CN107375145B - Cosmetic matrix, preparation method and application thereof, eye cream and preparation method thereof - Google Patents

Cosmetic matrix, preparation method and application thereof, eye cream and preparation method thereof Download PDF

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CN107375145B
CN107375145B CN201710678389.9A CN201710678389A CN107375145B CN 107375145 B CN107375145 B CN 107375145B CN 201710678389 A CN201710678389 A CN 201710678389A CN 107375145 B CN107375145 B CN 107375145B
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extract
eye cream
cosmetic
mass
water
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CN107375145A (en
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王娟
裴运林
聂艳峰
刘露
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Guangzhou Marubi Biotechnology Co ltd
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Guangzhou Marubi Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention discloses a cosmetic matrix, a preparation method and application thereof, eye cream and a preparation method thereof, and relates to the technical field of cosmetics. The cosmetic matrix is mainly prepared from the following raw materials in percentage by mass: 10-20% of tea extract-coated boswellia serrata extract, 5-10% of citrus peel extract, 10-20% of date seed, 55-10% of acetyl tetrapeptide, 3-6% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-6% of polygonum cuspidatum root extract, 1-3% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water. The invention solves the technical problems of poor effects of removing dark eye circles and improving skin brightness of the existing eye cosmetics. The substrate can effectively reduce melanin and improve skin brightness through the cooperation of the raw materials, and the melanin of skin around eyes can be obviously reduced and the eyes can be brightened by applying the eye cream containing the substrate.

Description

Cosmetic matrix, preparation method and application thereof, eye cream and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a cosmetic matrix, a preparation method and application thereof, and eye cream and a preparation method thereof.
Background
The eyes are the parts of the face which are exposed to the age at the earliest, and the eyes which face to the face are vigorous, so that the whole face of the user is more youthful. The sub-ocular region is very sensitive and subject to irritation. It is nearly ten times thinner than skin in other parts of the body, with few sebaceous glands, and is therefore more prone to dryness and irritation. Dark circles are mostly inherited, but also due to the following factors: stress, unhealthy diet, vitamin and mineral deficiencies, smoking, alcohol consumption, uv damage, evidence of blood vessels and capillaries under the skin, irritation, and natural melanin. All or just some of these factors, coupled with the ever thinner dry skin and the effects of earth's gravity, pull on the skin and make the dark circles appear larger, dull and fatiguing.
The main causes of dark circles are poor blood circulation and blood leakage in delicate tissues around the eyes, and poor sleep also aggravates dark circles, which are the second major concern of consumers following wrinkles in european countries and several countries around the world. Therefore, a cosmetic for effectively removing black eyes is also important. The existing eye cosmetics have poor black eye circle removing effect, the melanin reducing effect on skin around eyes after use is limited, and meanwhile, the general eye cosmetics cannot well play a role in improving the skin brightness around eyes.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
The invention aims to provide a cosmetic matrix, which can effectively reduce melanin and improve skin brightness through the cooperation of raw materials, and can effectively relieve dark circles after being applied.
The second purpose of the invention is to provide a preparation method of the cosmetic matrix, which can obtain uniform and stable emulsion, has the advantages of simple method and easy operation, and is suitable for standardized production and popularization and application.
The invention also aims to provide the application of the cosmetic matrix in preparing skin-care cosmetics.
The invention also provides an eye cream containing the cosmetic base, which can effectively reduce melanin of skin around eyes after being applied on the eye cream, has the effect of brightening the eyes, and is a cosmetic for effectively removing black eyes.
The fifth purpose of the invention is to provide a preparation method of the eye cream, and the uniform and stable cream cosmetic can be obtained by using the method, so that the eye cream has the advantages of simple method and easy operation, and is suitable for standardized production and popularization and application.
In order to achieve the above purpose of the present invention, the following technical solutions are adopted:
the cosmetic matrix is mainly prepared from the following raw materials in percentage by mass: 10-20% of tea extract-coated boswellia serrata extract, 5-10% of citrus peel extract, 10-20% of date seed, 55-10% of acetyl tetrapeptide, 3-6% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-6% of polygonum cuspidatum root extract, 1-3% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
Preferably, on the basis of the technical scheme provided by the invention, the matrix is mainly prepared from the following component raw materials in percentage by mass: 12-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 12-18% of date seed, 56-10% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
Preferably, on the basis of the technical scheme provided by the invention, the matrix is mainly prepared from the following raw materials in percentage by mass: 15-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 16-18% of date seed, 56-8% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
Further, on the basis of the technical scheme provided by the invention, the mass ratio of the wild soybean protein to the hydrolyzed rice protein to the superoxide dismutase in the mixture of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase is (0.1-1) to (5-10) to (0.1-1).
A preparation method of the cosmetic matrix comprises the following steps:
the raw materials with the formula ratio are fully mixed, heated, kept warm, homogenized and cooled to obtain the cosmetic matrix.
Further, on the basis of the technical scheme provided by the invention, the preparation method of the cosmetic matrix comprises the following steps:
(a) heating water with the formula amount to 85-90 ℃, preserving heat for 20-30 min, and cooling to 30-35 ℃;
(b) adding the other raw materials into the cooled water in the step (a), stirring and homogenizing for 5-10 min at the stirring speed of 1000-3000 r/min, and removing residues to obtain the cosmetic matrix.
An application of the cosmetic matrix in preparing skin care cosmetics is provided.
The eye cream comprises the cosmetic base, wherein the cosmetic base accounts for 20-30% of the eye cream by mass.
Further, on the basis of the technical scheme provided by the invention, the eye cream is mainly prepared from the following raw materials in percentage by mass: 20-30% of a cosmetic matrix, 2-3% of PEG-60 hydrogenated castor oil, 61-2% of cetostearyl alcohol polyether, 1-2% of behenyl alcohol, 2-3% of shea butter, 3-4% of dioctyl carbonate, 3-4% of glycerol tri (ethyl hexanoate), 0.5-1% of tocopherol acetate, 8-10% of glycerol, 5-7% of butanediol, 0.5-0.8% of carbomer, 0.3-0.6% of triethanolamine and the balance of water.
Further, on the basis of the technical scheme provided by the invention, the eye cream also comprises a preservative and essence;
the preservative is 0.1-0.3% of the eye cream by mass;
the essence accounts for 0.01-0.03% of the eye cream by mass.
A preparation method of the eye cream comprises the following steps:
mixing PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopheryl acetate, heating, keeping the temperature to obtain an oily raw material, mixing the oily raw material with glycerol, butanediol, carbomer, triethanolamine and water, heating, keeping the temperature to obtain an aqueous raw material, homogenizing, cooling, adding a cosmetic matrix, optionally a preservative and essence, and removing residues to obtain the eye cream.
Preferably, on the basis of the technical scheme provided by the invention, the preparation method of the eye cream comprises the following steps:
(a) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring and heating to 75-85 ℃, and keeping the temperature for later use to obtain an oil phase raw material;
(b) adding glycerol, butanediol, carbomer and triethanolamine into a water phase pot, stirring and heating to 80-90 ℃, and keeping the temperature for later use to obtain a water phase raw material;
(c) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, and stirring and homogenizing for 5-10 min at the stirring speed of 1000-3000 r/min;
(d) and after homogenizing, continuously stirring and cooling to 40-45 ℃, adding a cosmetic matrix, and optionally a preservative and essence, stirring for 10-15 min, and removing residues to obtain the eye cream.
Compared with the prior art, the invention has the following beneficial effects:
(1) the cosmetic matrix disclosed by the invention is prepared by reasonably matching a tea extract coated boswellia serrata extract, an orange peel extract, date seeds, acetyl tetrapeptide-5, wild soybean protein, a hydrolyzed rice protein and superoxide dismutase mixture, a polygonum cuspidatum root extract and ascorbyl tetraisopalmitate, and optimizing the formula amount of the cosmetic matrix, so that the effects of the components can be fully matched and complemented in a synergistic manner, the antioxidation effect is obvious, the melanin can be remarkably reduced, the skin color is lightened, and the black eye can be effectively relieved after the cosmetic matrix is applied.
(2) The cosmetic matrix can be used as a raw material to be added into skin care cosmetics such as essence, emulsion, cream and the like, and has a good effect of improving dark circles.
(3) The eye cream disclosed by the invention can effectively reduce melanin of skin around the eyes and brighten the skin color around the eyes by adding the cosmetic matrix with a specific content, can effectively relieve dark circles after being smeared, and is a cosmetic for efficiently removing the dark circles.
(4) The cosmetic matrix and the eye cream have the advantages of simple preparation process, convenient use, capability of obtaining uniform and stable emulsion and cream products, simple method and easy operation, and are suitable for standardized production, popularization and application.
Detailed Description
Embodiments of the present invention will be described in detail below with reference to examples, but it will be understood by those skilled in the art that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
According to a first aspect of the invention, a cosmetic base is provided, which is mainly prepared from the following raw materials in percentage by mass: 10-20% of tea extract-coated boswellia serrata extract, 5-10% of citrus peel extract, 10-20% of date seed, 55-10% of acetyl tetrapeptide, 3-6% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-6% of polygonum cuspidatum root extract, 1-3% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
Tea extract coated boswellia serrata extract
Tea (CAMELLIA SINENSIS) extract is coated with BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, preferably from Naolys, france, pH: 4.5-7.5, the mastic extract is coated by white tea extract, the white tea extract is extracted by white tea as raw material, the main components comprise theanine (flavanol), phenolic acid, flavonol, depside acid, etc., wherein the catechin compound accounts for 65-80% of the total amount of tea polyphenol, the main active component of the mastic extract is from miraculous Indian mastic and contains 40% of mastic acid which is an active ingredient of allergy relieving.
The tea (CAMELLIA SINENSIS) extract is coated with BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract typically but not limited to, in mass percent, e.g., 10%, 11%, 12%, 13%, 14%, 15%, 16%, 17%, 18%, 19%, or 20%.
The tea (CAMELLIA SINENSIS) extract is used for wrapping theaflavin compound and boswellic acid in BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, and can effectively relieve dark eye circles and reduce fine wrinkles in eyes.
Citrus peel extract
Citrus (Citrus RETICULATA) pericarp extract is extracted from CITRUS peel, which contains multiple essential nutrients and beneficial substances, and is rich in physiologically active components including flavonoids, flavanones, dietary fiber, essential oil, carotene, and saccharides. The extract of pericarp of CITRUS (Citrus RETICULATA) can be selected from commercially available products, preferably extract of pericarp of CITRUS (Citrus RETICULATA) produced by Nippon Populus L.
Typical but not limiting percentages by mass of CITRUS (CITRUS RETICULATA) peel extract are for example 5%, 6%, 7%, 8%, 9% or 10%.
The extract of pericarp of Citrus RETICULATA (Citrus RETICULATA) can brighten skin and increase skin transparency.
Date seed
Date (Phoenix DACTYLIFERA) seed is a water-soluble plant extract from date palm seed. The date (Phoenix DACTYLIFERA) seed is commercially available, preferably from IBR (Albizia) with pH: 3.0-5.0.
Typical but not limiting mass percentages of date palm (PHOENIX DACTYLIFERA) seeds are for example 10%, 11%, 12%, 13%, 14%, 15%, 16%, 17%, 18%, 19% or 20%.
The date (Phoenix DACTYLIFERA) seed can slow down cell proliferation and simultaneously prevent oxidative damage, so that the aging can be comprehensively slowed down, and in-vitro tests show that the cream added with the raw material has very obvious effects of relieving dark circles and acne rosacea.
Acetyl tetrapeptide-5
Acetyl tetrapeptide-5 may be selected from commercially available products, preferably available from the pharmaceutical, pH: 5.4-6.4, refractive index: 1.320-1.440.
Typical but not limiting mass percentages of acetyl tetrapeptide-5 are, for example, 5%, 6%, 7%, 8%, 9%, or 10%.
The acetyl tetrapeptide-5 can inhibit capillary permeability and promote lymphatic microcirculation, thereby achieving the effects of relieving under-eye puffiness and dark circles.
Mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase
The mixture of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase is a mixture formed by mixing the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase (SOD) in any proportion, the wild soybean protein and the hydrolyzed rice protein are purely natural soybean and rice polypeptides, and the superoxide dismutase (SOD) is extracted from a natural yeast strain by using a biotechnology.
The soy protein, hydrolyzed rice protein and superoxide dismutase mixture is preferably available from DSM, switzerland, PH: 5.3-6.3, refractive index: 1.366-1.370.
Typical but not limiting percentages by mass of the mixture are, for example, 3%, 4%, 5% or 6%.
The pure natural soybean and rice polypeptide and the superoxide dismutase extracted from the natural yeast strain by utilizing the biotechnology can promote the circulation of capillary vessels and improve the dark circles.
Polygonum cuspidatum root extract
The rhizoma Polygoni Cuspidati (Polygonum CUSPIDATUM) root extract is prepared from rhizoma Polygoni Cuspidati (Polygonum CUSPIDATUM) of Polygonaceae of Polygonum of perennial herb, and has effects of promoting blood circulation, removing blood stasis, dredging channels and relieving cough. Rhizoma Polygoni Cuspidati contains multiple bioactive substances, and resveratrol is one of its main active ingredients. The extract of rhizoma Polygoni Cuspidati (Polygonum CUSPIDATUM) root can be obtained from commercially available products, preferably from BIOLAND, pH: 4.0-6.0, refractive index: 1.340-1.380.
Typical but not limiting mass percentages of the extract of the root of POLYGONUM CUSPIDATUM (POLYGONUM CUSPIDATUM) are, for example, 3%, 4%, 5% or 6%.
The extract of the root of Polygonum CUSPIDATUM (Polygonum CUSPIDATUM) can inhibit skin pigmentation through various mechanisms, including initial signal transmission and gene expression, as well as melanin production and final melanin transfer, and has strong antioxidant effect.
Ascorbyl tetraisopalmitate
Ascorbyl tetraisopalmitate palmitic acid is esterified with natural ingredients such as L-ascorbic acid and may be selected from commercially available products, preferably available from japanese sun light company, refractive index: 1.459-1.465.
Typical but not limiting percentages by mass of ascorbyl tetraisopalmitate are for example 1%, 1.5%, 2%, 2.5% or 3%.
The ascorbyl tetraisopalmitate can inhibit intracellular tyrosinase activity and melanin generation, and can improve skin color.
PEG-40 hydrogenated Castor oil
PEG-40 hydrogenated castor oil is a white waxy surfactant, and may be selected from commercially available products, preferably from Basff.
Typical but not limiting mass percentages of PEG-40 hydrogenated castor oil are for example 1%, 1.2%, 1.4%, 1.6%, 1.8% or 2%.
Water (W)
The water is preferably deionized water.
By "consisting essentially of" as used herein is meant that it may include, in addition to the recited materials, other materials that impart different properties to the substrate. In addition, the term "consisting essentially of" as used herein may be replaced by "being" or "consisting of … …" as used herein in the closed-loop fashion.
For example, other components such as preservatives may also be included.
It is to be noted that the balance of water means that the balance of the raw materials of the matrix of the present invention excluding the tea extract-coated boswellia serrata extract, the citrus peel extract, the date seed, the acetyl tetrapeptide-5, the wild soybean protein, the hydrolyzed rice protein and superoxide dismutase mixture, the polygonum cuspidatum root extract, ascorbyl tetraisopalmitate, PEG-40 hydrogenated castor oil and optionally other components is water, and the sum of the mass percentages of water-coated boswellia serrata extract, the citrus peel extract, the date seed, the acetyl tetrapeptide-5, the wild soybean protein, the hydrolyzed rice protein and superoxide dismutase mixture, the polygonum cuspidatum root extract, ascorbyl tetraisopalmitate, PEG-40 hydrogenated castor oil and optionally other components is 100%.
The invention screens the functional components through tests, researches the improvement effect of the functional components on the dark circles, finds that the functional components have the improvement effect on the dark circles of the eyes to different degrees, considers the reasonable collocation of the functional components, the cosmetic matrix can exert excellent effect by optimizing the formula amount of each component in synergistic cooperation, the cosmetic matrix of the invention is prepared by selecting tea extract with specific content to wrap boswellia serrata extract, citrus peel extract, date seed, acetyl tetrapeptide-5, wild soybean protein, hydrolyzed rice protein and superoxide dismutase mixture, polygonum cuspidatum root extract and ascorbyl tetraisopalmitate, the effects of the components can be mutually cooperated and complemented, the antioxidation effect is obvious, the melanin can be obviously reduced, the skin color can be brightened, and the black eye can be effectively relieved after the black eye cream is smeared.
In a preferred embodiment, the matrix is mainly prepared from the following component raw materials in percentage by mass: 12-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 12-18% of date seed, 56-10% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
In a preferred embodiment, the matrix is mainly prepared from the following raw materials in percentage by mass: 15-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 16-18% of date seed, 56-8% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
By optimizing the mixture ratio of the components, the antioxidant effect and black eye removing effect of the matrix can be further enhanced.
In a preferred embodiment, the mass ratio of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase in the mixture of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase is (0.1-1): (5-10): (0.1-1).
Typical but non-limiting mass ratios of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase are, for example, 0.1:5:0.1, 0.2:5:0.2, 0.5:5:0.5, 0.6:5:0.6, 1:5:1, 0.1:8:0.2, 0.5:8:0.5, 1:8:1 or 1:10: 1.
The black eye removing matrix with better effect can be obtained by the mixture with a specific proportion.
According to a second aspect of the present invention, there is provided a process for the preparation of the cosmetic base described above, comprising the steps of:
the raw materials with the formula ratio are fully mixed, heated, kept warm, homogenized and cooled to obtain the cosmetic matrix.
Preferably, the mixing and heating process can be performed by a stirring and heating method, homogenization is also called homogenization, and is a treatment process for micronizing and homogenizing a dispersion in a suspension (or emulsion) system, the treatment process simultaneously plays a role in reducing the size of the dispersion and improving the distribution uniformity of the dispersion, and the homogenization process is preferably performed under the high-speed condition that the rotating speed is more than 1000 r/min.
Through mixing, heating, heat preservation and homogenization, the active ingredients can be fully mixed, the active ingredients can be fully released, and a uniform and stable emulsion matrix which is light yellow can be obtained.
In a preferred embodiment, the method of making the cosmetic base comprises the steps of:
(a) heating water with the formula amount to 85-90 ℃, preserving heat for 20-30 min, and cooling to 30-35 ℃;
(b) adding the other raw materials into the cooled water in the step (a), stirring and homogenizing for 5-10 min at the stirring speed of 1000-3000 r/min, and removing residues to obtain the cosmetic matrix.
Other raw materials refer to all other raw materials of the matrix raw material except for water.
Typical but non-limiting heating temperatures for step (a) are 85 ℃, 86 ℃, 87 ℃, 88 ℃, 89 ℃ or 90 ℃.
Typical but non-limiting incubation times for step (a) are 20min, 22min, 24min, 26min, 28min or 30 min.
Typical but non-limiting cooling temperatures for step (a) are 30 ℃, 31 ℃, 32 ℃, 33 ℃, 34 ℃ or 35 ℃.
Typical but non-limiting homogenization times for step (b) are 5min, 6min, 7min, 8min, 9min or 10 min.
The stirring speed of step (b) is typically, but not limited to, 1000r/min, 1500r/min, 2000r/min, 2500r/min or 3000 r/min.
The deslagging is preferably performed by adopting a filtering mode, and is preferably performed by adopting 200-mesh and 300-mesh filter cloth.
Under certain conditions, water is firstly subjected to high-temperature, heat preservation and cooling treatment, and then other raw materials are added for homogenization under certain conditions, so that the damage of high temperature to effective components in the preparation process can be avoided, the active components in the water are retained, and a uniform and stable matrix is obtained.
According to a third aspect of the present invention, there is provided the use of a cosmetic base as described above in the manufacture of a skin care cosmetic product.
Typical, but non-limiting, skin care cosmetic products include essences, lotions, or creams.
According to a fourth aspect of the invention, the eye cream comprises the cosmetic base, and the cosmetic base accounts for 20-30% of the eye cream by mass.
Typical but non-limiting mass percentages of the base in the eye cream are for example 20%, 22%, 24%, 26%, 28% or 30%.
The matrix of the invention is added into the eye cream in a specific proportion, which can bring the effect of obviously relieving black eye and brighten the color of the skin around the eyes.
A typical eye cream is mainly prepared from the following raw materials in percentage by mass: 20-30% of a cosmetic matrix, 2-3% of PEG-60 hydrogenated castor oil, 61-2% of cetostearyl alcohol polyether, 1-2% of behenyl alcohol, 2-3% of shea butter, 3-4% of dioctyl carbonate, 3-4% of glycerol tri (ethyl hexanoate), 0.5-1% of tocopherol acetate, 8-10% of glycerol, 5-7% of butanediol, 0.5-0.8% of carbomer, 0.3-0.6% of triethanolamine and the balance of water.
Typical but not limiting mass percentages of the cosmetic base are for example 20%, 22%, 24%, 26%, 28% or 30%.
Typical but not limiting mass percentages of PEG-60 hydrogenated castor oil are for example 2%, 2.2%, 2.4%, 2.6%, 2.8% or 3%.
Typical but not limiting percentages by mass of ceteareth-6 are, for example, 1%, 1.2%, 1.4%, 1.6%, 1.8% or 2%.
Typical but not limiting percentages by mass of behenyl alcohol are for example 1%, 1.2%, 1.4%, 1.6%, 1.8% or 2%.
Typical but not limiting percentages by mass of shea butter are for example 2%, 2.2%, 2.4%, 2.6%, 2.8% or 3%.
Typical but not limiting mass percentages of dioctyl carbonate are, for example, 3%, 3.2%, 3.4%, 3.6%, 3.8%, or 4%.
Typical but not limiting percentages by mass of glycerol tri (ethylhexanoate) are, for example, 3%, 3.2%, 3.4%, 3.6%, 3.8% or 4%.
Typical but not limiting mass percentages of tocopherol acetate are for example 0.5%, 0.6%, 0.7%, 0.8%, 0.9% or 1%.
Typical but not limiting mass percentages of glycerol are for example 8%, 8.2%, 8.4%, 8.6%, 8.8%, 9%, 9.2%, 9.4%, 9.6%, 9.8% or 10%.
Typical but non-limiting mass percentages of butanediol are for example 5%, 5.2%, 5.4%, 5.6%, 5.8%, 6%, 6.2%, 6.4%, 6.6%, 6.8% or 7%.
Typical but not limiting percentages by mass of carbomer are for example 0.5%, 0.6%, 0.7% or 0.8%.
Typical but not limiting percentages by mass of triethanolamine are for example 0.3%, 0.4%, 0.5% or 0.6%.
The water is preferably deionized water.
By "consisting essentially of it is meant that it may include, in addition to the materials, other materials which impart different characteristics to the eye cream. In addition, the term "consisting essentially of" as used herein may be replaced by "being" or "consisting of … …" as used herein in the closed-loop fashion.
For example, other components such as preservatives, fragrances, and the like may also be included.
It is to be noted that the balance of water means that the balance of the raw materials of the eye cream of the present invention excluding the cosmetic base, PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethylhexanoate), tocopherol acetate, glycerol, butylene glycol, carbomer, triethanolamine and optionally other components is water, and the sum of the mass percentages of water and the cosmetic base, PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethylhexanoate), tocopherol acetate, glycerol, butylene glycol, carbomer, triethanolamine and optionally other components is 100%.
The eye cream disclosed by the invention can obtain an obvious black eye removing effect by adding the matrix disclosed by the invention with a specific content, and meanwhile, the eye cream is mutually cooperated with other eye cream raw materials, so that the best eye removing effect can be obtained, the skin brightness around eyes can be obviously improved, fine lines of eyes can be slowed down, and the eye cream is an ideal eye cream product with an efficient black eye removing effect and a good comprehensive effect.
In a preferred embodiment, the eye cream further comprises a preservative and a fragrance;
the preservative accounts for 0.1-0.3% of the eye cream by mass;
the essence accounts for 0.01-0.03% of the eye cream by mass.
Typical but not limiting percentages by mass of preservatives are for example 0.1%, 0.2% or 0.3%.
Typical but not limiting mass percentages of perfume are for example 0.01%, 0.02% or 0.03%.
By adding the preservative and the essence, the shelf life of the eye cream can be prolonged, the fragrance of the eye cream can be improved, and the comprehensive performance of the eye cream can be optimized.
According to a fifth aspect of the present invention, there is provided a method for preparing the above eye cream, comprising the steps of:
mixing PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopheryl acetate, heating, keeping the temperature to obtain an oily raw material, mixing the oily raw material with glycerol, butanediol, carbomer, triethanolamine and water, heating, keeping the temperature to obtain an aqueous raw material, homogenizing, cooling, adding a cosmetic matrix, optionally a preservative and essence, and removing residues to obtain the eye cream.
Preferably, in particular, the method for preparing the above eye cream comprises the following steps:
(a) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring and heating to 75-85 ℃, and keeping the temperature for later use to obtain an oil phase raw material;
(b) adding glycerol, butanediol, carbomer and triethanolamine into a water phase pot, stirring and heating to 80-90 ℃, and keeping the temperature for later use to obtain a water phase raw material;
(c) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, and stirring and homogenizing for 5-10 min at the stirring speed of 1000-3000 r/min;
(d) and after homogenizing, continuously stirring and cooling to 40-45 ℃, adding a cosmetic matrix, and optionally a preservative and essence, stirring for 10-15 min, and removing residues to obtain the eye cream.
Typical but non-limiting temperature increases for step (a) are 75 deg.C, 76 deg.C, 77 deg.C, 78 deg.C, 79 deg.C, 80 deg.C, 81 deg.C, 82 deg.C, 83 deg.C, 84 deg.C or 85 deg.C.
Typical but non-limiting temperature increases for step (b) are 80 deg.C, 81 deg.C, 82 deg.C, 83 deg.C, 84 deg.C, 85 deg.C, 86 deg.C, 87 deg.C, 88 deg.C, 89 deg.C or 90 deg.C.
Typical but non-limiting homogenization times for step (c) are 5min, 6min, 7min, 8min, 9min or 10 min.
The stirring speed of step (c) is typically, but not limited to, 1000r/min, 1500r/min, 2000r/min, 2500r/min or 3000 r/min.
Typical but non-limiting temperature reductions for step (d) are 40 ℃, 41 ℃, 42 ℃, 43 ℃, 44 ℃ or 45 ℃. Typical but non-limiting stirring times are 10min, 11min, 12min, 13min, 14min or 15 min.
The deslagging is preferably performed by adopting a filtering mode, and is preferably performed by adopting a 200-mesh filter cloth.
The water-based raw materials and the oily raw materials are respectively obtained under certain conditions, then are mixed and homogenized, and finally the matrix is added, so that the damage of high temperature to the effective components in the matrix in the preparation process can be avoided, the active components in the matrix can be better reserved, and the uniform and stable eye cream product can be finally obtained.
For further understanding of the present invention, the method and effects of the present invention will be described in further detail with reference to specific examples. All the raw materials related to the invention can be obtained commercially.
Tea (CAMELLIA SINENSIS) extract-encapsulated BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract was obtained from Naolys, france, pH: 4.5 to 7.5;
citrus (Citrus RETICULATA) pericarp extract was obtained from Nippon mono-pill company;
date (PHOENIX DACTYLIFERA) seeds were purchased from IBR (erbia) corporation, pH: 3.0-5.0;
acetyl tetrapeptide-5 was purchased from the zhhai federal pharmaceutical, pH: 5.4-6.4, refractive index: 1.320-1.440;
a mixture of wild soybean (GLYCINE SOJA) protein, hydrolyzed rice protein and superoxide dismutase (SOD) was purchased from DSM, switzerland, pH: 5.3-6.3, refractive index: 1.366 to 1.370, wherein the mass ratio of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase is (0.1 to 1): 5 to 10): 0.1 to 1;
polygonum CUSPIDATUM (Polygonum CUSPIDATUM) root extract is obtained from BIOLAND, pH: 4.0-6.0, refractive index: 1.340-1.380;
ascorbyl tetraisopalmitate was purchased from japanese sun company, refractive index: 1.459 to 1.465;
PEG-40 hydrogenated castor oil was purchased from Pasteur. Other raw materials are all commercial products.
Example 1
A cosmetic matrix is prepared from the following raw materials in percentage by mass: 10% of tea extract-coated boswellia serrata extract, 5% of citrus peel extract, 10% of date seed, 510% of acetyl tetrapeptide, 6% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3% of polygonum cuspidatum root extract, 1% of ascorbyl tetraisopalmitate, 1% of PEG-40 hydrogenated castor oil and 54% of deionized water.
The preparation method of the cosmetic matrix comprises the following specific steps:
(1) heating 54% deionized water to 85 deg.C, maintaining the temperature for 20min, and cooling to 35 deg.C;
(2) adding 10% tea (CAMELLIA SINENSIS) extract coated BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, 5% CITRUS (CITRUS RETICULATA) pericarp extract, 10% date (PHOENIX DACTYLIFERA) seed, 10% acetyl tetrapeptide-5, 6% wild soybean (GLYCINE SOJA) protein, hydrolyzed rice protein, superoxide dismutase (SOD) mixture, 3% giant knotweed (POLYGONUM CUSPIDATUM) root extract, 1% ascorbyl tetraisopalmitate and 1% PEG-40 hydrogenated castor oil into the water in step (1), homogenizing for 10min at a homogenizing speed of 3000r/min, and filtering through 300 mesh filter cloth to obtain the cosmetic matrix.
Example 2
A cosmetic matrix is prepared from the following raw materials in percentage by mass: 13% of tea extract-coated boswellia serrata extract, 7% of citrus peel extract, 12% of date seed, 57% of acetyl tetrapeptide, 5% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 4% of polygonum cuspidatum root extract, 1% of ascorbyl tetraisopalmitate, 1% of PEG-40 hydrogenated castor oil and 50% of deionized water.
The preparation method of the cosmetic matrix comprises the following specific steps:
(1) heating 50% deionized water to 90 deg.C, maintaining the temperature for 25min, and cooling to 30 deg.C;
(2) adding 13% tea (CAMELLIA SINENSIS) extract coated BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, 7% CITRUS (CITRUS RETICULATA) pericarp extract, 12% date (PHOENIX DACTYLIFERA) seed, 7% acetyl tetrapeptide-5, 5% wild soybean (GLYCINE SOJA) protein, hydrolyzed rice protein, superoxide dismutase (SOD), 4% giant knotweed (POLYGONUM CUSPIDATUM) root extract, 1% ascorbyl tetraisopalmitate and 1% PEG-40 hydrogenated castor oil into the water in step (1), homogenizing for 10min at a homogenizing speed of 1000r/min, and filtering through 300 mesh filter cloth to obtain the cosmetic matrix.
Example 3
A cosmetic matrix is prepared from the following raw materials in percentage by mass: 15% of tea extract-coated boswellia serrata extract, 7% of citrus peel extract, 15% of date seed, 57% of acetyl tetrapeptide, 5% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 4% of polygonum cuspidatum root extract, 2% of ascorbyl tetraisopalmitate, 2% of PEG-40 hydrogenated castor oil and 43% of deionized water.
The preparation method of the cosmetic matrix comprises the following specific steps:
(1) 43% deionized water was heated to 87 ℃, held for 30min, and then cooled to 35 ℃.
(2) Adding 15% tea (CAMELLIA SINENSIS) extract coated BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, 7% CITRUS (CITRUS RETICULATA) pericarp extract, 15% date (PHOENIX DACTYLIFERA) seed, 7% acetyl tetrapeptide-5, 5% wild soybean (GLYCINE SOJA) protein, hydrolyzed rice protein, superoxide dismutase (SOD), 4% giant knotweed (POLYGONUM CUSPIDATUM) root extract, 2% ascorbyl tetraisopalmitate and 2% PEG-40 hydrogenated castor oil into the water in step (1), homogenizing for 8min at a homogenization speed of 2000r/min, and filtering through 300 mesh filter cloth to obtain the cosmetic matrix.
Example 4
A cosmetic matrix is prepared from the following raw materials in percentage by mass: 20% of tea extract-coated boswellia serrata extract, 10% of citrus peel extract, 20% of date seed, 510% of acetyl tetrapeptide, 6% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 6% of polygonum cuspidatum root extract, 3% of ascorbyl tetraisopalmitate, 2% of PEG-40 hydrogenated castor oil and 23% of deionized water.
The preparation method of the cosmetic matrix comprises the following specific steps:
(1) heating 23% deionized water to 88 deg.C, maintaining the temperature for 25min, and cooling to 32 deg.C.
(2) Adding 20% tea (CAMELLIA SINENSIS) extract coated BOSWELLIA SERRATA (BOSWELLIA SERRATA) extract, 10% CITRUS (CITRUS RETICULATA) pericarp extract, 20% date (PHOENIX DACTYLIFERA) seed, 10% acetyl tetrapeptide-5, 6% wild soybean (GLYCINE SOJA) protein, hydrolyzed rice protein, superoxide dismutase (SOD), 6% giant knotweed (POLYGONUM CUSPIDATUM) root extract, 3% ascorbyl tetraisopalmitate and 2% PEG-40 hydrogenated castor oil into the water in step (1), homogenizing for 5min at a homogenizing speed of 3000r/min, and filtering through 300 mesh filter cloth to obtain the cosmetic matrix.
Example 5
An eye cream containing a cosmetic base, which consists of the following components in percentage by mass:
Figure BDA0001374461810000171
Figure BDA0001374461810000181
the preparation method of the eye cream comprises the following steps:
(1) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring at the rotating speed of 1000r/min, heating to 75 ℃, and keeping the temperature for 10min for later use to obtain an oil phase raw material;
(2) adding glycerol, butanediol, carbomer, triethanolamine and water into a water phase pot, stirring at 1000r/min, heating to 90 deg.C, and keeping the temperature for 15min to obtain water phase raw material;
(3) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, stirring and homogenizing for 5min, wherein the stirring speed is 3000 r/min;
(4) and after homogenizing, continuously stirring and cooling to 45 ℃, adding the cosmetic matrix, the preservative and the essence, stirring for 15min, filtering by using a 200-mesh filter cloth, and discharging to obtain the eye cream.
Example 6
An eye cream containing a cosmetic base, which consists of the following components in percentage by mass:
Figure BDA0001374461810000182
Figure BDA0001374461810000191
the preparation method of the eye cream comprises the following steps:
(1) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring at the rotating speed of 1000r/min, heating to 85 ℃, and keeping the temperature for 10min for later use to obtain an oil phase raw material;
(2) adding glycerol, butanediol, carbomer, triethanolamine and water into a water phase pot, stirring at 1000r/min, heating to 85 deg.C, and keeping the temperature for 15min to obtain water phase raw material;
(3) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, stirring and homogenizing for 10min, wherein the stirring speed is 1000 r/min;
(4) and after homogenizing, continuously stirring and cooling to 45 ℃, adding the cosmetic matrix, the preservative and the essence, stirring for 10min, filtering by using a 200-mesh filter cloth, and discharging to obtain the eye cream.
Example 7
An eye cream containing a cosmetic base, which consists of the following components in percentage by mass:
Figure BDA0001374461810000192
Figure BDA0001374461810000201
the preparation method of the eye cream comprises the following steps:
(1) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring at the rotating speed of 1000r/min, heating to 80 ℃, and keeping the temperature for 10min for later use to obtain an oil phase raw material;
(2) adding glycerol, butanediol, carbomer, triethanolamine and water into a water phase pot, stirring at 1000r/min, heating to 80 deg.C, and keeping the temperature for 15min to obtain water phase raw material;
(3) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, stirring and homogenizing for 8min, wherein the stirring speed is 2000 r/min;
(4) and after homogenizing, continuously stirring and cooling to 40 ℃, adding the cosmetic matrix, the preservative and the essence, stirring for 10min, filtering by using a 200-mesh filter cloth, and discharging to obtain the eye cream.
Example 8
An eye cream containing a cosmetic base, which consists of the following components in percentage by mass:
Figure BDA0001374461810000202
Figure BDA0001374461810000211
the preparation method of the eye cream comprises the following steps:
(1) adding PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopherol acetate into an oil phase pot, stirring at the rotating speed of 1000r/min, heating to 85 ℃, and keeping the temperature for 10min for later use to obtain an oil phase raw material;
(2) adding glycerol, butanediol, carbomer, triethanolamine and water into a water phase pot, stirring at 1000r/min, heating to 90 deg.C, and keeping the temperature for 15min to obtain water phase raw material;
(3) pumping the water phase raw material into an emulsifying pot, pumping into an oil phase pot, stirring and homogenizing for 5min, wherein the stirring speed is 3000 r/min;
(4) and after homogenizing, continuously stirring and cooling to 45 ℃, adding the cosmetic matrix, the preservative and the essence, stirring for 15min, filtering by using a 200-mesh filter cloth, and discharging to obtain the eye cream.
Comparative example 1
An eye cream containing no cosmetic base, the rest components were the same as in example 5, and the preparation method was the same as in example 5.
Comparative example 2
An eye cream containing a cosmetic base, wherein the cosmetic base is prepared from the following raw materials in percentage by mass: 5% of citrus peel extract, 10% of date seed, 510% of acetyl tetrapeptide, 6% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3% of polygonum cuspidatum root extract, 1% of ascorbyl tetraisopalmitate, 1% of PEG-40 hydrogenated castor oil and 64% of deionized water.
The other components were the same as in example 5, and the preparation method was the same as in example 5.
Comparative example 3
An eye cream containing a cosmetic base, wherein the cosmetic base is prepared from the following raw materials in percentage by mass: 13% of tea extract-coated boswellia serrata extract, 7% of citrus peel extract, 57% of acetyl tetrapeptide, 5% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 4% of polygonum cuspidatum root extract, 1% of ascorbyl tetraisopalmitate, 1% of PEG-40 hydrogenated castor oil and 62% of deionized water.
The other components were the same as in example 6, and the preparation method was the same as in example 6.
Comparative example 4
An eye cream containing a cosmetic base, wherein the cosmetic base is prepared from the following raw materials in percentage by mass: 15% of tea extract-coated boswellia serrata extract, 7% of citrus peel extract, 15% of date seed, 57% of acetyl tetrapeptide, 4% of polygonum cuspidatum root extract, 2% of ascorbyl tetraisopalmitate, 2% of PEG-40 hydrogenated castor oil and 48% of deionized water.
The other components were the same as in example 7, and the preparation method was the same as in example 7.
Comparative example 5
An eye cream containing a cosmetic base, wherein the cosmetic base is prepared from the following raw materials in percentage by mass: 20% of tea extract-coated boswellia serrata extract, 10% of citrus peel extract, 20% of date seed, 510% of acetyl tetrapeptide, 6% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3% of ascorbyl tetraisopalmitate, 2% of PEG-40 hydrogenated castor oil and 29% of deionized water.
The other components were the same as in example 8, and the preparation method was the same as in example 8.
Comparative example 6
An eye cream containing a cosmetic base, wherein the cosmetic base is prepared from the following raw materials in percentage by mass: 6% of tea extract-coated boswellia serrata extract, 15% of citrus peel extract, 8% of date seed, 53% of acetyl tetrapeptide, 10% of mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 1% of polygonum cuspidatum root extract, 5% of ascorbyl tetraisopalmitate, 1% of PEG-40 hydrogenated castor oil and 51% of deionized water.
The other components were the same as in example 5, and the preparation method was the same as in example 5.
Test examples
Eye cream trial effect test:
the test population: 35 healthy Chinese adult females with dark skin color, color spots, black eyes and other problems around eyes are selected, wherein the age is 25-60 years, and the average age is 40.5 +/-9.1 years.
The test method comprises the following steps: after the face is cleaned and the skin is refreshed in the morning and evening, a proper amount of the face cleaning cream is applied to the periphery of eyes in the examples 5 to 8 and the comparative examples 1 to 6, and the face cleaning cream is uniformly applied and massaged until the face cleaning cream is absorbed. Before trial, the melanin value, the skin color L value and the skin color b value of the eye skin are tested after 8 weeks of trial, VISIA photographing and visual evaluation are carried out, and the ITA is calculated.
The test results of examples 5 to 8 and comparative examples 1 to 6 are as follows.
Table 1 example 5 test results (eye cream with base)
Before use After use Variations in
Melanin pigment 191.24 178.70 -12.54
Skin color L value 58.66 60.04 1.38
ITA° 26.15 28.61 2.46
Description of the drawings: the value of melanin of skin around eyes is reduced, which indicates that the test object has the efficacy of reducing the melanin content around eyes. The value of skin brightness L around eyes is increased, which suggests that the subject has the efficacy of improving skin brightness. The increase in ITA ° indicates that the subject has improved black eye efficacy.
Table 2 example 6 test results (eye cream with base)
Before use After use Variations in
Melanin pigment 187.22 165.33 -21.89
Skin color L value 60.24 63.27 3.03
ITA° 25.12 27.22 2.12
Table 3 example 7 test results (eye cream with base)
Figure BDA0001374461810000231
Figure BDA0001374461810000241
Table 4 example 8 test results (eye cream with base)
Before use After use Variations in
Melanin pigment 190.22 178.01 -12.21
Skin color L value 60.27 62.46 2.19
ITA° 25.12 27.03 1.91
TABLE 5 test results of comparative example 1 (eye cream without base)
Before use After use Variations in
Melanin pigment 177.72 180.22 2.5
Skin color L value 57.78 56.99 -0.79
ITA° 24.98 25.01 0.03
Table 6 test results of comparative example 2 (eye cream with base)
Before use After use Variations in
Melanin pigment 187.47 181.45 -6.02
Skin color L value 58.46 58.78 0.32
ITA° 27.38 28.48 1.10
TABLE 7 test results of comparative example 3 (eye cream with base)
Figure BDA0001374461810000242
Figure BDA0001374461810000251
Table 8 comparative example 4 test results (eye cream with base)
Before use After use Variations in
Melanin pigment 190.64 185.80 -4.84
Skin color L value 59.35 60.21 0.86
ITA° 27.34 28.78 1.44
TABLE 9 test results of comparative example 5 (eye cream with base)
Before use After use Variations in
Melanin pigment 188.32 179.85 -8.47
Skin color L value 53.48 54.02 0.54
ITA° 24.82 26.13 1.31
TABLE 10 test results of comparative example 6 (eye cream with base)
Before use After use Variations in
Melanin pigment 188.56 179.03 -9.53
Skin color L value 57.38 58.26 0.88
ITA° 27.72 29.67 1.95
As can be seen from tables 1 to 10, the melanin values of examples 5 to 8 are decreased, and the skin color L and ITA are both significantly increased, compared with comparative example 1, and thus, the eye cream using the base of the present invention has the effects of significantly relieving dark circles and lightening the skin color around the eyes. The eye cream using the base of example 7 has the best black eye removing effect and brightness improving effect.
Comparative example 2 compared to example 5, the substrate did not contain tea extract to encapsulate boswellia serrata extract; comparative example 3 compared to example 6, the matrix contained no date seeds; comparative example 4 compared to example 7, the matrix contained no soy protein, hydrolyzed rice protein and superoxide dismutase mixture; comparative example 5 compared with example 8, the matrix does not contain the polygonum cuspidatum root extract, and the reduction degree of the melanin value before and after use, the increase degree of the skin color L x value and the ITA ° are reduced in different degrees, so that the active ingredients of the cosmetic matrix have a synergistic effect, and no significant effect can be obtained by reducing one of the ingredients.
In comparison with example 5, the ratio of the components of the base material was different from that of the present invention, and the degree of decrease in melanin value before and after use, the degree of increase in skin color L x and ITA ° were also decreased, and thus it was found that the cosmetic base material of the present invention could achieve significant effects of relieving dark circles and lightening skin color by the mutual matching of the components in a specific ratio.
In conclusion, the cosmetic matrix disclosed by the invention is prepared by reasonably matching a tea extract coated boswellia serrata extract, an orange peel extract, date seed, acetyl tetrapeptide-5, wild soybean protein, a hydrolyzed rice protein and superoxide dismutase mixture, a polygonum cuspidatum root extract and ascorbyl tetraisopalmitate, and optimizing the formula amount of the matrix, so that the effects of the components have a mutual synergistic effect and a better effect is achieved, the components are fully coordinated and complemented, the antioxidation effect is obvious, melanin can be remarkably reduced, the skin color is brightened, and the black eye circle can be effectively relieved after the matrix is applied.
While particular embodiments of the present invention have been illustrated and described, it would be obvious that various other changes and modifications can be made without departing from the spirit and scope of the invention. It is therefore intended to cover in the appended claims all such changes and modifications that are within the scope of this invention.

Claims (10)

1. The cosmetic matrix is characterized by being prepared from the following raw materials in percentage by mass: 10-20% of tea extract-coated boswellia serrata extract, 5-10% of citrus peel extract, 10-20% of date seed, 55-10% of acetyl tetrapeptide, 3-6% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-6% of polygonum cuspidatum root extract, 1-3% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water;
the mass ratio of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase in the mixture of the wild soybean protein, the hydrolyzed rice protein and the superoxide dismutase is (0.1-1): (5-10): (0.1-1).
2. The cosmetic base according to claim 1, wherein the base is prepared from the following raw materials in percentage by mass: 12-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 12-18% of date seed, 56-10% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
3. The cosmetic base according to claim 1, wherein the base is prepared from the following raw materials in percentage by mass: 15-18% of tea extract-coated boswellia serrata extract, 8-10% of citrus peel extract, 16-18% of date seed, 56-8% of acetyl tetrapeptide, 3-5% of a mixture of wild soybean protein, hydrolyzed rice protein and superoxide dismutase, 3-5% of polygonum cuspidatum root extract, 1-2% of ascorbyl tetraisopalmitate, 1-2% of PEG-40 hydrogenated castor oil and the balance of water.
4. A process for the preparation of a cosmetic base according to any one of claims 1 to 3, characterized in that it comprises the following steps:
the raw materials with the formula ratio are fully mixed, heated, kept warm, homogenized and cooled to obtain the cosmetic matrix.
5. A process for the preparation of a cosmetic base according to claim 4, characterized in that it comprises the following steps:
(a) heating water with the formula amount to 85-90 ℃, preserving heat for 20-30 min, and cooling to 30-35 ℃;
(b) adding the other raw materials into the cooled water in the step (a), stirring and homogenizing for 5-10 min at the stirring speed of 1000-3000 r/min, and removing residues to obtain the cosmetic matrix.
6. Use of the cosmetic base according to any one of claims 1 to 3 for the preparation of a skin-care cosmetic.
7. An eye cream comprising the cosmetic base according to any one of claims 1 to 3, wherein the cosmetic base is present in the eye cream in an amount of 20 to 30% by weight.
8. The eye cream according to claim 7, wherein the eye cream is mainly prepared from the following raw materials in percentage by mass: 20-30% of a cosmetic matrix, 2-3% of PEG-60 hydrogenated castor oil, 61-2% of cetostearyl alcohol polyether, 1-2% of behenyl alcohol, 2-3% of shea butter, 3-4% of dioctyl carbonate, 3-4% of glycerol tri (ethyl hexanoate), 0.5-1% of tocopherol acetate, 8-10% of glycerol, 5-7% of butanediol, 0.5-0.8% of carbomer, 0.3-0.6% of triethanolamine and the balance of water.
9. The eye cream according to claim 8, wherein the eye cream further comprises a preservative and a fragrance;
the preservative is 0.1-0.3% of the eye cream by mass;
the essence accounts for 0.01-0.03% of the eye cream by mass.
10. A method for preparing the eye cream as claimed in claim 8 or 9, comprising the steps of:
mixing PEG-60 hydrogenated castor oil, ceteareth-6, behenyl alcohol, shea butter, dioctyl carbonate, glycerol tri (ethyl hexanoate) and tocopheryl acetate, heating, keeping the temperature to obtain an oily raw material, mixing the oily raw material with glycerol, butanediol, carbomer, triethanolamine and water, heating, keeping the temperature to obtain an aqueous raw material, homogenizing, cooling, adding a cosmetic matrix, optionally a preservative and essence, and removing residues to obtain the eye cream.
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CN109602654A (en) * 2018-12-25 2019-04-12 广州葆妍生物科技有限公司 A kind of composition and its preparation method and application with eye-care function
CN111939113A (en) * 2019-05-16 2020-11-17 广州玉鑫商业运营管理有限公司 Multi-effect eye muscle activating base solution and preparation method thereof
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CN111514085B (en) * 2020-05-18 2021-05-11 高宝化妆品(中国)有限公司 Moisturizing composition containing date seed extract and mask
CN114159316B (en) * 2021-11-24 2024-06-11 珀莱雅化妆品股份有限公司 Microcapsule liposome for caring skin around eyes and preparation method thereof

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