, in particular to a repairing composition, essence water and essence emulsion containing the composition.
Background
The skin is the first barrier of the human body from the external environment and protects various barriers and organs in the body from invasion by external physical, mechanical, chemical and pathogenic microorganisms. The skin barrier is mainly composed of a variety of substances such as the sebaceous membrane, the keratin of the stratum corneum, lipids, etc.
The term "sensitive muscle" in the mouth of a person, known as "sensitive skin", refers to a state of hyperreactivity of the skin under physiological or pathological conditions, which occurs mainly in the face. The clinical manifestations of sensitive muscles are mainly burning, stinging, itching and tightness feeling when the skin is stimulated by physical, chemical or mental factors, and sometimes accompanied by erythema, desquamation, telangiectasia and the like.
At present, the most effective solution to skin sensitivity is to use medicines, but long-term use of medicines is easy to generate drug resistance, so that the situation that sensitive muscles of users cannot be relieved can be caused. Or some medicines, hormone, and the long-term use of the medicine can lead to hormone-dependent dermatitis. Therefore, there is still a need for improvement.
Disclosure of Invention
In order to develop a long-acting repair product for sensitive muscles, the application provides a repair composition and essence water and essence emulsion containing the composition.
In a first aspect, the present application provides a repair composition, which adopts the following technical scheme:
the repairing composition is prepared from the following raw materials in parts by weight: 4-6 parts of component A,2-4 parts of component B,1-3 parts of component C and 0.2-0.6 part of glucan;
the component A is prepared from the following raw materials in percentage by mass: 1.5 to 2.5 percent of dendrobium candidum stem extract, 4.8 to 6.0 percent of taxus cuspidata leaf extract, 4.5 to 5.8 percent of licorice root extract, 10 to 14 percent of other plant extract, 0.5 to 1.2 percent of humectant A and water which are supplemented to 100 percent;
the component B is prepared from the following raw materials in percentage by mass: 0.8-1.5% of extract of Fanghua flowers, 1.5-3.0% of other flower extracts, 30-45% of humectant A,0.12-0.35% of thickener A,0.35-0.5% of antibacterial agent and water to 100%;
the component C is prepared from the following raw materials in percentage by mass: 2.5-3.5% of radix ophiopogonis extract, 0.8-1.5% of radix scutellariae extract, 1.2-2.2% of radix paeoniae extract, 8-12% of additional plant extract, 48-55% of humectant A and water to be supplemented to 100%.
The composition is prepared by jointly matching a plurality of specific plant extracts, the plant extracts are used as active ingredients, the dependence of the product on chemical synthetic products is greatly reduced, the safety of the product is greatly improved, and sensitive muscles can be used with confidence. In addition, the skin has higher acceptance to natural plant extracts than chemical synthetic products, has good use feeling, and can not generate dependence feeling after long-term use.
By adopting the technical scheme, under the specific proportion of the dendrobium candidum stem extract, the inula flower extract and the ophiopogon root extract, a plurality of macromolecules and small molecules with different sizes act on the skin of a user together, permeate into different cortex layers on the skin layer by layer, and have good permeability and efficacy. Thereby leading various external and supplementary nutrient substances to deeply permeate into the skin layer, nourishing the skin and supplementing various nutrient substances which are missing of the skin, and further repairing the skin barrier. Under the conditions of long-term use and long-term accumulation, ruddy complexion, smooth skin, difficult reddening and relatively firm skin barrier, thereby improving the resistance effect on severe environment.
Treatment for relieving inflammation is also one of the important parts of repair. Under the specific collocation, the inventor finds that the composition acts in essence water and essence milk, has more remarkable treatment effect on inflammation and pain of sensitive muscle users, and further plays a good repairing role.
Preferably, the other plant extracts comprise one or more of radix stephaniae tetrandrae extract, horse chestnut extract and rhizoma smilacis glabrae root extract;
the other flower extracts comprise one or more of flos Rosae Multiflorae extract and flos Chrysanthemi extract;
the additional plant extract comprises one or more of radix et caulis Opuntiae Dillenii extract and oat bran extract.
Preferably, in the component a, the other plant extracts include tetrandra root extract, hippocastanum extract, and glabrous greenbrier rhizome extract, and the mass ratio of the tetrandra root extract, the hippocastanum extract, the glabrous greenbrier rhizome extract, and the glabrous greenbrier rhizome extract to the glabrous greenbrier rhizome extract is 0.33:1:1:1, a step of;
the other flower extracts comprise flos Rosae Multiflorae extract and flos Chrysanthemi extract, wherein the mass ratio of flos Rosae Multiflorae extract to flos Chrysanthemi extract is 1:1:1, a step of;
the additional plant extracts comprise cactus extract and oat bran extract, and the mass ratio of the cactus extract to the oat bran extract to the dwarf lilyturf tuber root extract is 7:3:3.
by adopting the technical scheme, the prepared composition acts in products such as essence water, essence milk, essence cream and the like, strongly resists the release of inflammatory mediators and inhibits the damage of the inflammatory mediators to normal cells; reducing the loss of skin moisture, enhancing the skin barrier function, improving the self-protection capability of the skin and reducing the sensitivity; the method has the advantages of removing excessive free radicals, weakening the damage of the free radicals to the cell membranes of mast cells and basophils, and playing roles in resisting sensitization and relieving itching, thereby playing a good repairing role.
Preferably, the humectant A comprises one or more of 1, 2-hexanediol, ethylhexyl glycerol, glycerol and butanediol.
Preferably, the humectant A in the component A comprises 0.4-0.8% of 1, 2-hexanediol and 0.1-0.4% of ethylhexyl glycerol by weight of the total mass of the component A; the humectant A of the component B comprises 30-45% of glycerin by weight of the total mass of the component B; the humectant A in the component C comprises butanediol accounting for 48-55% of the total mass of the component C.
Preferably, the humectant A in the component A comprises 0.5% of 1, 2-hexanediol and 0.2% of ethylhexyl glycerin by weight of the total mass of the component A; the humectant A of the component B comprises glycerin accounting for 40% of the total mass of the component B; the humectant A in the component C comprises 50% of butanediol by weight of the total mass of the component C.
The oil, sweat and fat discharged from the skin form the sebum membrane of the skin together, improper cleaning and excessive cleaning are main reasons for damaging the sebum membrane, and particularly for dry sensitive muscles, the sebum membrane is more barren, and the sebum membrane needs to be repaired by moisturizing.
One premise here is that the user will use the product containing the composition after cleansing, applying the toner. At this point, the user surface has been replenished with a quantity of extraneous water.
Firstly, under the common cooperation of dendrobium candidum stem extract, inula flower extract and ophiopogon root extract, the original way of forming a film and locking water by macromolecules is widened into a mode of combining small molecules on the original basis for moisture absorption and coexistence, and the sebum membrane repair is assisted from multiple aspects.
On the basis, the dendrobium polysaccharide and the ophiopogon polysaccharide are matched with a specific type of humectant, so that the effect of the dendrobium polysaccharide and the ophiopogon polysaccharide on the skin is further promoted. Specifically, the polar groups of the polysaccharide form hydrogen bonds with water molecules for binding moisture, thereby providing the skin with filling moisture. In addition, dendrobium polysaccharide and ophiopogon polysaccharide can form a uniform film on the surface of the skin more quickly, so that the speed of external supplementing water and the speed of the skin evaporating in the air from water is slowed down. The water is not only locked, but also is supplemented, so that the long-acting water retention is realized, thereby providing good repairing conditions for the sebum membrane, and repairing under mild and proper conditions.
In a second aspect, the present application provides a essence lotion comprising the composition, which adopts the following technical scheme:
the essence water containing the composition is prepared from the following raw materials in percentage by mass: 8-12% of humectant B,0.1-0.5% of preservative, 0.2-0.5% of thickener B,0.1-0.3% of pH regulator, 0.1-0.3% of skin conditioning agent, 9-12% of composition and water to 100%.
Preferably, the humectant B comprises one or more of 1, 3-propylene glycol and betaine.
Preferably, a preparation process of essence water containing the composition comprises the following steps:
step 1): mixing water, humectant B, thickener B, skin conditioner, and 15-25% antiseptic together until uniform, adjusting temperature to 80-90deg.C, and maintaining for 18-30min to obtain water semi-finished product.
Step 2): cooling to 32-42 ℃, then adding the pH regulator, the composition and the rest preservative into the semi-finished product, and uniformly stirring;
step 3): and filtering and discharging after the plates are qualified to obtain a water material body, and filling after aging and inspection of the water material body to obtain a finished product.
By adopting the technical scheme, the composition is prepared by being mixed into essence water, and a specific humectant is selected for auxiliary matching. The specific moisturizer is used as a basis for moisturizing, and the moisturizer penetrates to different cortex parts of the skin along with the composition to fill the skin with moisture. The composition has the effect of effectively locking water when the composition is cooperated with the humectant to supplement water, so that the sebum membrane is repaired.
In a third aspect, the present application provides an essence emulsion comprising the composition, which adopts the following technical scheme:
the essence emulsion containing the composition is prepared from the following raw materials in percentage by mass: 10-13% humectant C,2-6% emollient, 1.0-1.5% thickener C,0-0.6% antioxidant, 0.1-0.5% preservative, 0.1-0.3% skin conditioning agent, 9-12% composition, water make up to 100%.
Preferably, the humectant C comprises one or more of propylene glycol, glycerin, betaine.
Preferably, an essence emulsion comprising the composition comprises the following preparation methods:
step 01): mixing water, humectant C, 45-55% thickener, skin conditioner, and 15-25% antiseptic together until stirring, adjusting temperature to 80-90deg.C, and maintaining for 18-30min to obtain milk semi-finished product;
step 02): regulating temperature to 68-78deg.C, adding emollient, antioxidant and residual thickener into milk semi-finished product, homogenizing for 4-8min;
step 03): continuously adjusting the temperature to 35-45 ℃, adding the composition and the rest preservative, and uniformly mixing;
step 04): and (5) filtering and discharging after the plates are qualified to obtain a milk material body, and filling after aging and inspection of the milk material body to obtain a finished product.
By adopting the technical scheme, the essence emulsion is thicker than the essence water in texture, has good long-acting moisturizing effect, but is easy to generate skin-feel. The composition is applied to the essence milk and is matched with a specific humectant, so that the refreshing feeling of the essence milk is improved. Because the composition has the function of rapid permeation, the essence emulsion permeates into the skin before the skin feel is generated, the skin absorbs rapidly, and then a layer of uniform film water locking is formed. The sense of freshness slows down the condition of stuffy pox, is favorable for repairing sensitive muscles, and improves good use experience.
In summary, the present application has the following beneficial effects:
1. under the specific proportion of dendrobium candidum stem extract, inula flower extract and ophiopogon root extract, various macromolecules and small molecules with different sizes act on the skin of a user together, permeate into different cortex layers on the skin layer by layer, and have good permeability and efficacy. Thereby leading various external and supplementary nutrient substances to deeply permeate into the skin layer, nourishing the skin and supplementing various nutrient substances which are missing of the skin, and further repairing the skin barrier. Under the conditions of long-term use and long-term accumulation, ruddy complexion, smooth skin, difficult reddening and relatively firm skin barrier, thereby improving the resistance effect on severe environment.
2. The prepared composition acts in products such as essence water, essence milk, essence cream and the like, strongly resists the release of inflammatory mediators and inhibits the damage of the inflammatory mediators to normal cells; reducing the loss of skin moisture, enhancing the skin barrier function, improving the self-protection capability of the skin and reducing the sensitivity; the method has the advantages of removing excessive free radicals, weakening the damage of the free radicals to the cell membranes of mast cells and basophils, and playing roles in resisting sensitization and relieving itching, thereby playing a good repairing role.
3. Under the mutual cooperation of the dendrobium candidum stem extract, the inula flower extract and the ophiopogon root extract, the water is locked and supplemented, so that the long-acting water-moist maintenance is realized, good repairing conditions are provided for sebum membranes, and the repairing is carried out under mild and proper conditions.
Detailed Description
The present application is described in further detail below with reference to examples.
The plant extracts used in the following preparation examples are all commercial dry products, and after purchase, floating dust is cleaned by water and dried and then put into use; the other preparation examples, examples and comparative examples all use commercially available raw materials.
Preparation example
Preparation example 1
The repairing composition is prepared from the following raw materials: 5kg of component A,3kg of component B,2kg of component C and 0.5kg of glucan. And (3) putting the component A, the component B, the component C and the glucan into a stirring kettle, and uniformly mixing to obtain the composition.
The component A comprises the following raw materials: dendrobium officinale (Dendrobium officinale) stem extract, taxus cuspidata (Taxus cuspidata) leaf extract, glycyrrhiza glabra (Glycyrrhiza glabra) root extract, other plant extracts, humectant A and water. And uniformly mixing the raw materials to obtain the component A.
The other plant extracts are radix Stephaniae Tetrandrae (STEPHANIATETRANDRA) extract, aesculus hippocastanum (Aesculus hippocastanum) extract, and rhizoma Smilacis Glabrae (Smilax glabra) root extract. The mass ratio of the stephania tetrandra extract, the aesculus hippocastanum extract, the glabrous greenbrier rhizome extract and the glabrous greenbrier rhizome extract is 0.33:1:1:1.
the component B comprises the following raw materials: extract of flos Lonicerae (jasminum unificiense), other flower extract, humectant A, thickener A, antibacterial agent and water. And uniformly mixing the raw materials to obtain the component B.
The other flower extracts are flos Rosae Multiflorae (Rosaceae) flower extract and flos Chrysanthemi (Bellispernins) flower extract. The mass ratio of the flos rosae multiflorae extract to the extract of the flos chrysanthemi in the formula is 1:1:1.
the thickener A is xanthan gum; the antibacterial agent is potassium benzoate and potassium sorbate, and the mass ratio of the potassium benzoate to the potassium sorbate is 1:1.
the component C comprises the following raw materials: radix Ophiopogonis (OPHIOPOGUANGJAPONICUS) root extract, scutellariae radix (Scutellaria baicalensis) root extract, radix Paeoniae (PaeoniaeAALBIFLORA) root extract, additional plant extract, humectant A and water. And uniformly mixing the raw materials to obtain the component C.
The additional plant extract is Opuntia dillenii (Opuntia dillenii) extract and Avena sativa (AVENASATIVA) bran extract. The mass ratio of the cactus extract to the oat bran extract to the dwarf lilyturf tuber root extract is 7:3:3.
the humectant A in the component A is 1, 2-hexanediol and ethylhexyl glycerin, wherein the 1, 2-hexanediol accounts for 0.5% of the total mass percent of the component A, and the ethylhexyl glycerin accounts for 0.2% of the total mass percent of the component A.
The humectant A of the component B comprises glycerin, and the glycerin accounts for 40% of the total mass percent of the component B.
The humectant A in the component C comprises butanediol accounting for 50% of the total mass of the component C.
The glucan is beta-glucan.
Preparation example 2
A repairing composition was different from preparation example 1 in that the amount of component A was 4kg, the amount of component B was 2kg, the amount of component C was 1kg, and the amount of glucan was 0.2kg.
The amounts of the various materials used in component A, B, C vary and are specifically described in tables 1-3.
Preparation example 3
A repairing composition was different from preparation example 1 in that the amount of component A was 6kg, the amount of component B was 4kg, the amount of component C was 3kg, and the amount of glucan was 0.6kg.
The amounts of the various materials used in component A, B, C vary and are specifically described in tables 1-3.
TABLE 1 component A
TABLE 2 composition B
TABLE 3 composition C
Preparation example 4
A repairing composition which is different from that of preparation example 1,
in the component A, other plant extracts are radix stephaniae tetrandrae extract, european horse chestnut extract and glabrous greenbrier rhizome extract, and the mass ratio of the radix stephaniae tetrandrae extract, the European horse chestnut extract, the glabrous greenbrier rhizome extract to the glabrous greenbrier rhizome extract is 1:0.5:0.8:1, a step of; the amount of water used is adjusted accordingly. Namely, the usage amount of the tetrandra root extract is 5.5kg, the usage amount of the aesculus hippocastanum extract is 2.8kg, the usage amount of the glabrous greenbrier rhizome extract is 4.4kg, and the usage amount of the glabrous greenbrier rhizome extract is 5.5kg.
In component B, the other flower extracts are flos Rosae Multiflorae extract and flos Chrysanthemi extract. The mass ratio of the flos rosae multiflorae extract to the extract of the flos chrysanthemi in the formula is 0.5:2:1, a step of; the amount of water used is adjusted accordingly. The usage amount of flos Rosae Multiflorae extract is 0.5kg, the usage amount of flos Chrysanthemi extract is 2kg, and the usage amount of Sufang flower extract is 1kg.
The additional plant extract is cactus extract and oat bran extract. The mass ratio of the cactus extract to the oat bran extract to the dwarf lilyturf tuber root extract is 1:3:1, a step of; the amount of water used is adjusted accordingly. The usage amount of the cactus extract is 3kg, the usage amount of the oat bran extract is 9kg, and the usage amount of the radix ophiopogonis extract is 3kg.
Preparation example 5
A repairing composition is different from preparation 1 in that the other plant extracts in component A are radix Platycodi root extract, the usage amount is 14kg, and the water usage amount is adjusted accordingly. The other flower extracts in component B are calendula extract; the amount of water used is adjusted accordingly. The additional plant extract in component C is herba Portulacae extract; the amount of water used is adjusted accordingly.
The humectant A is glycerin.
Preparation example 6
A repairing composition is different from preparation 1 in that the Dendrobium officinale stem extract in component A is replaced with an extract of Eucalyptus globulus leaf of equal quality.
Preparation example 7
A repairing composition is different from preparation 1 in that the extract of Sufang flower in component A is replaced with an extract of herba Taraxaci of equal quality.
Preparation example 8
A repairing composition is different from preparation 1 in that the extract of Fanghua flower in component A is replaced with an equal quality extract of grape seed.
Preparation example 9
A repairing composition was different from preparation example 1 in that the amount of component A used was 1kg, the amount of component B used was 6kg, and the amount of component C used was 3.5kg.
Examples
Example 1
An essence water containing the composition, humectant B, antiseptic, thickener B, pH regulator, skin conditioner, composition and water.
The humectant B is 1, 3-propylene glycol and betaine, the dosage of 1, 3-propylene glycol is 8kg, and the dosage of betaine is 1.2kg.
The preservative is a substance formed by mixing phenoxyethanol, 1, 2-hexanediol and chlorpheniramine and methylparaben. The amount of phenoxyethanol was 0.21kg, the amount of 1, 2-hexanediol was 0.1kg, and the amount of chlorobenzeneglycolether was 0.09kg. The amount of methylparaben used was 0.1kg.
The thickener B is xanthan gum and carbomer, the using amount of the xanthan gum is 0.2kg, and the using amount of the carbomer is 0.18kg.
The pH regulator is arginine.
The skin conditioner is allantoin.
The composition was prepared according to preparation example 1.
The specific amounts of the remaining materials are shown in Table 4.
The embodiment of the application also discloses a preparation method of the essence water containing the composition, which comprises the following steps:
step 1): clean the emulsifying pot and various using devices.
Step 2): mixing water, humectant B, thickener B, skin conditioner and methylparaben together to uniformity, adjusting temperature to 80deg.C, and maintaining for 20min to obtain water semi-finished product.
Step 3): cooling to 40deg.C, adding pH regulator, composition and rest antiseptic into the semi-finished product, and stirring.
Step 4): filtering and discharging after the plates are qualified to obtain a water material body, aging the water material body for 24 hours, sampling and checking, and performing semi-finished product physicochemical and microorganism detection.
Step 5): and after the detection is qualified, filling, packaging and code spraying are carried out within a week to obtain a finished product.
Example 2
Essence water containing the composition is different from example 1 in the amount of each raw material, and the composition is prepared in example 2, specifically shown in table 4.
A preparation method of essence water containing the composition is different from that of example 1,
and 2) adjusting the temperature to 90 ℃ in the step 2), and preserving the heat for 18min.
The temperature in step 3) was adjusted to 42 ℃.
Example 3
Essence water containing the composition is different from example 1 in the amount of each raw material, and the composition is prepared in example 3, specifically shown in table 4.
A preparation method of essence water containing the composition is different from that of example 1,
and 2) adjusting the temperature to 80 ℃ in the step 2), and preserving the heat for 30min.
The temperature in step 3) was adjusted to 32 ℃.
TABLE 4 Table 4
Example 4
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 4.
Example 5
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 5.
Example 6
An essence emulsion containing the composition comprises the following raw materials: moisturizer C, emollient, thickener C, antioxidant, preservative, skin conditioner, composition, and water.
The humectant C is propylene glycol, glycerol, and betaine. The amount of propylene glycol was 5kg, the amount of glycerin was 5kg, and the amount of betaine was 1.2kg.
The emollient is cyclohexane siloxane, cyclopenta-dimethyl siloxane, polydimethylsiloxane, caprylic capric triglyceride. The amount of cyclohexasiloxane used was 0.66kg, the amount of cyclopentadimethicone used was 1.34kg, the amount of dimethicone used was 1kg, and the amount of caprylic/capric triglyceride used was 1kg.
The thickener C is a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, water and sorbitan oleate and an ammonium acryloyldimethyl taurate/VP copolymer. The amount of sodium acrylate/sodium acryloyldimethyl taurate copolymer used was 0.225kg, the amount of isohexadecane used was 0.135kg, the amount of polysorbate-80 used was 0.045kg, the amount of water used was 0.18kg, the amount of sorbitan oleate used was 0.015kg, and the amount of ammonium acryloyldimethyl taurate/VP copolymer used was 0.6kg.
The antioxidant is tocopheryl acetate.
The preservative is a substance formed by mixing phenoxyethanol, 1, 2-hexanediol and chlorpheniramine and methylparaben. The amount of phenoxyethanol was 0.21kg, the amount of 1, 2-hexanediol was 0.1kg, and the amount of chlorobenzeneglycolether was 0.09kg. The amount of methylparaben used was 0.1kg.
The skin conditioner is allantoin.
The composition was prepared according to preparation example 1.
The specific amounts of the remaining materials are shown in Table 5.
The application also discloses a preparation method of the essence emulsion containing the composition, which comprises the following steps:
step 01): clean the emulsifying pot and various using devices.
Step 02): mixing water, humectant C, ammonium acryloyldimethyl taurate/VP copolymer, skin conditioner and methylparaben together, stirring, adjusting temperature to 80deg.C, and maintaining for 20min to obtain milk semi-product.
Step 03): regulating the temperature to 75deg.C, adding emollient, antioxidant and residual thickener into the semi-finished product, and homogenizing for 5min.
Step 04): continuously adjusting the temperature to 40 ℃, adding the composition and the rest preservative, and uniformly mixing.
Step 05): and (5) filtering and discharging after the plates are qualified to obtain a milk material body, aging the milk material body for 24 hours, and sampling and inspecting the milk material body to perform semi-finished product physicochemical and microorganism detection.
Step 06): and after the detection is qualified, filling, packaging and code spraying are carried out within a week to obtain a finished product.
Example 7
An essential emulsion comprising the composition is different from example 6 in the amount of each raw material, and is specifically shown in table 5.
The composition was prepared according to preparation 2.
Example 8
An essential emulsion comprising the composition is different from example 6 in the amount of each raw material, and is specifically shown in table 5.
The composition was prepared according to preparation 3.
TABLE 5
Comparative example
Comparative example 1
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 6.
Comparative example 2
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 7.
Comparative example 3
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 8.
Comparative example 4
Essence water containing the composition was different from example 1 in that the composition was prepared in preparation example 9.
Performance test
1. Skin moisture content detection: 24 slightly sensitive muscle volunteers aged 25-35 were selected, two volunteers in one group, one group of volunteers using one of the products of examples 1-8, comparative examples 1-4. During the test period, the volunteers use the corresponding products once after basic face cleansing and skin toner every morning and evening, and other skin care products and cosmetics are not used additionally. Skin moisture content was measured with a skin moisture content tester before use, after 1h of first use, after 8 weeks of use.
2. Osmotic effect: 10 pieces of cosmetic cotton are prepared, and the cosmetic cotton is piled up in a stack. Taking 2ml of the samples of examples 1-5 and comparative examples 1-4, dripping the samples onto the surface of the cosmetic cotton from top to bottom, and recording the time required for no flowing liquid to drip onto the surface of the first cosmetic cotton sheet by naked eyes; then, the number of pieces of cosmetic cotton penetrating from top to bottom was examined.
3. Appearance and sense of use of sensitive muscles: the first volunteer examined was observed for facial condition after 8 weeks of use and recorded for erythema, redness, rash, etc. Meanwhile, the volunteer is asked to feel in use, and the conditions of absorption speed, moisture retention, moistening degree and the like are recorded.
The above test data are shown in Table 6.
TABLE 6-1
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TABLE 6-2
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As can be seen from the test data of examples 1-8 in Table 6, after the products of examples 1-8 are applied to the faces of volunteers, the moisture of the faces is greatly improved when the products are used for 1h, which indicates that the products of the application have good moisturizing effect. After the face mask is continuously used for 8 weeks, the water content of the face is greatly improved compared with that before the face mask is used, so that the face mask has good water locking effect and skin moisture improving effect, and a good environment is provided for repairing the sebum membrane. The excellent effect of the products of examples 1-8 on skin repair was further verified by combining the appearance and the use feeling detection data, the volunteers had good use experience, and the sensitive muscles of the volunteers were also relieved and presented with a healthy state.
The method has the advantages that under the specific proportion of the dendrobium candidum stem extract, the inula flower extract and the ophiopogon root extract, a macromolecular film forming and water locking mode and a small molecular moisture absorption co-existence moisturizing mode are achieved, so that the skin is kept long-acting moist, and the sebum membrane is repaired under proper conditions.
From the examination data of the permeation effects of examples 1 to 5 in Table 6-1, it can be seen that the essence water of examples 1 to 5 has a rapid permeation rate and also has a good permeation effect. The method shows that under the specific proportion of the dendrobium candidum stem extract, the inula flower extract and the ophiopogon root extract, the permeation is facilitated by the combination of various molecules, so that nutrients are supplemented into different cortex to nourish the skin, and the skin can be repaired.
As can be seen from comparison of the test data of examples 1-3 and examples 4-5 in Table 6, further limiting the amount of component A, B, C and the choice of materials is advantageous in improving the product effect to some extent.
As can be seen from comparison of the test data of example 1 with comparative examples 1-3 in Table 6, the water content of the face was less elevated after 1h and 8 weeks after use of the products of comparative examples 1-3, to a degree far less than that of the volunteer from example 1. The method shows that the prepared composition can play a good repairing effect only by being applied to skin care products under the common coordination of dendrobium candidum stem extract, inula flower extract and ophiopogon root extract. And by combining the detection data of the comparative example 4, it can be seen that the three components are matched under the specific use amount, and the ideal effect can be achieved.
The present embodiment is merely illustrative of the present application and is not intended to be limiting, and those skilled in the art, after having read the present specification, may make modifications to the present embodiment without creative contribution as required, but is protected by patent laws within the scope of the claims of the present application.

Claims (6)

1. The repairing composition is characterized by being prepared from the following raw materials in parts by weight: 4-6 parts of component A,2-4 parts of component B,1-3 parts of component C and 0.2-0.6 part of glucan;
the component A is prepared from the following raw materials in percentage by mass: 1.5 to 2.5 percent of dendrobium candidum stem extract, 4.8 to 6.0 percent of taxus cuspidata leaf extract, 4.5 to 5.8 percent of licorice root extract, 10 to 14 percent of other plant extract, 0.5 to 1.2 percent of humectant A and water which are supplemented to 100 percent;
the component B is prepared from the following raw materials in percentage by mass: 0.8-1.5% of extract of Fanghua flowers, 1.5-3.0% of other flower extracts, 30-45% of humectant A,0.12-0.35% of thickener A,0.35-0.5% of antibacterial agent and water to 100%;
the component C is prepared from the following raw materials in percentage by mass: 2.5-3.5% of radix ophiopogonis extract, 0.8-1.5% of radix scutellariae extract, 1.2-2.2% of radix paeoniae extract, 8-12% of additional plant extract, 48-55% of humectant A and water to be supplemented to 100%;
in the component A, other plant extracts comprise tetrandra root extract, horse chestnut extract and glabrous greenbrier rhizome extract, and the mass ratio of the tetrandra root extract, the horse chestnut extract, the glabrous greenbrier rhizome extract and the glabrous greenbrier rhizome extract is 0.33:1:1:1, a step of;
the other flower extracts comprise flos Rosae Multiflorae extract and flos Chrysanthemi extract, and the mass ratio of flos Rosae Multiflorae extract to flos Chrysanthemi extract is 1:1:1, a step of;
the additional plant extracts comprise cactus extract and oat bran extract, and the mass ratio of the cactus extract to the oat bran extract to the dwarf lilyturf tuber root extract is 7:3:3, a step of;
the humectant A comprises one or more of 1, 2-hexanediol, ethylhexyl glycerol, glycerol and butanediol.
2. A repair composition according to claim 1, characterized in that: the humectant A in the component A comprises 0.5% of 1, 2-hexanediol and 0.2% of ethylhexyl glycerin by weight percentage of the total mass of the component A; the humectant A of the component B comprises glycerin accounting for 40% of the total mass of the component B; the humectant A in the component C comprises 50% of butanediol by weight of the total mass of the component C.
3. A essence containing the repairing composition as claimed in any one of claims 1 to 2, characterized by being prepared from the following raw materials in mass percent: 8-12% of humectant B,0.1-0.5% of preservative, 0.2-0.5% of thickener B,0.1-0.3% of pH regulator, 0.1-0.3% of skin conditioning agent, 9-12% of repairing composition and water to 100%; a repair composition employing the repair composition of any one of claims 1-2.
4. The essence of water according to claim 3, characterized in that: the humectant B comprises one or more of 1, 3-propylene glycol and betaine.
5. An essential emulsion comprising the repairing composition according to any one of claims 1 to 2, characterized by being prepared from the following raw materials in percentage by mass: 10-13% of humectant C,2-6% of emollient, 1.0-1.5% of thickener C,0-0.6% of antioxidant, 0.1-0.5% of preservative, 0.1-0.3% of skin conditioning agent, 9-12% of repairing composition and water to 100%; a composition employing a composition according to any one of claims 1-2.
6. The cream as claimed in claim 5, wherein: the humectant C comprises one or more of propylene glycol, glycerol and betaine.
CN202210841427.9A 2022-07-18 2022-07-18 Repairing composition and essence lotion and essence emulsion containing same Active CN114983909B (en)

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CN115581653B (en) * 2022-09-30 2023-08-04 广州市博之越精细化工有限公司 Shumin repair agent and application thereof
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CN111110617A (en) * 2020-01-19 2020-05-08 朱志辉 Skin care product prepared from Chinese medicinal extract and its preparation method
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