CN111568810A - Edible velvet lipstick and preparation method thereof - Google Patents

Edible velvet lipstick and preparation method thereof Download PDF

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Publication number
CN111568810A
CN111568810A CN202010424197.7A CN202010424197A CN111568810A CN 111568810 A CN111568810 A CN 111568810A CN 202010424197 A CN202010424197 A CN 202010424197A CN 111568810 A CN111568810 A CN 111568810A
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parts
edible
seed oil
lipstick
velvet
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Chinese (zh)
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傅建斌
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/347—Phenols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06—Lipsticks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/001—Preparations for care of the lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74—Biological properties of particular ingredients
    • A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782—Enzyme inhibitors; Enzyme antagonists

Abstract

The invention discloses an edible velvet lipstick, which relates to the technical field of cosmetics and is prepared from the following components: thickening agent, plant conditioning humectant, emollient, colorant, antioxidant, and edible essence. The lipstick disclosed by the invention is natural in gloss, soft in lip feel and good in moisturizing effect; meanwhile, because the raw materials adopted in the production are all pure natural products, no toxic chemical additive is used, the product can be eaten, the taste is relatively proper, and the product also has the health care, eating and moistening effects.

Description

Edible velvet lipstick and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to an edible velvet lipstick and a preparation method thereof.
Background
The hottest word in the beauty industry in 2019 is CBD (cannabidiol), from Unilever to asherian (EsteeLauder), eurey (L' oreal CO.), and traditional beauty and personal care companies are catching up with the "most important trend in the next 10 years": CBD makes skin and protects skin.
Cannabidiol (CBD) is a compound naturally occurring in the flowers of cannabis, a long history of cannabis as a drug dating back several thousand years ago. Today, the therapeutic properties of CBD are being tested and confirmed by scientists and physicians around the world. CBD is a safe, non-addictive substance. Is one of over one hundred "phytocannabinoids". These "phytocannabinoids" are characteristic of cannabis and confer a powerful therapeutic effect on cannabis. By digging deeply into our physiological functions, CBD can relieve chronic pain, anxiety, inflammation, depression and many other symptoms.
Many lipsticks are inedible depending on their ingredients, and typical preservatives used for lipsticks are methyl paraben and propyl paraben, most of which are organic synthetic pigments or inorganic pigments, most of which are mineral waxes and synthetic waxes, and most of which are mineral oils which may cause serious harm to the body if used for a long time.
To remedy the deficiencies of the prior art, the lipstick made in accordance with the present invention is primarily composed of hemp seed oil, primarily extracted from the leaves and stems of the hemp plant, also known as hemp (CANNABIS SATIVA) seed oil, which is commonly described as "super food" and contains important nutritional components including amino acids, fibers, Omega-3 and Omega-6 fatty acids, as well as a range of important vitamins and minerals. Researches show that the hemp seed oil has obvious effects on reducing cholesterol, resisting oxidation, eliminating free radicals in human bodies and the like, is safe and nontoxic, and is functional grease with high utilization value. Other raw materials adopted in the production are all pure natural vegetable oil raw materials.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide the edible velvet lipstick and the preparation method thereof, so that the prepared lipstick has silky and soft lip feeling, rich and full color and luster and good moisturizing effect; meanwhile, because the raw materials adopted in the production are all pure natural products, no toxic chemical additive is used, the product can be eaten, the taste is relatively proper, and the product also has the health care, eating and moistening effects.
In order to achieve the purpose, the invention adopts the following technical scheme:
an edible velvet lipstick and a preparation method thereof, wherein the edible velvet lipstick comprises the following components: thickening agent, plant conditioning humectant, emollient, colorant, antioxidant, and edible essence.
Preferably, the thickener is a mixture of candelilla wax, beeswax, carnauba wax and glycolipids.
Preferably, the plant conditioning moisturizer is hemp seed oil, cannabidiol, cocoa butter, gardenia oil, carrot seed oil, macadamia nut seed oil, jojoba seed oil and crambe abyssinica seed oil.
Preferably, the emollient is: the plant lanolin comprises the following components: avocado fat: 47 parts of glyceryl rosinate: 48 parts of olive oil unsaponifiable matter and 5 parts of olive oil unsaponifiable matter. Is natural semi-solid lanolin substitute. Has similar appearance and properties to lanolin. Water retention, moisture retention and stabilization of the emulsification system. By oral mucosal irritation test. Ecosert state: is recognized as a natural raw material.
Preferably, the colorant is edible pigment, and the plant pigment is capsanthin, carotene, lycopene or seabuckthorn yellow pigment. The color number of the pigment is: CI15850, CI 19140, CI 45410 and CI45380 are one or a mixture of colors.
Preferably, the antioxidant is tocopherol, a fat-soluble vitamin, the hydrolysate of which is tocopherol, being one of the most predominant antioxidants. The tocopherol can promote the secretion of sex hormone, so that the vitality and the quantity of sperms of the male are increased; increase female estrogen concentration, improve fertility, prevent abortion, and can be used for preventing and treating male infertility, burn, cold injury, capillary hemorrhage, climacteric syndrome, and skin care.
Preferably, the edible essence is edible essence (material), and the fragrance type is one or two mixed fragrance types of strawberry, juicy peach, apple, chocolate, orange and grape.
Preferably, the hemp seed oil is extracted mainly from the flower leaves and stems of the hemp plant, also known as hemp seed oil, generally described as "super food", containing important nutritional components including amino acids, fibers, Omega-3 and Omega-6 fatty acids, as well as a range of important vitamins and minerals. Researches show that the hemp seed oil has obvious effects on reducing cholesterol, resisting oxidation, eliminating free radicals in human bodies and the like, is safe and nontoxic, and is functional grease with high utilization value.
Preferably, cannabidiol, also known as cannabis leaf extract, is a compound naturally occurring in the flowers of cannabis sativa, which has a long history as a drug dating back several thousand years ago. Today, the therapeutic properties of CBD are being tested and confirmed by scientists and physicians around the world. CBD is a safe, non-addictive substance. Is one of over one hundred "phytocannabinoids". These "phytocannabinoids" are characteristic of cannabis and confer a powerful therapeutic effect on cannabis. By digging deeply into our physiological functions, CBD can relieve chronic pain, anxiety, inflammation, depression and many other symptoms.
Preferably, the candelilla wax is a natural plant wax, and the candelilla wax is extracted from the bark of the particular candelilla shrub in northern mexico, southern texas, california, and the like.
The beeswax is also called beeswax, and is a fatty substance secreted by 4 pairs of wax glands on the abdomen of worker bees of the proper age in a bee colony.
The carnauba wax is very hard in texture, has extremely high gloss, is extremely easy to emulsify, has good oil retention, and has the greatest advantage of having extremely high gloss and extraordinary hardness which are not possessed by other waxes. In addition, it has polishing property, which makes it an indispensable natural raw material in the industries of candy production, pharmacy, leather and the like.
The glycolipid is also a component constituting a cell membrane, is associated with cell recognition and surface antigenicity, and functions as a lip protection film in lipstick.
The cocoa seed butter is excellent basic oil of cosmetics, can nourish skin, and has good permeability. The extract can promote skin metabolism, and has anti-aging effect in combination with antioxidant effect; can inhibit histamine release, and has anti-allergy and relieving effects; has inhibitory effect on metalloprotease, and has anti-inflammatory effect.
The flower oil of Gardenia jasminoides is a unique flower of Hill, is a precious source of active substances, is also an important plant recorded in the traditional Boriniya pharmacopoeia, and the original resident of Boriniya prepares the Tilia flower into a medicament capable of treating migraine, earache, wound and mosquito and insect bite, and can even be used for treating eczema. The Tarsie gardenia oil is very easy to be absorbed by the skin, is a good product for repairing the skin after being exposed to the sun, is also a very excellent natural moisturizing product, can obtain the evidence from the glittering healthy and glossy skin of a creek female and silky smooth skin, is lipophilic vegetable oil, can be used in the formula of a soothing, detoxifying and purifying skin care product, and has the moisturizing and repairing properties.
The carrot seed oil has strong oxidation resistance, has an effect of eliminating singlet oxygen, can be used as an auxiliary antioxidant for cosmetics, can promote the proliferation of fibroblasts, inhibit the activity of collagenase, and can resist ageing and wrinkle; has effect in inhibiting melanocyte activity, and can be used for whitening skin; meanwhile, the moisturizing cream has a good moisturizing effect.
The macadamia nut seed oil is also called as macadamia nut oil, contains high amount of oil, is especially characterized by being rich in unsaturated fatty acid, mainly contains oleic acid and palmitic acid, is edible nut with better quality in the world, is called as 'dried fruit queen' and 'king of nut in the world' in vegetarian, can prevent heart disease, can regulate and control blood sugar level and improve lipid metabolism of diabetics, and is a good fat supplement source for the diabetics. Can also effectively moisturize and protect the skin, and is a good sunscreen and skin-care product.
The jojoba seed oil, also called jojoba oil, is obtained from jojoba fruit, has unsaturated higher alcohol and fatty acid as main ingredients, has good stability, is easy to fuse with skin, has superior oxidation resistance, and contains abundant vitamins, and has effects of nourishing and softening skin.
The crambe seed oil in the deep sea, also called crambe seed oil, is rich in oil nutrient components, can enable the skin to be balanced and moisturized and keep healthy, can strengthen the delicate cell membrane, enables the cells to obtain sufficient nourishment, and effectively removes wastes in the cells; has good dispersibility, and can be used as emollient.
An edible velvet lipstick is characterized in that the edible velvet lipstick is prepared from edible oil, natural edible wax and natural pigment.
The paint specifically comprises the following components in parts by weight: 25-30 parts of hemp seed oil, 0.5-1 part of cannabidiol, 8-10 parts of candelilla wax, 5-7 parts of beeswax, 5-7 parts of carnauba wax, 4-5 parts of glycolipid, 5-7 parts of cocoa seed fat, 5-6 parts of flower oil of gardenia schidigera, 5-6 parts of carrot seed oil, 6-8 parts of macadamia nut seed oil, 6-8 parts of jojoba seed oil, 6-8 parts of crambe abyssinica seed oil, 5-8 parts of vegetable lanolin, 3-4 parts of edible pigment, 0.5-1 part of tocopherol and 0.1-0.2 part of edible essence.
Preferably, the preparation method of cannabidiol extraction comprises the following steps:
(1) pulverizing flower, leaf and fruit of Cannabis plant, and mixing with enzyme to obtain substance A;
(2) ultrasonically extracting the substance A with an organic solvent, and filtering to obtain filter residue B and filtrate C;
(3) extracting the filter residue B with an organic solvent to obtain a substance D;
(4) mixing the filtrate C and the substance D, concentrating, and drying.
The cannabidiol is extracted from flowers, leaves and fruits of cannabis plants, has high nutritive value, and is beneficial to health.
More preferably, the mass ratio of the flowers, leaves and fruits of the cannabis plant to the enzyme in the step (1) is 10-30:1, the enzymolysis temperature is 25-55 ℃, and the pH value is adjusted to 4.0-6.0.
More preferably, the mass-to-volume ratio of the substance A to the organic solvent in the step (2) is 1:50-100 g/mL.
More preferably, the mass-to-volume ratio of the filtrate B to the organic solvent in the step (3) is 1:20-40 g/mL.
More preferably, the enzyme in step (1) is one or more of pectinase, cellulase, protease and amylase.
More preferably, the enzyme in the step (1) is a mixture of cellulase, pectinase, protease and amylase, and the mass ratio of the four enzymes is 1:2-3:0.5-1: 1-2.
More preferably, the organic solvent in step (2) is a mixed solvent of formic acid and ethanol with a volume fraction of 70-90%.
More preferably, the organic solvent in the step (2) is a mixed solvent of formic acid and ethanol with the volume fraction of 70-90%, and the volume ratio of the formic acid to the ethanol with the volume fraction of 70-90% is 1: 6-9.
More preferably, the ultrasonic power in step (2) is 100-300w, and the ultrasonic time is 20-40 min.
More preferably, the organic solvent in the step (3) is a mixed solvent of acetone and 80-95% by volume of ethanol.
More preferably, the organic solvent in the step (3) is a mixed solvent of acetone and 80-95% by volume of ethanol, and the volume ratio of the acetone to the 80-95% by volume of ethanol is 1: 2-4.
The invention also discloses a preparation method of the edible velvet lipstick, which comprises the following steps:
1) weighing edible pigment and the hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists during grinding, thus preparing the hemp seed oil color paste.
2) Weighing candelilla wax, beeswax, carnauba wax, cannabidiol, glycolipid, cannabis sativa seed oil, cocoa butter, flower oil of cape jasmine, carrot seed oil, macadamia nut seed oil, jojoba seed oil, crambe seed oil, plant lanolin, tocopherol and edible essence according to the mass ratio, mixing and heating until the components are completely dissolved, then cooling the temperature to 75 ℃, adding the cannabis sativa seed oil color paste prepared in the step 1), mixing and stirring uniformly, adding cannabidiol at 65 ℃, mixing and stirring uniformly, and then cooling the temperature to 55 ℃ to prepare a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, taking out the lipstick mold, and demolding to obtain the edible velvet lipstick.
The invention has the beneficial effects that:
1. since cannabidiol can be used to help treat various other diseases, for example: seizures, inflammatory pain, psychosis or psychiatric disorders, inflammatory bowel disease, nausea, migraine, depression, anxiety, pain, muscle spasm, glaucoma, insomnia, anorexia, and the like. Therefore, the use of lipstick containing cannabidiol can inhibit and relieve the above mental disorders, inflammatory bowel disease, nausea, migraine, depression, anxiety, pain, muscle spasm, glaucoma, insomnia, anorexia, etc.
2. Hemp seed contains about 25-35% of oil, 20-25% of protein, 20-30% of carbohydrate, and abundant trace elements. The content of unsaturated fatty acids in the hemp seed oil is about 90%, wherein the content of essential fatty acids is about 80%. The ratio of omega-6 to omega-3 polyunsaturated fatty acids is about 3: 1, which is the ideal ratio for human fatty acid intake, and also contains gamma-linolenic acid and abundant tocopherols and phytosterols. Researches show that the hemp seed oil has obvious effects on reducing cholesterol, resisting oxidation, eliminating free radicals in human bodies and the like, is safe and nontoxic, and is functional grease with high utilization value.
3. The edible pigment toner is a colored toner extracted from roots, stems, leaves, flowers or fruits of plants, and can be converted into a mutagen under ultraviolet irradiation to cause cancer relative to a chemically synthesized artificial toner, and the plant toner does not contain heavy metal and preservatives harmful to human bodies, does not produce any side effect on human bodies, has quick metabolism even if being absorbed by the human bodies, high safety, matte color and luster, high plumpness and good coloring effect; the moisture of the lip skin is easy to evaporate into the air, the natural vegetable oil can be used for keeping the moisture of the skin, the moisture is stably locked in the skin for a long time and is not lost, the natural vegetable oil is milder and has no stimulation compared with the common components such as mineral oil, glycerin and the like, the moisturizing function is enhanced, and the natural vegetable oil becomes a barrier for locking the evaporation of free water on the basis of not hindering the breathing of the lip skin; compared with the prior art, the lipstick disclosed by the invention is natural in gloss, soft in lip feel and good in moisturizing effect; meanwhile, because the raw materials adopted in the production are all pure natural products, no toxic chemical additive is used, the product can be eaten, the taste is relatively proper, and the product also has the health care, eating and moistening effects.
Detailed Description
The invention will be further described with reference to specific embodiments, and the advantages and features of the invention will become apparent as the description proceeds. These examples are illustrative only and do not limit the scope of the present invention in any way. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Example 1
The edible velvet lipstick comprises the following components in parts by weight: 25.9 parts of hemp seed oil, 1 part of Cannabidiol (CBD), 8 parts of candelilla wax, 7 parts of beeswax, 7 parts of carnauba (Copelicia CERIFERA) wax, 4 parts of glycolipid, 5 parts of cocoa (Theobroma CACAO) seed fat, 6 parts of flower oil of Gardenia jasminoides Ellis (GARDENIA TAHITENSIS), 6 parts of carrot (Daucus CAROTA SATIVA) seed oil, 6 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 6 parts of jojoba (Simdsia CHINENSIS) seed oil, 6 parts of CRAMBE ABYSSINICA (Crambe ABYSSINICA) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 1 part of tocopherol (vitamin E) and 0.1 part of edible essence (material).
The method for preparing Cannabidiol (CBD) extract comprises the following steps:
(1) pulverizing flower, leaf and fruit of Cannabis plant, and mixing with enzyme to obtain substance A;
(2) ultrasonically extracting the substance A with an organic solvent, and filtering to obtain filter residue B and filtrate C;
(3) extracting the filter residue B with an organic solvent to obtain a substance D;
(4) mixing the filtrate C and the substance D, concentrating, and drying.
The preparation method of the edible velvet lipstick comprises the following steps:
1) weighing edible pigment and the hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists during grinding, thus preparing the hemp seed oil color paste.
2) Weighing candelilla wax, beeswax, carnauba (Copellicia CERIFERA) wax, Cannabidiol (CBD), glycolipid, cannabis SATIVA oil, cocoa (Theobroma CACACAAO) seed fat, Gardenia jasminoides ellis (GARDENIA TAHITENSIS) flower oil, carrot (Daucus CAROTA SATIVA) seed oil, macadamia nut (MACADAMIA TERNIFOLIA) seed oil, jojoba (Simmondsia CHINENSIS) seed oil, CRAMBE ABYSSINICA (Crabyssinica) seed oil, vegetable lanolin, tocopherol (vitamin E) and edible essence according to the mass ratio, mixing and heating until the mixture is completely dissolved, then cooling to 75 ℃, adding the cannabis SATIVA color paste prepared in the step 1) into the mixture and mixing and stirring uniformly, adding Cannabidiol (CBD) at 65 ℃, mixing and stirring uniformly, and then cooling to 55 ℃, and preparing a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, taking out the lipstick mold, and demolding to obtain the edible velvet lipstick.
Example 2
The edible velvet lipstick comprises the following components in parts by weight: the components by weight ratio are as follows: 28 parts of hemp seed oil, 0.5 part of Cannabidiol (CBD), 9 parts of candelilla wax, 7 parts of beeswax, 5.8 parts of carnauba (Copellicia CERIFERA) wax, 4 parts of glycolipid, 6 parts of cocoa (Theobroma CACAO) seed fat, 6 parts of flower oil of Gardenia tashaiensis (GARDENIA TAHITENSIS), 8 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 8 parts of jojoba (Simmondsia CHINENSIS) seed oil, 8 parts of CRAMBE abysica (Crambe abysica) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 0.5 part of tocopherol (vitamin E) and 0.2 part of edible essence (material).
The method for preparing Cannabidiol (CBD) extract comprises the following steps:
(1) pulverizing flower, leaf and fruit of Cannabis plant, and mixing with enzyme to obtain substance A;
(2) ultrasonically extracting the substance A with an organic solvent, and filtering to obtain filter residue B and filtrate C;
(3) extracting the filter residue B with an organic solvent to obtain a substance D;
(4) mixing the filtrate C and the substance D, concentrating, and drying.
A preparation method of edible velvet lipstick comprises the following steps:
1) weighing edible pigment and the hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists during grinding, thus preparing the hemp seed oil color paste.
2) Weighing candelilla wax, beeswax, carnauba (Copellicia CERIFERA) wax, Cannabidiol (CBD), glycolipid, cannabis SATIVA oil, cocoa (Theobroma CACACAAO) seed fat, Gardenia jasminoides ellis (GARDENIA TAHITENSIS) flower oil, carrot (Daucus CAROTA SATIVA) seed oil, macadamia nut (MACADAMIA TERNIFOLIA) seed oil, jojoba (Simmondsia CHINENSIS) seed oil, CRAMBE ABYSSINICA (Crabyssinica) seed oil, vegetable lanolin, tocopherol (vitamin E) and edible essence according to the mass ratio, mixing and heating until the mixture is completely dissolved, then cooling to 75 ℃, adding the cannabis SATIVA color paste prepared in the step 1) into the mixture and mixing and stirring uniformly, adding Cannabidiol (CBD) at 65 ℃, mixing and stirring uniformly, and then cooling to 55 ℃, and preparing a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, taking out the lipstick mold, and demolding to obtain the edible velvet lipstick.
Example 3
The edible velvet lipstick comprises the following components in parts by weight: the components by weight ratio are as follows: 29 parts of hemp seed oil, 0.5 part of Cannabidiol (CBD), 9 parts of candelilla wax, 7 parts of beeswax, 5.8 parts of carnauba (Copelicia CERIFERA) wax, 4 parts of glycolipid, 5 parts of cocoa (Theobroma CACAO) seed fat, 6 parts of flower oil of Gardenia tasajia (GARDENIA TAHITENSIS), 6 parts of carrot (Daucus CAROTA SATIVA) seed oil, 6 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 6 parts of jojoba (SIMDSIA CHINENSIS) seed oil, 6 parts of CRAMBE ABYSSINICA (Crambre ABYSSINICA) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 0.5 part of tocopherol (vitamin E) and 0.2 part of edible essence (material).
Wherein the edible pigment is capsanthin, carotene, lycopene, and seabuckthorn yellow. The color number of the pigment is: a mixture of CI15850, CI 19140, CI 45410 and CI45380 in a mass ratio of 2: 1:1: 2;
the method for preparing Cannabidiol (CBD) extract comprises the following steps:
(1) pulverizing flowers, leaves and fruits of cannabis plants, mixing with enzyme at a mass ratio of 20:1, and performing enzymolysis at 40 deg.C to obtain substance A, wherein the enzyme is a mixture of cellulase, pectinase, protease and amylase, and the mass ratio of the four enzymes is 1:3:0.5: 1;
(2) ultrasonically extracting the substance A by using an organic solvent according to the mass volume ratio of 1:70g/mL, wherein the ultrasonic power is 200w, the ultrasonic time is 30min, and filtering to obtain filter residue B and filtrate C, wherein the organic solvent is a mixed solvent of formic acid and ethanol with the volume fraction of 80%, and the volume ratio of the two is 1: 8;
(3) extracting the filter residue B by using an organic solvent according to the mass volume ratio of 1:30g/mL to obtain a substance D, wherein the organic solvent is a mixed solvent of acetone and 90% ethanol by volume fraction, and the volume ratio of the acetone to the ethanol is 1: 3;
(4) mixing the filtrate C and the substance D, concentrating, and drying.
A preparation method of edible velvet lipstick comprises the following steps:
1) weighing edible pigment and the hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists during grinding, thus preparing the hemp seed oil color paste.
2) Weighing candelilla wax, beeswax, carnauba (Copellicia CERIFERA) wax, Cannabidiol (CBD), glycolipid, cannabis SATIVA oil, cocoa (Theobroma CACACAAO) seed fat, Gardenia jasminoides ellis (GARDENIA TAHITENSIS) flower oil, carrot (Daucus CAROTA SATIVA) seed oil, macadamia nut (MACADAMIA TERNIFOLIA) seed oil, jojoba (Simmondsia CHINENSIS) seed oil, CRAMBE ABYSSINICA (Crabyssinica) seed oil, vegetable lanolin, tocopherol (vitamin E) and edible essence according to the mass ratio, mixing and heating until the mixture is completely dissolved, then cooling to 75 ℃, adding the cannabis SATIVA color paste prepared in the step 1) into the mixture and mixing and stirring uniformly, adding Cannabidiol (CBD) at 65 ℃, mixing and stirring uniformly, and then cooling to 55 ℃, and preparing a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, taking out the lipstick mold, and demolding to obtain the edible velvet lipstick.
Example 4
The edible velvet lipstick comprises the following components in parts by weight: the components by weight ratio are as follows: 30 parts of hemp seed oil, 1 part of Cannabidiol (CBD), 8 parts of candelilla wax, 5 parts of beeswax, 6 parts of carnauba (Copelicia CERIFERA) wax, 4 parts of glycolipid, 5 parts of cocoa (Theobroma CACAO) seed fat, 6 parts of flower oil of Gardenia tassella (GARDENIA TAHITENSIS), 6 parts of carrot (Daucus CAROTA SATIVA) seed oil, 6 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 6.9 parts of jojoba (Simmondsia CHINENSIS) seed oil, 6 parts of CRAMBE ABYSSINICA (Crabyssinica) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 1 part of tocopherol (vitamin E) and 0.1 part of edible essence (material).
The method for preparing Cannabidiol (CBD) extract comprises the following steps:
(1) pulverizing flowers, leaves and fruits of cannabis plants, mixing with enzyme at a mass ratio of 15:1, and performing enzymolysis at 40 deg.C to obtain substance A, wherein the enzyme is a mixture of cellulase, pectinase, protease and amylase, and the mass ratio of the four enzymes is 1:2.5:1: 2;
(2) ultrasonically extracting the substance A by using an organic solvent according to the mass volume ratio of 1:60g/mL, wherein the ultrasonic power is 200w, the ultrasonic time is 30min, and filtering to obtain filter residue B and filtrate C, wherein the organic solvent is a mixed solvent of formic acid and ethanol with the volume fraction of 85%, and the volume ratio of the two is 1: 8;
(3) extracting the filter residue B by using an organic solvent according to the mass volume ratio of 1:30g/mL to obtain a substance D, wherein the organic solvent is a mixed solvent of acetone and 90% ethanol by volume fraction, and the volume ratio of the acetone to the ethanol is 1: 3;
(4) mixing the filtrate C and the substance D, concentrating, and drying.
A preparation method of edible velvet lipstick comprises the following steps:
1) weighing edible pigment and the hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists during grinding, thus preparing the hemp seed oil color paste.
2) Weighing candelilla wax, beeswax, carnauba (Copellicia CERIFERA) wax, Cannabidiol (CBD), glycolipid, cannabis SATIVA oil, cocoa (Theobroma CACACAAO) seed fat, Gardenia jasminoides ellis (GARDENIA TAHITENSIS) flower oil, carrot (Daucus CAROTA SATIVA) seed oil, macadamia nut (MACADAMIA TERNIFOLIA) seed oil, jojoba (Simmondsia CHINENSIS) seed oil, CRAMBE ABYSSINICA (Crabyssinica) seed oil, vegetable lanolin, tocopherol (vitamin E) and edible essence according to the mass ratio, mixing and heating until the mixture is completely dissolved, then cooling to 75 ℃, adding the cannabis SATIVA color paste prepared in the step 1) into the mixture and mixing and stirring uniformly, adding Cannabidiol (CBD) at 65 ℃, mixing and stirring uniformly, and then cooling to 55 ℃, and preparing a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, taking out the lipstick mold, and demolding to obtain the edible velvet lipstick.
Comparative example 1
The difference from the embodiment 4 is only that the weight parts of the components are different, and the rest conditions are the same, and the specific points are as follows:
30 parts of hemp seed oil, 1 part of Cannabidiol (CBD), 8 parts of candelilla wax, 5 parts of beeswax, 6 parts of carnauba (Copelicia CERIFERA) wax, 4 parts of glycolipid, 5 parts of cocoa (Theobroma CACAO) seed fat, 6 parts of flower oil of Gardenia tassella (GARDENIA TAHITENSIS), 6 parts of carrot (Daucus CAROTA SATIVA) seed oil, 6 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 6.9 parts of jojoba (Simmondsia CHINENSIS) seed oil, 6 parts of CRAMBE ABYSSINICA (Crabyssinica) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 1 part of tocopherol (vitamin E) and 0.1 part of edible essence (material).
Comparative example 2
The only difference from example 4 is that no carrot (Daucus CAROTA SATIVA) seed oil was added, and the conditions were the same.
Comparative example 3
The difference from the example 4 is only that in the preparation process of the Cannabidiol (CBD) extract, the mass ratio of the cellulase, the pectinase, the protease and the amylase in the step (1) is 1:1:2:3, and the rest conditions are the same.
Comparative example 4
The only difference from example 4 is that in the preparation of the Cannabidiol (CBD) extract, the volume ratio of formic acid and 85% volume fraction ethanol in step (2) is 1:2, and the rest conditions are the same.
Comparative example 5
The only difference from example 4 is that in the preparation of Cannabidiol (CBD) extract, the volume ratio of acetone to 90% volume fraction ethanol in step (3) is 2:1, and the rest conditions are the same.
Comparative example 6
The difference from example 4 is only that the feeding sequence of each raw material is different in the preparation process of the edible velvet lipstick, and the rest conditions are the same.
8 parts of candelilla wax, 5 parts of beeswax, 6 parts of carnauba (copericia CERIFERA) wax, 4 parts of glycolipid, 5 parts of cocoa (THEOBROMA CACAO) seed fat, 30 parts of hemp seed oil, 6 parts of flower oil of gardenia (GARDENIA TAHITENSIS), 6 parts of carrot (DAUCUS CAROTA SATIVA) seed oil, 6 parts of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 6.9 parts of jojoba (SIMMONDSIA CHINENSIS) seed oil, 6 parts of CRAMBE ABYSSINICA (CRAMBE ABYSSINICA) seed oil, 5 parts of vegetable lanolin, 4 parts of edible pigment, 1 part of tocopherol (vitamin E), 0.1 part of edible essence (material) and 1 part of Cannabidiol (CBD).
Test example 1
The products prepared in examples 1 to 4 and comparative examples 1 to 6 were subjected to a moisturizing efficacy test, which was performed by referring to "guide for evaluating moisturizing efficacy of cosmetic QB/T4256-2011", and skin moisture content was measured 30min, 60min and 120min after application using a Corneometer moisture test probe of a moisture tester CK MPA10, respectively, and the results are shown in table 1.
Table 1 product moisturization efficacy testing
Figure BDA0002498048850000141
Figure BDA0002498048850000151
Test example 2 acute oral toxicity test
100 healthy mice, male and female halves, were randomly selected and divided into 10 groups of 10 mice each (each of examples 1-4 and comparative examples 1-6), fasted for 16h without restriction of water. The dose of lipstick administered to each mouse was 0, 1000mg/kg, 3000mg/kg, 4000mg/kg, 5000mg/kg, respectively. The lipstick was administered to mice in one time by oral administration, and then the general state, toxic manifestation and death of the mice were closely observed and recorded for 14 days. After 14 days, all groups of test mice have normal water intake and food intake, have no poisoning and death condition, have normal skin, hair and eyes, and have no phenomena of tremor, convulsion, diarrhea, coma and the like. The acute toxicity grading marks show that the half oral lethal dose LD of the test object is more than or equal to 5000mg/kg and is actually nontoxic, the maximum dose group in the test is 5000mg/kg, animal death does not occur, and the half oral lethal dose is more than 5000mg/kg, so that the lipsticks prepared in the examples 1-4 and the comparative examples 1-6 can be determined to be actually nontoxic and can be used for human body tests.
Test example 3 sensory evaluation
100 female volunteers with healthy lips were selected and randomly divided into 10 groups of 10 persons, and the lipsticks of examples 1-4 and comparative examples 1-6 were tried respectively, without any lip care product on the day before trial, continuously used for 1 week for 3 times a day, once in the morning, at noon and evening, and used for the same time. And (4) scoring the ductility, the viscosity, the moistening and the discoloration effects of the product, and taking an average value. Grading standard: 5 points- -very satisfactory; 4 min-satisfaction; 3 minutes- -general; score 2- -unsatisfied; score 1- -very unsatisfactory. The results are shown in Table 2.
TABLE 2 sensory evaluation results of the products
Figure BDA0002498048850000161
The technical means disclosed by the scheme of the invention are not limited to the technical means disclosed by the technical means, and the technical scheme also comprises the technical scheme formed by any combination of the technical characteristics. While the foregoing is directed to embodiments of the present invention, it will be appreciated by those skilled in the art that various changes may be made in the embodiments without departing from the principles of the invention, and that such changes and modifications are intended to be included within the scope of the invention.

Claims (10)

1. An edible velvet lipstick is characterized by being prepared from the following components: thickening agent, plant conditioning humectant, emollient, colorant, antioxidant, and edible essence.
2. An edible velvet lipstick according to claim 1 wherein said thickening agent is a mixture of candelilla wax, beeswax, carnauba wax and glycolipids; the plant conditioning humectant consists of hemp seed oil, cannabidiol, cocoa butter, flower oil of Gardenia jasminoides Ellis, carrot seed oil, macadamia nut seed oil, jojoba seed oil and two sections of deep sea camelina sativa seed oil; the emollient is vegetable lanolin; the colorant is edible pigment; the antioxidant is tocopherol.
3. The edible velvet lipstick according to claim 2, wherein the edible pigments are capsanthin, carotene, lycopene, seabuckthorn yellow; the color number of the pigment is: CI15850, CI 19140, CI 45410 and CI45380 are one or a mixture of colors.
4. The edible velvet lipstick according to claim 2, which is prepared from the following components in parts by weight: 25-30 parts of hemp seed oil, 0.5-1 part of cannabidiol, 8-10 parts of candelilla wax, 5-7 parts of beeswax, 5-7 parts of carnauba wax, 4-5 parts of glycolipid, 5-7 parts of cocoa seed fat, 5-6 parts of flower oil of gardenia schidigera, 5-6 parts of carrot seed oil, 6-8 parts of macadamia nut seed oil, 6-8 parts of jojoba seed oil, 6-8 parts of crambe abyssinica seed oil, 5-8 parts of vegetable lanolin, 3-4 parts of edible pigment, 0.5-1 part of tocopherol and 0.1-0.2 part of edible essence.
5. The edible velvet lipstick according to claim 4, wherein the vegetable lanolin is composed of the following components in parts by weight: 47 parts of avocado fat, 48 parts of glyceryl rosinate and 5 parts of olive oil unsaponifiable matter.
6. The edible velvet lipstick according to claim 1, wherein the cannabidiol extract is prepared by a method comprising the steps of:
(1) pulverizing flower, leaf and fruit of Cannabis plant, and mixing with enzyme to obtain substance A;
(2) ultrasonically extracting the substance A with an organic solvent, and filtering to obtain filter residue B and filtrate C;
(3) extracting the filter residue B with an organic solvent to obtain a substance D;
(4) mixing the filtrate C and the substance D, concentrating, and drying to obtain cannabidiol.
7. The edible velvet lipstick according to claim 6, wherein the mass ratio of the flowers, leaves, fruits and enzymes of the cannabis plant in the step (1) is 10-30:1, the enzymolysis temperature is 25-55 ℃, and the pH value is adjusted to 4.0-6.0; the mass-volume ratio of the substance A to the organic solvent in the step (2) is 1:50-100 g/mL; the mass-volume ratio of the filtrate B to the organic solvent in the step (3) is 1:20-40 g/mL.
8. The edible velvet lipstick according to claim 6, wherein the enzyme in step (1) is one or more of pectinase, cellulase, protease and amylase; the organic solvent in the step (2) is a mixed solvent of formic acid and ethanol with the volume fraction of 70-90%; the organic solvent in the step (3) is a mixed solvent of acetone and 80-95% of ethanol by volume fraction.
9. The edible velvet lipstick according to claim 6, wherein the enzyme is a mixture of cellulase, pectinase, protease and amylase, and the mass ratio of the four enzymes is 1:2-3:0.5-1: 1-2; the volume ratio of the formic acid to the ethanol with the volume fraction of 70-90% is 1: 6-9; the volume ratio of the acetone to the ethanol with the volume fraction of 80-95% is 1: 2-4.
10. A method of preparing an edible velvet lipstick according to any one of claims 2-9, comprising the steps of:
1) weighing edible pigment and hemp seed oil, mixing and stirring according to the mass ratio of 1:4, and then circularly grinding by using a colloid mill until no granular sensation exists in grinding to prepare hemp seed oil color paste;
2) weighing candelilla wax, beeswax, carnauba wax, cannabidiol, glycolipid, cannabis sativa seed oil, cocoa butter, flower oil of cape jasmine, carrot seed oil, macadamia nut seed oil, jojoba seed oil, crambe seed oil, plant lanolin, tocopherol and edible essence according to the mass ratio, mixing and heating until the components are completely dissolved, then cooling the temperature to 75 ℃, adding the cannabis sativa seed oil color paste prepared in the step 1), mixing and stirring uniformly, adding cannabidiol at 65 ℃, mixing and stirring uniformly, and then cooling the temperature to 55 ℃ to prepare a semi-finished lipstick paste;
3) stirring and heating the semi-finished lipstick body prepared in the step 2) to 80-90 ℃ until the lipstick body is dissolved;
4) pouring the mixture dissolved in the step 3) into a lipstick mold, keeping for 7-15 seconds, cooling to-3 to-9 ℃, cooling for 5 minutes, taking out the lipstick mold, demolding, inserting a lipstick tube, and pulling out to obtain the edible velvet lipstick.
CN202010424197.7A 2020-05-19 2020-05-19 Edible velvet lipstick and preparation method thereof Pending CN111568810A (en)

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CN103494739A (en) * 2013-09-29 2014-01-08 娇时化妆品（杭州）有限公司 Plant essence type rouge allure lipstick
CN108125808A (en) * 2017-12-25 2018-06-08 广州丽彦妆生物科技有限公司 A kind of oil and fat of sacha inchi edible health moistens lipstick and preparation method thereof
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Application publication date: 20200825