CN114632028A - Lifting and tightening face cream and preparation method thereof - Google Patents

Lifting and tightening face cream and preparation method thereof Download PDF

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Publication number
CN114632028A
CN114632028A CN202210325912.0A CN202210325912A CN114632028A CN 114632028 A CN114632028 A CN 114632028A CN 202210325912 A CN202210325912 A CN 202210325912A CN 114632028 A CN114632028 A CN 114632028A
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phase
composition
stirring
humectant
filler
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CN114632028B (en
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叶晓纯
杜万锋
黄振振
曹波
杨菊
李金印
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Guangzhou Youjiyuan Cosmetics Co ltd
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Guangzhou Youjiyuan Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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    • A61K8/26Aluminium; Compounds thereof
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
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    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
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    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
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    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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    • A61Q19/00Preparations for care of the skin
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract

The invention discloses a lifting tightening cream, which comprises: the phase A comprises a solvent, a humectant, a thickening agent and a skin conditioning agent, wherein the thickening agent in the phase A consists of carbomer, sodium polyacrylate grafted starch and xanthan gum; the phase B1 comprises emulsifier, thickener, detergent, emollient, and filler; the filler in phase B1 consists of polydimethylsiloxane and polysiloxane-11; the phase B2 comprises mica as filler, titanium dioxide and bismuth oxychloride; the phase C1 comprises a stabilizer; the C2 phase comprises emollient and filler, and the filler in the C2 phase is polymethylsilsesquioxane; the C3 phase comprises a pH regulator and a solvent; the phase D comprises antioxidant and humectant; phase E comprises humectant and skin conditioner. The lifting tightening cream disclosed by the invention is strong in moisturizing capability, capable of forming a lifting effect on skin, tightening and plumping the skin, slightly waterproof, soft, glutinous and fine in texture, simple in preparation method and process and easy to control in quality.

Description

Lifting and tightening face cream and preparation method thereof
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to lifting and tightening face cream and a preparation method thereof.
Background
With the development of economy, people are pursuing higher and higher life, including requirements on form. However, the skin care products on the market are various in types, and the forms of the skin care products include liquid, emulsion and solid; the types of the skin-smoothing lotion include smoothing toner, essence, emulsion, cream, facial mask and the like; the effects include moisture retention, whitening, acne removal, yellow removal, wrinkle removal, allergy resistance and the like. The ability to select an appropriate skin care product is critical to skin care. On the other hand, as women age, more and more skin problems occur, such as loose skin, sagging skin, etc., which have long plagued the average consumer. For high-end consumers, the users can select a mode of injecting a wrinkle resistant needle and the like to pull the skin, but the injection of the wrinkle resistant needle is expensive and has certain risks, and the injection of the wrinkle resistant needle is not a routine choice for ordinary consumers. The general public consumers tend to apply skin care products to care the skin. In order to meet the high-end skin care requirements of common consumers, the high-end skin care product has good market prospect in research and development.
Disclosure of Invention
In order to overcome the defects of the prior art, one of the purposes of the invention is to provide a lifting and tightening face cream which has strong moisture retention capacity, can form a lifting effect on skin to tighten and tighten the skin, has a micro-waterproof effect, prevents a skin care layer from being easily taken away by water, sweat and the like, maintains the skin for a long time, has soft, glutinous and fine texture, and is a high-end upgrading face cream.
The invention also aims to provide a preparation method of the lifting and tightening cream, which has simple process and easily controlled quality.
One of the purposes of the invention is realized by adopting the following technical scheme:
a lifting and tightening cream comprises a phase A, a phase B, a phase C, a phase D, a phase E, a phase F and a phase G, and comprises the following components in percentage by weight in the cream:
the phase A comprises a solvent and the balance; 5-11% of a humectant; 0.2 to 0.8 percent of thickening agent; 0.1-0.3% of skin conditioner; the thickening agent in the phase A consists of carbomer, sodium polyacrylate grafted starch and xanthan gum;
the B phase comprises a B1 phase and a B2 phase; the B1 phase comprises 1.4-3.5% of emulsifier; 1.5 to 4.2 percent of thickening agent; 2-5% of a cleaning agent; 5-18.5% of emollient; 5-15% of a filler; the filler in phase B1 consists of polydimethylsiloxane and polysiloxane-11; the phase B2 comprises 1-2.9% of filler, and the filler in the phase B2 comprises mica, titanium dioxide and bismuth oxychloride;
the C phase comprises a C1 phase, a C2 phase and a C3 phase; the C1 phase comprises 0.8-1.2% of stabilizer; the C2 phase comprises 0.8-1.5% of emollient and 0.8-1.5% of filler, and the filler in the C2 phase is polymethylsilsesquioxane; the C3 phase comprises pH regulator 0.15-0.5% and solvent 0.5-2%;
the phase D comprises 0.3-0.6% of antioxidant and 1-5.6% of humectant;
the phase E comprises 0.5 to 2 percent of humectant and 0.6 to 4.5 percent of skin conditioner;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% of colorant.
The tightening cream provided by the invention comprises multiple components, each component is accurately blended into different phases, and the multiple components such as the humectant, the emulsifier, the thickener, the filler, the emollient, the skin conditioner, the cleanser and the like are ingeniously matched, so that the formed cream is soft, glutinous and thick in texture, excellent in moisturizing capability, micro-waterproof, moist and not greasy, can make the skin plump and compact, and meets the high-end skin care requirements of common mass consumers. Wherein, the addition of the sodium polyacrylate grafted starch can not only improve the softness of the product. More importantly, the skin can be lifted and tightened, and the sodium polyacrylate grafted starch takes hydrophilic and semi-rigid starch macromolecules as a skeleton, and has polysaccharide compounds, intermolecular forces and reactivity by introducing different functional groups and adjusting the proportion of hydrophilic and lipophilic chain segment structures. Based on this characteristic, when the sodium polyacrylate grafted starch is spread on the skin, the skin is fixed like a rigid structure, so that the skin has a tight feeling. Meanwhile, the sodium polyacrylate grafted starch is an amphoteric compound, is hydrophilic and lipophilic, can be tightly attached to a water-based end, has a more excellent water holding effect, can be well filled in gaps among skin cells, and enables the skin to be fuller and firmer. In addition, the special filling agent and the sodium polyacrylate grafted starch are compounded, so that the skin is firmer and fuller, the filling agent can brighten the skin color, adjust the skin color and enable the skin to be in a healthy state, and meanwhile, the product has natural use feeling, is easy to extend and apply. On the other hand, the filler has a hydrophobic function, and can block moisture to a certain extent, so that the product has a micro-waterproof function. The product of the invention can realize skin tightening, and simultaneously, the skin does not feel tight and uncomfortable, because the invention also adds a proper amount of humectant, emollient and skin conditioner, and the components can relieve and soften the skin. In addition, a large amount of grease (mainly emollient in B1 phase and C2 phase) is added into the formula, and the grease further improves the waterproof function of the product.
Further, in the phase a, the solvent is water; the humectant is a combination of glycerin, butanediol and sodium hyaluronate; the skin conditioning agent is allantoin.
The cream disclosed by the invention has excellent moisturizing effect, the glycerin, the butanediol and the sodium hyaluronate in the phase A are easily absorbed by skin, and the hyaluronic acid is a linear polysaccharide structure consisting of the repeated structures of N-caproyl glucosamine and D-glucuronic acid. The reduction and destruction of the hyaluronic acid (hyaluronic acid) HA content in the skin can cause the skin to lose water, wrinkle and lose elasticity, causing the aging of the human epidermis. The moisturizer disclosed by the invention comprises sodium hyaluronate as an efficient moisturizer, and can delay skin aging.
Further, in the phase B1, the emulsifier is lauryl PEG-10 tris (trimethylsiloxy) silylethyl dimethicone, PEG-20 methyl glucose sesquistearate and a combination of glyceryl stearate and PEG-100 stearate; the thickening agent is a composition of cetostearyl alcohol and behenyl alcohol; the cleanser is a composition of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; the emollient is a composition of dimethicone, C12-15 alcohol benzoate, isohexadecane, polydimethylsiloxane, dimethiconol, cyclohexasiloxane, cyclopentadimethylsiloxane and octyl methicone.
The cleanser component is added into the face cream, and lauric acid in the cleanser component can enable the skin to be more delicate.
Further, in the C1 phase, the stabilizer is a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate; in the C2 phase, the emollient is a combination of cyclohexasiloxane and cyclopentadimethylsiloxane; the filler is polymethylsilsesquioxane; in the C3 phase, the pH adjusting agent is aminomethyl propanol; the solvent is water.
Further, in the phase D, the antioxidant is p-hydroxyacetophenone, and the p-hydroxyacetophenone has the effects of resisting oxidation and relieving the skin. In the invention, the p-hydroxyacetophenone can be used as a substitute of the traditional preservative, has the functions of antisepsis and synergism, and has excellent stability in high and low pH and temperature ranges. Further, in the D phase, the humectant is a combination of butylene glycol and 1, 2-hexanediol.
Further, in the E phase, the humectant is a trimethylpentanediol/adipic acid/glycerol crosspolymer; the skin conditioner comprises lactobacillus/soybean milk fermentation product filtrate, butanediol, 1, 2-pentanediol, hydroxypropyl tetrahydropyrane triol, 1, 2-hexanediol, hexapeptide-9 and arginine/lysine polypeptide. Arginine/lysine polypeptide and hexapeptide-9 have synergistic effects, and the addition of lysine makes the skin more firm.
Further, in the phase F, the fragrance is a perfume; in the G phase, the colorant is caramel color.
Further, the lifting tightening cream comprises an A phase, a B phase, a C phase, a D phase, an E phase, an F phase and a G phase, and the lifting tightening cream comprises the following components in percentage by weight:
the phase A comprises: water, the balance; humectant: 3-5% of glycerin, 2-5% of butanediol and 0.01-0.05% of sodium hyaluronate; thickening agent: carbomer 0.1-0.5%, sodium polyacrylate grafted starch 0.05-0.15%, and xanthan gum 0.05-0.15%; 0.1-0.3% of skin conditioner allantoin;
the B1 phase comprises: emulsifier: lauryl PEG-10 tris (trimethylsiloxy) silylethyl polydimethylsiloxane 0.1-0.5%, PEG-20 methyl glucose sesquistearate 0.8-1.5%, glyceryl stearate and PEG-100 stearate 0.5-1.5%; thickening agent: 0.5-1.2% of cetearyl alcohol and 1-3% of behenyl alcohol; cleaning agent: 2-5% of a combination of lauric, myristic, palmitic, stearic and arachidic acids; and (3) an emollient: 1-3% of simethicone, 0.5-2% of C12-15 alcohol benzoate, 2-6% of isohexadecane, 0.3-0.6% of composition of polydimethylsiloxane and dimethiconol, 1-5% of composition of cyclohexasiloxane and cyclopentadecyldimethylsiloxane and 0.5-1.5% of octyl methicone; filling agent: 5-15% of a composition of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filling agent: 0.5-1.5% of a combination of mica, titanium dioxide and triethoxyoctylsilane, 0.5-1.2% of a combination of mica and titanium dioxide, and 0.05-0.15% of a combination of bismuth oxychloride and ethylhexyl hydroxystearate;
the C1 phase includes: a stabilizer: 0.8-1.2% of the composition of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: and (3) an emollient: 0.8 to 1.5% of a composition of cyclohexasiloxane and cyclopentadimethicone, filler: 0.8 to 1.5 percent of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: 0.15-0.5% of aminomethyl propanol, solvent: 0.5 to 2 percent of water;
the phase D comprises: antioxidant: 0.3-0.6% of p-hydroxyacetophenone, and humectant: 1-5% of butanediol and 0.1-0.6% of 1, 2-hexanediol;
the phase E comprises: humectant: 0.5-2% of trimethylpentanediol/adipic acid/glycerin crosspolymer, skin conditioning agent: lactobacillus/soybean milk fermentation product filtrate, 0.5-2% composition of butanediol and 1, 2-pentanediol, 0.1-0.8% composition of hydroxypropyl tetrahydropyrane triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.05-1.5% composition of butanediol and hexapeptide-9, and 0.005-0.015% arginine/lysine polypeptide;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% of colorant.
The second purpose of the invention is realized by adopting the following technical scheme:
a preparation method of a lifting and tightening face cream comprises the following steps:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 85-88 ℃, and homogenizing for 3-5 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 80-85 deg.C, homogenizing until no particles are dissolved completely (stirring for 3-5 min);
adding the raw material of the B2 phase into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under the condition of rapid stirring, homogenizing and uniformly stirring;
adding C1 phase raw materials, stirring, and homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding the C3 phase, stirring uniformly, keeping the temperature for 20 minutes, and stirring and cooling;
independently heating the phase D to 60-65 ℃, stirring and dissolving until the phase D is completely transparent and free of particles, adding the phase D into an emulsifying pot when the temperature of a material body in the emulsifying pot is reduced to 65 ℃, and uniformly stirring;
continuously stirring and cooling to below 45 ℃, sequentially adding the phase E, and uniformly stirring;
adding the phase F, and uniformly stirring;
adding G phase for color matching, and stirring.
In the preparation process, the temperature, the stirring time and the heat preservation time are very critical, and improper operation can affect the forming of the product, the skin feeling of the product and even generate peculiar smell. Particularly, the preparation of the B1 phase is particularly important, ester substances exist in the B1 phase, and the ester substances are deteriorated and generate peculiar smell after being heated and stirred for a long time; too short time, uneven and insufficient stirring of the particles, which affects the sense.
Compared with the prior art, the invention has the beneficial effects that:
(1) the lifting tightening face cream provided by the invention is an upgraded version of a common face cream, each component and the using amount of the components are accurately blended, and the face cream has texture and soft, glutinous and fine skin feel. The face cream can brighten skin color, enables skin to be full and compact, can provide rich and nourishing natural grease for skin, provides continuous moistening for dry skin, enables a user to feel continuous full feeling and comfortable skin feeling during smearing, moistens and moisturizes, is soft and moist but not greasy, has a certain waterproof effect, and is soft, glutinous and fine.
(2) The preparation method of the lifting and tightening face cream provided by the invention is simple to operate and easy to control the quality.
Drawings
FIG. 1 is a diagram of a product for lifting and firming a cream provided in example 1 of the present invention;
fig. 2 is a diagram showing the trial effect of the lifting tightening cream provided in embodiment 1 of the present invention.
Detailed Description
The present invention is further described with reference to the accompanying drawings and the detailed description, and it should be noted that, in the case of no conflict, any combination between the embodiments or technical features described below may form a new embodiment. The raw materials, equipments and the like used in the following examples are commercially available unless otherwise specified.
A lifting firming cream is prepared from phase A, phase B, phase C, phase D, phase E, phase F and phase G raw materials, and the specific formula is shown in table 1 below.
Table 1 formula table for pull-up firming creams of examples 1-3
Figure BDA0003573465910000071
Figure BDA0003573465910000081
Figure BDA0003573465910000091
Figure BDA0003573465910000101
Figure BDA0003573465910000111
Figure BDA0003573465910000121
The lifting and tightening creams of examples 1-3 were prepared as follows:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 87 ℃, and homogenizing for 4 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 82 deg.C, stirring for 4min, wherein the B1 phase raw material is in homogeneous state, and the material is completely dissolved without particles for use;
adding the raw material of the B2 phase into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under the condition of rapid stirring, homogenizing and uniformly stirring;
adding C1 phase raw materials, stirring, and homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding the C3 phase, stirring uniformly, keeping the temperature for 20 minutes, and stirring and cooling;
independently heating the phase D to 62 ℃, stirring and dissolving until the phase D is completely transparent and free of particles, adding the phase D into an emulsifying pot when the temperature of a material body in the emulsifying pot is reduced to 65 ℃, and uniformly stirring;
continuously stirring and cooling to below 45 ℃, sequentially adding the phase E, and uniformly stirring;
adding the phase F, and uniformly stirring;
adding G phase for color matching, and stirring to obtain the final product.
Comparative example 1
Comparative example 1 differs from example 1 in that the "sodium polyacrylate grafted starch" in phase A was replaced with "polyacrylate crosspolymer-6", and polyacrylate crosspolymer-6 was used in an amount of 0.08%, the remainder being the same as in example 1.
Comparative example 2
Comparative example 1 differs from example 1 in that the filler in B2 phase is omitted and the rest is the same as example 1.
Comparative example 3
Comparative example 1 is different from example 1 in that the fillers in the B1 phase and the C2 phase are omitted, and the rest is the same as example 1.
Comparative example 4
Comparative example 4 is different from example 1 in that the emulsifier "lauryl PEG-10 tris (trimethylsiloxy) silylethyl polydimethylsiloxane" in phase B1 was omitted and the amount of "PEG-20 methyl glucose sesquistearate" was adjusted to 1.5% and the same as in example 1.
Comparative example 5
Comparative example 5 differs from example 1 in that the detergent in phase B1 was omitted and the same as example 1.
Comparative example 6
Comparative example 6 differs from example 1 in that the emollients "dimethicone" and "isohexadecane" in phase B1 were omitted and the amount of the emollients "cyclohexasiloxane, cyclopentadecyldimethicone" in phase B1 was adjusted to 8%, the remainder being the same as example 1.
Evaluation of Effect
90 test persons of 45 to 55 years old were selected, divided into 9 groups on average, and 10 persons in each group were tried with the cream samples of examples 1 to 3 and comparative examples 1 to 9, respectively. The facial skin of these test persons had varying degrees of fine lines and had poor skin elasticity. After the test persons cleaned the facial skin with the same cleanser every day, 2g of the cream samples of examples 1 to 3 and comparative examples 1 to 9 were uniformly applied to the facial skin, and the effects were counted for 7 days, 14 days, and 28 days, and the results are shown in table 2 below.
Evaluation criteria: the tested person self-recites the use feeling and compares the skin texture map through a computer to identify the skin tightening and pulling effect.
The method has the following advantages: the skin becomes firmer and more elastic than before trial use, and fine lines are reduced.
And (4) invalidation: the skin did not change any more than before the experiment.
Table 2 usage effect recording table
Figure BDA0003573465910000141
From the record in table 2, it can be seen that the lifting and tightening cream provided by the embodiment of the present invention has an effective rate of over 80% after being used for 28 days, and can make the skin become full and tight, recover elasticity, and lighten fine wrinkles, while the formula of the comparative example is changed, and the effect is reduced to different degrees. In addition, the tested person has high evaluation on the face cream of the embodiment of the invention, and the skin feel is good, so that the tested person is willing to use the face cream for a long time. Fig. 1-2 are product diagrams of examples 1-2 of the present invention, and it can be seen that the cream of example 1 is soft, glutinous, and thick, and has a fine texture.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.

Claims (10)

1. The lifting and tightening cream is characterized by comprising an A phase, a B phase, a C phase, a D phase, an E phase, an F phase and a G phase, wherein the weight percentages of the A phase, the B phase, the C phase, the D phase, the E phase, the F phase and the G phase in the cream are as follows:
the phase A comprises a solvent and the balance; 5-11% of a humectant; 0.2 to 0.8 percent of thickening agent; 0.1-0.3% of skin conditioner; the thickening agent in the phase A consists of carbomer, sodium polyacrylate grafted starch and xanthan gum;
the B phase comprises a B1 phase and a B2 phase; the B1 phase comprises 1.4-3.5% of emulsifier; 1.5 to 4.2 percent of thickening agent; 2-5% of a cleaning agent; 5-18.5% of emollient; 5-15% of a filler; the filler in phase B1 consists of polydimethylsiloxane and polysiloxane-11; the phase B2 comprises 1-2.9% of filler, and the filler in the phase B2 comprises mica, titanium dioxide and bismuth oxychloride;
the C phase comprises a C1 phase, a C2 phase and a C3 phase; the C1 phase comprises 0.8-1.2% of stabilizer; the C2 phase comprises 0.8-1.5% of emollient and 0.8-1.5% of filler, and the filler in the C2 phase is polymethylsilsesquioxane; the C3 phase comprises pH regulator 0.15-0.5% and solvent 0.5-2%;
the phase D comprises 0.3-0.6% of antioxidant and 1-5.6% of humectant;
the phase E comprises 0.5 to 2 percent of humectant and 0.6 to 4.5 percent of skin conditioner;
the phase F comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% of colorant.
2. The lift-tightening cream of claim 1, wherein in the a phase, the solvent is water; the humectant is a combination of glycerin, butanediol and sodium hyaluronate; the skin conditioning agent is allantoin.
3. The lift-tightening cream of claim 1, wherein in phase B1, the emulsifier is lauryl PEG-10 tris (trimethylsiloxy) silylethyl polydimethylsiloxane, PEG-20 methylgluco-sesquistearate, and a combination of glyceryl stearate and PEG-100 stearate; the thickening agent is a composition of cetearyl alcohol and behenyl alcohol; the cleanser is a composition of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; the emollient is a composition of dimethicone, C12-15 alcohol benzoate, isohexadecane, polydimethylsiloxane, dimethiconol, cyclohexasiloxane, cyclopentadimethylsiloxane and octyl methicone.
4. The lift-tightening cream of claim 1, wherein in the C1 phase, the stabilizer is a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, and sorbitan oleate; in the C2 phase, the emollient is a combination of cyclohexasiloxane and cyclopentadimethylsiloxane; the filler is polymethylsilsesquioxane; in the C3 phase, the pH adjusting agent is aminomethyl propanol; the solvent is water.
5. The lift-tightening cream of claim 1, wherein in the D phase, the antioxidant is p-hydroxyacetophenone; the humectant is a combination of butanediol and 1, 2-hexanediol.
6. The lift-tightening cream of claim 1, wherein in the E phase, the humectant is a trimethylpentanediol/adipic acid/glycerin crosspolymer; the skin conditioner comprises lactobacillus/soybean milk fermentation product filtrate, butanediol, 1, 2-pentanediol, hydroxypropyl tetrahydropyrane triol, 1, 2-hexanediol, hexapeptide-9 and arginine/lysine polypeptide.
7. The lift-tightening cream of claim 1, wherein in the F phase, the fragrance is a perfume; in the G phase, the colorant is caramel color.
8. The lift-tightening cream according to claim 1, comprising phases a, B, C, D, E, F and G, in percentages by weight in the cream:
the phase A comprises: water, the balance; humectant: 3-5% of glycerin, 2-5% of butanediol and 0.01-0.05% of sodium hyaluronate; thickening agent: carbomer 0.1-0.5%, sodium polyacrylate grafted starch 0.05-0.15%, and xanthan gum 0.05-0.15%; 0.1-0.3% of skin conditioner allantoin;
the B1 phase comprises: emulsifier: lauryl PEG-10 tris (trimethylsiloxy) silylethyl polydimethylsiloxane 0.1-0.5%, PEG-20 methyl glucose sesquistearate 0.8-1.5%, glyceryl stearate and PEG-100 stearate 0.5-1.5%; thickening agent: 0.5-1.2% of cetearyl alcohol and 1-3% of behenyl alcohol; cleaning agent: 2-5% of a combination of lauric, myristic, palmitic, stearic and arachidic acids; and (3) an emollient: 1-3% of simethicone, 0.5-2% of C12-15 alcohol benzoate, 2-6% of isohexadecane, 0.3-0.6% of composition of polydimethylsiloxane and dimethiconol, 1-5% of composition of cyclohexasiloxane and cyclopentadecyldimethylsiloxane and 0.5-1.5% of octyl methicone; filling agent: 5-15% of a composition of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filling agent: 0.5-1.5% of a combination of mica, titanium dioxide and triethoxyoctylsilane, 0.5-1.2% of a combination of mica and titanium dioxide, and 0.05-0.15% of a combination of bismuth oxychloride and ethylhexyl hydroxystearate;
the C1 phase includes: a stabilizer: 0.8-1.2% of the composition of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: and (3) an emollient: 0.8 to 1.5% of a composition of cyclohexasiloxane and cyclopentadimethicone, filler: 0.8 to 1.5 percent of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: 0.15-0.5% of aminomethyl propanol, solvent: 0.5 to 2 percent of water;
the phase D comprises: antioxidant: 0.3-0.6% of p-hydroxyacetophenone, and humectant: 1-5% of butanediol and 0.1-0.6% of 1, 2-hexanediol;
the phase E comprises: humectant: 0.5-2% of trimethylpentanediol/adipic acid/glycerin crosspolymer, skin conditioner: lactobacillus/soybean milk fermentation product filtrate, 0.5-2% composition of butanediol and 1, 2-pentanediol, 0.1-0.8% composition of hydroxypropyl tetrahydropyrane triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.05-1.5% composition of butanediol and hexapeptide-9, and 0.005-0.015% arginine/lysine polypeptide;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% of colorant.
9. The lift-tightening cream according to claim 1, comprising phases a, B, C, D, E, F and G, in weight percent in the cream:
the phase A comprises: water, the rest; humectant: 4% of glycerin, 3% of butanediol and 0.03% of sodium hyaluronate; thickening agent: carbomer 0.3%, sodium polyacrylate grafted starch 0.08%, xanthan gum 0.05%; allantoin as skin conditioner 0.2%;
the B1 phase comprises: emulsifier: lauryl PEG-10 tris (trimethylsiloxy) silylethyl polydimethylsiloxane 0.3%, PEG-20 methylgluco sesquistearate 1.2%, glyceryl stearate and PEG-100 stearate 0.8% in combination; thickening agent: cetearyl alcohol 0.8%, behenyl alcohol 2%; cleaning agent: 2.5% of a combination of lauric, myristic, palmitic, stearic and arachidic acid; and (3) an emollient: 2% of dimethicone, 0.5% of C12-15 alcohol benzoate, 4% of isohexadecane, 0.5% of a composition of polydimethylsiloxane and dimethiconol, 2% of a composition of cyclohexasiloxane and cyclopentadecyldimethicone, and 1% of octyl methicone; filling agent: 12% of a combination of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filling agent: 1% of a composition of mica, titanium dioxide and triethoxyoctylsilane, 0.8% of a composition of mica and titanium dioxide, and 0.08% of a composition of bismuth oxychloride and ethylhexyl hydroxystearate;
the C1 phase includes: a stabilizer: 1% of a composition of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: and (3) an emollient: composition of cyclohexasiloxane and cyclopentadimethicone 1%, filler: 1% of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: aminomethyl propanol 0.33%, solvent: 0.5 to 2 percent of water;
the phase D comprises: antioxidant: 0.5% of p-hydroxyacetophenone, and a humectant: 2% of butanediol and 0.5% of 1, 2-hexanediol;
the phase E comprises: humectant: 1% of trimethylpentanediol/adipic acid/glycerol crosspolymer, skin conditioner: lactobacillus/soy milk fermentation product filtrate, 0.5% composition of butylene glycol and 1, 2-pentanediol, 0.5% composition of hydroxypropyl tetrahydropyran triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.1% composition of butylene glycol and hexapeptide-9, 0.01% arginine/lysine polypeptide;
the F phase comprises fragrance 0.04%;
the G phase includes colorant 0.00429%.
10. A method of making a lift-tightening cream according to any one of claims 1 to 9, comprising the steps of:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 85-88 ℃, and homogenizing for 3-5 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 80-85 ℃, and stirring for 3-5 min;
adding the raw material of the B2 phase into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under the condition of rapid stirring, homogenizing and uniformly stirring;
adding C1 phase raw materials, stirring, and homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding the C3 phase, stirring uniformly, keeping the temperature for 20 minutes, and stirring and cooling;
independently heating the phase D to 60-65 ℃, stirring and dissolving until the phase D is completely transparent and free of particles, adding the phase D into an emulsifying pot when the temperature of a material body in the emulsifying pot is reduced to 65 ℃, and uniformly stirring;
continuously stirring and cooling to below 45 ℃, sequentially adding the phase E, and uniformly stirring;
adding the phase F, and uniformly stirring;
adding G phase for color matching, and stirring.
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