KR101944764B1 - High moisturized cosmetical composition using natural plant extract and lipstick comprising the same - Google Patents

Abstract

The present invention relates to a high moisturizing cosmetic composition using natural extracts and a lipstick comprising the same, which can provide high moisturizing properties through natural extracts by mixing a Smilax china leaf extract, a Poria cocos extract, a sea cucumber extract, a spirulina extract, a Scutellaria baicalensis extract, and a liriope rhizome leaf extract at a certain mixing ratio to form a composition; has excellent fragrance and color functions by adding any one selected from a first mixture obtained by mixing a forsythia fruit extract and a morus bark extract at a weight ratio of 1:1, a second mixture obtained by mixing a green tea leaf extract and a dandelion extract at a weight ratio of 1:1, a third mixture obtained by mixing a lithospermum extract and a juniper extract at a weight ratio of 1:1, or a retinispora extract; and can also extend the service life of a cosmetic composition and a cosmetic product comprising the same by a natural preservative by adding a fourth mixture obtained by mixing a Japanese pepper extract, a moss extract, a Pulsatilla extract, and a grapefruit seed extract.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a cosmetic composition containing a natural extract and a lipstick containing the same,

The present invention provides skin protection and high moisturizing properties by the pharmacological effect of natural extracts by mixing with a certain blending ratio of a green leaf extract, a sea bream extract, a sea cucumber extract, a spirulina extract, a golden extract and a marshmallow leaf extract,

A first mixture obtained by mixing together an agaricus extract and an extract of Mulberry bark extract in a weight ratio of 1: 1; A green tea leaf extract and a dandelion extract are blended in a weight ratio of 1: 1; A third mixture obtained by mixing the herb extract and the juniper extract at a weight ratio of 1: 1; Or an extract of Chamaecyparis obtusa, it is possible to provide skin protection, fragrance and color development function by the pharmacological effect of the natural extract,

The present invention relates to a cosmetic composition comprising a natural preservative and a fourth mixture prepared by mixing a mixture of the natural extract, the natural extract, the acid extract, the moss extract, the Baechuong extract and the grapefruit seed extract. ≪ / RTI >

Make-up can be divided into base make-up and point make-up as a means of expressing social status and protecting oneself from the surrounding environment.

The present invention relates to point make-up, and in particular relates to lip make-up.

The lip make-up modifies the shape of the lip to balance the upper lip and the lower lip as a whole, and not only makes the lips more distinct, but also uses various colors to enhance the color of the face.

Lip products on the lips are divided into lip care and therapeutic lip care and makeup products. Products intended for make-up generally include liptint, lipgloss, lipstick, and lipliner.

The present invention relates to a lipstick of the above products, and more particularly, to a cosmetic composition for imparting high moisturizing properties to the lipstick and a lipstick comprising the cosmetic composition.

In general, lipstick consists of oil base material and coloring agents.

In oil-based lipstick, solid wax is divided into natural wax and mineral wax. It is used to provide stick form of lipstick at room temperature.

Natural waxes include carnauba wax, beeswax, candelilla wax, and japan wax. Mineral waxes include solid paraffin, microcrystalline wax, ceresin, and hydrocarbon wax.

Oil is a liquid type that dissolves in human body temperature and is divided into natural oil and synthetic oil.

Natural oils used in lipstick include cocoa butter, castor oil, jojoba oil, macadamia nut oil and lanolin oil. The synthetic oils include petrolatum, liquid paraffin, synthetic fatty acid, And hydrocarbon-based oils such as esters. Among these oils, the most viscous oil in lipstick molding is castor oil, which is used in most lipstick manufacturing.

Conventional lipsticks were prepared by adding moisturizing agents such as glycerin, propylene glycol, butylene glycol, ceramide, polyethylene wax and the like in order to impart a moisturizing function. However, in the present invention, skin protection, And to provide a cosmetic composition and a lipstick using the cosmetic composition, which can improve the moisturizing characteristic and improve the fragrance and coloring function by the natural extract to enhance the satisfaction of the consumer.

Korean Registered Patent No. 10-1233857 (Registered on March 20, 2013) Korean Registered Patent No. 10-1566820 (Registration date 2015.11.02) Korean Patent Publication No. 10-2016-0096323 (Publication date 2016.08.16)

The present invention provides skin protection and high moisturizing properties by the pharmacological effect of natural extracts by mixing with a certain blending ratio of a green leaf extract, a sea bream extract, a sea cucumber extract, a spirulina extract, a golden extract and a marshmallow leaf extract,

A first mixture obtained by mixing together an agaricus extract and an extract of Mulberry bark extract in a weight ratio of 1: 1; A green tea leaf extract and a dandelion extract are blended in a weight ratio of 1: 1; A third mixture obtained by mixing the herb extract and the juniper extract at a weight ratio of 1: 1; Or an extract of Chamaecyparis obtusa, it is possible to provide skin protection, fragrance and color development function by the pharmacological effect of the natural extract,

The present invention relates to a cosmetic composition comprising a natural preservative and a fourth mixture prepared by mixing a mixture of the natural extract, the natural extract, the acid extract, the moss extract, the Baechuong extract and the grapefruit seed extract. It is an object of the present invention to provide a lipstick containing a lipstick.

In order to achieve the above object,

In the present invention, a mixture obtained by mixing citron tree and ethanol at a weight ratio of 1: 1.5-3 is leached at room temperature for 20 to 30 hours to obtain a primary extract, followed by filtration. The same procedure is repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours at 0.1 to 0.3 mPA with a vacuum rotation evaporator, lyophilized for 2 to 4 days using a freeze dryer, 0.01 to 70 wt% of ground powdered leaf extract,

The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator Concentrated to a concentration of 0.1 to 0.3 mPA under reduced pressure for 5 to 7 hours, lyophilized for 2 to 4 days using a freeze dryer, and then pulverized to a size of 30 to 50 mesh in an amount of 0.01 to 70 wt%

The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 0.01 ~ 70 wt% of sea cucumber extract crushed with 30 ~ 50 mesh,

The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dried for 2 to 4 days, and then spray-dried with 0.01 to 70 wt% of Spirulina extract pulverized into 30 to 50 mesh,

The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, the extract is pulverized to 30 ~ 50 mesh and 0.01 ~ 70 wt%

Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying Dried for 2 to 4 days, and then mixed with 0.01 to 70 wt% of marshmallow leaf extract pulverized into 30 to 50 mesh, to provide a moisturizing cosmetic composition using the natural extract.

Also provided is a lipstick of high moisturizing property which is prepared by adding the above-mentioned high moisture-sensitive cosmetic composition at 0.1 to 50 wt% with respect to the total weight of the cosmetic.

The high moisture cosmetic composition using the natural extract according to the present invention and the lipstick containing the same have the following effects.

first. The high moisture cosmetic composition according to the present invention can provide a high moisturizing function while enhancing the stability of use such as skin stability by natural materials using a natural extract having excellent moisturizing properties such as a natural extract of green tea leaf.

second. The high moisture-reducing cosmetic composition according to the present invention comprises a first mixture obtained by mixing a combination of an almond extract and an extract of Morus alba extract, in a weight ratio of 1: 1; A green tea leaf extract and a dandelion extract are blended in a weight ratio of 1: 1; A third mixture obtained by mixing the herb extract and the juniper extract at a weight ratio of 1: 1; Or by adding an extract of Chrysanthemum morifolium, it is possible to provide a lipstick excellent in flavor and color expression through a natural material.

third. The antimicrobial and antioxidant functions contained in the natural extract have an additional advantage that they can be used more cleanly and safely due to blocking of bacterial infection and the like.

fourth. It has an advantage that the health condition of the lip skin by the pharmacological action of the natural extract can be maintained continuously.

fifth. It is possible to solve the problem that the use and storage period, which is a disadvantage of the cosmetic composition containing natural extract, is short, by using a natural preservative which is free of skin irritation and can ensure safety of use.

The above-described technical construction will be described in more detail.

As described above,

The high moisture cosmetic composition using the natural substance according to the present invention,

The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 0.01 ~ 70 wt% of leaf extract,

The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator Concentrated to a concentration of 0.1 to 0.3 mPA under reduced pressure for 5 to 7 hours, lyophilized for 2 to 4 days using a freeze dryer, and then pulverized to a size of 30 to 50 mesh in an amount of 0.01 to 70 wt%

The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, Freeze dryer for 2 ~ 4 days and then dried at 30 ~ 50 mesh, 0.01 ~ 70 wt% of sea cucumber extract,

The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using a dryer, the spirulina extract was pulverized to 30 ~ 50 mesh, 0.01 ~ 70 wt%

The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After lyophilization, 0.01 ~ 70 wt% of the golden extract was pulverized with 30 ~ 50 mesh,

Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After lyophilization for 2 ~ 4 days, it is mixed with 0.01 ~ 70 wt% of marshmallow leaf extract which is pulverized with 30 ~ 50 mesh.

Hereinafter, natural extracts constituting the cosmetic composition will be described in more detail.

<Persimmon leaf extract>

Smilax china is a vine shrub belonging to the lily family. In one room, it is called Sukyegye, Sukjeonggyeong, and Sanygrae. It is known that roots and trees are effective for relieving symptoms such as fever, detoxification, diuretic, improving physical strength and dermatitis, nephritis, cystitis, antibacterial effect, arthritis and breast cancer.

In the present invention, an ethanol extract of Persimmon leaves is used.

That is, the mixture of lupine leaves and ethanol is mixed at a ratio of 1: 1.5-3 by weight to form a mixture. The mixture is then leached at room temperature for 20 to 30 hours to obtain a first extract, which is then filtered, The filtrate was concentrated, concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA, dried for 2 to 4 days using a freeze dryer, Use a homogenizer that is pulverized to 30 to 50 mesh.

As a specific example of the above-mentioned limpid leaf extraction, 1,000 g of light leaf is mixed with 2.5 L of 80% ethanol, and the mixture is then leached for 24 hours to obtain a primary extract, which is then filtered.

The same procedure is followed to obtain a secondary extract and a tertiary extract.

The primary extract, the secondary extract and the tertiary extract were mixed and concentrated under reduced pressure at 62 ° C and 0.2 mPA with a vacuum rotation evaporator for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract was dried for 3 days, and then pulverized to 40 mesh to prepare powdered lucidum leaves extract.

<Extract of Bokryeong>

Bokyeong is a type of mushroom belonging to the Vaccine family, which grows parasitically from roots after 3 to 10 years after cutting the pine tree. The main components of Byeongryeong are carbohydrate, moisture, crude fiber, minerals and trace amount of protein. Among the carbohydrates, pachyman is the most abundant carbohydrate. Pachymic acid, tumulosic acid, dehydrotumulosic acid, ergosterol, eburicoic acid, dehydroeburicoic acid, trametenolic aicd .

The extracts of Bombyx mori were prepared by mixing the bamboo shoot powder and ethanol at a weight ratio of 1: 9 to 12, and then the mixture was subjected to sonication extraction. The extract was filtered with a filter paper, Is concentrated under reduced pressure using a vacuum rotation evaporator for 5 to 7 hours under a condition of 0.1 to 0.3 mPA and dried for 2 to 4 days using a freeze dryer.

As a concrete example of the extract, 1000 g of finely pulverized seeds are pulverized using a pulverizer into 10 L of 70% ethanol and subjected to sonication. After extraction, filter with filter paper (Whatman No 3. filterpaper). The filtered extract was concentrated under reduced pressure using a vacuum rotation evaporator at 62 캜 and 0.2 mPA for 5 hours to obtain 1 L of an extract. At this time, sonication is performed by generating ultrasonic waves at 60 kHz for 30 minutes by using an ultrasonic dispersing machine, and then storing it at room temperature under dark condition for 72 hours.

Next, 1 L of the extract was dried for 3 days, and then pulverized to 40 mesh to prepare powdered lucidum leaves extract.

<Sea cucumber extract>

Sea cucumber is a generic term for sea cucumbers belonging to the sea cucumber river. There are three kinds of sea cucumbers in Korea, red ginseng, blue ginseng and black ginseng. Sea cucumbers act as amino acid and iron (Fe), phosphorus (P) and bile components such as cysteine, histidine and lysine to prevent anemia and liver. Taurine (Taurine) is contained in the gallbladder and liver to detoxify the function of strengthening, cholesterol lowering, heart function and improve vision is said to be effective in the recovery.

The raw sea cucumber contains water, protein, carbohydrate, ash, calcium, phosphorus, iron, lysine, vitamin 1, B2, essential amino acid, erythrocyte thionin, glutamic acid, glycine, tryptophan and taurine. Sea cucumber extracts from sea cucumbers contain chondroitin, a type of mucopolysaccharide. Chondroitin plays a role in accumulating moisture and nutrients in the skin. Chondroitin sulfate is a major component of viscous polysaccharides and is a mucopolysaccharide found in animal cartilage, nervous tissue and intercellular tissue. Chondroitin sulfate does not exist in vivo but is bound to proteins to form a chondroitin sulfate protein complex. It is the basis for living somatic cells in vivo, such as collagen, elastin, hyaluronic acid, etc., It gives resilience. Chondroitin sulfate, which is contained in sea cucumber extract, keeps moisturizing function by storing moisture in the skin. It also stores a large amount of amino acid, protein and iodine ingredient to save skin wrinkles, prevent aging, skin whitening efficacy, .

The sea cucumber extracts were prepared by mixing sea cucumber and ethanol at a weight ratio of 1:10 to 12, preparing a mixture, extracting the mixture at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm in a shaking incubator, The supernatant obtained by centrifugation at 7,500 to 8,500 rpm for 15 to 25 minutes was filtered with a filter paper, and the resulting extract was filtered with a vacuum rotation evaporator under the condition of 0.1 to 0.3 mPA at 5 to 7 And dried in a freeze dryer for 2 to 4 days and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of the above sea cucumber extract, 1,000 g of sea cucumber is placed in 10 L of 50% ethanol and extracted at 160 rpm at 26 캜 for 60 hours in a shaking incubator to obtain an extract. The extract is centrifuged at 7,000 rpm for 30 minutes in a centrifuge. The supernatant obtained by centrifugation is filtered with filter paper (Whatman No. 3 filter paper). The filtered extract was concentrated under reduced pressure at 62 DEG C and 0.2 mPA for 5 hours by a vacuum rotation evaporator to obtain 1 L of an extract.

Next, 1 L of the extract was dried for 3 days using a freeze dryer, and then pulverized into 40 mesh to prepare a powdered sea cucumber extract.

<Spirulina extract>

Spirulina (Spirulina platensis) is one of the oldest algae on Earth, the first photosynthetic creature that was born about 3.5 billion years ago.

It is a kind of cyanobacteria that grows in hot water of high alkalinity and high seawater and strong alkalinity. It is composed of 60-70% protein, 6-9% lipid, 15-20% carbohydrate and a large amount Vitamins, minerals, and fiber.

Spirulina contains about 65% pure protein in its whole ingredients and contains 50 essential nutrients including protein, phosphorus, fat, vitamins and minerals which are the five essential nutrients. It contains SOD, which is a powerful natural antioxidant. It is known to be effective in improving skin health, antioxidant activity, and improving blood cholesterol.

Spirulina contains a variety of nutrient sources and is registered as a health food for the KFDA. Spirulina is added to the skin to increase the activity of the skin, while providing excellent moisturizing effect on the skin to keep the skin healthy .

The spirulina extract was prepared by mixing spirulina with distilled water at a weight ratio of 1:35 to 45 to prepare a mixture. The mixture was extracted from the shaker culture at 120 to 160 rpm at 24 to 26 ° C for 65 to 75 hours, and the extract was centrifuged at 7,500 After centrifugation at 8,500 rpm for 15 to 25 minutes, the supernatant and the precipitate were repeatedly separated three times, and only the supernatant was collected

As a specific example of the above Spirulina extract, 1,000 g of Spirulina is added to 40 L of distilled water and extracted at 160 rpm at 26 DEG C for 70 hours in a shaking incubator to obtain an extract.

The extract is centrifuged at 7,000 rpm for 30 minutes in a centrifuge to separate the supernatant and the precipitate first.

The precipitate is again centrifuged at 7,000 rpm for 30 minutes in a centrifuge to separate the supernatant and the precipitate secondarily.

The precipitate is further centrifuged at 7,000 rpm for 30 minutes in a centrifuge to separate the supernatant and the precipitate from the supernatant.

Only the supernatant obtained through centrifugation is collected and used as Spirulina extract.

At this time, the obtained extract is dried for 3 days by using a freeze dryer, and then the spirulina extract is pulverized to 40 mesh.

<Golden extract>

Golden (Scutellaria baicalensis) is a perennial plant belonging to the botanical tree of the botanical plant. It is called money, a little bit, and an organism, and it uses taste, and the property is cold and nontoxic. It mainly uses roots. Gold is known as a potent pharmacologic crop and has been used as an alternative medicine for anti-inflammatory, anti-cancer and soothing effects.

The gold extract was prepared by mixing gold and methanol at a weight ratio of 1: 4 to 6, preparing a mixture, refluxing the mixture at 65 to 75 ° C for 20 to 30 hours, extracting the mixture for 4 to 6 minutes at 3,500 to 4,500 rpm The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 to 4 days and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of the gold extract, dried gold is finely pulverized, and 1,000 g of gold fine powder and 5 L of 70% ethanol are mixed, followed by reflux extraction at 72 ° C for 15 hours.

The extract is centrifuged at 3,500 rpm for 10 minutes, and the supernatant is collected and filtered with filter paper (Whatman No. 3 filter paper). The filtered extract was concentrated under reduced pressure at 62 DEG C and 0.2 mPA for 5 hours by a vacuum rotation evaporator to obtain 1 L of an extract.

At this time, the obtained extract was dried for 3 days using a freeze dryer, and then pulverized to a size of 40 mesh to prepare a golden extract.

<MacMonkey Leaf Extract>

Liriope platyphylla tubers belong to the lily family and are perennial herbs and widely distributed in the temperate zone from the subtropical. At the end of the beard roots of Maekmundong, a short spindle root is mixed and used as a herbal medicine and medicinal herb. In recent years, it is also used for landscape.

It is used for treatment of chronic kidney disease, chronic bronchitis, chronic sore throat, and pulmonary tuberculosis. The contents of polyphenol compounds and flavonoid compounds were higher than those of root extracts.

MacMonkey leaf extracts were washed with water, dried in a freeze dryer, processed into powder, powdered MacMonkey leaves and distilled water were mixed at a weight ratio of 1:10 to 12, The resulting extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPA by a vacuum rotation evaporator, and the concentrate was concentrated in a freeze drier And dried in a freeze dryer for 2 to 4 days and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of the manganese leaf extract, the leaf of Liriope platyphylla is washed with water after removing soil and foreign matter, dried in a freeze dryer, and then used as a powder.

1,000 g of powdery manganese leaves were mixed with 10 L of distilled water to prepare a mixture, and the mixture was reflux-extracted at 80 캜 for 3 hours.

Filter the extract with filter paper.

The filtered extract was concentrated under reduced pressure at 62 DEG C and 0.2 mPA for 5 hours using a vacuum rotation evaporator to obtain 1 L of an extract.

At this time, the obtained extract was dried for 3 days by using a freeze dryer, and then pulverized into 40 mesh to prepare a gentian lentil extract.

The cosmetic composition according to Example 1 is composed of a mixture of a bright red leaf extract, a royal jelly extract, a sea cucumber extract, a spirulina extract, a golden extract and a mung bean leaf extract.

In other words,

50% by weight of leaf extract;

10 wt% of ginseng extract;

Sea cucumber extract 10 wt%;

Spirulina extract 10 wt%;

10 wt% of gold extract;

10% by weight of Macmunococcus aureus extract to prepare a cosmetic composition according to the present invention.

In order to enhance the fragrance and coloring function of the cosmetic composition according to the present invention, a first mixture obtained by mixing together a 1:

At this time, the amount of the first mixture may be further added in an amount of 0.01 to 20 wt% based on the total weight of the cosmetic composition.

<Alcoholic extract>

It is a deciduous broad-leaved shrub with dried forsythia species. Ingredients include oleanolic acid and lignan glycoside in fruits.

The roots are used for medicinal purposes, and the stem and leaves are used for medicinal purposes. The extracts from the forsythia fruit skin are used for detoxification, dermatitis, drainage, inflammation and diuretic.

In addition, Forsythia suspensa is known as a medicinal product with excellent therapeutic effect against acute nephritis, laryngitis, fever, ulcer, tonsillitis and gonorrhea. Essential oils of almonds have been reported to have antiviral, antioxidant, antibacterial, anti-inflammatory, anti-inflammatory effects.

The dried persimmon extracts were washed in a drier at a temperature of 55 to 65 ° C for 20 to 26 hours, and then the dried persimmon leaves and distilled water were mixed in a ratio of 1:10 to 15 by weight, and the mixture was heated for 2 to 4 hours The extracted filtrate was concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA and dried for 2 to 4 days using a freeze dryer And then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a concrete example of the extract of the above-mentioned tangle, the ties were washed cleanly and dried in a dryer at 62 ° C for 22 hours. Then, 1,000 g of each of the extracts was placed in a pan and 12 L of distilled water was added to the extract for 3 hours to obtain an extract. Filtered and the filtrate was concentrated under reduced pressure at 62 ° C and 0.2 mPA for 5 hours using a vacuum rotation evaporator to obtain 1 L of an extract.

At this time, the obtained extract is dried for 3 days by using a freeze dryer, and then the resulting extract is pulverized to 40 mesh.

<Manganese extract>

Morus alba refers to the root bark parts of Morus alba L., M. bomloycis Koidzumi, M. lu Koidzumi, or other inbred plants and is mainly exported to Korea, China and Japan.

The main ingredient is flavonoids, which exhibit hypotensive effects. Known pharmacological actions of bovine alfalfa include blood pressure lowering, blood sugar lowering, antibacterial action, and diuretic anti-inflammatory action.

In the extract of Miscanthus sinensis L., the mixture is mixed at a ratio of 1:10 to 15, and then the mixture is extracted at room temperature for 70 to 74 hours, and the extracted extract is centrifuged to take the supernatant.

The supernatant obtained by repeating this process twice was mixed, filtered, concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA, and then freeze-dried using a freeze dryer Dried for 2 to 4 days, and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of the above extract of Mulberry bark, 70% ethanol is added to the mulberry bark at 10 times the weight of the mulberry bark and the mixture is extracted at room temperature for 72 hours to obtain an extract, which is centrifuged to take the supernatant. The supernatant obtained by repeating the same two times was called Whatman No. &quot; 2 and a sterilizing filter, and concentrated under reduced pressure at 62 DEG C and 0.2 mPA with a vacuum rotation evaporator for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract was dried for 3 days, and then pulverized to 40 mesh to prepare a powdery mulberry bark extract.

The cosmetic composition according to the second embodiment is prepared by further adding a first mixture obtained by mixing together a 1:

50% by weight of leaf extract;

Ginseng extract 9 wt%;

Sea cucumber extract 9 wt%;

Spirulina extract 9 wt%;

9 wt% of gold extract;

9 m.

And 5 wt% of a first mixture prepared by mixing the extract of Allium cepa L. and extract of Allium cepaceri L. (1: 1).

In order to enhance the fragrance and coloring function of the cosmetic composition according to the present invention, a second mixture in which a green tea leaf extract and a dandelion extract are mixed at a weight ratio of 1: 1 is further added to prepare a cosmetic composition.

At this time, the amount of the second mixture may be further added in an amount of 0.01 to 20 wt% based on the total weight of the cosmetic composition.

<Green tea leaf extract>

The contents of green tea were 9.2 ~ 11.8% in water content, 4.9 ~ 6.1% in crude protein, 5.2 ~ 6.3% in crude fat, 22.5 ~ 26.4% in protein content and 50.4 ~ 55.1% in carbohydrate. / 100 g), sodium (340 ~ 580 mg / 100 g) and magnesium (242 ~ 320 mg / 100 g).

(-) - epicatechin (EGC), epicatechin-3-gallate (ECG) and epigallocatechin-3-gallate (ECG) are the major physiologically active components of green tea. gallate (EGCG). These polyphenols have been shown to have various effects such as anti-inflammation, anti-cancer and whitening. Especially, these green tea catechins have passed through the blood-brain barrier and are involved in the metabolism regulation of the central nervous system .

Green tea leaf extracts were prepared by thoroughly washing the green tea leaves with distilled water and drying at 25 to 26 ° C for 23 to 26 hours. The dried green tea leaves were pulverized using a pulverizer, and the pulverized green tea leaf powder and ethanol were mixed at 1: The extract was filtered and concentrated under reduced pressure using a vacuum rotation evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA, It is dried in a freeze dryer for 2 to 4 days and then pulverized into 30 to 50 mesh using a homogenizer.

As a specific example of green tea leaf extract, green tea leaves are cleanly washed with distilled water and then dried at 25 ° C for 24 hours. Dried green tea leaves are pulverized using a pulverizer, and 10 g of 95% ethanol is added to 1,000 g of green tea leaf powder and extracted with stirring at room temperature for 24 hours. Filter paper No. 4, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract is dried for 3 days and then pulverized to 40 mesh to prepare a powdery green tea leaf extract.

<Dandelion extract>

Dandelion is a plant commonly found in mountains and fields around the country and around the roads. It is recorded as a medicinal substance to heat in Donguibogam, and it is recorded as medicinal substance to reinforce bones and muscles and to remove poison.

It is processed food of Min-dal, and many forms of food such as pellets, pellets, and extract are developed. It also acts to inhibit fungal viruses. It is used in cosmetics such as remedies for bathing and bathing products. It also contains nutrients such as vitamin C and amino acids. It is used as a cosmetic additive for nutritional creams, whitening creams, and contains organic acids, and the extract is also used as a preservative in cosmetics.

The dandelion extract is prepared by crushing the dandelion into leaves and roots and crushing with a homogenizer to prepare a powder. The dandelion powder and the distilled water are mixed in a weight ratio of 1:10 to 15, and the mixture is shaken in a shaking incubator at 24 to 28 ° C for 30 to 60 hours The extracts were filtered and concentrated under reduced pressure using a vacuum rotation evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA and then freeze-dried using a freeze dryer , Dried for 2 to 4 days, and then pulverized to a size of 30 to 50 mesh using a homogenizer.

A specific example of the above-mentioned dandelion extract is as follows: Dandelion is divided into leaves and roots and homogenized to prepare a powder. 1,000 g of dandelion powder and 10 L of distilled water are mixed, and the mixture is heated in a shaking incubator at 26 DEG C for 160 hours rpm to obtain an extract. 4, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract is dried for 3 days, and then pulverized into 40 mesh to prepare a powdered dandelion extract.

The cosmetic composition according to Example 3 was prepared by further adding a first mixture prepared by mixing green tea extract and dandelion extract at a weight ratio of 1: 1 in order to enhance the fragrance and color development function.

50% by weight of leaf extract;

Ginseng extract 9 wt%;

Sea cucumber extract 9 wt%;

Spirulina extract 9 wt%;

9 wt% of gold extract;

9 m.

5 wt% of a second mixture prepared by mixing 1: 1 green tea extract and dandelion extract.

In order to enhance the fragrance and coloring function of the cosmetic composition according to the present invention, a cosmetic composition is prepared by further adding a third mixture obtained by mixing a herb extract and a jochen extract at a weight ratio of 1: 1.

At this time, the amount of the third mixture may be further added in an amount of 0.01 to 20 wt% based on the total weight of the cosmetic composition.

<Herbicide extract>

(Lithospermum erythrorhizon Sieb. Et Zucc., Gromwell) It is a perennial plant called plant, grass, shaggy, or rosewood.

In the past, it has been used for the treatment of eczema, burns, frostbite, etc. The roots were used for the prevention of measles, hematemesis, hemorrhoids and constipation.

The root, which is the root of the dirt, gives the lipstick a soft color, which alleviates the inherent color of the vegetable ingredient. Natural pigments are mainly used as carotenoids, anthocyanin, chlorophyll, betalain pigments, and red pigments, and red pigments are most widely used among food colors. A representative example of a natural coloring matter is a red coloring matter derived from the seedling used for the production of redness.

The herbicidal extracts were prepared by mixing the powdery mash powder and ethanol in a weight ratio of 1:10 to 15, then extracting the mixture at room temperature for 22 to 26 hours with stirring, filtering the extract, filtering the mixture at a reduced pressure of 0.1 to 0.3 mPa for 5 to 7 hours It is concentrated in a vacuum rotary evaporator, dried in a freeze dryer for 2 to 4 days, and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a concrete example of the extract of grasses, 10 g of 95% ethanol is added to 1,000 g of ground powder, and the mixture is extracted with stirring at room temperature for 24 hours. Filter paper No. 4, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract is dried for 3 days, and then pulverized to a size of 40 mesh to prepare a powdery shoot extract.

<Junjoo extract>

The juniper trees are short - leaved, rounded seoulensis (var. Seoulensis), leafy endless modesta, beachhead juniper (ver. Koreana) growing on the beach, , communis), and fruit juvenile (J. communis var. nipponica). In oriental medicine, it is called a nursery and is used for the treatment of sweating, diuretic, neuralgia, and rheumatism. The essential oil of seeds is used for rheumatism and as a spice for Yangju Jin.

The main constituents of juniper were (+) - catechin, quercetin-3-O-α-L-rhamnopyranoside, isoconiferin and umbelliferone and quercetin-3-O-β-D-rutinoside.

The juniper extract was prepared by mixing juniper and ethanol at a weight ratio of 1: 2 ~ 6, and then extracting the mixture at room temperature for 22 to 26 hours with stirring. The extract was filtered and concentrated under reduced pressure of 0.1 to 0.3 mPA for 5 to 7 hours, concentrated using a vacuum rotation evaporator, dried in a freeze dryer for 2 to 4 days, and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of Junjung Ju extract, 4 L of 80% ethanol is added to 1,000 g of Junjou, and the mixture is extracted with stirring at room temperature for 24 hours. Filter paper No. 4, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract was dried for 3 days, and then pulverized into 40 mesh to prepare a powdered junken extract.

The cosmetic composition according to Example 4 is prepared by further adding a third mixture obtained by mixing the herb extract and the juniper extract at a weight ratio of 1: 1 in order to enhance the fragrance and coloring function.

50% by weight of leaf extract;

Ginseng extract 9 wt%;

Sea cucumber extract 9 wt%;

Spirulina extract 9 wt%;

9 wt% of gold extract;

9 m.

5% by weight of a third mixture prepared by mixing 1: 1 mixture of a seed extract and a juniper extract.

In the present invention, in order to enhance the fragrance and coloring function of the cosmetic composition, a cosmetic composition is prepared by further adding a cypress extract.

At this time, the amount of the extract of Clostridium perfringens extract may be further added in an amount of 0.01 to 20 wt% based on the total weight of the cosmetic composition.

&Lt; RTI ID = 0.0 >

Chamaecyparis obtusa is an evergreen conifer belonging to the Cupressaceae. Essential oil extracts from Quercus monkeys have been reported to be effective in relieving stress, improving psychological stability, strengthening cardiopulmonary function, and bronchial asthma. In addition, it is known that it has anti-itching effect of atopic dermatitis and antimicrobial activity against skin microorganism.

The extracts were obtained by extracting the extracts from the leaves of Chenopodium ambrosioides L. and the distilled water at a weight ratio of 1:10 to 20, and then the mixture was extracted with a hot water extractor for 2 to 4 hours. The extract was filtered, , Concentrated under reduced pressure using a vacuum rotation evaporator for 5 to 7 hours, dried for 2 to 4 days using a freeze dryer, and then pulverized into 30 to 50 mesh using a homogenizer .

As a specific example of the above-mentioned extract, 5 L of distilled water is added to 500 g of a perilla leaf, and the mixture is extracted with a hot-water extractor for 3 hours to obtain an extract. Filter paper No. 4, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

Next, 1 L of the extract was dried for 3 days, and then pulverized to 40 mesh to prepare a powdery cotton seed extract.

The cosmetic composition according to Example 5 was prepared by further adding a Leaf Leaf Extract to enhance flavor and color development.

50% by weight of leaf extract;

Ginseng extract 9 wt%;

Sea cucumber extract 9 wt%;

Spirulina extract 9 wt%;

9 wt% of gold extract;

9 m.

And 5 wt% of Prunus mume extract.

In the present invention, in order to prolong the preservation period of the cosmetic composition composed of the natural extract, 0.1 to 50 wt% of an acanthoxylum extract, 0.1 to 50 wt% of a moss extract, 0.1 to 50 wt% wt% of a fourth mixture is further added thereto to prepare a cosmetic composition.

At this time, the amount of the fourth mixture may be further added in an amount of 0.01 to 3 wt% based on the total weight of the cosmetic composition.

<Sancho extract>

Zanthoxylum schinfolium (Zanthoxylum schinfolium) is a species native to the altitude less than 1,000m altitude in Korea and its fruit is used as vegetable oil resources and various seasonings, and seed oil is also used as a lubricant for millet.

Sancho is the fruit of the sancho (Japanese apricot) tree. The fruit skin contains 2 ~ 4% of essential oil. Its main ingredients are dipentene (dl-limonene), citronellal, l-β-phellandrene, geraniol, citronellol Respectively. The fruit contains xanthoxine, a phlegmatic toxin, xanthoxine acid, a paralytic component, sterol campesterol, stigmasterol, and β-sitosterol.

The mixture was mixed at a ratio of 1:10 to 15 by weight, and the mixture was stirred at room temperature for 22 to 26 hours. The extract was filtered, concentrated under reduced pressure using a vacuum rotation evaporator, Use a freeze dryer to dry for 2 to 4 days and then use a homogenizer to pulverize the mixture into 30 to 50 mesh.

As a specific example of the above-mentioned ACS extract, 1,000 g of anthracnose and 10 L of methanol are mixed and extracted with stirring at room temperature for 24 hours. Filter paper No. 2, and concentrated under reduced pressure using a vacuum rotation evaporator at 62 DEG C and 0.2 mPA for 5 hours to obtain 1 L of an extract.

<Moss extract>

Moss has been reported to have excellent antimicrobial and antioxidant effects. When mosses are added to water, the acidity of the surrounding water is increased by the object of mosses in the body, thereby reducing the bacterial activity and preventing the deterioration of water.

There are lichen (moss, moss, Musci), umbrella (liverwort, Hepaticae), and horny lichen (hornwort, Anthocerotae). These lichens inhibit microbial propagation and are highly valuable as natural preservatives because of their antioxidant action.

The moss extract was washed with hot water at 55 to 65 ° C and then dried by hot air blow. The moss was mixed with 100% methanol at a weight ratio of 1:10 to 15, Cooled at 62 ° C for 5 to 7 hours,

The extract is filtered, concentrated under reduced pressure using a vacuum rotation evaporator, dried in a freeze dryer for 2 to 4 days and then pulverized in a homogenizer to a size of 30 to 50 mesh use.

As a specific example of the moss extract, a moss mixture obtained by mixing moss, large feather moss and feather moss at the same weight ratio is dewatered by water washing and then dried by hot air drying at 62 ° C for 6 hours. 1,000 g of the pulverized dried sample and 10 L of 100% methanol are mixed in a reflux condenser equipped with a cooling tube and reflux cooled for extraction at 58 ° C. for 7 hours.

The extract was filtered with a pore size filter paper having a pore size of 5 μm and concentrated under reduced pressure at 62 ° C. and 0.2 mPA using a vacuum rotation evaporator for 5 hours to obtain 1 L of an extract.

<Baekhyon extract>

It is a perennial plant belonging to the ranunculaceae family. It is distributed in all parts of Korea and also in northeast China. This herbal medicine has been commonly applied to toothache, fever, and water, and has been used for anti-inflammation, astringency, hemostasis, dysentery, detoxification, scrotum, antibacterial, sedation, and anticancer. It has been reported that this material has been widely used for anti-inflammation, analgesic, antipyretic, and detoxification purposes in Korea.

The Baekhwong extract is washed with water, dried in a freeze dryer, processed into a powder form, powdered Baekjong and distilled water are mixed at a weight ratio of 1:10 to 12, The resulting extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa with a vacuum rotation evaporator, dryer for 2 to 4 days and then pulverized to a size of 30 to 50 mesh using a homogenizer.

As a specific example of the Baechuonggong extract, 1,000 g of Baekhwong in the form of powder is mixed with 10 L of distilled water to form a mixture, and the mixture is reflux-extracted at 80 ° C for 3 hours.

Filter the extract with filter paper.

The filtered extract was concentrated under reduced pressure at 62 DEG C and 0.2 mPA for 5 hours using a vacuum rotation evaporator to obtain 1 L of an extract.

At this time, the obtained extract was dried for 3 days using a freeze dryer, and then pulverized to a size of 40 mesh to produce Baechutong extract.

<Grapefruit seed extract>

Grapefruit is juicy and has a bit of sour taste. Grapefruit seed extract is a natural antimicrobial material, and its main components are ascorbic acid, palmitic acid, glucoside, and naringin glycocortoferol, which inhibit mycotoxin biosynthesis and growth of fungal strains.

The grapefruit seed extract is prepared by mixing grapefruit seed with ethanol at a weight ratio of 1: 5 to 10, refluxing and cooling at 60 to 62 ° C for 2 to 3 hours, centrifuging at 10,000 × g for 20 to 40 minutes, The filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dried for 2 to 4 days using a freeze dryer, Use a powder of 30 to 50 mesh.

The fourth mixture was tested for antiseptic activity against the bacterial strains Staphylococcus aureus KCCM 11335, Escherichia coli, Pseudomonas aeruginosa KCCM 11802, Candida albicans KCCM 11282 and Aspagillus niger KCCM 60143 which are problematic in cosmetics.

E. coli, KCCM 40271), Candida albicans (C. albicans KCCM 11282), fungi (E. coli KCCM 11282), and yeast strains of Staphylococcus aureus (S. aureus, KCCM 11335), Pseudomonas aeroginosa (P. aeroginosa, KCCM 11802) and Escherichia coli Aspergillus niger (A. niger KCCM 60143) was cultured, and the bacteria were cultured in a shaking incubator adjusted at 37 ° C and fungi at 26 ° C and 250 rpm.

The number of viable cells was measured on days 1, 3 and 7 after inoculation with the bacterial strain thus cultured. As a result, no viable cells were detected.

The cosmetic composition according to Example 6 was prepared by further adding a fourth mixture composed of an acidulant extract, a moss extract, a bamboo shoot extract, and a grapefruit seed extract in order to prolong the storage period.

52% by weight of leaf extract;

Ginseng extract 9 wt%;

Sea cucumber extract 9 wt%;

Spirulina extract 9 wt%;

9 wt% of gold extract;

9 m.

3 wt% of a fourth mixture, which was prepared by mixing the extracts of Sancho, moss, Baechutong and grapefruit seeds at the same weight ratio.

Hereinafter, production examples of lipsticks using the cosmetic composition shown in Examples 1 to 6 will be described with reference to Examples 7 to 11.

The lipstick was prepared using the cosmetic composition of Example 1,

80 g of ceresin wax,

80 g of Candelilla wax,

20 g of Microcrystalline wax,

149 g of polyglyceryl-2 triisostearate,

40 g of dipentaerythrityl hexahydroxystearate / hexastearate / hexarosinate, 40 g of dipentaerythrityl hexahydroxystearate /

100 g of diisostearyl malate,

Octyl palmitate, Stearalkonium hectorite, 30 g of propylene carbonate,

0.5 g of Propylparaben,

0.5 g of Ethylparaben,

950 g of a lipstick composition (A) (1,000 g) consisting of a mixture of 500 g of liquid paraffin or caprylic / capric triglyceride,

The highly moisturizing lipstick composition prepared by mixing 50 g of the cosmetic composition (B) of Example 1 was molded into a lipstick shape, and then the molded body was placed in a cooling chamber maintained at 4 캜 for 17 hours and,

Removed from the cooling chamber, maintained in an incubator maintained at 45 캜 for 5 hours,

And then taken out from the incubator, put in the cooling chamber again, and held for 6 hours to complete the lipstick.

In this Example, a lipstick is prepared through the same procedure as in Example 7, except that 50 g of the cosmetic composition of Example 2 is used to make a lipstick when using the cosmetic composition (B).

In this Example, a lipstick is prepared in the same manner as in Example 7 except that, in using the cosmetic composition (B), 50 g of the cosmetic composition of Example 3 is used to make a lipstick.

In this Example, a lipstick was prepared in the same manner as in Example 7, except that, in using the cosmetic composition (B), 50 g of the cosmetic composition of Example 4 was used to prepare a lipstick.

In this Example, a lipstick was prepared in the same manner as in Example 7, except that, in using the cosmetic composition (B), 50 g of the cosmetic composition of Example 5 was used to make a lipstick.

In this Example, a lipstick was prepared in the same manner as in Example 7, except that 50 g of the cosmetic composition of Example 6 was used to prepare a lipstick in the case of using the cosmetic composition (B).

[ Test Example 1 ]

The lipstick was prepared in the same manner as in Example 7 except that the lipstick was prepared using only 100 wt% of the lipstick composition (A) without using the cosmetic composition (B).

The lipstick thus prepared was determined as Comparative Example 1 for comparison with the above Examples 7 to 12 for moisturizing properties, flavor and hue development, and preservation period extension.

The feeling of use and the water loss (TWEL) of the lipstick according to Examples 7 to 12 and the lipstick according to Comparative Example 1 were measured. The results are shown in Tables 1 and 2 below.

<Feeling test>

The lipsticks shown in Examples 6 to 10 and the lipstick shown in Comparative Example 1 were used for 20 days for 20 women (5 persons for each generation) for 50 days.

And satisfaction with use of moisture, moisturizing power, incense, color, etc. were evaluated in a comprehensive manner and classified into very satisfied ◎, satisfactory ◯, normal □, dissatisfied △, and very unsatisfactory ×. If the total score is 100 points or more, the total score is ◎. If the score is more than 75 and less than 90 points, it is satisfied. ○ If the score is 50 or more, the score is less than 75 points. □ If the score is less than 40 points, Very unsatisfactory ×.

age Example 7 Example 8 Example 9 Example 10 Example 11 Comparative Example 1 20's ○ ○ ○ ○ □ ○ 30s ○ ◎ ◎ ◎ ○ ○ 40s ◎ ◎ ◎ ◎ ○ △ 50s ◎ ◎ ◎ ◎ ◎ △

&Lt; Measurement of water loss (TWEL) >

The subjects were 20 women in their 20s and 50s (5 women in each generation). The subjects were stabilized for 30 minutes to 1 hour in an environment with a temperature of 23 ~ 27 ℃ and a relative humidity of 40 ~ 60% The experiment was conducted in the same place.

Water loss (TWEL) was measured before use of the lipstick of Examples 7 to 11 and the lipstick of Comparative Example 1, 1 hour after use, and 3 hours after use.

Using the Corneometer CM 825 (Courage and Khazaka, Germany), the probe was brought into close contact with the surface of the measurement site and then lightly pressed. The displayed value was expressed in arbitrary units (AU) .

Using a Tewarmeter TM 210 (Courgae and Khazaka, Germany), a device for comparing transepidermal water loss (TWEL), the probe was placed vertically on the site of measurement and maintained horizontal for more than 15 seconds, m ² h) was measured.

Corneometry and tewarmeter measurements were performed 5 times each time and the mean values were obtained and analyzed. Table 2 summarizes the measurement results.

Water loss (g / m ² h) Before use After 1 hour After 3 hours Example 7 6.0 5.8 5.2 Example 8 6.0 5.9 5.6 Example 9 6.0 5.9 5.7 Example 10 6.0 5.9 5.6 Example 11 6.0 5.9 5.6 Comparative Example 1 6.0 6.2 6.3

As a result of comparing the amount of water loss, the greatest difference was found between the lipstick of Example 7 and the lipstick of Comparative Example 1, and it was confirmed that the lipsticks shown in Examples 8 to 11 showed almost similar water loss. Also, it was confirmed that the lipsticks shown in Examples 7 to 11 according to the present invention had decreased water loss with the lapse of time.

The moisturizing cosmetic composition using the natural extract according to the present invention and the lipstick containing the natural extract can enhance the functionality of moisturizing, flavor and color development by using natural extracts, so that the safety of the inherent use of natural materials and the function of lipstick are harmonized, It is highly likely to be used industrially.

Claims (7)

The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 50 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator After concentrating under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 10 wt% of bamboo shoot extract pulverized into 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using a freeze dryer, 10 wt% of sea cucumber extract crushed into 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 10 wt% of Spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days 10 wt% of the golden extract was pulverized into 30 to 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying Dried for 2 to 4 days, and then 10 wt% of marshmallow leaf extract pulverized into 30 to 50 mesh.
The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 50 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator The mixture was concentrated under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 9 wt% of bamboo shoot extract pulverized to 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 9 wt% of sea cucumber extract crushed by 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 9 wt% of spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, 9 wt% of gold extract pulverized with 30 ~ 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After drying for 2 ~ 4 days, 9 wt% of mung bean leaf extract, pulverized with 30 ~ 50 mesh,
The dried bridges are dried in a drier at a temperature of 55 to 65 ° C for 20 to 26 hours, mixed with dried bridges and distilled water at a ratio of 1:10 to 15, heated in a hot water bath for 2 to 4 hours for extraction, The resulting filtrate was concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours at 0.1 to 0.3 mPA, dried for 2 to 4 days using a freeze dryer, A 30-50 mesh pulverized alum extract;
The mixture was mixed at a ratio of 1:10 to 15 by weight of ethanol, and then the mixture was extracted at room temperature for 70 to 74 hours. The extracted extract was centrifuged to obtain supernatant. The supernatant obtained by repeating this procedure twice, The mixture was filtered, concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours under a condition of 0.1 to 0.3 mPA, dried for 2 to 4 days using a freeze dryer, Wherein the composition comprises 5 wt% of a first mixture of 100 wt% mixed with 1 wt% of an extract of Mulberry bark extract, which is in the form of a powder obtained by pulverizing the mixture into 30 to 50 mesh.
The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 50 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator The mixture was concentrated under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 9 wt% of bamboo shoot extract pulverized to 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 9 wt% of sea cucumber extract crushed by 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 9 wt% of spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, 9 wt% of gold extract pulverized with 30 ~ 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After drying for 2 ~ 4 days, 9 wt% of mung bean leaf extract, pulverized with 30 ~ 50 mesh,
The green tea leaves were cleaned with distilled water and dried at 25 to 26 ° C for 23 to 26 hours. The dried green tea leaves were pulverized using a pulverizer, and the pulverized green tea leaf powder and ethanol were mixed at a ratio of 1:10 to 15 After mixing, the mixture was extracted with stirring at room temperature for 22 to 26 hours. The extract was filtered, concentrated under reduced pressure using a vacuum rotation evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA, ), Dried for 2 ~ 4 days, and then pulverized with a homogenizer to 30 ~ 50 mesh; powdery green tea leaf extract;
Dandelion powder was mixed with distilled water at a ratio of 1:10 to 15, and the mixture was shaken in a shaking incubator at 24 to 28 ° C for 30 to 60 hours at 160 rpm , And the extract was filtered and concentrated under reduced pressure using a vacuum rotary evaporator for 5 to 7 hours under the condition of 0.1 to 0.3 mPA. And 5 wt% of a second mixture of 100 wt% of a mixture of dandelion extracts in the form of powder obtained by pulverizing the mixture to 30 to 50 mesh using a homogenizer in a weight ratio of 1: 1. Wherein the cosmetic composition is a cosmetic composition.
The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 50 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator The mixture was concentrated under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 9 wt% of bamboo shoot extract pulverized to 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 9 wt% of sea cucumber extract crushed by 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 9 wt% of spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, 9 wt% of gold extract pulverized with 30 ~ 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After drying for 2 ~ 4 days, 9 wt% of mung bean leaf extract, pulverized with 30 ~ 50 mesh,
The powder was mixed with ethanol at a weight ratio of 1:10 to 15, and then the mixture was extracted with stirring at room temperature for 22 to 26 hours. The extract was filtered, washed with a vacuum (0.1 to 0.3 mPa) dried in a freeze dryer for 2 to 4 days, and then pulverized with a homogenizer to a size of 30 to 50 mesh;
The extracts were filtered and washed with vacuum rotation (0.1-0.3 mPa) for 5-7 hours. The extracts were filtered, washed with water, evaporator), dried for 2 to 4 days using a freeze dryer, and then pulverized to a size of 30 to 50 mesh using a homogenizer to prepare a powder mixture of juniper extract at a ratio of 1: 1 by weight And 5 wt% of a third mixture of 100 wt% of the cosmetic composition.
The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 50 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator The mixture was concentrated under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 9 wt% of bamboo shoot extract pulverized to 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 9 wt% of sea cucumber extract crushed by 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 9 wt% of spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, 9 wt% of gold extract pulverized with 30 ~ 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After drying for 2 ~ 4 days, 9 ~ 10 wt%
The extracts were obtained by extracting the mixture with a hot water extractor for 2 to 4 hours, filtering the extract, filtering the extracts at a concentration of 0.1 to 0.3 mPa for 5 to 7 hours The mixture was concentrated under reduced pressure using a vacuum rotation evaporator, dried for 2 to 4 days using a freeze dryer, and then pulverized with a homogenizer to a size of 30 to 50 mesh to obtain 5 wt% The cosmetic composition according to claim 1,
The mixture obtained by mixing lime leaf and ethanol at a weight ratio of 1: 1.5-3 was leached at room temperature for 20 to 30 hours to obtain a primary extract, which was then filtered. The same procedure was repeated twice, The mixture was concentrated under reduced pressure for 5 to 7 hours with a vacuum rotation evaporator at 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, pulverized to 30 to 50 mesh, 52 wt% of leaf extract,
The mixture obtained by mixing the fine powder of bamboo shoot with ethanol at a weight ratio of 1: 9 to 12 is extracted by sonication. The extract is filtered with a filter paper, and the filtered extract is concentrated by a vacuum rotation evaporator The mixture was concentrated under reduced pressure for 5 to 7 hours under the conditions of 0.1 to 0.3 mPA, lyophilized for 2 to 4 days using a freeze dryer, 9 wt% of bamboo shoot extract pulverized to 30 to 50 mesh,
The mixture of sea cucumber and ethanol at a weight ratio of 1:10 to 12 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, After drying for 2 ~ 4 days using freeze dryer, 9 wt% of sea cucumber extract crushed by 30 ~ 50 mesh,
The mixture of Spirulina and distilled water at a ratio of 1: 35 to 45 is extracted at a shaking incubator at 24 to 26 ° C for 65 to 75 hours at 120 to 160 rpm and the extract is centrifuged at 7,500 to 8,500 rpm for 15 to 25 minutes The supernatant obtained by centrifugation was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by a vacuum rotation evaporator, dryer for 2 ~ 4 days, 9 wt% of spirulina extract pulverized with 30 ~ 50 mesh,
The mixture obtained by mixing gold and methanol at a weight ratio of 1: 4 to 6 was refluxed at 65 to 75 ° C for 20 to 30 hours, and the extract was centrifuged at 3,500 to 4,500 rpm for 4 to 6 minutes, The mixture was filtered through filter paper and the filtrate was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by vacuum rotation evaporator and dried in a freeze dryer for 2 to 4 days After drying, 9 wt% of gold extract pulverized with 30 ~ 50 mesh,
Dried in a freeze dryer and processed into a powder form. Powdered manganese leaves and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying After drying for 2 ~ 4 days, 9 wt% of mung bean leaf extract, pulverized with 30 ~ 50 mesh,
The mixture was mixed with methanol at a weight ratio of 1:10 to 15, and then the mixture was extracted with stirring at room temperature for 22 to 26 hours. The extract was filtered, concentrated under reduced pressure using a vacuum rotation evaporator, dryer for 2 ~ 4 days and then powdered with 30 ~ 50 mesh using a homogenizer.
The moss was washed with hot air at 55 to 65 ° C and then pulverized. The pulverized moss and 100% methanol were mixed at a weight ratio of 1:10 to 15, and the mixture was cooled to a temperature of 58 to 62 ° C at a temperature of 58 to 62 ° C The extract was filtered, concentrated under reduced pressure using a vacuum rotation evaporator, dried in a freeze dryer for 2 to 4 days, and then homogenized in a homogenizer for 30 ~ Powdery mash extract powder 25 wt% ground by 50 mesh;
Dried in a freeze drier, processed into powder form, powdered Baekjong and distilled water were mixed at a weight ratio of 1:10 to 12 times, and the mixture was refluxed at 75 to 85 ° C for 2 to 4 hours The extract was filtered with a filter paper, and the filtered extract was concentrated under reduced pressure for 5 to 7 hours under a condition of 0.1 to 0.3 mPa by using a vacuum rotation evaporator, followed by freeze drying Dried for 2 ~ 4 days and then pulverized with 30 ~ 50 mesh using a homogenizer.
After mixing the grapefruit seeds and ethanol at a weight ratio of 1: 5 to 10, the mixture was refluxed for 2 to 3 hours at a temperature of 60 to 62 ° C, centrifuged at 10,000 × g for 20 to 40 minutes, Concentrate under reduced pressure (0.1-0.3 mPa) for 5 ~ 7 hours using a vacuum rotation evaporator, dry for 2 ~ 4 days using a freeze dryer, and homogenize at 30 ~ 50 mesh And 3 wt% of a fourth mixture of 100 wt% composed of a mixture of 25 wt% of a grapefruit seed extract in the form of pulverized powder.
A moisturizing lipstick characterized in that it comprises 0.1 to 50 wt% of any one cosmetic composition selected from the claims 1 to 6 based on the total weight of the cosmetic.