CN110840791B - Lip color cosmetic product and preparation method thereof - Google Patents
Lip color cosmetic product and preparation method thereof Download PDFInfo
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- CN110840791B CN110840791B CN201911237930.8A CN201911237930A CN110840791B CN 110840791 B CN110840791 B CN 110840791B CN 201911237930 A CN201911237930 A CN 201911237930A CN 110840791 B CN110840791 B CN 110840791B
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
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Abstract
The invention belongs to the technical field of cosmetics, and provides a lip color cosmetic product and a preparation method thereof. The lip color cosmetic product comprises the following components in parts by weight: 1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride and 0.5-1.5 parts of coconut fatty acid monoethanolamide, wherein the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water. Through above-mentioned technical scheme, solved among the prior art lip makeup product and moistened the degree poorly, the problem that lip skin is dry desquamate easily after using.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and relates to a lip color cosmetic product and a preparation method thereof.
Background
Unlike other skin regions, the skin of the lips is the weakest part of the human skin and is vulnerable to the external environment, which accelerates the aging process. The lip skin has thin cutin, no accessory organs such as hair follicles and sebaceous glands, and a plurality of salivary glands are distributed in the cuticle, the cuticle and the granular layer are thin, and the granular melanin is less than that of the common skin. The lip color cosmetic product can not only trace lips and endow the lips with gorgeous color, brightness and aesthetic feeling, but also play a role in protecting the lips, so the lip color cosmetic product is popular with vast women.
Lip color cosmetics on the market at present are various in color number and variety and rich in color, and are necessary beauty cosmetics for girls. However, the lips on which lipstick is applied tend to dry due to the user's work for a long time. Therefore, the existing lip color cosmetic products have the problems of poor moisturizing degree and easy dryness and desquamation of lip skin after long-term use.
Disclosure of Invention
The invention provides a lip color cosmetic product and a preparation method thereof, and solves the problems that the lip color cosmetic product in the prior art is poor in moistening degree and the skin of lips is easy to dry and peel after use.
The technical scheme of the invention is realized as follows:
the lip color cosmetic product comprises the following components in parts by weight:
1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride, 0.5-1.5 parts of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water.
As a further technical scheme, the paint comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride, 1 part of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water.
As a further technical scheme, the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain the modified mica.
As a further technical scheme, the natural pigment comprises one or more of grape skin red, roselle red, mulberry red and blackcurrant red.
As a further technical scheme, the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract.
The invention also provides a preparation method of the lip color cosmetic product, which comprises the following steps:
s1, weighing the components according to the formula of the lip color cosmetic product for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and uniformly stirring and dispersing to obtain the lip color cosmetic product.
As a further technical proposal, the stirring speed in the step S3 is 200 r/min.
As a further technical proposal, the stirring speed in the step S4 is 800 r/min.
As a further technical proposal, the stirring speed in the step S5 is 500 r/min.
The working principle and the beneficial effects of the invention are as follows:
1. according to the invention, the specific formula and the preparation method are compatible, so that the prepared lip color cosmetic product is smooth and uniform in texture, smooth in surface, strict in color and luster, moderate in hardness and not prone to bending and breaking.
2. According to the invention, the yttrium oxide and the oxidized bait are adopted to modify the mica, and then the modified mica is added into the lip color cosmetic product, so that the hardness, the color and the texture of the lip color cosmetic product can be obviously improved. The yttrium oxide and the oxidized bait are adopted to modify mica, the obtained modified mica has good colorability and crystal transparency, and when the modified mica is added into a lip color cosmetic product, the modified mica has good hyperchromic and color-retaining effects on natural pigments, so that the prepared lip color cosmetic product is strict, uniform and full in color. The addition of the modified mica promotes the dispersion of the pigment in the lip color cosmetic product, so that the components in the lip color cosmetic product are dispersed more uniformly, the lip color cosmetic product is smooth in texture and moderate in hardness, and the lip color cosmetic product is not easy to break in the using process.
3. According to the invention, the poloxamer is added into the lip color cosmetic product, so that the color and the wettability of the lip color cosmetic product can be obviously improved. The water solubility of the natural pigment is poor, and the poloxamer is added, so that the dispersion of the natural pigment in water is promoted in the process of preparing the natural pigment solution, and when the oil phase is slowly added into the natural pigment solution, the hydrophilic group and the hydrophobic group in the poloxamer molecule respectively interact with the natural pigment solution and the oil phase, so that the compatibility of the natural pigment solution and the oil phase interface is changed, the dispersion of the natural pigment in the lip color cosmetic product is further promoted, the color of the lip color cosmetic product is more uniform and full, the poloxamer has good hydrophilicity, and the lip color cosmetic product has a better moisturizing effect.
4. According to the invention, the mahonia stem extract and the hesperetin are added into the lip color cosmetic product, so that the smell of the lip color cosmetic product can be obviously improved. The mahonia stem extract is also compatible with hesperetin, so that the prepared lip color cosmetic product has light sweet taste and is popular with consumers. The mahonia stem extract also has a good antioxidation effect, and is added into a lip color cosmetic product to endow the lip color cosmetic product with an antioxidation function, so that the lip skin is better protected, and the practicability is stronger.
5. In the invention, the pentaerythritol tri-hydroxystearate and the cholesteryl hydroxystearate are added into the lip color cosmetic product, so that the texture and the moisture of the lip color cosmetic product can be obviously improved. The mutual compatibility of the polypentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can obviously improve the surface tension among various constituent phases in the lip color cosmetic product to form a uniform and stable dispersion system, so that the lip color cosmetic product has smooth and uniform texture; the mutual compatibility of the poly pentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can efficiently keep moisture, and has good skin moistening effect, thereby improving the moistening degree of the lip color cosmetic product.
6. In the invention, the potassium abietyl hydrolyzed soy protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide are added into the lip color cosmetic product, so that the wettability and the hardness of the lip color cosmetic product can be obviously improved. The potassium abietyl hydrolyzed soybean protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide have synergistic effect and strong permeability, and can effectively promote the absorption of active ingredients, thereby improving the wettability of the lip color cosmetic product, and the lip color cosmetic product is compatible with other components in the formula, thereby obviously improving the hardness of the lip color cosmetic product.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The lip color cosmetic product comprises the following components in parts by weight:
1 part of natural pigment, 2 parts of bitter orange peel oil, 5 parts of modified mica, 3 parts of poloxamer, 1 part of polyethylene glycol, 0.5 part of palm oil, 0.5 part of cane sugar, 0.5 part of tartaric acid, 2 parts of dipentaerythritol tri-polyhydroxy stearate, 2 parts of cholesterol hydroxy stearate, 0.1 part of hesperetin, 0.8 part of mahonia stem extract, 0.5 part of potassium abietyl hydrolyzed soybean protein, 0.5 part of dioctadecyl dimethyl ammonium chloride and 0.5 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method comprises the following steps:
s1, weighing the components according to the formula for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring at the speed of 200r/min until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing at the speed of 800r/min to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and stirring and dispersing uniformly at the speed of 500r/min to obtain the lip color cosmetic product.
Example 2
The lip color cosmetic product comprises the following components in parts by weight:
10 parts of natural pigment, 15 parts of bitter orange peel oil, 10 parts of modified mica, 8 parts of poloxamer, 5 parts of polyethylene glycol, 2 parts of palm oil, 2 parts of sucrose, 2 parts of tartaric acid, 5 parts of dipentaerythritol tri-polyhydroxystearate, 5 parts of cholesterol hydroxystearate, 0.5 part of hesperetin, 2.5 parts of mahonia stem extract, 1.5 parts of potassium abietyl hydrolyzed soybean protein, 1.5 parts of dioctadecyl dimethyl ammonium chloride and 1.5 parts of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 3
The lip color cosmetic product comprises the following components in parts by weight:
3 parts of natural pigment, 6 parts of bitter orange peel oil, 6 parts of modified mica, 4 parts of poloxamer, 2 parts of polyethylene glycol, 1.2 parts of palm oil, 1 part of sucrose, 1 part of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesterol hydroxystearate, 0.2 part of hesperetin, 1.3 parts of mahonia stem extract, 0.8 part of potassium abietyl hydrolyzed soybean protein, 0.8 part of dioctadecyl dimethyl ammonium chloride and 0.8 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating and concentrating the filtrate, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 4
The lip color cosmetic product comprises the following components in parts by weight:
7 parts of natural pigment, 10 parts of bitter orange peel oil, 8 parts of modified mica, 6 parts of poloxamer, 4 parts of polyethylene glycol, 1.5 parts of palm oil, 1.5 parts of cane sugar, 1.5 parts of tartaric acid, 4 parts of dipentaerythritol tri-hydroxystearate, 4 parts of cholesteryl hydroxystearate, 0.4 part of hesperetin, 2.1 parts of mahonia stem extract, 1.2 parts of potassium abietyl hydrolyzed soybean protein, 1.2 parts of dioctadecyl dimethyl ammonium chloride and 1.2 parts of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 5
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wetly grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 6
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 2.5 parts of mica, 0.2 part of yttrium oxide, 0.2 part of erbium oxide and 3 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating and concentrating the filtrate, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 7
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 10 parts of mica, 0.5 part of yttrium oxide, 0.5 part of erbium oxide and 8 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1.
Example 8
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is roselle red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 9
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is mulberry red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 10
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is blackcurrant red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1.
Comparative example 1
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesteryl hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of abietyl hydrolyzed soybean protein potassium, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as the example 1 except that mica is added and modified mica is not added in the step S5.
Comparative example 2
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1 except that poloxamer is not added in step S2.
Comparative example 3
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1 except that the mahonia stem extract is not added in step S5.
Comparative example 4
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxystearate, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as the example 1 except that no hesperetin is added in the step S5.
Comparative example 5
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 0.3 part of hesperetin, 1.6 parts of a mahonia stem extract, 1 part of abietyl hydrolyzed soybean protein potassium, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
in the preparation method, no dipentaerythritol tri-polyhydroxystearate or cholesteryl hydroxystearate is added in step S3, and the rest steps are the same as in example 1.
Comparative example 6
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxystearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin and 1.6 parts of mahonia stem extract;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
in the preparation method, step S4 does not add abietyl hydrolyzed soybean protein potassium, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and the rest steps are the same as in example 1.
The lip color cosmetic products prepared in examples 1-10 and comparative examples 1-6 were subjected to the following performance tests:
1. and (3) microbial detection: items such as total bacteria, total mold/yeast, heat-resistant coliform, staphylococcus aureus and pseudomonas aeruginosa in the sample are detected according to the method specified in technical specifications for cosmetic safety (2015), and the detection results are shown in the following table:
TABLE 1 results of microbiological examination of lip color cosmetic products prepared in examples 1-10 and comparative examples 1-6
Note: in the above table, indicates no detection, and indicates no detection.
The data in table 1 show that the total number of bacteria in the mask liquid products of examples 1 to 7 and comparative examples 7 to 12 is less than 10/mL, the total number of mold/yeast is less than 10/mL, heat-resistant coliform bacteria, staphylococcus aureus and pseudomonas aeruginosa are not detected, and the microbial test result shows that the products meet the requirements of technical cosmetic safety specifications (2015 edition), which indicates that the lip color cosmetic products prepared by the invention are safe and reliable.
2. Heavy metals: detecting the contents of chromium, arsenic, cadmium, antimony and lead in the sample according to a method specified in GB/T35828-2018 inductively coupled plasma mass spectrometry for determining chromium, arsenic, cadmium, antimony and lead in cosmetics, wherein the detection standard refers to GB7916-87 cosmetic hygienic standard, and the detection results are shown in the following table:
table 2 determination results of heavy metal content of lip color cosmetic products prepared in examples 1 to 10 and comparative examples 1 to 6
Note: in the above table, a indicates no detection.
As can be seen from the data in Table 2, no heavy metal such as chromium, arsenic, cadmium, antimony, lead and the like is detected in the lip color cosmetic products of examples 1 to 10 and comparative examples 1 to 6, and the lip color cosmetic products meet the requirements of GB7916-87 cosmetic hygienic Standard.
3. Sensory evaluation: selecting 100 female volunteers, wherein the female volunteers are 25-40 years old, scoring the texture, color, hardness, moistening degree, smell and the like of the lip color cosmetic products of examples 1-10 and comparative examples 1-6 according to sensory evaluation indexes, wherein the scoring standard is 0-10 points, the closer the lip color cosmetic products to the scoring standard, the higher the score, and on the contrary, the lower the score, the sensory evaluation indexes are shown in table 3, and the scoring results are shown in table 4:
TABLE 3 sensory evaluation index
| Item | Evaluation index |
| Texture of | Smooth surface, pearly luster, smooth and uniform paste texture, no air holes and no granular sensation |
| Color | Bright color, soft and beautiful color, uniform and natural color |
| Hardness of | Is not easy to bend and break, but is not too soft and too hard |
| Degree of wetness | After being coated, the coating is not dry, greasy, caking and good in moistening degree |
| Smell(s) | Has light sweet taste, no pungent flavor and petroleum smell, and thick cured meat flavor |
TABLE 4 Scoring situation
The data in table 4 show that the scores of the texture, color, hardness, moisture and smell of the lip color cosmetic products of examples 1-10 of the present invention are all over 9 points, which are higher than the scores of the lip color cosmetic products of comparative examples 1-6, and thus, the lip color cosmetic products prepared in examples 1-10 of the present invention have the advantages of smooth and uniform texture, smooth surface, proper color, moderate hardness, and less possibility of bending and breaking, the skin is not greasy and has good moisture after the use of the lip color cosmetic products of the present invention, and meanwhile, the lip color cosmetic products prepared in the examples of the present invention have good smell, have light sweet taste after the use, and are suitable for wide consumers.
Compared with the lip color cosmetic products of examples 1-10, the lip color cosmetic product of comparative example 1 has relatively poor wettability and texture because mica is not modified in the lip color cosmetic product of comparative example 1, which indicates that after the mica is modified by yttrium oxide and bait oxide, the lip color cosmetic product can be added to the lip color cosmetic product to obviously improve the hardness, color and texture of the lip color cosmetic product. The yttrium oxide and the oxidized bait are adopted to modify mica, the obtained modified mica has good colorability and crystal transparency, and when the modified mica is added into a lip color cosmetic product, the modified mica has good hyperchromic and color-retaining effects on natural pigments, so that the prepared lip color cosmetic product is strict, uniform and full in color. The addition of the modified mica also promotes the dispersion of pigments in the lip color cosmetic product, so that the components in the lip color cosmetic product are dispersed more uniformly, and the lip color cosmetic product has smooth texture and moderate hardness and is not easy to break off in the using process.
Compared with examples 1-10, the lip color cosmetic product of comparative example 2 has relatively poor color and luster and wettability, because poloxamer is not added to the lip color cosmetic product of comparative example 2, which indicates that the color and luster and wettability of the lip color cosmetic product can be remarkably improved by adding poloxamer to the lip color cosmetic product. The water solubility of the natural pigment is poor, and the poloxamer is added, so that the dispersion of the natural pigment in water is promoted in the process of preparing the natural pigment solution, and when the oil phase is slowly added into the natural pigment solution, the hydrophilic group and the hydrophobic group in the poloxamer molecule respectively interact with the natural pigment solution and the oil phase, so that the compatibility of the natural pigment solution and the oil phase interface is changed, the dispersion of the natural pigment in the lip color cosmetic product is further promoted, the color of the lip color cosmetic product is more uniform and full, the poloxamer has good hydrophilicity, and the lip color cosmetic product has a better moisturizing effect.
Compared with examples 1-10, the lip color cosmetic products of comparative example 3 and comparative example 4 have slightly poorer odor, because the mahonia dubia extract is not added in the lip color cosmetic product of comparative example 3, and the hesperetin is not added in the lip color cosmetic product of comparative example 4, which indicates that the odor of the lip color cosmetic product can be obviously improved by adding the mahonia dubia extract and the hesperetin to the lip color cosmetic product. The mahonia stem extract is also compatible with hesperetin, so that the prepared lip color cosmetic product has light sweet taste and is popular with consumers. The mahonia stem extract also has a good antioxidation effect, and is added into a lip color cosmetic product to endow the lip color cosmetic product with an antioxidation function, so that the lip skin is better protected, and the practicability is stronger.
Compared with examples 1-10, the lip color cosmetic product of comparative example 5 has a slightly poorer texture and wettability, because the lip color cosmetic product of comparative example 5 is not added with the polypentaerythritol tri-polyhydroxystearate and the cholesteryl hydroxystearate, which shows that the addition of the polypentaerythritol tri-polyhydroxystearate and the cholesteryl hydroxystearate to the lip color cosmetic product can obviously improve the texture and the wettability of the lip color cosmetic product. The mutual compatibility of the polypentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can obviously improve the surface tension among various constituent phases in the lip color cosmetic product to form a uniform and stable dispersion system, so that the lip color cosmetic product has smooth and uniform texture; the mutual compatibility of the poly pentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can efficiently keep moisture, and has good skin moistening effect, thereby improving the moistening degree of the lip color cosmetic product.
Compared with examples 1-10, the lip color cosmetic product of comparative example 6 has poorer wettability and hardness, because potassium abietyl hydrolyzed soy protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide are not added in the lip color cosmetic product of comparative example 6, which indicates that the wettability and hardness of the lip color cosmetic product can be obviously improved by adding the potassium abietyl hydrolyzed soy protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide into the lip color cosmetic product. The potassium abietyl hydrolyzed soybean protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide have synergistic effect and strong permeability, and can effectively promote the absorption of active ingredients, thereby improving the wettability of the lip color cosmetic product, and the lip color cosmetic product is compatible with other components in the formula, thereby obviously improving the hardness of the lip color cosmetic product.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions, improvements, etc. within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The lip color cosmetic product is characterized by comprising the following components in parts by weight:
1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride, 0.5-1.5 parts of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water;
the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica;
the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract.
2. The lip color cosmetic product according to claim 1, comprising the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesteryl hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride, 1 part of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water.
3. The lip color cosmetic product of claim 1, wherein the natural pigments comprise one or more of grape skin red, hibiscus sabdariffa red, mulberry red, and blackcurrant red.
4. A preparation method of a lip color cosmetic product is characterized by comprising the following steps:
s1, weighing the components according to the formula of the lip color cosmetic product as claimed in any one of claims 1 to 3 for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and uniformly stirring and dispersing to obtain the lip color cosmetic product.
5. The method for preparing a lip color cosmetic product according to claim 4, wherein the stirring speed in step S3 is 200 r/min.
6. The method for preparing a lip color cosmetic product according to claim 4, wherein the stirring speed in step S4 is 800 r/min.
7. The method for preparing a lip color cosmetic according to claim 4, wherein the stirring speed in step S5 is 500 r/min.
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| FR3011178A1 (en) * | 2013-10-01 | 2015-04-03 | Oreal | LIQUID COMPOSITION COMPRISING A NON-VOLATILE OIL, 12-HYDROXYSTEARIC ACID, AN ADDITIONAL WAX, A VINYLPYRROLIDONE COPOLYMER AND A SILICA AEROGEL |
| CN105168031A (en) * | 2015-10-14 | 2015-12-23 | 广州市花安堂生物科技有限公司 | Lip gloss containing multi-colored particles and preparation method thereof |
| CN107648108A (en) * | 2017-10-18 | 2018-02-02 | 佛山娇芙生物科技有限公司 | A kind of non-sticky cup liquid lipstick and preparation method thereof |
| CN109806197A (en) * | 2019-02-27 | 2019-05-28 | 广州尚姿化妆品有限公司 | A kind of multiple plant cyanines extraction lip gloss and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3011178A1 (en) * | 2013-10-01 | 2015-04-03 | Oreal | LIQUID COMPOSITION COMPRISING A NON-VOLATILE OIL, 12-HYDROXYSTEARIC ACID, AN ADDITIONAL WAX, A VINYLPYRROLIDONE COPOLYMER AND A SILICA AEROGEL |
| CN105168031A (en) * | 2015-10-14 | 2015-12-23 | 广州市花安堂生物科技有限公司 | Lip gloss containing multi-colored particles and preparation method thereof |
| CN107648108A (en) * | 2017-10-18 | 2018-02-02 | 佛山娇芙生物科技有限公司 | A kind of non-sticky cup liquid lipstick and preparation method thereof |
| CN109806197A (en) * | 2019-02-27 | 2019-05-28 | 广州尚姿化妆品有限公司 | A kind of multiple plant cyanines extraction lip gloss and preparation method thereof |
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