CN106074280A - The preparation method and applications of purple Chinese cabbage anthocyanidin - Google Patents
The preparation method and applications of purple Chinese cabbage anthocyanidin Download PDFInfo
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- CN106074280A CN106074280A CN201610550074.1A CN201610550074A CN106074280A CN 106074280 A CN106074280 A CN 106074280A CN 201610550074 A CN201610550074 A CN 201610550074A CN 106074280 A CN106074280 A CN 106074280A
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- chinese cabbage
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention provides the preparation method and applications of purple Chinese cabbage anthocyanidin, be applied particularly to the preparation of antioxidation cosmetic product and color make-up.The preparation method of purple Chinese cabbage anthocyanidin is: break into serosity after being cleaned by purple Chinese cabbage, adds ethanol solution, regulates PH, extracts 6h, extracts 2 times, and centrifugation goes out supernatant, concentrating under reduced pressure, purification, lyophilization, makes lyophilized powder.Purple Chinese cabbage anthocyanidin is a kind of antioxidant being effective against free radical, can prevent skin from crossing presenility, and oxidation resistance is apparently higher than vitamin C and vitamin E.Purple Chinese cabbage anthocyanidin is alternatively arranged as a kind of natural pigment and adds in cosmetics, plays the effect of skin protection and coloring simultaneously.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to the preparation method and applications of purple Chinese cabbage anthocyanidin.
Background technology
The rich content of anthocyanidin in purple Chinese cabbage, its extraction and purification process is ripe, low cost, and is applied to cosmetics
In can play good cosmetology effect, therefore from purple Chinese cabbage, extract anthocyanidin be applied in cosmetics to have very
Wide application prospect.
Skin is directly exposed in external environment, subjects the oxidative pressure from external environment.Ultraviolet (UV), chemistry
The oxidative pressure such as material, environmental pollution makes skin be highly prone to oxidative damage, and when using antioxidation cosmetic product, people are universal
A kind of antioxidation means selected.And the selection for antioxidant is just particularly important.The better antioxidant of effect is such as
It is on the high side for superoxides gasification enzyme, and its effect of cheap vitamin E is the most less obvious.
Pigment used by cosmetics is generally organic synthesis pigment, inorganic pigment, animals and plants natural pigment and pearlescent pigment.
And for various reasons, most of producers can select some cheap organic synthesis pigment, inorganic pigments, this can be to skin
Cause bigger injury.Therefore, find cost relatively low and the pigment of Nantural non-toxic is inexorable trend.
Chinese invention patent application number 201310584138.6, invention entitled " a kind of defying age containing polyphenoils protects
Skin frost " disclose a kind of anti-aging skin cream, it is made up of the raw material of following parts by weight: Caulis et Folium Brassicae capitatae extract 15-20 part, Semen Juglandis
Extract 8-12 part, Fructus Lycii extract 6-9 part, vitamin E 4-7 part, give birth to alcohol 3-6 part, squalane 3-9 part, octadecanol 2-6
Part, lanoline 4-8 part, xanthan gum 2-4 part, triethanolamine 2-7 part, vaseline 8-16 part, capriloyl glycine 3-5 part, the third ammonia
Acid 3-6 part, deionized water 30-45 part.This invention anti-aging skin cream containing polyphenoils, has an advantage in that the battalion in Caulis et Folium Brassicae capitatae
Forming point, not only content is high, and very comprehensive, mainly includes protein, carbohydrate, fat, mineral, vitamin C
With carotene etc., to improving skin, delay senility has significant role.
Chinese invention patent application number 201510822906.6, invention entitled " a kind of natural colour lipstick " discloses one
Kind of natural colour lipstick, described natural colour lipstick is mainly made up of by weight following component: natural pigment 3～7 parts, natural
Wax 15～20 parts, natural oil 40～70 parts, natural perfume material 2～5 parts, other natural function | raw additive 1～3 parts.This invention
Advantage be use extracted form natural plant juice as colouring substance, do not use the compound of synthetic, to human non-toxic,
And lip mucosa can be lubricated, anaphylaxis will not be produced.
Instantly society, due to safety and the effectiveness of natural plant composition, people increasingly hanker after using natural planting
Thing effective ingredient product.But, not all plant component can play useful effectiveness, therefore, selects which kind of plant
Which kind of effective ingredient adds in cosmetics so that it is the safest but also problem being to solve of playing effectiveness.
Summary of the invention
For problem mentioned above, the invention provides a kind of not only safety added in cosmetics but also can play
The natural plant composition of its useful effectiveness.The concrete technical scheme of the present invention is as follows:
The invention provides the application in preparing antioxidation cosmetic product, color make-up of the purple Chinese cabbage anthocyanidin, described purple
The preparation method of Chinese cabbage anthocyanidin comprises the steps:
(1) purple Chinese cabbage is cleaned up, break into serosity；
(2) add the 25%-30% ethanol solution of 12-15 times of purple Chinese cabbage amount, mix homogeneously, add citric acid regulation
PH to 2.8-3.5；
(3) extracting 6h under 15-30 DEG C of dark surrounds, extraction time 2 times, low-temperature centrifugation isolates supernatant；
(4) supernatant vacuum-concentrcted below 40 DEG C, to ethanol noresidue, is obtained concentrated solution；
(5) concentrated solution is purified according to common anthocyanidin purifying process, obtains purple Chinese cabbage anthocyanidin concentrated solution；
(6) the purple Chinese cabbage anthocyanidin concentrated solution in frozen drying step (5) at-35 DEG C, makes purple big
Chinese cabbage anthocyanidin lyophilized powder.
The purple of Chinese cabbage is by caused by anthocyan material, and anthocyanidin has antioxidation and eliminates the functions such as free radical,
Also have delaying skin aging and improve the effect of body immunity, can be applicable in antioxidation cosmetic product.Flower in purple Chinese cabbage
The content of blue or green element is stepped up from inside to outside, is wherein distributed mainly on the 1-4 layer of outer foil, and green-purple leaf is most external
Blade, anthocyanidin content is up to 82.83mg/kg.
Anthocyanidin is a kind of water colo(u)r, is one of primary pigments constituting petal and fruit color, can be along with carefully
The soda acid of cytosol changes color, and Cell sap is that acidity is the reddest, and Cell sap is that alkalescence is the most blue.Anthocyanidin can be natural as one
Pigment adds in food, safety non-toxic.And the purple Chinese cabbage anthocyanidin of the present invention can play tinction as natural pigment and make
While with, also there is the effect of skin care, add in color make-up, safety non-toxic, and also can protect skin, prevent and alleviate
The infringement that skin is produced by life-time service cosmetics.
Further, described antioxidation cosmetic product contain 10 parts of purple Chinese cabbage anthocyanidin concentrated solutions.
Further, the dosage form of described antioxidation cosmetic product is frost, emulsion, facial film.
The invention provides a kind of antioxygen defrost, described antioxygen defrost includes the raw material of following weight parts:
Purple Chinese cabbage anthocyanidin concentrated solution: 10,
Semen Lini oil: 4,
Oleum helianthi: 3.5,
Osmanthus essential oil: 2,
Pyrrolidone sodium carboxylate: 3,
Hydroxylated milk glyceride: 3,
Cetearyl alcohol: 1.2,
Glycerin mono-fatty acid ester: 0.8,
PGML: 1.4,
Hydroxypropyl starch phosphate: 0.3,
Phenoxyethanol: 0.15,
Trihydroxy tristerin: 0.6,
Lanoline: 1.4,
Allantoin: 2.8,
Deionized water: 65.85.
Antioxygen defrost is prepared according to the preparation method of cream general in prior art.
The mode that purple Chinese cabbage anthocyanidin is applied in color make-up is for join in cosmetics with lyophilized powder form.
Further, described color make-up is lipstick, eye shadow, rouge.
The invention provides a kind of lipstick containing purple Chinese cabbage anthocyanidin, described lipstick includes the former of following weight parts
Material: purple Chinese cabbage anthocyanidin 3-15 part, wax 6-12 part, oils and fats 8-12 part, quintessence oil 0.5-1.5 part.
Further, described wax be weight part ratio be (2-3): (1-4): (1-2): the Brazil wax of (2-3), Cera Flava,
Fructus Canarii albi wax, the mixture of laurel wax.
Further, at least two during described oils and fats is American Avocado Tree oil, Oleum Vitis viniferae, Oleum Cocois, lecithin, lanoline.
Further, described quintessence oil be weight part ratio be (0.1-0.4): (0.2-0.8): the egg HUAJING of (0.2-0.3)
Oil, Cymbidium ensifolium (L.) Sw. quintessence oil, the mixture of camellia essential oil.
The preparation method of lipstick is: wax and oils and fats are heated to about 85 DEG C, are uniformly mixed, and is cooled to 50 DEG C, adds purple
Color Chinese cabbage anthocyanidin lyophilized powder, stirs, and adds quintessence oil, is uniformly mixed, pours in mould, and cooling and demolding is packed.
The advantage of the preparation method and applications of purple Chinese cabbage anthocyanidin of the present invention and having the beneficial effect that:
(1) preparation method and applications of purple Chinese cabbage anthocyanidin of the present invention, the extraction raw material purple chosen
Chinese cabbage is cheap, wide material sources, and the content of anthocyanidin is high；
(2) preparation method and applications of purple Chinese cabbage anthocyanidin of the present invention, can be by purple Chinese cabbage cyanine
Element adds to and plays antioxidative effect in cosmetics, is effective against free radical；
(3) purple Chinese cabbage anthocyanidin can add in cosmetics as a kind of natural pigment, play simultaneously skin protection with
The effect of coloring.
Detailed description of the invention
In order to make those skilled in the art be more fully understood that technical scheme, below in conjunction with embodiment to this
Bright technical scheme is described in further detail.
The preparation of embodiment 1 purple Chinese cabbage anthocyanidin
Take 1kg purple Chinese cabbage to clean up, break into serosity, add 28% ethanol solution of 13 times of purple Chinese cabbage amounts,
Mix homogeneously, add citric acid regulation PH to 2.8-3.5, under 15-30 DEG C of dark surrounds extract 6h, extraction time 2 times, low temperature from
The heart isolates supernatant, to ethanol noresidue, supernatant vacuum-concentrcted below 40 DEG C is obtained concentrated solution, is pressed by concentrated solution
It is purified according to common anthocyanidin purifying process, obtains purple Chinese cabbage anthocyanidin concentrated solution, take purple Chinese cabbage anthocyanidin and concentrate
Liquid half amount frozen drying at-35 DEG C, makes purple Chinese cabbage anthocyanidin lyophilized powder.
The preparation of embodiment 2 antioxygen defrost
Table 1 antioxygen defrost formula forms
Antioxygen defrost is prepared according to the preparation method of cream general in prior art.
The preparation of embodiment 3 lipstick
Table 2 lipstick formula forms
The preparation method of lipstick is: wax and oils and fats are heated to about 85 DEG C, are uniformly mixed, and is cooled to 50 DEG C, adds
Purple Chinese cabbage anthocyanidin lyophilized powder, stirs, and adds quintessence oil, is uniformly mixed, pours in mould, cooling and demolding bag
Dress.
Embodiment 4 antioxygen defrost efficacy assessments is tested
1. test specimen
Antioxygen defrost that embodiment 2 prepares and blank group facial cream, commercially available antioxidation facial cream and blank sample go from
Sub-water.
2. test method
Scavenging ability of DPPH free radical measures: take 2ml test specimen, adds dehydrated alcohol 2mL and 0.02%DPPH ethanol
Solution 0.8ml, vibrate mix homogeneously, and under room temperature, lucifuge places 30min, measures absorbance, calculate clearance rate under 518nm.Table 3
For antioxygen defrost efficacy assessments result table.
Clearance rate %=((blank absorbency-sample light absorption value)/blank absorbency) × 100
Table 3 antioxygen defrost efficacy assessments result
| Test specimen | Embodiment 2 antioxygen defrost | Blank group facial cream | Commercially available antioxygen defrost |
| Clearance rate/% | 74.34 | 8.79 | 34.86 |
As can be seen from result of Table 3, the purple Chinese cabbage that the present invention prepares is applied in cosmetics, cosmetics can be made to possess good
The good ability removing free radical, it is possible to play good antioxidation, it is possible to clear most free radical, effectively protects
Skin avoids the infringement that free radical causes.Under the same terms, commercially available its free radical scavenging activity of antioxygen defrost only has 34.86%, far
Less than the 74.34% of the antioxygen defrost that embodiment 2 prepares, therefore the purple Chinese cabbage that the present invention prepares is applied in cosmetics, its
Oxidation resistance is better than general commercially available antioxygen defrost.
Embodiment 5 lipstick efficacy assessments is tested
The lipstick preparing embodiment 3 carries out efficacy assessments test, choose 20-40 year female volunteers 35, experimental group
1-5 uses the lipstick of A-E group, and matched group 1 uses blank group lipstick, and matched group 2 uses commercially available lipstick.Using method: will
Lipstick is applied directly to lip, in smear rear 0h, 2h, 4h, 6h measure lipstick persistence, i.e. the residual volume of lipstick on lip；
In smearing rear 0h, 2h, 4h, 6h moist degree with scoring form evaluation lipstick.Table 4 is lipstick efficacy assessments result of the test table.
Table 4 lipstick efficacy assessments result of the test
Moisten the moist degree of degree: 1=low；It is relatively low that 2=moistens degree；It is general that 3=moistens degree；4=moistens degree height.
The result that lipstick residual volume changes over time from table 4, uses the purple Chinese cabbage anthocyanidin of the present invention
The lipstick being prepared as, its persistence is better than commercially available general lipstick, it is possible to preferably keep dressing.The result of degree is moistened in contrast can
Seeing, the moist degree of commercially available lipstick is relatively low, and the lipstick using the purple Chinese cabbage anthocyanidin of the present invention to be prepared as, moisten degree height,
Can be good at protecting lip fragility skin, give lip water moisture feeling.
The crowd of the cosmetics that the purple Chinese cabbage anthocyanidin of the use present invention is prepared as, equal nobody occurs any bad
Reaction, the cosmetics safety that the purple Chinese cabbage anthocyanidin of the present invention is prepared as is non-stimulated, can life-time service.
Embodiment described above only have expressed the several embodiments of the present invention, and it describes more concrete and detailed, but also
Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that, for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these broadly fall into the guarantor of the present invention
Protect scope.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. purple Chinese cabbage anthocyanidin application in preparing antioxidation cosmetic product, color make-up, described purple Chinese cabbage anthocyanidin
Preparation method comprises the steps:
(1) purple Chinese cabbage is cleaned up, break into serosity；
(2) add the 25%-30% ethanol solution of 12-15 times of purple Chinese cabbage amount, mix homogeneously, add citric acid regulation PH extremely
2.8-3.5；
(3) extracting 6h under 15-30 DEG C of dark surrounds, extraction time 2 times, low-temperature centrifugation isolates supernatant；
(4) supernatant vacuum-concentrcted below 40 DEG C, to ethanol noresidue, is obtained concentrated solution；
(5) concentrated solution is purified according to common anthocyanidin purifying process, obtains purple Chinese cabbage anthocyanidin concentrated solution；
(6) the purple Chinese cabbage anthocyanidin concentrated solution in frozen drying step (5) at-35 DEG C, makes purple Chinese cabbage
Anthocyanidin lyophilized powder.
Application the most according to claim 1, it is characterised in that described antioxidation cosmetic product contain 10 portions of purple DABAI cauliflowers
Blue or green element concentrated solution.
Application the most according to claim 2, it is characterised in that the dosage form of described antioxidation cosmetic product is frost, emulsion, face
Film.
Application the most according to claim 3, it is characterised in that described antioxygen defrost includes the raw material of following weight parts:
Purple Chinese cabbage anthocyanidin concentrated solution: 10,
Semen Lini oil: 4,
Oleum helianthi: 3.5,
Osmanthus essential oil: 2,
Pyrrolidone sodium carboxylate: 3,
Hydroxylated milk glyceride: 3,
Cetearyl alcohol: 1.2,
Glycerin mono-fatty acid ester: 0.8,
PGML: 1.4,
Hydroxypropyl starch phosphate: 0.3,
Phenoxyethanol: 0.15,
Trihydroxy tristerin: 0.6,
Lanoline: 1.4,
Allantoin: 2.8,
Deionized water: 65.85.
Application the most according to claim 1, it is characterised in that described color make-up contains purple Chinese cabbage anthocyanidin lyophilized powder.
Application the most according to claim 5, it is characterised in that described color make-up is lipstick, eye shadow, rouge.
Application the most according to claim 6, it is characterised in that described lipstick includes the raw material of following weight parts: purple is big
Chinese cabbage anthocyanidin 3-15 part, wax 6-12 part, oils and fats 8-12 part, quintessence oil 0.5-1.5 part.
Lipstick the most according to claim 7, it is characterised in that described wax be weight part ratio be (2-3): (1-4): (1-2):
(2-3) Brazil wax, Cera Flava, Fructus Canarii albi wax, the mixture of laurel wax.
Lipstick the most according to claim 7, it is characterised in that described oils and fats is American Avocado Tree oil, Oleum Vitis viniferae, Oleum Cocois, ovum
At least two in phospholipid, lanoline.
Lipstick the most according to claim 7, it is characterised in that described quintessence oil be weight part ratio be (0.1-0.4): (0.2-
0.8): the Flos Plumeriae Acutifoliae quintessence oil of (0.2-0.3), Cymbidium ensifolium (L.) Sw. quintessence oil, the mixture of camellia essential oil.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107137324A (en) * | 2017-07-06 | 2017-09-08 | 山西大学 | A kind of humidity-preserving type lipstick and preparation method thereof |
| CN108403512A (en) * | 2018-04-27 | 2018-08-17 | 长沙理工大学 | A kind of lipstick and preparation method thereof with healthcare function |
| CN113164363A (en) * | 2018-11-26 | 2021-07-23 | 高露洁-棕榄公司 | Personal care compositions |
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| CN103342692A (en) * | 2013-07-24 | 2013-10-09 | 青岛蓝莓生物科技有限公司 | Method for extracting blueberry anthocyanin |
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| CN1813667A (en) * | 2005-11-23 | 2006-08-09 | 云南农业大学 | Natural red cyanidin cosmetics |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107137324A (en) * | 2017-07-06 | 2017-09-08 | 山西大学 | A kind of humidity-preserving type lipstick and preparation method thereof |
| CN108403512A (en) * | 2018-04-27 | 2018-08-17 | 长沙理工大学 | A kind of lipstick and preparation method thereof with healthcare function |
| CN113164363A (en) * | 2018-11-26 | 2021-07-23 | 高露洁-棕榄公司 | Personal care compositions |
| CN113164363B (en) * | 2018-11-26 | 2023-12-08 | 高露洁-棕榄公司 | Personal care compositions |
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