CN110840789B - Color-changing lipstick containing plant pigment and preparation method thereof - Google Patents
Color-changing lipstick containing plant pigment and preparation method thereof Download PDFInfo
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- CN110840789B CN110840789B CN201911204738.9A CN201911204738A CN110840789B CN 110840789 B CN110840789 B CN 110840789B CN 201911204738 A CN201911204738 A CN 201911204738A CN 110840789 B CN110840789 B CN 110840789B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention provides a color-changing lipstick containing plant pigment and a preparation method thereof. The color-changing lipstick comprises the following raw materials in parts by weight: 15-30 parts of natural wax, 60-90 parts of natural vegetable oil, 0.05-5 parts of vegetable pigment, 0.05-5 parts of antioxidant and 0.05-5 parts of color-changing powder; the plant pigment comprises one or more of radix Ipomoeae extract, radix Betae extract, radix Raphani extract, Bolete Spirulina extract, and Curcuma rhizome extract. The color-changing lipstick containing the plant pigment has the synergistic effect due to the mutual matching of the components, and can achieve the effects of moistening and beautifying lips, keeping moisture, preventing the lips from being cracked and skinned, reducing fine wrinkles and dry wrinkles of the lips, and enabling the lips to be glossy and colored.
Description
Technical Field
The invention belongs to the field of cosmetics, relates to a color-changing lipstick and a preparation method thereof, and particularly relates to a color-changing lipstick containing plant pigments and a preparation method thereof.
Background
Lipstick is one kind of lipstick, and can moisten and color lips and correct lip contour. Women are the leading forces of the lipstick consumer market. Researches show that the market is good at applying the color rule and caters to the pursuit of beauty of women, thereby increasing the sales volume of lipstick. However, most of lipsticks in the market are coated on lips to display the same color as the apparent color of the lipsticks, and the coating color of products with unique apparent colors such as cyan, yellow, blue and the like is not the color which is loved by consumers. According to different people and different preferences on the appearance color of the product, the lipstick with different appearance colors is selected and smeared to form moist and colored lipstick, so that the pursuit of the unique beauty of the women can be better shown.
On the other hand, the lipstick in the market at present mainly comprises mineral oil, chemical synthetic oil, surfactant, various synthetic waxes, lakes, essence and the like, and generally contains a large amount of synthetic pigments to color lipstick products. The lipstick is daily used by women, after the lipstick is coated, a large amount of paste containing toner remains on lips, the paste is inevitably mistakenly eaten to be inedible toner when the lips are closed or eaten, heavy metals, polycyclic aromatic hydrocarbons, mineral oil, preservatives and the like possibly exist in the product, and certain potential safety hazards exist after the product is mistakenly eaten for a long time. Most of the natural lip products in the market are lip balms, so that the coloring capability is poor, and the requirement of showing the makeup of women cannot be met.
CN107753321A discloses a color-changing lipstick which comprises the following components in parts by weight: 40-50 parts of isooctyl palmitate, 20-30 parts of cosmetic white oil, 20-30 parts of isooctyl isostearyl alcohol, 1-3 parts of dibutyl ethyl hexanoyl glutamine, 1-3 parts of hydroxystearic acid, 0.5-1 part of dibutyl lauroyl glutamine, 0.5-1 part of phenoxyethanol and natural pigment. The lipstick contains a large amount of mineral oil and chemical synthetic oil, after the lipstick is smeared, a large amount of paste is remained on lips, certain potential safety hazards exist after long-term eating by mistake, and the effects of moisturizing the lips and improving lip lines are poor.
CN109077963A discloses a rose flower fragrance type color-changing lipstick. The rose-fragrance-containing color-changing lipstick disclosed by the invention adopts natural beeswax as a substrate, and is prepared by adding shea butter, olive extract, carnauba wax, corn oil, castor bean oil, European sweet cherry fruit extract and eosin pigment. The color-changing lipstick can enable lips to be ruddy and glossy to a certain degree, but wax is single, the moistening degree and the toughness of the lipstick are poor, and when the non-plant pigment eosin acid pigment is added, the content of color components such as coloring agent is too high, so that the color-changing lipstick has slight irritation on the lips, and the problems of cracking and peeling of the lips cannot be well solved.
Therefore, the color-changing lipstick which can fade lip wrinkles, nourish lips, has saturated color and long-term and lasting effect and can protect female lip health has important significance.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a color-changing lipstick and a preparation method thereof, in particular to a color-changing lipstick containing plant pigments and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the invention provides a color-changing lipstick containing plant pigments, which comprises the following raw materials in parts by weight: 15-30 parts of natural wax, 60-90 parts of natural vegetable oil, 0.05-5 parts of vegetable pigment, 0.05-5 parts of antioxidant and 0.05-5 parts of color-changing powder;
the plant pigment comprises one or more of radix Ipomoeae extract, radix Betae extract, radix Raphani extract, Bolete Spirulina extract, and Curcuma rhizome extract.
In the present invention, the natural wax is 15 to 30 parts, and may be, for example, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts, 30 parts.
In the present invention, the natural vegetable oil or fat may be 60 to 90 parts, for example, 60 parts, 61 parts, 62 parts, 63 parts, 64 parts, 65 parts, 66 parts, 67 parts, 68 parts, 69 parts, 70 parts, 71 parts, 72 parts, 73 parts, 74 parts, 75 parts, 76 parts, 77 parts, 78 parts, 79 parts, 80 parts, 81 parts, 82 parts, 83 parts, 84 parts, 85 parts, 86 parts, 87 parts, 88 parts, 89 parts, 90 parts.
In the present invention, the plant pigment is 0.05 to 5 parts, and may be, for example, 0.05 part, 0.06 part, 0.07 part, 0.08 part, 0.09 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part, 1.2 part, 1.4 part, 1.6 part, 1.8 part, 2 parts, 2.2 parts, 2.4 parts, 2.6 parts, 2.8 parts, 3 parts, 3.2 parts, 3.4 parts, 3.6 parts, 3.8 parts, 4 parts, 4.2 parts, 4.4 parts, 4.6 parts, 4.8 parts, 5 parts.
In the present invention, the antioxidant is 0.05 to 5 parts, and may be, for example, 0.05 parts, 0.06 parts, 0.07 parts, 0.08 parts, 0.09 parts, 0.1 parts, 0.2 parts, 0.3 parts, 0.4 parts, 0.5 parts, 0.6 parts, 0.7 parts, 0.8 parts, 0.9 parts, 1 part, 1.2 parts, 1.4 parts, 1.6 parts, 1.8 parts, 2 parts, 2.2 parts, 2.4 parts, 2.6 parts, 2.8 parts, 3 parts, 3.2 parts, 3.4 parts, 3.6 parts, 3.8 parts, 4 parts, 4.2 parts, 4.4 parts, 4.6 parts, 4.8 parts, 5 parts.
In the present invention, the color-changing powder is 0.05 to 5 parts, and may be, for example, 0.05 part, 0.06 part, 0.07 part, 0.08 part, 0.09 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part, 1.2 part, 1.4 part, 1.6 part, 1.8 part, 2 parts, 2.2 parts, 2.4 parts, 2.6 parts, 2.8 parts, 3 parts, 3.2 parts, 3.4 parts, 3.6 parts, 3.8 parts, 4 parts, 4.2 parts, 4.4 parts, 4.6 parts, 4.8 parts, 5 parts.
In the lipstick, the wax is natural wax, and the main raw materials are all pure natural plant components, so that the lipstick is nontoxic, free of heavy metal elements and safe and healthy in components.
In the invention, the oil is natural vegetable oil, contains abundant monounsaturated fatty acid (oleic acid), polyunsaturated fatty acid (linoleic acid and linolenic acid), multiple vitamins, minerals and antioxidants, and can form a hydrophobic film on the surface of lip skin to moisten and smooth the skin, inhibit the evaporation of skin moisture and promote the absorption of effective components.
The plant pigment is sweet potato root extract, beet root extract, radish root extract, Bonnate spirulina extract or turmeric root extract. The plant pigments belong to natural pigments, have no toxic or side effect and high safety, and can respectively play roles of enhancing the immune function of a human body, resisting oxidation and preserving moisture.
The sweet potato root extract can enhance the activity of superoxide dismutase and catalase, enhance the oxidation resistance of lip skin, improve the activity of superoxide dismutase (SOD) so as to reduce the formation of free radicals, clear DPPH free radicals, superoxide free radicals and hydroxyl free radicals, reduce the damage of the free radicals to the skin and effectively delay the aging of the skin.
The beetroot extract, natural hygroscopic factor, strong hygroscopicity, can provide a large amount of moisture for skin, is very important for protein formation, DNA repair, and enzyme activity, and can be combined with other components to relieve skin allergy, so that the beetroot extract is an ideal sedative humectant. Can balance cell osmotic pressure, and can help cells to restore to balance and moisture state when skin encounters adverse environment, cell osmotic pressure is unbalanced, and cells lose water.
The radish root extract is a pure natural product extracted from the root of radish, contains protein, saccharide, a large amount of vitamin C and iron calcium, can be used as an astringent and a skin conditioner, and can accelerate skin metabolism, balance oil and smooth lip wrinkles.
The Bonnate spirulina extract comprises vegetable protein, various vitamins and minerals such as essential fatty acid, phytochrome, SOD and the like, can moisten the lip skin, enables the lip skin to be rich in elasticity, moisturizes, is soft, smooth and tender, and provides nutrient components for the lip skin. In addition, the facial mask also has the effects of promoting the synthesis of collagen and elastin, increasing the elasticity and the tightness of lip skin, and moisturizing and conditioning the lip skin.
The turmeric root extract and turmeric have strong antioxidant function, can eliminate free radicals, has the oxidation valence of 1.6 times of VE and 2.33 times of flavonoids of 2.75 times of VC, can capture free radicals, and has the function of resisting aging in one day. Turmeric also has the effects of enhancing body defense function, resisting inflammation, and neutralizing toxins entering lips.
The color change is caused because the pH value is changed due to the body temperature, and the color change powder plays a role of an acid-base indicator in the lipstick, so that the color is changed; the color produced by different pH values is different, the pH value of saliva of each person is different, and the pH value of lips is different, so that the color of the color-changing lipstick coated on each person is different.
Preferably, the color-changing lipstick comprises the following raw materials in parts by weight: 20-30 parts of natural wax, 65-80 parts of natural vegetable oil, 0.1-3 parts of vegetable pigment, 0.15-5 parts of antioxidant and 0.2-3 parts of color-changing powder.
Preferably, the color-changing lipstick comprises the following components in parts by weight: 22-28 parts of natural wax, 68-78 parts of natural vegetable oil, 0.1-2.5 parts of vegetable pigment, 0.15-3 parts of antioxidant and 0.2-2.5 parts of color-changing powder.
Preferably, the natural wax comprises any one of beeswax, candelilla wax or carnauba wax or a combination of at least two of these.
Preferably, the natural wax is a combination of at least two of beeswax, candelilla wax or carnauba wax.
As a preferred technical scheme of the invention, the natural wax is a combination of beeswax, candelilla wax and carnauba wax. The beeswax can improve the hardness of lipstick, in addition, the most obvious effect of the beeswax is antibiosis and antiphlogosis, the antibacterial components rich in the beeswax have inhibition and killing effects on various pathogenic bacteria, the multiple oxidation-resistant components contained in the beeswax can effectively eliminate redundant free radicals in the body, meanwhile, the components such as vitamins, aromatic substances and the like contained in the beeswax can keep the skin soft and moist, and in addition, the antibacterial components contained in the beeswax can inhibit and kill bacteria on the surface of the skin and can promote the regeneration of skin cells. The candelilla wax can improve the overall quality of ductility, pigment dispersibility, falling resistance and the like. Meanwhile, the lipstick is natural in luster and very soft in lip feeling. The carnauba wax is very hard in texture, has extremely high gloss, is extremely easy to emulsify, has good oil retention, and has the greatest advantage of having extremely high brightness and extraordinary hardness which are not possessed by other waxes. The three natural waxes are mutually matched, have a synergistic effect, not only enable the lipstick to have good moistening degree so as to improve lip lines, have good lip protecting effect, but also ensure the toughness of the lipstick, the lipstick cannot break when the lipstick falls off straightly at a height of about two meters, reduce the transportation loss and can be completely used by consumers when the lipstick is used.
Preferably, the natural vegetable oil comprises any one of shea butter, castor oil, squalane, jojoba oil, meadowfoam seed oil or olive oil or a combination of at least two of them.
Preferably, the natural vegetable oil is a combination of shea butter, castor oil, squalane, jojoba oil, meadowfoam seed oil and olive oil.
In a preferred embodiment of the present invention, the natural vegetable oil or fat is a combination of the above six vegetable oils or fats, and has a synergistic effect, and the natural vegetable oil or fat imparts an optimum viscosity to lipstick and enhances the coloring property to lips. In addition, the anti-chapping effect of the lip skin can be enhanced, the anti-chapping cream is non-toxic, has good moisturizing and moistening effects on the lip skin, and can lighten lip wrinkles and nourish lips. Has good effects of moisturizing, moistening, resisting oxidation, delaying aging, etc., and highlights the anti-chapping effect of lipstick, so that the lip skin is moist, smooth, ruddy and healthy.
Preferably, the plant pigment is a combination of at least two of sweet potato root extract, beet root extract, radish root extract, bonatespirulina extract or turmeric root extract.
As the preferable technical scheme of the invention, the plant pigment is the mutual matching of the two pigments, and the synergistic effect is realized, so that the color degree of the lipstick is fuller, and the color effect is further improved. The lip gloss cleanser can further moisten and beautify lips, prevent the lips from being dry cracked and skinned, reduce fine wrinkles and dry wrinkles of the lips and enable the lips to be glossy.
Preferably, the antioxidant comprises any one of pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate), butylated hydroxytoluene or tocopherol or a combination of at least two of them.
Preferably, the variable color powder comprises any one of CI 45380, CI 45410 or CI 45370, or a combination of at least two thereof.
Preferably, the color-changing lipstick further comprises edible essence;
preferably, the edible essence is 0.05-0.1 part by weight of the color-changing lipstick.
In the invention, the edible essence is 0.05-0.1 part by weight, such as 0.05 part, 0.06 part, 0.07 part, 0.08 part, 0.09 part and 0.1 part.
Preferably, the color-changing lipstick comprises the following raw materials in parts by weight: 10-15 parts of beeswax, 2-5 parts of candelilla wax, 5-10 parts of carnauba wax, 20-25 parts of shea butter, 15-20 parts of castor oil, 10-18 parts of white chinlon oil, 2-5 parts of squalane, 3-6 parts of olive oil, 10-15 parts of jojoba seed oil, 0.05-5 parts of plant pigment, 0.05-5 parts of antioxidant and 0.05-5 parts of color-changing powder.
In a second aspect, the present invention provides a preparation method of the color-changing lipstick containing plant pigments, specifically comprising the following steps:
(1) mixing and grinding the plant pigment and part of natural plant oil to obtain plant pigment color paste; mixing the color-changing powder with part of natural vegetable oil, and homogenizing and dispersing to obtain color-changing color paste;
(2) and (2) mixing and stirring the natural wax and the residual natural vegetable oil for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time, and filling and molding to obtain the color-changing lipstick containing the plant pigment.
The preparation method of the invention is that the plant pigment and the color-changing powder are respectively mixed with part of the natural plant oil and fat and then mixed with the natural wax, the residual natural plant oil and fat and the antioxidant, so that the natural wax can be colored more quickly in the later period, and the natural wax is completely mixed with other components, thereby the color of the lipstick is more uniform without generating variegated color.
Preferably, the mass of the natural vegetable oil and fat mixed with the vegetable pigment in the step (1) is 5 to 15% of the total mass of the natural vegetable oil and fat, and may be, for example, 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%, 13%, 14%, 15%.
Preferably, the temperature for mixing the plant pigment and the partial natural vegetable oil and fat in the step (1) is 20-40 deg.C, such as 20 deg.C, 22 deg.C, 24 deg.C, 26 deg.C, 28 deg.C, 30 deg.C, 32 deg.C, 34 deg.C, 36 deg.C, 38 deg.C, and 40 deg.C.
Preferably, the mixing time of the plant pigment and the part of the natural plant oil in the step (1) is 5-10min, such as 5min, 6min, 7min, 8min, 9min, and 10 min.
Preferably, the rotation speed for grinding the plant pigment and the part of the natural plant oil in the step (1) is 400-600r/min, such as 400r/min, 450r/min, 500r/min, 550r/min and 600 r/min.
Preferably, the time for grinding the plant pigment and part of the natural plant oil in the step (1) is 10-20min, such as 10min, 12min, 14min, 16min, 18min, 20 min.
Preferably, the mass of the natural vegetable oil and fat mixed with the color-changing powder in the step (1) is 5 to 15% of the total mass of the natural vegetable oil and fat, and may be, for example, 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%, 13%, 14%, 15%.
Preferably, the temperature for mixing the discoloring powder and part of the natural vegetable oil and fat in step (1) is 20-40 deg.C, such as 20 deg.C, 22 deg.C, 24 deg.C, 26 deg.C, 28 deg.C, 30 deg.C, 32 deg.C, 34 deg.C, 36 deg.C, 38 deg.C, 40 deg.C.
Preferably, the time for mixing the discoloring powder and part of the natural vegetable oil and fat in the step (1) is 5-10min, such as 5min, 6min, 7min, 8min, 9min, 10 min.
Preferably, the rotation speed for homogeneously dispersing the discolouring powder and part of the natural vegetable oil and fat in the step (1) is 600-800r/min, such as 600r/min, 650r/min, 700r/min, 750r/min and 800 r/min.
Preferably, the time for homogenizing and dispersing the discoloring powder and part of the natural vegetable oil and fat in the step (1) is 20-30min, such as 20min, 22min, 24min, 26min, 28min and 30 min.
Preferably, the temperature for homogeneously dispersing the toner and part of the natural vegetable oil and fat in step (1) is 60-80 deg.C, such as 60 deg.C, 62 deg.C, 64 deg.C, 66 deg.C, 68 deg.C, 70 deg.C, 72 deg.C, 74 deg.C, 76 deg.C, 78 deg.C, 80 deg.C.
Preferably, the temperature of the primary mixing and stirring in the step (2) is 85 to 90 ℃, for example, 85 ℃, 86 ℃, 87 ℃, 88 ℃, 89 ℃, 90 ℃.
Preferably, the temperature of the secondary mixing and stirring in step (2) is 80-85 deg.C, such as 81 deg.C, 82 deg.C, 83 deg.C, 84 deg.C, 85 deg.C.
Preferably, the filling and forming in the step (2) is specifically: heating and melting the semi-finished lipstick body obtained after the secondary mixing and stirring, injecting into a mould, cooling and demoulding;
preferably, the melting temperature is 75-80 ℃, for example, 75 ℃, 76 ℃, 77 ℃, 78 ℃, 79 ℃, 80 ℃.
Preferably, the cooling temperature is 10-20 ℃, for example, 10 ℃, 12 ℃, 14 ℃, 16 ℃, 18 ℃, 20 ℃.
Preferably, the preparation method of the color-changing lipstick containing plant pigments specifically comprises the following steps:
(1) mixing the plant pigment and part of natural plant oil according to the formula amount at 20-40 ℃ for 5-10min, and then grinding in a high-speed grinder at the rotating speed of 400-600r/min for 10-20min to obtain plant pigment color paste; mixing the color-changing powder and part of the natural vegetable oil for 5-10min at 20-40 ℃, and then homogenizing and dispersing for 20-30min in a high-speed homogenizer at the speed of 600-800r/min to obtain color-changing color paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 85-90 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 80-85 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 10-20 ℃, and demolding to obtain the color-changing lipstick containing the plant pigment.
Compared with the prior art, the invention has the following beneficial effects:
(1) the color-changing lipstick containing the plant pigment is composed of natural wax, natural vegetable oil, the plant pigment, an antioxidant and color-changing powder, and the components are matched with each other, so that the color-changing lipstick has a synergistic effect, can moisten and beautify lips, moisturize and prevent the lips from cracking and peeling, and reduce fine wrinkles and dry wrinkles of the lips.
(2) The color-changing lipstick containing the plant pigment can immediately sense the pH value of the lips or saliva and gradually change different effects suitable for users, the natural effect is adjusted according to each user, so the color-changing lipstick is suitable for people with any lip color, the lips can be enabled to look fresh, full and shiny, and the contained natural plant ruddy components can play a role in improving the lip color after long-term use.
Detailed Description
The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
Example 1
The embodiment provides a color-changing lipstick containing plant pigments, which comprises the following components in parts by weight:
the preparation method of the color-changing lipstick containing the plant pigment comprises the following steps:
(1) mixing the plant pigment and 9 parts of castor oil according to the formula amount at 40 ℃ for 10min, and grinding in a high-speed grinder at the rotating speed of 600r/min for 10min to obtain plant pigment color paste; mixing the color-changing powder and 9 parts of castor oil at 40 ℃ for 10min, and then homogenizing and dispersing for 20min at 600r/min in a high-speed homogenizer to obtain color-changing paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 90 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 85 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 20 ℃ and demolding to obtain the color-changing lipstick containing the plant pigment.
Example 2
The embodiment provides a color-changing lipstick containing plant pigments, which comprises the following components in parts by weight:
the preparation method of the color-changing lipstick containing the plant pigment comprises the following steps:
(1) mixing the plant pigment and 8 parts of castor oil according to the formula amount at 40 ℃ for 10min, and grinding in a high-speed grinder at the rotating speed of 500r/min for 10min to obtain plant pigment color paste; mixing the color-changing powder and 8 parts of castor oil at 40 ℃ for 10min, and then homogenizing and dispersing for 20min at 600r/min in a high-speed homogenizer to obtain color-changing paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 85 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 80 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 20 ℃, and demolding to obtain the color-changing lipstick containing the plant pigment.
Example 3
The embodiment provides a color-changing lipstick containing plant pigments, which comprises the following components in parts by weight:
the preparation method of the color-changing lipstick containing the plant pigment comprises the following steps:
(1) mixing the plant pigment and 8 parts of castor oil according to the formula amount at 40 ℃ for 10min, and grinding in a high-speed grinder at the rotating speed of 500r/min for 10min to obtain plant pigment color paste; mixing the color-changing powder and 8 parts of castor oil at 40 ℃ for 10min, and then homogenizing and dispersing for 20min at 600r/min in a high-speed homogenizer to obtain color-changing paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 85 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 80 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 20 ℃, and demolding to obtain the color-changing lipstick containing the plant pigment.
Example 4
The embodiment provides a color-changing lipstick containing plant pigments, which comprises the following components in parts by weight:
the preparation method of the color-changing lipstick containing the plant pigment comprises the following steps:
(1) mixing the plant pigment and 7.5 parts of castor oil according to the formula amount at 30 ℃ for 10min, and grinding in a high-speed grinder at the rotating speed of 500r/min for 10min to obtain plant pigment color paste; mixing the color-changing powder and 7.5 parts of castor oil at 40 ℃ for 10min, and then homogenizing and dispersing for 20min in a high-speed homogenizer at 600r/min to obtain color-changing color paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 85 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 80 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 20 ℃, and demolding to obtain the color-changing lipstick containing the plant pigment.
Example 5
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural wax does not contain carnauba wax, the beeswax is 18 parts, and the candelilla wax is 7.5 parts; the contents of other components and the preparation method are the same as example 1.
Example 6
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural wax does not contain candelilla wax, the beeswax is 17.25 parts, and the carnauba wax is 6.75 parts; the contents of other components and the preparation method are the same as example 1.
Example 7
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural wax does not contain beeswax, the candelilla wax is 12 parts, and the carnauba wax is 13.5 parts; the contents of other components and the preparation method are the same as example 1.
Example 8
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain shea butter, and 22.2 parts of castor oil, 6.2 parts of vegetable squalane, 16.2 parts of jojoba oil, 19.434 parts of chinaroot greenbrier seed oil and 8.2 parts of olive oil; the contents of other components and the preparation method are the same as example 1.
Example 9
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain castor oil, and the natural vegetable oil contains 24.6 parts of shea butter, 5.6 parts of vegetable squalane, 15.6 parts of jojoba oil, 18.834 parts of chinaroot greenbrier seed oil and 7.6 parts of olive oil; the contents of other components and the preparation method are the same as example 1.
Example 10
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain plant squalane, and 21.4 parts of shea butter, 18.4 parts of castor oil, 12.4 parts of jojoba oil, 15.634 parts of meadowfoam seed oil and 4.4 parts of olive oil; the contents of other components and the preparation method are the same as example 1.
Example 11
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain jojoba oil, and 23.4 parts of shea butter, 20.4 parts of castor oil, 4.4 parts of plant squalane, 17.634 parts of chinlon oil and 6.4 parts of olive oil; the contents of other components and the preparation method are the same as example 1.
Example 12
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain meadowfoam seed oil, and the natural vegetable oil contains 24 parts of shea butter, 21 parts of castor oil, 5 parts of plant squalane, 15 parts of jojoba oil and 7 parts of olive oil; the contents of other components and the preparation method are the same as example 1.
Example 13
This example provides a color-changing lipstick containing plant pigments, which is different from example 1 in that: the natural vegetable oil does not contain olive oil, and 21.8 parts of shea butter, 18.8 parts of castor oil, 2.8 parts of plant squalane, 12.8 parts of jojoba oil and 16.034 parts of meadowfoam seed oil; the contents of other components and the preparation method are the same as example 1.
Comparative example 1
This comparative example provides a lipstick, differing from example 1 in that: the color-changing lipstick does not contain plant pigment; the contents of other components and the preparation method are the same as example 1.
Comparative example 2
This comparative example provides a lipstick, differing from example 1 in that: the color-changing lipstick does not contain a color-changing powder; the contents of other components and the preparation method are the same as example 1.
Comparative example 3
This comparative example provides a lipstick, differing from example 1 in that: the color-changing lipstick does not contain plant pigment and color-changing powder; the contents of other components and the preparation method are the same as example 1.
Comparative example 4
This comparative example provides a lipstick, differing from example 1 in that: replacing 1.016 parts of beta-carotene by the plant pigment radish root extract and the beet root extract; the contents of other components and the preparation method are the same as example 1.
Comparative example 5
The comparative example provides a lipstick, and the color-changing lipstick comprises the following components in parts by weight:
the preparation method of the color-changing lipstick provided by the comparative example is the same as that of the example 1.
Comparative example 6
The comparative example provides a lipstick, and the color-changing lipstick comprises the following components in parts by weight:
the preparation method of the color-changing lipstick provided by the comparative example is the same as that of example 1.
Test example 1
Experiment of acute toxicity of mouse by mouth
According to the method of Hoen, 65 healthy mice were selected and randomly divided into 13 groups of 5 mice each. Average body weight of female mice (19.8 + -1.6) g, male mice (18.7 + -1.8) g. The samples to be tested are the color-changing lipstick containing plant pigments prepared in the embodiments 1-13 of the invention, the set dosage is respectively 21.5g/(kg · bw), 10.0g/(kg · bw), 4.64g/(kg · bw) and 2.15g/(kg · bw), after the test substances are orally taken once, the toxic reaction and death condition of the animals are observed within two weeks, and the test result of half lethal dose of mice is shown in table 1.
TABLE 1
The experimental result of the oral acute toxicity experiment of the mouse shows that: all groups of mice have no abnormal reaction in an observation period, the growth condition is good, no death occurs, the final weight of female mice is (20.2 +/-1.6) g, the final weight of male mice is (18.9 +/-1.8) g, and LD50 is more than 21.5 g/(kg-bw); grading standard according to acute toxicity. The color-changing lipstick containing plant pigment belongs to a nontoxic substance and can reach the edible level.
Test example 2
Lipstick Effect test
Selecting 95 healthy female volunteers, wherein the female volunteers are 20-40 years old and divided into 19 groups, 5 persons in each group have no serious system diseases, immunodeficiency or autoimmune diseases, no allergy to cosmetics, no acute inflammation on the face, no hormone medicine or immunosuppressant, no other clinical tests, no external preparation, the color-changing lipstick containing plant pigments provided by the embodiment 1-13 and the lipstick prepared by the comparative example 1-5 are respectively coated on the lip skins of the volunteers in the group, and the effect of the lip skin of the volunteers is detected after 2 hours.
Lip moisture content (%) was measured using a skin moisture loss tester (Tewameter TM 300) and skin elasticity of lips was measured using a skin elasticity tester (Cutomer MPA 580), and the result was expressed as a ratio of the springback value Ur to the maximum tensile value Uf of the skin, and the closer to 1 the value, the better the skin elasticity. And a spectrocolorimeter (CM-2500c) was used to determine the change in lip color (greater delta L, greater delta L indicates more residual lips, more saturated colors, better gloss) as shown in table 2:
TABLE 2
From the above test data, it is understood that the color-changed lipsticks containing plant pigments prepared in examples 1 to 13 of the present invention have a moisture retention rate of 41.5% or more, an elasticity parameter of Ur/Uf of 0.81 or more, and the closer to 1 the value, the better the elasticity of the lip skin. The fact fully shows that the components of the color-changing lipstick containing the plant pigment are matched with each other, have the synergistic effect and can achieve the effect of moistening and beautifying lips. The lip color change (delta L) value is more than 2 in the embodiment, and is obviously higher than the comparative example value, which shows that the color saturation, the glossiness and the moistening degree of the lip of the color-changing lipstick containing the plant pigment are obviously improved after the color-changing lipstick is used, so that the lip is more glossy and colored, and the effects of keeping moisture, preventing the lip from being cracked and skinned and reducing fine wrinkles and dry wrinkles of the lip are achieved.
Test example 3
Experiment of product efficacy
The color-changing lipsticks containing phytochrome prepared in examples 1 to 13 and the lipsticks prepared in comparative examples 1 to 6 were tried for test effect by the opinion score method. Test objects: each experimental group was 10 professionally trained women (20-45 years old); test area: a lip portion; frequency of use: once a day for 1 week; and (3) testing items: lip staining, anaphylactic reaction and satisfaction degree, and recording the number of the tested people respectively, wherein the specific test results are shown in table 3:
TABLE 3
The above tests show that the lipstick prepared in examples 1-13 has a significantly better lip dyeing effect than the lipstick prepared in comparative examples 1-6, and the color-changing lipstick containing plant pigments of the invention has a significant effect on lip dyeing; the lipsticks prepared in examples 1 to 13 have no allergic reaction, and it can be seen that the color-changed lipsticks containing plant pigments according to the present invention have no allergy and discomfort to the human body after use; the lipstick prepared in examples 1-13 was used in a satisfactory proportion of persons of 88% or more, and the test subjects in comparative example 1 generally indicated that the lipstick was not attractive enough in appearance and not developed in color when applied, the test subjects in comparative example 2 generally indicated that the lipstick was not developed when applied, and the test subjects in comparative example 3 generally indicated that the lipstick was not a lipstick product and was a lip gloss. Comparative example 4 appearance color saturation was too poor. Neither comparative examples 5, 6 are experiences with acceptable lipstick products.
Test example 4
Product appearance and stability testing
The color-changed lipsticks containing plant pigments prepared in examples 1 to 13 and the lipsticks prepared in comparative examples 1 to 6 were subjected to a stability test for their test effects, test standards: GB/T26513 + 2011, test method: detecting sensory indexes and physical and chemical indexes of the lipstick, and testing an instrument: the constant temperature drying oven and the heat resistance test method are as follows: placing the test sample at 45 +/-1 ℃ for 24h, and observing whether the lipstick has obvious change or not and can be normally used or not after the temperature is restored to the room temperature; the cold resistance test method comprises the following steps: the test sample is placed at (-5 to-10) DEG C for 25h, whether the lipstick has obvious change or not and can be normally used is observed after the temperature is restored to the room temperature, wherein the appearance color represents the color of the lipstick, the smearing color represents the color displayed by the lipstick smeared on lips, the results of sensory test and physicochemical index test are shown in Table 4, and the microbial index and the heavy metal index are shown in Table 5:
TABLE 4
TABLE 4
From the above test results, it is clear that the color-changeable lipsticks containing plant pigments prepared in examples 1 to 13 have high stability and safety, and meet the requirements for production quantity. In conclusion, the color-changing lipstick containing the plant pigment has normal stability, safety and sensory experience. In addition, the appearance color and the painting color of the product are controllable, and the appearance color and the painting color which are loved by consumers can be debugged. On the premise of safety and stability, the requirement of consumers on lipstick color is met. The color-changing lipstick with the plant pigment can be used for beautifying and permanently strengthening natural colors of two lips, can immediately sense the pH values of the two lips and gradually change different ruddy effects suitable for users, the natural ruddy effects are adjusted according to each user, so that the color-changing lipstick is suitable for people with any lip color, the two lips are enabled to be fresh, full and shiny, and the natural plant ruddy components are contained, so that the color-changing lipstick can play a role in improving the lip color after being used for a long time.
The applicant states that the present invention is described by the above examples to describe the color-changeable lipstick containing plant pigments and the method for preparing the same, but the present invention is not limited to the above examples, that is, it is not meant to be construed that the present invention is necessarily implemented by the above examples. It should be understood by those skilled in the art that any modifications of the present invention, equivalent substitutions of the raw materials of the product of the present invention, and the addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (24)
1. The color-changing lipstick containing plant pigments is characterized by comprising the following raw materials in parts by weight: 15-30 parts of natural wax, 60-90 parts of natural vegetable oil, 0.05-5 parts of vegetable pigment, 0.05-5 parts of antioxidant and 0.05-5 parts of color-changing powder;
the plant pigment comprises at least two of sweet potato root extract, beet root extract, radix Raphani extract, Bolete Spirulina extract or Curcuma rhizome extract;
the natural wax consists of 10-15 parts of beeswax, 2-5 parts of candelilla wax and 5-10 parts of carnauba wax;
the natural vegetable oil consists of 20-25 parts of shea butter, 15-20 parts of castor oil, 10-18 parts of chinlon oil, 2-5 parts of plant squalane, 3-6 parts of olive oil and 10-15 parts of jojoba seed oil;
the color-changing powder comprises any one of CI 45380, CI 45410 or CI 45370 or a combination of at least two of the foregoing.
2. The color-changing lipstick containing plant pigments according to claim 1, characterized in that the color-changing lipstick comprises the following raw materials in parts by weight: 20-30 parts of natural wax, 65-80 parts of natural vegetable oil, 0.1-3 parts of vegetable pigment, 0.15-5 parts of antioxidant and 0.2-3 parts of color-changing powder.
3. The color-changing lipstick containing plant pigments according to claim 2, characterized in that the color-changing lipstick comprises the following raw materials in parts by weight: 22-28 parts of natural wax, 68-78 parts of natural vegetable oil, 0.1-2.5 parts of vegetable pigment, 0.15-3 parts of antioxidant and 0.2-2.5 parts of color-changing powder.
4. The color-changing lipstick containing plant pigment according to claim 1, wherein said antioxidant comprises any one of pentaerythritol tetrakis (bis-t-butylhydroxyhydrocinnamate), butylated hydroxytoluene, or tocopherol or a combination of at least two thereof.
5. The color-changing lipstick containing plant pigments according to claim 1, characterized in that said color-changing lipstick further comprises a flavor.
6. The color-changing lipstick containing plant pigment according to claim 5, wherein the weight portion of said flavor in said color-changing lipstick is 0.05-0.1.
7. The method for producing a color-changing lipstick containing plant pigments according to any one of claims 1 to 6, comprising the steps of:
(1) mixing and grinding the plant pigment and part of natural plant oil to obtain plant pigment color paste; mixing the color-changing powder with part of natural vegetable oil, and homogenizing and dispersing to obtain color-changing color paste;
(2) and (2) mixing and stirring the natural wax and the residual natural vegetable oil for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time, and filling and molding to obtain the color-changing lipstick containing the plant pigment.
8. The process for producing a color-changing lipstick containing a plant pigment according to claim 7, wherein the mass of the natural vegetable oil or fat blended with the plant pigment in the step (1) is 5 to 15% of the total mass of the natural vegetable oil or fat.
9. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the temperature of mixing the vegetable pigments with a part of natural vegetable oils and fats in the step (1) is 20 to 40 ℃.
10. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the mixing time of the vegetable pigments and the part of natural vegetable oils and fats in the step (1) is 5 to 10 min.
11. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the rotation speed for grinding the plant pigments and the part of natural plant oil and fat in the step (1) is 400-600 r/min.
12. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the time for grinding the plant pigments and a part of natural vegetable oils and fats in the step (1) is 10 to 20 min.
13. The process for producing a color-changing lipstick containing a vegetable pigment according to claim 7, wherein the natural vegetable oils and fats mixed with the color-changing powder in the step (1) account for 5 to 15% by mass of the total mass of the natural vegetable oils and fats.
14. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the temperature at which the color-changing powder and a part of natural vegetable oil or fat are mixed in the step (1) is 20 to 40 ℃.
15. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the time for mixing the color-changing powder and a part of the natural vegetable oil or fat in the step (1) is 5 to 10 min.
16. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the rotation speed for homogeneously dispersing the color-changing powder and part of the natural vegetable oil and fat in the step (1) is 600-800 r/min.
17. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the time for homogeneously dispersing the color-changing powder and a part of the natural vegetable oil and fat in the step (1) is 20 to 30 min.
18. The method for preparing color-changing lipstick containing vegetable pigments according to claim 7, wherein the temperature at which the color-changing powder and a part of the natural vegetable oil or fat are homogeneously dispersed in the step (1) is 60 to 80 ℃.
19. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the temperature of the primary mixing and stirring in the step (2) is 85 to 90 ℃.
20. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the temperature of the secondary mixing and stirring in step (2) is 80-85 ℃.
21. The method for preparing color-changing lipstick containing plant pigments according to claim 7, wherein the filling molding of the step (2) is specifically: and heating and melting the semi-finished lipstick body obtained after the secondary mixing and stirring, injecting into a mold, cooling and demolding.
22. The method of claim 21, wherein the melting temperature is 75 to 80 ℃.
23. The method of claim 21, wherein the cooling temperature is 10-20 ℃.
24. The method for preparing a color-changing lipstick containing plant pigments according to claim 7, wherein the method for preparing a color-changing lipstick containing plant pigments comprises the steps of:
(1) mixing the plant pigment and part of natural plant oil according to the formula amount at 20-40 ℃ for 5-10min, and then grinding in a high-speed grinder at the rotating speed of 400-600r/min for 10-20min to obtain plant pigment color paste;
mixing the color-changing powder and part of the natural vegetable oil for 5-10min at 20-40 ℃, and then homogenizing and dispersing for 20-30min in a high-speed homogenizer at the speed of 600-800r/min to obtain color-changing color paste;
(2) mixing and stirring the natural wax and the residual natural vegetable oil at 85-90 ℃ for the first time, adding the antioxidant, the plant pigment color paste and the color-changing color paste obtained in the step (1), mixing and stirring for the second time at 80-85 ℃, heating to fully melt uniformly, injecting into a mold, cooling at 10-20 ℃, and demolding to obtain the color-changing lipstick containing the plant pigment.
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| GB202004239D0 (en) * | 2020-03-24 | 2020-05-06 | Givaudan Sa | Pigment |
| CN111568842B (en) * | 2020-05-28 | 2023-04-07 | 杭州心悦化妆品有限公司 | Natural color-changing lipstick and preparation method thereof |
| CN112043638A (en) * | 2020-09-18 | 2020-12-08 | 山东易孚得生物科技有限公司 | Perilla frutescens and schisandra chinensis flavored lipstick and preparation method thereof |
| CN112675073A (en) * | 2020-12-26 | 2021-04-20 | 广州集妍化妆品科技有限公司 | Velvet texture composition and lipstick |
| CN115957165A (en) * | 2023-01-17 | 2023-04-14 | 广东茂名健康职业学院 | Edible lipstick and preparation method thereof |
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