CN110354033A - A kind of thousand change lipstick of red cherry discoloration and preparation method thereof eaten - Google Patents

A kind of thousand change lipstick of red cherry discoloration and preparation method thereof eaten Download PDF

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Publication number
CN110354033A
CN110354033A CN201910652174.9A CN201910652174A CN110354033A CN 110354033 A CN110354033 A CN 110354033A CN 201910652174 A CN201910652174 A CN 201910652174A CN 110354033 A CN110354033 A CN 110354033A
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China
Prior art keywords
parts
lipstick
oil
substance
discoloration
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CN201910652174.9A
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Chinese (zh)
Inventor
杨菊
曹波
傅建斌
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GUANGDONG BAILICHEN BIOTECHNOLOGY Co.,Ltd.
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Kingway Cosmetics Technology Guangzhou Co Ltd
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Priority to CN201910652174.9A priority Critical patent/CN110354033A/en
Publication of CN110354033A publication Critical patent/CN110354033A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/927Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

Abstract

The present invention relates to a kind of lipsticks, and in particular to the red cherry discoloration thousand that one kind can be eaten becomes lipstick and preparation method thereof.It includes following component that the discoloration thousand, which becomes lipstick: thickener, moisturizer, colorant, gean seed oil, gean berry extract, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed oil of deep-sea, glycerol caprylate and ethylhexyl palmitate.The present invention has the advantages that moisturizing, anticracking, using effect are good.

Description

A kind of thousand change lipstick of red cherry discoloration and preparation method thereof eaten
Technical field
The present invention relates to cosmetic technical fields, and in particular to the red cherry discoloration thousand that one kind can be eaten becomes lipstick and its preparation Method.
Background technique
Lipstick is one kind of most original, the most common lipstick, usually solid, and quality is more dry than lip gloss and lip honey and hard. Lipstick has become the common cosmetics of China's modern female.One layer of just right lipstick is applied on lip can make one to seem especially It is coquettish.Color saturation is high, and color mileage is strong, and due to being that solid is generally not easy since cheilogramma is too deep and excessive, often Lip shape, lip color are modified with it.The face cream of daily smearing, which is coated on dry lip, not to be acted on.Lip needs relatively to moisten, Hold time it is relatively permanent, lip surface can be rested on and impervious skin care item, here it is lip gloss.Though lip gloss cannot be said Effect is omnipotent, but the special requirement for being really directed to skin of lip of its main component for containing, can lock water for lips Divide and barrier is provided.
Much lipsticks are inedible, this depends primarily on its ingredient.For example, the main component packet of many lipsticks Wax, oil and pigment etc. are contained, if very big injury may be caused to body by being used for a long time.Oil and wax all have stronger suction Attached property, can be by noxious substances such as dust, virus, bacteriums in air on lip mucosa, when people is careless with food Into internal, the sick probability of human body is increased.The common dyestuff of lipstick is the non-food coloring being harmful to the human body, expert mostly Experiments prove that certain poor quality dyestuffs also contain carcinogenic chemical analysis.In addition, preservative and antioxidant can also be added to In lipstick, for a long time, unnecessary damage can be caused to human body.Also, although the lipstick of commercially available various brands all must in advance Safety testing must be passed through, but since color is different and the difference of base material formulation, in addition people's constitution is multifarious.Therefore, Some lipsticks still hide anaphylactoid danger to user.Lip allergy caused by lipstick has been one serious and universal The problem of, about 10% it is for women after will appear that lip is dry and cracked, burn, swelling, itch, exfoliation, mild pain etc..Cause This, lipstick is actually a kind of chemical substance of complexity, and there is the hidden danger not paid attention to for people for the behind of fresh colour.
To solve the above-mentioned problems, occur many lipsticks done using pure plant raw material, these lipsticks in the market It is edible.One of raw material is gean, and gean system rosaceae originates in Europe and western part of Asia, Cultivation is experienced all sorts of in existing Eurasian and North America, and kind is also more, and fruit type is big, flavor grace, eats raw or can processed, and cherry juice can refine sugar slurry, sugar Glue and fruit wine;Kernel can extract oil, like apricot kernel oil.
For sweet cherry oil generally by squeezing gean come what is extracted, cherry tree needs the time of 3-4 to produce Its first generation fruit, 7 years will be mature, and the best fruit of output is known as the good reputation of " all kinds of fruits first ".Sweet cherry oil is claimed For the essence of the Nature, sweet cherry oil has outstanding nourishing, moisture-retaining capacity.For allowing your skin to seem in cosmetics 100% health and youth.It is absolutely marvellous using cherry kernel oil effect on your skin, hair and nail.This is one A stable soothing oil, oleic acid, natural, δ, α and Gamma-Tocopherol and vitamin E and A with high-content.It Also contain a kind of polyunsaturated fatty acid, is called eleostearic eleostearic acid, this is a kind of conjugate linolenic acid, can prevent purple Outer line absorption forms a barrier in skin or hair quality surface, protects hair and protects your skin old from sunburn and skin Change.It the use of lipstick made of sweet cherry oil is the lipstick that can directly eat.
Chinese patent application CN 109125130A discloses a kind of edible fruit lip gloss and preparation method thereof, water Fruit lip gloss is prepared by the component of following quality proportionings: cera alba: 7-8%;Babassu (COPERNICIA CERIFERA) wax: 7-8%;Apple (PYRUS MALUS) pericarp wax: 4-5%;Lecithin: 4-5%;Jojoba esters: 2- 3%;Jojoba (SIMMONDSIA CHINENSIS) seed oil: 5-6%;Queensland nut (MACADAMIA TERNIFOLIA) seed Oil: 10-15%;Grape (VITIS VINIFERA) seed oil: 10-15%;Diisooctadecanol malate: 5-10%;Coconut oil Ethylhexyl: 11.8-36.4%;Tocopherol acetate: 1-2%;Butyrospermum parkii (BUTYROSPERMUM PARKII) fruit fatty oil: 4-5%;Double more acyl group adipate ester -2:4-5% of-two glycerol;Fruit extract: 0.5-1%;Essence: 0.1-0.2%.Fruit Extract is strawberry berry extract, gean berry extract or sweet orange fruit powder.The raw material that the patent uses all is pure natural Product can be used for eating, but moisturizing, effect of anti-cracking need to be further increased.
Therefore, a kind of red cherry discoloration thousand eaten that can solve above-mentioned technical problem of exploitation becomes lipstick and its preparation Method is very important.
Summary of the invention
There is provided that a kind of moisturizing, anticracking, using effect is good eats the purpose of the present invention is overcome the deficiencies in the prior art Red cherry discoloration thousand become lipsticks and preparation method thereof.
The present invention is achieved by the following technical programs:
A kind of thousand change lipstick of red cherry discoloration and preparation method thereof eaten, it includes such as the following group that the discoloration thousand, which becomes lipsticks, Point: thickener, moisturizer, colorant, gean seed oil, gean berry extract, plant wool oil, coconut oil second The own ester of base, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed oil of deep-sea, glycerol caprylate and ethylhexyl palmitate.
Preferably, the thickener is the mixture of babassu vegetable wax, beeswax and glycolipid.
Preferably, the moisturizer is sweet orange pericarp wax, olive saualane, three (octyldodecanol) citrates, plant Object lanolin, Viamerine 2500, three isostearate of polyglycereol -2 mixture.
The Viamerine 2500 derives from oleic acid, the linoleic acid, linolenic acid polyglycereol esters of whole plant, The linoleic plus oleic acid that Viamerine 2500 contains can play moist, moisture-keeping function, and skin moisture is prevented to be lost;And it is non- It is often readily permeable to inside skin, pro-skin feels fairly obvious.Can be absorbed is more than 200 times of skin itself of moisture.Paste skin It is very good, product greasy feeling is reduced, transdermal dehydration is reduced.
The plant lanolin derives from Butyrospermum parkii fruit rouge, Glyceryl rosinate and olive oil unsaponifiable matter.
Preferably, the colorant is the mixture of natural pigment color-change powder or natural pigment color-change powder and Oil Yellow.
It is highly preferred that the colorant is the mixture of natural pigment color-change powder, Oil Yellow.
The Oil Yellow is CI 12700, is the edible pigment extracted by lemon, colours for lipstick surface.
It is highly preferred that the natural pigment color-change powder is one of CI 45380, CI 45370, CI 45410 or more Kind, sweet cherry haematochrome, anthocyanidin, lycopene, corn yellow OB are derived from, natural food colour is belonged to.
It is highly preferred that the natural pigment color-change powder is one of CI 45380, CI 45370, CI 45410 or more Kind, the proportion of CI 45380, CI 45370 and CI 45410 are determined according to required color changeable effect.
The color changeable effect of product of the present invention be by natural pigment color-change powder CI 45380, CI 45370, CI 45410 this What three kinds of pigments were realized, CI 45380, CI 45370, CI 45410 under acidic environment in colourless, after CI 45380 meets skin Orange is shown since environment pH changes, shows pink since environment pH changes after the chance skin of CI 45370, after the chance skin of CI 45410 Different colours out can be changed so that product of the present invention be made to change with different skin pH value since environment pH changes aobvious rose Effect;The color changeable effect of product can freely arrange in pairs or groups these three color-change powder ratios, recall required color.
The plant wool oil is not saponified from Castor oil, Glyceryl rosinate, glyceryl oleate and olive oil Object.
It is highly preferred that the thousand change lipstick of discoloration includes the component of following parts by weight: gean (PRUNUS AVIUM) seed oil 20.3-35.55 parts, 8-9 parts of beeswax, 8-9 parts of wax of babassu (COPERNICIA CERIFERA), sweet orange 5-6 parts of pericarp wax of (CITRUS AURANTIUM DULCIS), 4-5 parts of berry extract of gean (PRUNUS AVIUM), olive 5-6 parts of olive saualane, 4-5 parts of glycolipid, three 4-5 parts of (octyldodecanol) citrates, 3-4 parts of plant lanolin, plant sheep 2-3 parts of crude oil, 5-6 parts of coconut oil ethylhexyl, 2-3 parts of seed oil of Queensland nut (MACADAMIA TERNIFOLIA), Jojoba 2-3 parts of seed oil of (SIMMONDSIA CHINENSIS), 2-3 parts of seed oil of two section shepherd's purse of deep-sea (CRAMBE ABYSSINICA), Viamerine 2500 4-5 part, 4-5 parts of three isostearate of polyglycereol -2,0.8-1 parts of glycerol caprylate, palm acid ethyl oneself 5-6 parts of ester, 0.1-0.5 parts of natural pigment color-change powder, 0.01-0.02 parts of Oil Yellow.
Preferably, it further includes edible essence that the discoloration thousand, which becomes lipstick,.
It is highly preferred that it further includes 0.05-0.2 parts of edible essence that the discoloration thousand, which becomes lipstick,.
Preferably, the preparation method of the gean berry extract includes the following steps:
(1) fruit of gean is taken, crushes, mixed with enzyme, obtain substance A;
(2) by substance A organic solvent ultrasonic extraction, filtering obtains filter residue B and liquor C;
(3) filter residue B is extracted with organic solvent, obtains substance D;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
Described gean (PRUNUS AVIUM) berry extract is obtained, nutritive value by extracting in sweet cherry fruit Height, it is good for health.
It is highly preferred that the fruit of gean described in step (1) and the mass ratio of enzyme are 10-30:1, hydrolysis temperature It is 25-55 DEG C, adjusts pH value 4.0-6.0.
It is highly preferred that the mass volume ratio of substance A described in step (2) and organic solvent is 1:50-100g/mL.
It is highly preferred that the mass volume ratio of liquor B described in step (3) and organic solvent is 1:20-40g/mL.
It is highly preferred that enzyme described in step (1) is one of pectase, cellulase, protease, amylase or several Kind.
It is highly preferred that enzyme described in step (1) is cellulase, the mixture of pectase, protease, amylase, four kinds The mass ratio of enzyme is 1:2-3:0.5-1:1-2.
It is highly preferred that the mixing for the ethyl alcohol that organic solvent is formic acid and volume fraction is 70-90% described in step (2) is molten Agent.
It is highly preferred that the mixing for the ethyl alcohol that organic solvent is formic acid and volume fraction is 70-90% described in step (2) is molten The volume ratio for the ethyl alcohol that agent, the formic acid and volume fraction are 70-90% is 1:6-9.
It is highly preferred that ultrasonic power 100-300w described in step (2), ultrasonic time 20-40min.
It is highly preferred that the mixing for the ethyl alcohol that organic solvent is acetone and volume fraction is 80-95% described in step (3) is molten Agent.
It is highly preferred that the mixing for the ethyl alcohol that organic solvent is acetone and volume fraction is 80-95% described in step (3) is molten The volume ratio for the ethyl alcohol that agent, the acetone and volume fraction are 80-95% is 1:2-4.
The invention further relates to the preparation methods that above-mentioned discoloration thousand becomes lipstick, which comprises the steps of:
Semi-finished product production:
S1 weighs natural pigment color-change powder, ethylhexyl palmitate, and mixing, grinding obtain substance A;
S2 weighs beeswax, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, and mixing obtains substance B;
S3 weighs gean seed oil, olive saualane, glycolipid, three (octyldodecanol) citrates, plant sheep Hair rouge, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea be oily, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, obtain substance C;
S4 mixes substance B and substance C, adds substance A, and Oil Yellow, edible essence is added to get semi-finished product in homogeneous Lipstick;
Finished product production:
By the semi-finished product lipstick pour into Rouge mold to get.
Preferably, mixing, grinding are performed under heating conditions in step S1 described in semi-finished product manufacturing process, heating temperature is 70-80 DEG C, heating time 10-15min.
It is highly preferred that being ground to no granular sensation in step S1 described in semi-finished product manufacturing process, it is colourless to be heated to surface It is bright.
Preferably, it being mixed in a heated condition in step S2 described in semi-finished product manufacturing process, heating temperature is 85-90 DEG C, Heating time is 5-15min.
Preferably, it being mixed in a heated condition in step S3 described in semi-finished product manufacturing process, heating temperature is 90-100 DEG C, Heating time is 10-15min.
It is completely dissolved it is highly preferred that being heated to substance in step S3 described in semi-finished product manufacturing process.
Preferably, substance B and substance C are mixed in step S4 described in semi-finished product manufacturing process, is cooled to 80-90 DEG C, it is cold But time 5-10min.
Preferably, add substance A in step S4 described in semi-finished product manufacturing process, be cooled to 70-80 DEG C, cooling time 5- 10min。
Preferably, Oil Yellow, edible essence are added in step S4 described in semi-finished product manufacturing process, is cooled to 50-60 DEG C, it is cold But time 5-15min is to get semi-finished product lipstick.
Preferably, the semi-finished product lipstick is heated to 80-90 DEG C in the finished product manufacturing process, heating time 5- 10min, stirring, is poured into Rouge mold, is cooled to -4~-8 DEG C, cooling time 5-15min to get.
The beneficial effects of the present invention are:
1. raw material of the invention is all food-grade, have good edible moisturizing effect: gean seed oil is referred to as The essence of the Nature, gean seed oil have good nourishing, moisture-retaining capacity.Lipstick produced by the present invention has good Moisten lip, effect of anti-cracking, keeps lip more satin beautiful.Using natural material and edible oil, allow user that can trust smearing, it can Edible, for mouthfeel also than convenient, fruit perfume (or spice), which is added, can more improve the mood of people.
2. gean fruit passes through enzymatic hydrolysis, ultrasound, extracting Combined Treatment during the extraction process, and using compound organic molten Agent, so that the effective component gean fruit extraction as much as possible for extracting, extracting in gean fruit The sweet cherry haematochrome synergistic effect of object and gean seed oil, natural pigment color-change powder, moistening effect are more significant.
3. the present invention is changed by different skin of lip pH values, change the effect of different colours out.
4. the present invention heats raw material using different heating temperature during the preparation process, specific sequence mixed raw material and Different temperature is cooling, and for lipstick gloss obtained naturally, lip sense is soft, using effect is more preferable.
Specific embodiment
The invention will now be further described with reference to specific embodiments, the advantages and features of the present invention will be with description and It is apparent.But examples are merely exemplary for these, and it is not intended to limit the scope of the present invention in any way.Those skilled in the art Member it should be understood that without departing from the spirit and scope of the invention can details to technical solution of the present invention and form into Row modifications or substitutions, but these modifications and replacement are fallen within the protection scope of the present invention.
Embodiment 1
A kind of thousand change lipstick of red cherry discoloration eaten includes the component of following parts by weight: gean seed oil 20.3 Part, 8 parts of beeswax, 8 parts of babassu vegetable wax, 5 parts of sweet orange pericarp wax, 4 parts of gean berry extract, olive saualane 5 Part, 4 parts of glycolipid, three 4 parts of (octyldodecanol) citrates, 3 parts of plant lanolin, 2 parts of plant wool oil, coconut oil ethyl 5 parts of own ester, 2 parts of oil of Queensland nut seed, 2 parts of jojoba seed oil, 2 parts of oil of two section shepherd's purse seed of deep-sea, gathers by 2,500 4 parts of Viamerine 4 parts, 0.8 part of glycerol caprylate, 5 parts of ethylhexyl palmitate, 45,380 0.1 parts of CI of three isostearate of glycerol -2.
The preparation method of gean berry extract includes the following steps:
(1) fruit of gean is taken, is crushed, is mixed, 25 DEG C of hydrolysis temperature, obtained according to mass ratio 10:1 with pectase Substance A;
(2) by substance A organic solvent according to mass volume ratio 1:50g/mL ultrasonic extraction, ultrasonic power 100w, ultrasound Time 20min, filtering, obtains filter residue B and liquor C, the mixed solvent for the ethyl alcohol that organic solvent is formic acid and volume fraction is 70%, The two volume ratio is 1:6;
(3) it is 1:20g/mL extracting according to mass volume ratio with organic solvent by filter residue B, obtains substance D, organic solvent third The mixed solvent for the ethyl alcohol that ketone and volume fraction are 80%, the two volume ratio are 1:2;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
The preparation method of thousand change lipstick of discoloration includes the following steps:
Semi-finished product production:
S1 weighs the CI 45380 of formula ratio, ethylhexyl palmitate, and mixing, grinding, stirring, heating temperature is 70 DEG C, Heating time is 10min, obtains substance A;
S2 weighs the beeswax of formula ratio, sweet orange pericarp wax, babassu vegetable wax, gean berry extract, mixes, stirs It mixes, heating temperature is 85 DEG C, and heating time 5min obtains substance B;
S3 weighs gean seed oil, glycolipid, olive saualane, three (octyldodecanol) citric acids of formula ratio Ester, plant wool oil, plant lanolin, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea Oil, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, stirring, heating temperature are 90 DEG C, Heating time is 10min, obtains substance C;
S4 mixes substance B and substance C, is cooled to 80 DEG C, keeps the temperature 5min, adds substance A, and homogeneous is cooled to 50 DEG C, Cooling 5min is to get semi-finished product lipstick.
Finished product production:
By semi-finished product lipstick heating, stir, heating temperature 80, DEG C, 5min is heated, is poured into Rouge mold, -4 It is cooling at DEG C, cooling 5min to get.
Embodiment 2
A kind of thousand change lipstick of red cherry discoloration eaten includes the component of following parts by weight: gean seed oil 35.55 Part, 9 parts of beeswax, 9 parts of babassu vegetable wax, 6 parts of sweet orange pericarp wax, 5 parts of gean berry extract, 6 parts of olive saualane, 5 parts of glycolipid, three 5 parts of (octyldodecanol) citrates, 4 parts of plant lanolin, 3 parts of plant wool oil, coconut oil ethyl hexyl 6 parts of ester, 3 parts of oil of Queensland nut seed, 3 parts of jojoba seed oil, 3 parts of oil of two section shepherd's purse seed of deep-sea, gathers sweet by 2,500 5 parts of Viamerine Oily 5 parts of -2 three isostearate, 1 part of glycerol caprylate, 6 parts of ethylhexyl palmitate, 45,410 0.5 parts of CI, Oil Yellow 0.02 Part, 0.05 part of edible essence.
The preparation method of gean berry extract includes the following steps:
(1) fruit of gean is taken, is crushed, mixed enzyme (cellulase, pectase with cellulase, pectase Mass ratio 1:2) it is mixed according to mass ratio 30:1,55 DEG C of hydrolysis temperature, obtain substance A;
(2) by substance A organic solvent according to mass volume ratio 1:100g/mL ultrasonic extraction, ultrasonic power 300w, ultrasound The filtering of time 40min, obtains filter residue B and liquor C, the mixed solvent for the ethyl alcohol that organic solvent is formic acid and volume fraction is 90%, The two volume ratio is 1:9;
(3) it is 1:40g/mL extracting according to mass volume ratio with organic solvent by filter residue B, obtains substance D, organic solvent third The mixed solvent for the ethyl alcohol that ketone and volume fraction are 95%, the two volume ratio are 1:4;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
The preparation method of thousand change lipstick of discoloration includes the following steps:
Semi-finished product production:
S1 weighs the CI 45410 of formula ratio, ethylhexyl palmitate, and mixing, grinding, stirring, heating temperature is 80 DEG C, Heating time is 15min, obtains substance A;
S2 weighs the beeswax of formula ratio, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, mixes, stirs It mixes, heating temperature is 90 DEG C, and heating time 15min obtains substance B;
S3 weighs gean seed oil, olive saualane, the glycolipid, three (octyldodecanol) citric acids of formula ratio Ester, plant lanolin, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea Oil, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, stirring, heating temperature are 100 DEG C, Heating time is 15min, obtains substance C;
S4 mixes substance B and substance C, is cooled to 90 DEG C, and cooling 10min adds substance A, homogeneous is cooled to 80 DEG C, Oil Yellow, edible essence is added in cooling 10min, is cooled to 60 DEG C, cooling 15min is to get semi-finished product lipstick.
Finished product production:
By semi-finished product lipstick heating, stirring, heating temperature is 90 DEG C, and heating time 10min pours into Rouge mold In, it is cooling at -8 DEG C, cooling time 15min to get.
Embodiment 3
A kind of thousand change lipstick of red cherry discoloration eaten includes the component of following parts by weight: 28 parts of oil of gean seed, 8.5 parts of beeswax, 8.5 parts of babassu vegetable wax, 5.5 parts of sweet orange pericarp wax, 4.5 parts of gean berry extract, olive spiny dogfish 5.5 parts of alkane, 4.5 parts of glycolipid, three 4.5 parts of (octyldodecanol) citrates, 3.5 parts of plant lanolin, plant wool oil 2.5 parts, 5.5 parts of coconut oil ethylhexyl, 2.5 parts of oil of Queensland nut seed, 2.5 parts of jojoba seed oil, two section shepherd's purse seed oil of deep-sea 2.5 parts, 2,500 4.5 parts of Viamerine, 4.5 parts of three isostearate of polyglycereol -2,0.9 part of glycerol caprylate, palmitinic acid second 5.5 parts, 0.3 part of natural pigment color-change powder, 0.015 part of Oil Yellow, 0.2 part of edible essence of the own ester of base.
Wherein, natural pigment color-change powder be CI 45380, CI 45370, CI 45410 mixture, three's mass ratio 1: 1:2;
The preparation method of gean berry extract includes the following steps:
(1) fruit of gean is taken, is crushed, is mixed with enzyme according to mass ratio 20:1,40 DEG C of hydrolysis temperature, obtain substance A, enzyme are the mixture of cellulase, pectase, protease, amylase, and the mass ratio of four kinds of enzymes is 1:3:0.5:1;
(2) by substance A organic solvent according to mass volume ratio 1:70g/mL ultrasonic extraction, ultrasonic power 200w, ultrasound Time 30min, filtering, obtains filter residue B and liquor C, the mixed solvent for the ethyl alcohol that organic solvent is formic acid and volume fraction is 80%, The two volume ratio is 1:8;
(3) it is 1:30g/mL extracting according to mass volume ratio with organic solvent by filter residue B, obtains substance D, organic solvent third The mixed solvent for the ethyl alcohol that ketone and volume fraction are 90%, the two volume ratio are 1:3;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
The preparation method of thousand change lipstick of discoloration includes the following steps:
Semi-finished product production:
S1 weighs natural pigment color-change powder, the ethylhexyl palmitate of formula ratio, and mixing, grinding are stirred, and heating temperature is 75 DEG C, heating time 12min obtains substance A;
S2 weighs the beeswax of formula ratio, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, mixes, stirs It mixes, heating temperature is 88 DEG C, and heating time 10min obtains substance B;
S3 weighs gean seed oil, olive saualane, the glycolipid, three (octyldodecanol) citric acids of formula ratio Ester, plant lanolin, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea Oil, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, stirring, heating temperature are 95 DEG C, Heating time is 13min, obtains substance C;
S4 mixes substance B and substance C, is cooled to 85 DEG C, cooling time, 8min, added substance A, and homogeneous is cooled to 75 DEG C, 7min, was added Oil Yellow, edible essence, was cooled to 55 DEG C, cooling time, 10min was to get semi-finished product lip cooling time Cream.
Finished product production:
By semi-finished product lipstick heating, stirring, heating temperature is 85 DEG C, and heating time 8min pours into Rouge mold In, it is cooling at -6 DEG C, cooling time 10min to get.
Embodiment 4
A kind of thousand change lipstick of red cherry discoloration eaten includes the component of following parts by weight: 30 parts of oil of gean seed, 8 parts of beeswax, 9 parts of babassu vegetable wax, 5 parts of sweet orange pericarp wax, 5 parts of gean berry extract, 5 parts of olive saualane, sugar 5 parts of rouge, three 5 parts of (octyldodecanol) citrates, 3 parts of plant lanolin, 3 parts of plant wool oil, coconut oil ethylhexyl 6 Part, 3 parts of oil of Queensland nut seed, 2 parts of jojoba seed oil, 3 parts of oil of two section shepherd's purse seed of deep-sea, gathers sweet by 2,500 5 parts of Viamerine Oily 4 parts of -2 three isostearate, 0.8 part of glycerol caprylate, 5.5 parts of ethylhexyl palmitate, 0.4 part of natural pigment color-change powder, 0.02 part of Oil Yellow, 0.1 part of edible essence.
Wherein, natural pigment color-change powder be CI 45380, CI 45370, CI 45410 mixture, three's mass ratio 2: 2:3;
The preparation method of gean berry extract includes the following steps:
(1) fruit of gean is taken, is crushed, is mixed with enzyme according to mass ratio 15:1,40 DEG C of hydrolysis temperature, obtain substance A, enzyme are the mixture of cellulase, pectase, protease, amylase, and the mass ratio of four kinds of enzymes is 1:2.5:1:2;
(2) by substance A organic solvent according to mass volume ratio 1:60g/mL ultrasonic extraction, ultrasonic power 200w, ultrasound Time 30min, filtering, obtains filter residue B and liquor C, the mixed solvent for the ethyl alcohol that organic solvent is formic acid and volume fraction is 85%, The two volume ratio is 1:8;
(3) it is 1:30g/mL extracting according to mass volume ratio with organic solvent by filter residue B, obtains substance D, organic solvent third The mixed solvent for the ethyl alcohol that ketone and volume fraction are 90%, the two volume ratio are 1:3;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
The preparation method of thousand change lipstick of discoloration includes the following steps:
Semi-finished product production:
S1 weighs natural pigment color-change powder, the ethylhexyl palmitate of formula ratio, and mixing, grinding are stirred, and heating temperature is 75 DEG C, heating time 15min obtains substance A;
S2 weighs the beeswax of formula ratio, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, mixes, stirs It mixes, heating temperature is 85 DEG C, and heating time 10min obtains substance B;
S3 weighs gean seed oil, olive saualane, the glycolipid, three (octyldodecanol) citric acids of formula ratio Ester, plant lanolin, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea Oil, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, stirring, heating temperature are 95 DEG C, Heating time is 12min, obtains substance C;
S4 mixes substance B and substance C, is cooled to 82 DEG C, cooling time, 5min, added substance A, and homogeneous is cooled to 75 DEG C, 8min, was added Oil Yellow, edible essence, was cooled to 55 DEG C, cooling time, 8min was to get semi-finished product lipstick cooling time.
Finished product production:
By semi-finished product lipstick heating, stirring, heating temperature is 80 DEG C, and heating time 7min pours into Rouge mold In, it is cooling at -5 DEG C, cooling time 10min to get.
Comparative example 1
It is only that each component parts by weight are different from the difference of embodiment 4, remaining condition is all the same, specific as follows:
A kind of thousand change lipstick of red cherry discoloration eaten includes the component of following parts by weight: 40 parts of oil of gean seed, 10 parts of beeswax, 6 parts of babassu vegetable wax, 10 parts of sweet orange pericarp wax, 8 parts of gean berry extract, 1 part of olive saualane, 2 parts of glycolipid, three 2 parts of (octyldodecanol) citrates, 5 parts of plant lanolin, 1 part of plant wool oil, coconut oil ethyl hexyl 8 parts of ester, 5 parts of oil of Queensland nut seed, 5 parts of jojoba seed oil, 1 part of oil of two section shepherd's purse seed of deep-sea, gathers sweet by 2,500 1 parts of Viamerine Oily 1 part of -2 three isostearate, 1.5 parts of glycerol caprylate, 8 parts of ethylhexyl palmitate, 1 part of natural pigment color-change powder, oil is molten It is 0.05 part, 0.1 part of edible essence yellow.
Comparative example 2
Difference with embodiment 4, which is only that, does not add gean seed oil, but is added to coconut oil, remaining condition It is all the same.
Comparative example 3
Difference with embodiment 4 is only that in the preparation process of gean berry extract, step (1) cellulase, Pectase, protease, amylase mass ratio be 1:1:2:3, remaining condition is all the same.
Comparative example 4
Difference with embodiment 4 is only that in the preparation process of gean berry extract, step (2) formic acid and volume The volume ratio for the ethyl alcohol that score is 85% is 1:2, remaining condition is all the same.
Comparative example 5
Difference with embodiment 4 is only that in the preparation process of gean berry extract, step (3) acetone and volume The volume ratio for the ethyl alcohol that score is 90% is 2:1, remaining condition is all the same.
Comparative example 6
Difference with embodiment 4 is only that discoloration thousand becomes in the preparation process of lipstick, and the order of addition of each raw material is different, Remaining condition is all the same, specific as follows:
The preparation method of thousand change lipstick of discoloration includes the following steps:
Semi-finished product production:
S1 weighs natural pigment color-change powder, the ethylhexyl palmitate of formula ratio, and mixing, grinding are stirred, and heating temperature is 75 DEG C, heating time 15min obtains substance A;
S2 weighs the beeswax of formula ratio, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, mixes, stirs It mixes, heating temperature is 85 DEG C, and heating time 10min obtains substance B;
S3 weighs gean seed oil, olive saualane, the glycolipid, three (octyldodecanol) citric acids of formula ratio Ester, plant lanolin, plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed of deep-sea Oil, Viamerine 2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, stirring, heating temperature are 95 DEG C, Heating time is 12min, obtains substance C;
S4 mixes substance A and substance C, is cooled to 82 DEG C, cooling time, 5min, added substance B, and homogeneous is cooled to 75 DEG C, 8min, was added Oil Yellow, edible essence, was cooled to 55 DEG C, cooling time, 8min was to get semi-finished product lipstick cooling time.
Finished product production:
By semi-finished product lipstick heating, stirring, heating temperature is 80 DEG C, and heating time 7min pours into Rouge mold In, it is cooling at -5 DEG C, cooling time 10min to get.
Test case 1
Product made from embodiment 1-4 and comparative example 1-6 is subjected to moisture-keeping efficacy test, test method refers to " cosmetics Moisture-keeping efficacy evaluation guide QB/T4256-2011 ", it is visited using the Corneometer moisture measurement of moisture tester CK MPA10 Head measures the moisture content of skin situation of 30min, 60min, 120min after smearing respectively, and the results are shown in Table 1.
The test of 1 product moisture-keeping efficacy of table
30min/% 60min/% 120min/%
Embodiment 1 33.5 30.8 26.9
Embodiment 2 33.2 30.1 27.4
Embodiment 3 36.6 33.5 29.4
Embodiment 4 35.8 33.1 30.3
Comparative example 1 32.4 27.0 24.9
Comparative example 2 31.9 28.2 23.8
Comparative example 3 32.0 27.8 24.1
Comparative example 4 31.5 28.3 25.0
Comparative example 5 32.8 28.4 25.6
Comparative example 6 31.7 27.4 24.8
2 acute oral toxicity test of test case
The healthy mice for randomly selecting 100 half male and half females, is randomly divided into 10 groups, every group 10 (embodiment 1-4 and right Each one group of ratio 1-6), fasting 16h, not water restriction.Every mouse give respectively lipstick dosage be 0,1000mg/kg, 3000mg/kg,4000mg/kg,5000mg/kg.Lipstick is disposably given to small white mouse with oral mode, then close observation And general state, poisoning manifestations and the death condition of small white mouse are recorded, it observes 14 days.After 14 days each group test small white mouse water inlet, Feed is normal, does not occur being poisoned and death condition, and skin, hair and eye exhibits are normal, atremia, convulsions, diarrhea, stupor Phenomena such as.The oral median lethal dose LD >=5000mg/kg of tested material known to acute toxicity classification mark is that reality is nontoxic, at this Maximum dose group is 5000mg/kg in test, animal dead does not occur, illustrates that its oral median lethal dose is greater than 5000mg/ Kg, therefore can determine that lipstick made from embodiment 1-4 and comparative example 1-6 is actually nontoxic, it can be used for human trial.
3 sensory evaluation of test case
The female volunteers for choosing 100 lip health, are randomly divided into 10 groups, every group of 10 people, respectively to embodiment 1-4 with And the lipstick of comparative example 1-6 is tried out, and is tried out the previous day without using any lip treatment products, is used continuously 1 week, an angel It is each primary in the morning, afternoon and evening and identical using the time with 3 times.To use the ductility of product, viscosity sense, moisture feeling, color changeable effect into Row scoring, is averaged.Standards of grading: 5 points -- it is very satisfied;4 points -- it is satisfied;3 points -- it is general;2 points -- it is dissatisfied;1 point -- It is very dissatisfied.The results are shown in Table 2.
2 product sensory evaluation result of table
Ductility Viscosity sense Moisture feeling Color changeable effect
Embodiment 1 4.7 4.6 4.6 4.4
Embodiment 2 4.7 4.7 4.7 4.5
Embodiment 3 4.9 4.8 4.7 4.9
Embodiment 4 4.8 4.9 4.8 5.0
Comparative example 1 4.5 4.5 4.4 4.8
Comparative example 2 4.0 4.0 3.9 4.7
Comparative example 3 4.1 4.2 4.1 4.5
Comparative example 4 4.0 3.8 4.0 4.4
Comparative example 5 4.1 4.3 4.2 4.3
Comparative example 6 4.5 4.6 4.5 4.4
The technical means disclosed in the embodiments of the present invention is not limited to the technical means disclosed in the above technical means, and further includes Technical solution consisting of any combination of the above technical features.The foregoing is a specific embodiment of the present invention, should refer to Out, for those skilled in the art, without departing from the principle of the present invention, can also make several Improvements and modifications, these modifications and embellishments are also considered to be within the scope of the present invention.

Claims (10)

1. the red cherry discoloration thousand that one kind can be eaten becomes lipstick, which is characterized in that it includes following component that the discoloration thousand, which becomes lipstick: being increased Thick dose, moisturizer, colorant, gean seed oil, gean berry extract, plant wool oil, coconut oil ethyl hexyl Ester, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed oil of deep-sea, glycerol caprylate and ethylhexyl palmitate.
2. discoloration thousand according to claim 1 becomes lipstick, which is characterized in that the thickener is babassu vegetable wax, bee Wax and glycolipid;The moisturizer is sweet orange pericarp wax, olive saualane, three (octyldodecanol) citrates, plant wool Three isostearate of rouge, Viamerine 2500 and polyglycereol -2;The colorant is natural pigment color-change powder or natural pigment The mixture of color-change powder and Oil Yellow;It further includes edible essence that the discoloration thousand, which becomes lipstick,.
3. discoloration thousand according to claim 2 becomes lipstick, which is characterized in that the natural pigment color-change powder is CI 45380, one of CI 45370, CI 45410 or a variety of.
4. discoloration thousand according to claim 2 becomes lipstick, which is characterized in that it includes following weight that the discoloration thousand, which becomes lipstick, The component of part: 20.3-35.55 parts of gean seed oil, 8-9 parts of beeswax, 8-9 parts of babassu vegetable wax, sweet orange pericarp wax 5-6 Part, 4-5 parts of gean berry extract, 5-6 parts of olive saualane, 4-5 parts of glycolipid, three (octyldodecanol) citrates 4-5 parts, 3-4 parts of plant lanolin, 2-3 parts of plant wool oil, 5-6 parts of coconut oil ethylhexyl, 2-3 parts of Queensland nut seed oil, 2-3 parts of jojoba seed oil, 2-3 parts of seed oil, Viamerine 2500 4-5 part of two section shepherd's purse of deep-sea, three isostearate of polyglycereol -2 4-5 parts, 0.8-1 parts of glycerol caprylate, 5-6 parts of ethylhexyl palmitate, 0.1-0.5 parts of natural pigment color-change powder, Oil Yellow 0.01-0.02 parts, 0.05-0.2 parts of edible essence.
5. discoloration thousand according to claim 1 becomes lipstick, which is characterized in that the preparation of the gean berry extract Method includes the following steps:
(1) fruit of gean is taken, crushes, mixed with enzyme, obtain substance A;
(2) by substance A organic solvent ultrasonic extraction, filtering obtains filter residue B and liquor C;
(3) filter residue B is extracted with organic solvent, obtains substance D;
(4) liquor C and substance D are mixed, concentration, it is dry to get.
6. discoloration thousand according to claim 5 becomes lipstick, which is characterized in that the fruit of gean described in step (1) The real mass ratio with enzyme is 10-30:1, and hydrolysis temperature is 25-55 DEG C, adjusts pH value 4.0-6.0;Substance A described in step (2) Mass volume ratio with organic solvent is 1:50-100g/mL;The mass volume ratio of liquor B and organic solvent described in step (3) For 1:20-40g/mL.
7. discoloration thousand according to claim 5 becomes lipstick, which is characterized in that enzyme described in step (1) is pectase, fiber One or more of plain enzyme, protease, amylase;Organic solvent described in step (2) is formic acid and volume fraction is 70- The mixed solvent of 90% ethyl alcohol;The ethyl alcohol that organic solvent is acetone and volume fraction is 80-95% described in step (3) mixes Bonding solvent.
8. discoloration thousand according to claim 7 becomes lipstick, which is characterized in that the enzyme is cellulase, pectase, albumen The mixture of enzyme, amylase, the mass ratio of four kinds of enzymes are 1:2-3:0.5-1:1-2;The formic acid and volume fraction are 70-90% Ethyl alcohol volume ratio be 1:6-9;The volume ratio for the ethyl alcohol that the acetone and volume fraction are 80-95% is 1:2-4.
9. the preparation method that a kind of any one of claim 2-8 discoloration thousand becomes lipstick, which is characterized in that including walking as follows It is rapid:
Semi-finished product production:
S1 weighs natural pigment color-change powder, ethylhexyl palmitate, and mixing, grinding obtain substance A;
S2 weighs beeswax, babassu vegetable wax, sweet orange pericarp wax, gean berry extract, and mixing obtains substance B;
S3 weigh gean seed oil, olive saualane, glycolipid, three (octyldodecanol) citrates, plant lanolin, Plant wool oil, coconut oil ethylhexyl, Queensland nut seed oil, jojoba seed oil, two section shepherd's purse seed oil of deep-sea, Viamerine2500, three isostearate of polyglycereol -2, glycerol caprylate, mixing, obtain substance C;
S4 mixes substance B and substance C, adds substance A, and Oil Yellow, edible essence is added to get semi-finished product lipstick in homogeneous;
Finished product production:
By the semi-finished product lipstick pour into Rouge mold to get.
10. preparation method according to claim 9, which is characterized in that adding in step S1 described in semi-finished product manufacturing process It mixed, ground under heat condition, heating temperature is 70-80 DEG C, heating time 10-15min;It is being heated in the step S2 Under the conditions of mix, heating temperature be 85-90 DEG C, heating time 5-15min;It is mixed in a heated condition in the step S3, Heating temperature is 90-100 DEG C, heating time 10-15min;Substance B and substance C are mixed in the step S4, are cooled to 80-90 DEG C, add substance A, homogeneous is cooled to 70-80 DEG C, and Oil Yellow, edible essence is added, be cooled to 50-60 DEG C to get Semi-finished product lipstick;The semi-finished product lipstick is heated to 80-90 DEG C in the finished product manufacturing process, Rouge mold is poured into stirring In, be cooled to -4~-8 DEG C to get.
CN201910652174.9A 2019-07-18 2019-07-18 A kind of thousand change lipstick of red cherry discoloration and preparation method thereof eaten Pending CN110354033A (en)

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CN110840789A (en) * 2019-11-29 2020-02-28 广州那比昂生物科技有限公司 Color-changing lipstick containing plant pigment and preparation method thereof
CN111218129A (en) * 2020-03-12 2020-06-02 运城学院 Method for extracting sweet cherry pigment
CN111568810A (en) * 2020-05-19 2020-08-25 傅建斌 Edible velvet lipstick and preparation method thereof
CN112426389A (en) * 2020-12-15 2021-03-02 邓守毅 Production process of red cherry lipstick
CN112870116A (en) * 2021-03-22 2021-06-01 皖南医学院 Lip balm for moistening, preserving moisture and repairing lips, preparation method of lip balm, lip balm for moistening, preserving moisture and repairing lips and preparation method of lip balm

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CN112870116A (en) * 2021-03-22 2021-06-01 皖南医学院 Lip balm for moistening, preserving moisture and repairing lips, preparation method of lip balm, lip balm for moistening, preserving moisture and repairing lips and preparation method of lip balm

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