CN110115691A - A kind of whitening and softening skin lotion of the product containing rice fermentation and preparation method thereof - Google Patents
A kind of whitening and softening skin lotion of the product containing rice fermentation and preparation method thereof Download PDFInfo
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- CN110115691A CN110115691A CN201910458979.XA CN201910458979A CN110115691A CN 110115691 A CN110115691 A CN 110115691A CN 201910458979 A CN201910458979 A CN 201910458979A CN 110115691 A CN110115691 A CN 110115691A
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The invention discloses whitening and softening skin lotions of a kind of product containing rice fermentation and preparation method thereof, belong to daily cosmetics technical field.In the whitening and softening skin lotion of the product containing rice fermentation, including Bacillus acidi lactici/rice fermentation product, maltitol and arginic mixture, because rice fermentation product is natural component, it is easy to absorb, it is nonirritant, it can obviously be moisturized the skin after, there is apparent whitening and softening skin effect；It is natural component, safe and non-stimulating, nourishes effect is good in addition, also containing yeast peptide, saussurea involucrata fermentation liquid and rice tunning filtrate in the whitening and softening skin lotion；The present invention also provides the methods for preparing mask sheet, control Bacillus acidi lactici/rice fermentation product, maltitol and ar-ginine mixtures and the mass ratio of rice tunning filtrate are 0.1-2:1 during the preparation process, make the lotion being prepared that there is better water lock effect, to make skin high resilience.
Description
Technical field
The invention belongs to daily cosmetics technical field, be related to a kind of product containing rice fermentation whitening and softening skin lotion and its
Preparation method.
Background technique
In modern society, the contacts of people are more and more, and possessing youth beautiful skin is gathered around desired by everyone
Have, for women, is even more important.The daily life of people thus is become along with people to the nursing moment of skin
Indispensable thing in work.With advancing age, skin degenerative, skin inevitably will appear some small situations, then plus
On by factors such as ultraviolet irradiation, air pollution, physical fatigues, skin can feel burnout, lose moist, cause water oil not
Balance, dry skin is coarse, lacks oil, moisture and nutrient necessary to supply skin operates.It nourishes when skin lacks, also can
A series of problems, such as accordingly causing spot, wrinkle, complexion dark yellow, matt.
Lotion is the most important step of basic skin care, and the effective components such as moisturizing, whitening and anti-aging in lotion can be more preferable
By percutaneous absorption, so, possess one bottle of good lotion and be very important.But the lotion occurred currently on the market, it is most
It is all containing a large amount of chemical substances, it is well known that many chemical substances have certain toxicity to the mankind, and are used for a long time to skin
There may be certain side effects for skin, cannot get ideal skin effect.
In the prior art, facial treatment milk and preparation method are widely reported.Such as Chinese patent application
201510713075.9 a kind of nourishing facial treatment milk is disclosed in comprising contain following components by percentage to the quality: thin
Intracellular growth factor 0.0001-0.001%, black bearberry leaf extract 0.5-5%, glycyrrhetinic acid 1-5%, allantoin 0.1-0.5%, horse
Oily 2-5%, sad Propylheptyl 5-10%, glucose aminoglucan 2-6%, alcohols 6-15%, carbomer 1-3%, carbonic acid two
Ethylhexyl 4-6%, surfactant 1-5%, preservative 0.01-1%, pH adjusting agent 0.01-5%, water surplus；Wherein cell
Growth factor, black bearberry leaf extract and glycyrrhetinic acid reasonable compatibility, collaboration play skin care, enhancing skin elasticity, reduce color
Element deposition, promotes cell repair and regenerated effect, to achieve the purpose that nourish shining skin；The invention provides its preparation simultaneously
Method, the activity of effective component in effective protection prescription, the effect for making it nourish shining skin is more significant, but in the invention not
There is the problem of concern improves skin elasticity.
For another example, a kind of blue lotus flower preserving moisture and protecting skin lotion, the skin care are disclosed in Chinese patent application 201610209367.3
Lotion is mainly made by the following raw material indicated according to parts by weight: cream wood 2-5 parts of fruit rouge, 5-10 parts of SIMMONDSIA CHINENSIS SEED OIL, saualane 2-7
Part, wax 1-5 parts natural emulsified, 8-12 parts of moisturizer, 50-70 parts of Lan Lianhua hydrosol, 3-15 parts of plant extraction liquid.The invention is also public
The preparation method of the indigo plant lotus flower preserving moisture and protecting skin lotion is opened.Product of the present invention is natural, mild, non-stimulated, can make moisturizing for a long time
Moisturizing is used, and has preferable replenishing water and preserving moisture effect to dry skin quality, sensitive skin quality etc., and have the work of whitening and softening skin whitening
With.It joined a certain amount of natural emulsified wax in this application, be easy to aggravate the greasy feeling of lotion, lotion is made clearly to spend reduction.
Therefore, develop one kind can with the tender skin of whitening effect, make skin have preferably elasticity, and can effectively water lock lotion
It is very necessary.
Summary of the invention
For above-mentioned problems of the prior art and deficiency, the present invention is intended to provide one kind can effective water lock, and
And the flexible lotion of skin can be made with whitening and softening skin.
The technical solution adopted by the present invention to solve the technical problems first is that: a kind of beauty of product containing rice fermentation is provided
Delicate skin lotion, the whitening and softening skin lotion includes following components by weight percentage: cetostearyl alcohol olive oleate
With the mixture 0.1-2% of the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation product, maltitol and arginic mixed
Object 0.1-2%, the mixture 0.1-2% of Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6, saussurea involucrata fermentation liquid 1-3% are closed,
Yeast peptide 1-5%, rice tunning filtrate 1-5% and excess water.
Preferably, the whitening and softening skin lotion includes following components by weight percentage: cetostearyl alcohol olive oil
The mixture 0.5-1.5% of acid esters and the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation product, maltitol and smart ammonia
The mixture 0.5-1.5% of acid, the mixture 0.5-1.5% of Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6, saussurea involucrata hair
Zymotic fluid 1.5-2.5%, yeast peptide 2-4%, rice tunning filtrate 2-4% and excess water.
Above-mentioned whitening and softening skin lotion further includes following components by weight percentage: butanediol 3-10%, trehalose 2-
6%, phytosterol/octyl dodecanol lauroyl glutamate ester 2-5%, glycine betaine 2-5%, overlay film saccharomycetes to make fermentation Product filtrate
1-5%, tranexamic acid 1-5%, niacinamide 1-3%, C13-16 isoparaffin 1-3%, (thylhexoic acid) ester of pentaerythrite four 1-
3%, dimethyl silicone polymer 1-3%, -10 1-3% of methyl gluceth, Cholesteryl hydroxystearate 0.1-2% are sweet
Oleyl alcohol methacrylate/stearyl alcohol methacrylate copolymer 0.1-2%, 1,2- pentanediol 0.1-2%, fertility
Phenol acetic acid esters 0.1-2%, docosyl alcohol 0.1-2%, Rheum officinale (RHEUM OFFICINALE) extract 0.1-2%, nanometer packet
Wrap up in ceramide 0.1-2%, preservative 0.1-2%, hydrolecithin 0.1-2%, -6 0.1- of polyacrylate cross-linked polymer
1%, carnosine 0.1-1%, xanthan gum 0.01-0.2%, carboxymethylchitosan 0.01-0.2%, beta glucan 0.01-
0.2%, Sodium Hyaluronate 0.01-0.2%, tremella (TREMELLA FUCIFORMIS) fruiting body extract 0.01-0.2%,
EDETATE SODIUM 0.01-0.2%, polyglutamic acid sodium 0.01-0.2% and essence 0.01-0.2%.
Preferably, the whitening and softening skin lotion further includes following components by weight percentage: butanediol 5-8%, sea
Algae sugar 3-5%, phytosterol/octyl dodecanol lauroyl glutamate ester 3-5%, glycine betaine 3-5%, overlay film saccharomycetes to make fermentation produce
Object filtrate 2-4%, tranexamic acid 2-4%, niacinamide 1.5-2.5%, C13-16 isoparaffin 1.5-2.5%, four (second of pentaerythrite
Base caproic acid) ester 1.5-2.5%, dimethyl silicone polymer 1.5-2.5%, -10 1.5-2.5% of methyl gluceth, cholesterine
Hydroxy stearic acid ester 0.5-1.5%, glycerol amide ethanol methyl acrylate/stearyl alcohol methacrylate copolymer 0.5-
1.5%, 1,2- pentanediol 0.5-1.5%, tocopherol acetate 0.5-1.5%, docosyl alcohol 0.5-1.5%, Rheum officinale
(RHEUM OFFICINALE) extract 0.5-1.5%, nano-encapsulated ceramide 0.5-1.5%, preservative 0.5-1.5%,
Hydrolecithin 0.5-1.5%, polyacrylate cross-linked polymer -6 0.5-0.8%, carnosine 0.5-0.8%, xanthan gum
0.05-0.15%, carboxymethylchitosan 0.05-0.15%, beta glucan 0.05-0.15%, Sodium Hyaluronate 0.05-
0.15%, tremella (TREMELLA FUCIFORMIS) fruiting body extract 0.05-0.15%, EDETATE SODIUM 0.05-0.15%,
Polyglutamic acid sodium 0.05-0.15% and essence 0.05-0.15%.
More preferably, the whitening and softening skin lotion of the above-mentioned product containing rice fermentation includes following components by weight percentage:
Butanediol 6-7%, trehalose 4-5%, phytosterol/octyl dodecanol lauroyl glutamate ester 4-5%, glycine betaine 4-5%, ferment
Female peptide 3-4%, rice tunning filtrate 3-4%, overlay film saccharomycetes to make fermentation Product filtrate 3-4%, tranexamic acid 3-4%, saussurea involucrata
Fermentation liquid 2-2.5%, niacinamide 2-2.5%, C13-16 isoparaffin 2-2.5%, (thylhexoic acid) ester of pentaerythrite four 2-
2.5%, dimethyl silicone polymer 2-2.5%, methyl gluceth -10 2-2.5%, Cholesteryl hydroxystearate 1-
1.5%, glycerol amide ethanol methyl acrylate/stearyl alcohol methacrylate copolymer 1-1.5%, 1,2- pentanediol 1-
1.5%, the mixture 1-1.5%, tocopherol acetate 1- of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb
1.5%, docosyl alcohol 1-1.5%, Bacillus acidi lactici/rice fermentation product, maltitol and arginic mixture 1-1.5% gather
The mixture 1-1.5% of sodium acrylate, C18-21 alkane and isodecanol polyethers -6, Rheum officinale (RHEUM OFFICINALE) extract
Object 1-1.5%, nano-encapsulated Cer EOS -1.5%, preservative 1-1.5%, hydrolecithin 1-1.5%, polyacrylate
Cross-linked polymer -6 0.6-0.7%, carnosine 0.6-0.7%, xanthan gum 0.1-0.15%, carboxymethylchitosan 0.1-
0.15%, beta glucan 0.1-0.15%, Sodium Hyaluronate 0.1-0.15%, tremella (TREMELLA FUCIFORMIS) are real
Body extract 0.1-0.15%, EDETATE SODIUM 0.1-0.15%, polyglutamic acid sodium 0.1-0.15%, essence 0.1-0.15% and water
Surplus.
In a preferred embodiment, the cetostearyl alcohol olive oleate and the smooth olive oleate mixing of sorb
The mass ratio of the mixture of object and Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6 is 1-10:1；
More preferably, the cetostearyl alcohol olive oleate and the smooth olive oil acid ester mixtures of sorb and polyacrylic acid
The mass ratio of the mixture of sodium, C18-21 alkane and isodecanol polyethers -6 is 3-6:1.
In a further preferred embodiment, the Bacillus acidi lactici/rice fermentation product, maltitol and arginine mixed
The mass ratio for closing object and rice tunning filtrate is 0.1-2:1；
More preferably, the Bacillus acidi lactici/rice fermentation product, maltitol and ar-ginine mixtures and rice ferment
The mass ratio of Product filtrate is 0.5-1:1.
The technical solution adopted by the present invention to solve the technical problems second is that: the present invention also provides described in one kind containing big
The preparation method of the whitening and softening skin lotion of rice tunning, comprising the following steps:
(1) by the butanediol of formulation dosage, trehalose, glycine betaine, tranexamic acid, niacinamide, methyl gluceth -10,
1,2- pentanediol, the mixture of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation produce
Object, maltitol and arginic mixture, hydrolecithin, polyacrylate cross-linked polymer -6, xanthan gum, hyaluronic acid
Sodium, tremella (TREMELLA FUCIFORMIS) fruiting body extract, EDETATE SODIUM and polyglutamic acid sodium are added in emulsifier unit,
After mixing evenly, it is kept the temperature after heating, obtains mixture A；
(2) by the phytosterol of formulation dosage/octyl dodecanol lauroyl glutamate ester, C13-16 isoparaffin, season penta
Tetrol four (thylhexoic acid) ester, dimethyl silicone polymer, Cholesteryl hydroxystearate, glycerol amide ethanol methyl acrylic acid
Ester/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water are added in dissolver, are warming up to dissolution
After stir evenly, keep the temperature, obtain mixture B；
(3) mixture B obtained in step (2) is added in mixture A and is stirred homogeneous 5-10 minutes, obtain mixture C,
Then the mixture of the Sodium Polyacrylate of formulation dosage, C18-21 alkane and isodecanol polyethers -6, which is added in mixture C, continues homogeneous
1-5 minutes, insulated and stirred obtained mixture D after cooling；
(4) yeast peptide, rice tunning filtrate, the overlay film saccharomycete hair of formulation dosage are added after object D cooling to be mixed
Ferment Product filtrate, saussurea involucrata fermentation liquid, Rheum officinale (RHEUM OFFICINALE) extract, nano-encapsulated ceramide, carnosine,
Carboxymethylchitosan, beta glucan, preservative and essence stir 10-30 minutes, continue to cool down, obtain mixture E；
(5) object E cooling to be mixed, filtering and discharging is to get the whitening and softening skin lotion for arriving the product of rice containing lactobacillus fermentation
Finished product.
Warming temperature described in above-mentioned steps (1) is 85-95 DEG C, and the insulated and stirred time is 20-40 minutes.
Warming temperature described in above-mentioned steps (2) is 80-90 DEG C, and the soaking time is 5-15 minutes.
The insulated and stirred time described in above-mentioned steps (3) is 10-30 minutes.
Cooling described in above-mentioned steps (4) is that temperature is down to 40-45 DEG C.
Cooling temperature described in above-mentioned steps (5) is 35-40 DEG C.
A kind of preparation method of the whitening and softening skin lotion of above-mentioned product containing rice fermentation, specifically includes the following steps:
(1) by the butanediol of formulation dosage, trehalose, glycine betaine, tranexamic acid, niacinamide, methyl gluceth -10,
1,2- pentanediol, the mixture of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation produce
Object, maltitol and arginic mixture, hydrolecithin, polyacrylate cross-linked polymer -6, xanthan gum, hyaluronic acid
Sodium, tremella (TREMELLA FUCIFORMIS) fruiting body extract, EDETATE SODIUM and polyglutamic acid sodium are added in emulsifier unit,
After mixing evenly, it is warming up to 85-95 DEG C, insulated and stirred 20-40 minutes, obtains mixture A；
(2) by the phytosterol of formulation dosage/octyl dodecanol lauroyl glutamate ester, C13-16 isoparaffin, season penta
Tetrol four (thylhexoic acid) ester, dimethyl silicone polymer, Cholesteryl hydroxystearate, glycerol amide ethanol methyl acrylic acid
Ester/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water are added in dissolver, are warming up to 80-90
DEG C dissolution after stir evenly, keep the temperature 5-15 minutes, obtain mixture B；
(3) mixture B obtained in step (2) is added in mixture A and is stirred homogeneous 5-10 minutes, obtain mixture C,
Then the mixture of the Sodium Polyacrylate of formulation dosage, C18-21 alkane and isodecanol polyethers -6, which is added in mixture C, continues homogeneous
1-5 minutes, insulated and stirred 10-30 minutes, mixture D is obtained after cooling；
(4) the yeast peptide of formulation dosage is added when object D temperature to be mixed is down to 40-45 DEG C, rice tunning filtrate, covers
Film saccharomycetes to make fermentation Product filtrate, saussurea involucrata fermentation liquid, Rheum officinale (RHEUM OFFICINALE) extract, nano-encapsulated nerve
Amide, carnosine, carboxymethylchitosan, beta glucan, preservative and essence stir 10-30 minutes, continue to cool down, obtain
To mixture E；
(5) object E to be mixed is cooled to 35-40 DEG C, and filtering and discharging is to get the whitening for arriving the product of rice containing lactobacillus fermentation
Tender skin lotion finished product.
Compared with prior art, the present invention beneficial effect is:
(1) contain rice fermentation product in facial treatment milk prepared by the present invention, be natural component, be easy to absorb, it is non-stimulated
Property, it can obviously be moisturized the skin after, there is apparent whitening and softening skin effect；
It (2) is day containing yeast peptide, saussurea involucrata fermentation liquid and rice tunning filtrate in the lotion prepared in the present invention
Right ingredient, safe and non-stimulating, nourishes effect is good；
(3) mask sheet prepared in the present invention controls Bacillus acidi lactici/rice fermentation product, maltitol during the preparation process
It is 0.1-2:1 with ar-ginine mixtures and the mass ratio of rice tunning filtrate, there is the lotion being prepared better
Water lock effect makes skin high resilience.
Specific embodiment
Beneficial effects of the present invention are further described by following embodiment, embodiment is only used for the purpose of illustration, no
It limits the scope of the invention, while the obvious change and modification that those of ordinary skill in the art are made according to the present invention
Comprising within the scope of the present invention, following component is in addition to especially indicating, in parts by weight.It is previously mentioned in following embodiment
Butanediol be purchased from U.S. OXEA, trehalose is purchased from the former chemistry of woods, trade name trehalose, phytosterol/octyl dodecanol laurel
Acyl glutamate is purchased from Japanese aginomoto, model ELDEW PS-203, and glycine betaine is purchased from Dupont, model BP-20, yeast
Peptide is purchased from the refined element in Chongqing, model TIA, and rice tunning filtrate is purchased from the refined element in Chongqing, the full ferment of trade name, overlay film saccharomycete hair
Ferment Product filtrate is purchased from Hubei Angel Yeast, trade name overlay film saccharomycetes to make fermentation Product filtrate, and tranexamic acid is purchased from Hunan Dongting Lake medicine
Industry, trade name tranexamic acid, saussurea involucrata fermentation liquid are purchased from Hubei Angel Yeast, model FS002, and niacinamide is purchased from Dutch Royal DSM,
Model Niacinamide PC, C13-16 isoparaffin is purchased from Japanese daylight, model X-Light I, four (ethyl hexyl of pentaerythrite
Acid) ester is purchased from that Japanese day is clear, and model SALACOS 5408, dimethyl silicone polymer is purchased from Dow corning, model PMX-
200, methyl gluceth -10 is purchased from U.S. Lu Borun, model GLUCAM E-10, and Cholesteryl hydroxystearate is purchased from
Japanese day is clear, model SALACOS HS, glycerol amide ethanol methyl acrylate/stearyl alcohol methacrylate copolymer purchase
Clear from Japanese day, model Ceracute L, 1,2- pentanediol is purchased from fragrant, the model Sendiol PG of German moral, and spermaceti is hard
Lipidol olive oleate and the smooth olive oil acid ester mixtures of sorb are purchased from Italy B&T, model olivem 1000, tocopherol
Acetic acid esters is purchased from purchased from German BASF, trade name Vitwas E, and docosyl alcohol is purchased from German BASF, model
Lanette 22, Bacillus acidi lactici/rice fermentation product, maltitol and ar-ginine mixtures are purchased from Japan Te Kenuobao, model
For Technolong rice ferment, Sodium Polyacrylate, C18-21 alkane and -6 mixture of isodecanol polyethers are celestial purchased from France
Graceful, model G57, Rheum officinale (RHEUM OFFICINALE) extract is purchased from the refined element in Chongqing, trade name rheum officinale ferment, nanometer
It wraps up ceramide and is purchased from South Korea Dou Shan, model HydroCeramide5, preservative is purchased from Britain's Bristol, model
MICROCARE PHDG, hydrolecithin are purchased from Japanese daylight, model Lecinol s-10, polyacrylate cross-linked polymeric
Object -6 purchased from France match Bick, model Sepimax zen, carnosine purchased from Shenzhen tie up fine jade, xanthan gum purchased from U.S. Si Bikai can,
Model Keldent, carboxymethylchitosan reveal purchased from the Shanghai spring, and model MHA micro, beta glucan is purchased from Ningbo
Uncommon Noah, trade name beta glucan, Sodium Hyaluronate are purchased from Shandong Fu Ruida, model HA-TLM 20-40, tremella
(TREMELLA FUCIFORMIS) fruiting body extract is purchased from Ningbo Xi Nuoya, and trade name tremella polysaccharides, EDETATE SODIUM is purchased from beauty
State Akzo Nobel, polyglutamic acid sodium are pacified purchased from Wuhan fine horse, trade name Polyurethane-epoxy resin sodium.
Instrument homogenizer used in following embodiment is purchased from Germany IKA, model T25；Blender is purchased from Germany
IKA, model RW20；Electronic scale is double outstanding purchased from Changshu, the double outstanding person 1000g of model；PH meter holds in the palm benefit purchased from Switzerland plum Teller &,
Model FE28；Thermostat water bath is purchased from the rich news in Shanghai, model HHS-11-1；Water purification machine is purchased from Zhejiang Qin Yuan, model RO-
1851；Beaker is purchased from Sichuan another name for Sichuan Province glass, 500mL.
The olivem 1000 being previously mentioned in following embodiment be mass ratio 60:40 cetostearyl alcohol olive oleate and
The mixture of the smooth olive oleate of sorb；Technolong rice ferment is the lactic acid bar of mass ratio 79.2:20:0.8
Bacterium/rice fermentation product, maltitol and arginic mixture；G57 ingredient be mass ratio 60:35:5 Sodium Polyacrylate,
- 6 mixture of C18-21 alkane and isodecanol polyethers；Saussurea involucrata fermentation liquid is the saccharomycetes to make fermentation Product filtrate and snow that mass ratio is 99:1
The mixture of lotus flower (SAUSSUREA INVOLUCRATA) extract；It is 5:40:3 that nano-encapsulated ceramide, which is mass ratio:
Cer NP, water, caprylic/capric triglyceride, glycerol, ceteareth -20, the Natrulon H-10 of 25:15:10:2 is hard
The mixture of resin acid ester and polysorbate -20；Preservative is Phenoxyethanol, decanediol and the pungent glycol that mass ratio is 92:4:4
Mixture.
Whitening and softening skin lotion of a kind of product containing rice fermentation of embodiment 1-5 and preparation method thereof
Preparation method: specifically includes the following steps:
(1) by the butanediol of formulation dosage, trehalose, glycine betaine, tranexamic acid, niacinamide, methyl gluceth -10,
1,2- pentanediol, the mixture of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation produce
Object, maltitol and arginic mixture, hydrolecithin, polyacrylate cross-linked polymer -6, xanthan gum, hyaluronic acid
Sodium, tremella (TREMELLA FUCIFORMIS) fruiting body extract, EDETATE SODIUM and polyglutamic acid sodium are added in emulsion pot, stir
After mixing uniformly, 90 DEG C are warming up to, insulated and stirred 30 minutes, obtains mixture A；
(2) by the phytosterol of formulation dosage/octyl dodecanol lauroyl glutamate ester, C13-16 isoparaffin, season penta
Tetrol four (thylhexoic acid) ester, dimethyl silicone polymer, Cholesteryl hydroxystearate, glycerol amide ethanol methyl acrylic acid
Ester/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water are added in oily phase pot, be warming up to 85 DEG C it is molten
It is stirred evenly after solution, keeps the temperature 10 minutes, obtain mixture B；
(3) mixture B obtained in step (2) is added in mixture A and is stirred homogeneous 6 minutes, obtain mixture C, so
The mixture of the Sodium Polyacrylate of formulation dosage, C18-21 alkane and isodecanol polyethers -6 is added continuation homogeneous 5 in mixture C and divides afterwards
Clock insulated and stirred 20 minutes, obtains mixture D after cooling；
(4) yeast peptide, the rice tunning filtrate, overlay film of formulation dosage are added when object D temperature to be mixed is down to 45 DEG C
Saccharomycetes to make fermentation Product filtrate, saussurea involucrata fermentation liquid, Rheum officinale (RHEUM OFFICINALE) extract, nano-encapsulated nerve acyl
Amine, carnosine, carboxymethylchitosan, beta glucan, preservative and essence stir 20 minutes, continue to cool down, be mixed
Object E；
(5) object E to be mixed is cooled to 38 DEG C, and filtering and discharging is tender to get the whitening to the product of rice containing lactobacillus fermentation
Skin lotion finished product.
Whitening and softening skin lotion of a kind of product containing rice fermentation of control group 1-5 and preparation method thereof
Compared with Example 1, difference is control group 1: control group 1 is not added with olivem 1000 and G57.
Compared with Example 1, difference is control group 2: the mass ratio of olivem 1000 and G57 is 0.5 in control group 2:
1, i.e., the percentage composition that the percentage composition of olivem 1000 is 0.5%, G57 is 1%.
Compared with Example 1, difference is control group 3: the mass ratio of olivem 1000 and G57 is 14 in control group 3:
1, i.e., the percentage composition that the percentage composition of olivem 1000 is 1.4%, G57 is 0.1%.
Compared with Example 1, difference is control group 4: control group 4 is not added with rice tunning filtrate, saussurea involucrata fermentation
Liquid, yeast peptide；
Compared with Example 1, difference is control group 5: control group 5 is not added with Technolong rice ferment.
Compared with Example 1, difference is control group 6: Technolong rice ferment and rice in control group 6
The mass ratio of tunning filtrate is 0.2:1, i.e., the percentage composition of Technolong rice ferment is 0.42%, rice
The percentage composition of tunning filtrate is 2.08%.
Compared with Example 1, difference is control group 7: Technolong rice ferment and rice in control group 7
The mass ratio of tunning filtrate is 5:1, i.e., the percentage composition of Technolong rice ferment is 2.08%, rice hair
The percentage composition of ferment Product filtrate is 0.42%.
Test assessment:
1, whitening spot-removing measure of merit
(1) Subject Population
Choose age bracket be 20-50 years old female volunteers 240, stochastic averagina is divided into 12 groups, every group 20.
(2) laboratory apparatus
German CK Multi probe skin measurement system MPA9, melanin and ferroheme test probe (Mexamter MX18).
(3) experimental method
After face cleaning, this product is taken to be applied to face to absorbing, without cleaning；It uses 3 times weekly, is used continuously 4 weeks；It is testing
Before, tested crowd need to use clear water cleaning face, with face tissue wiped clean, laboratory with constant temperature and constant humidity (20 ± 1 DEG C of temperature, it is wet
Degree 55 ± 3) in sit quietly 30 minutes after start to measure.The region 4*4cm in the middle part of the right face of each experimenter is chosen, it should with probe test
The average black cellulose content at four, region angle and intermediate total 5 positions.Then respectively whitening and softening skin lotion the 3rd on probation,
6,9,12 times when, test the average black cellulose content of every group of crowd respectively by the above process.
(4) evaluation method
By instrument test dermal melanin content, content reduces then explanation, and effectively, content increases or constant, illustrates nothing
Effect.
(5) experimental result
Melanin content the results are shown in Table 1
The Contrast on effect result of table 1 embodiment 1-5 and control group 1-7 product
Whitening is all had according to the lotion that the detection data of upper table 1 can be seen that the embodiment of the present invention and control group preparation
The effect of nti-freckle can be such that the melanin of skin reduces.But the lotion of embodiment preparation is reduced using rear dermal melanin
It becomes apparent from, therefore illustrates that the lotion whitening spot-removing effect of embodiment preparation is obvious.
2, water lock effect detection
(1) Subject Population
Choose age bracket be 20-50 years old female volunteers 240, stochastic averagina is divided into 12 groups, every group 20.
(2) laboratory apparatus
Tewameter TM300 calculates transdermal percentage of water loss (g/h/m by the difference of measurement water vapor pressure force gradient2),
Skin barrier is more intact, and TEWL value is lower, and skin water lock ability is better.
(3) experimental method
After face cleaning, this product is taken to be applied to face to absorbing, without cleaning；It uses 3 times weekly, is used continuously 4 weeks；It is testing
Before, tested crowd need to use clear water cleaning face, with face tissue wiped clean, laboratory with constant temperature and constant humidity (20 ± 1 DEG C of temperature, it is wet
Degree 55 ± 3) in sit quietly 30 minutes after start to measure.The region 4*4cm in the middle part of the right face of each experimenter is chosen, it should with probe test
The average capacitance value at four, region angle and intermediate total 5 positions.Then respectively after whitening and softening skin lotion on probation the
7,14,21,28 days, the average capacitance value of every group of crowd is tested respectively by the above process.
(4) evaluation method
TEWL value is lower, and skin water lock ability is better.
(5) experimental result
Water lock effect is shown in Table 2
The Contrast on effect result of table 2 embodiment 1-5 and control group 1-7 product
3, skin elasticity detects
(1) Subject Population
Choose age bracket be 20-50 years old female volunteers 240, stochastic averagina is divided into 12 groups, every group 20.
(2) laboratory apparatus
German CK company Cutometer dual MPA580 host, skin elasticity probe PVM600；
Test philosophy: based on suction and principle is stretched, a negative pressure is generated on the skin, skin is sucked into particular probe
Interior, the depth of sucking is measured by optic testing system.It include the transmitter and receiver of light, the ratio (transmitting of light in probe
The ratio between light and reception light) it is directly proportional to sucking depth, thus obtain the relationship of length and time that a skin is stretched
Then curve analyzes the elastic performance to determine skin by MPA software.
(3) experimental method
After face cleaning, this product is taken to be applied to face to absorbing, without cleaning；It uses 3 times weekly, is used continuously 4 weeks；It is testing
Before, tested crowd need to use clear water cleaning face, with face tissue wiped clean, laboratory with constant temperature and constant humidity (20 ± 1 DEG C of temperature, it is wet
Degree 55 ± 3) in sit quietly 30 minutes after start to measure.The region 4*4cm in the middle part of the right face of each experimenter is chosen, it should with probe test
The average elastic force of 3 positions of region upper, middle and lower.Then respectively at whitening and softening skin lotion the 3rd, 6,9,12 time on probation, by with top
Method tests the average elasticity value of every group of crowd respectively.Parameter setting: negative pressure -450mbar；M- 2s when negative pressure.
(4) evaluation method
R2=Ua/Uf, the springback capacity (Ua) of skin and the ratio between the maximum tension amount (Uf) when having a negative pressure, R2 number when no negative pressure
According to closer to 1, show that skin elasticity is better.
(5) experimental result
Skin elasticity effect is shown in Table 3
The Contrast on effect result of table 3 embodiment 1-5 and control group 1-7 product
Raising is all had according to the lotion that the detection data of upper table 3 can be seen that the embodiment of the present invention and control group preparation
The effect of elasticity.But the lotion of embodiment preparation is become apparent from using the elasticity improvement of rear skin, when ingredient a certain in component
Or several ingredients reduce the using effect that can significantly affect lotion, increasing skin elasticity by effect reduces, therefore illustrates embodiment
It is obvious that the lotion of preparation improves skin elasticity effect.
Above-mentioned detailed description is illustrating for wherein possible embodiments of the invention, and the embodiment is not to limit
The scope of the patents of the invention, all equivalence enforcements or change without departing from carried out by the present invention, is intended to be limited solely by technical solution of the present invention
Range.
Claims (10)
1. a kind of whitening and softening skin lotion of product containing rice fermentation, it is characterised in that: the whitening and softening skin lotion by weight hundred
Dividing includes following components than counting: the mixture 0.1-2% of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb, lactic acid
Bacillus/rice fermentation product, maltitol and arginic mixture 0.1-2%, Sodium Polyacrylate, C18-21 alkane and isodecanol
The mixture 0.1-2% of polyethers -6, saussurea involucrata fermentation liquid 1-3%, yeast peptide 1-5%, rice tunning filtrate 1-5% and surplus
Water.
2. the whitening and softening skin lotion of the product according to claim 1 containing rice fermentation, it is characterised in that: the whitening is tender
Skin lotion includes following components by weight percentage: the mixing of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb
Object 0.5-1.5%, Bacillus acidi lactici/rice fermentation product, maltitol and arginic mixture 0.5-1.5%, polyacrylic acid
The mixture 0.5-1.5% of sodium, C18-21 alkane and isodecanol polyethers -6, saussurea involucrata fermentation liquid 1.5-2.5%, yeast peptide 2-4%, rice
Rice tunning filtrate 2-4% and excess water.
3. the whitening and softening skin lotion of the product according to claim 1 containing rice fermentation, it is characterised in that: the whitening is tender
Skin lotion further includes following components by weight percentage: butanediol 3-10%, trehalose 2-6%, phytosterol/octyl 12
Alcohol lauroyl glutamate ester 2-5%, glycine betaine 2-5%, overlay film saccharomycetes to make fermentation Product filtrate 1-5%, tranexamic acid 1-5%, cigarette
Amide 1-3%, C13-16 isoparaffin 1-3%, pentaerythrite four (thylhexoic acid) ester 1-3%, dimethyl silicone polymer 1-
3%, methyl gluceth -10 1-3%, Cholesteryl hydroxystearate 0.1-2%, glycerol amide ethanol methyl acrylic acid
Ester/stearyl alcohol methacrylate copolymer 0.1-2%, 1,2- pentanediol 0.1-2%, tocopherol acetate 0.1-2%, behenyl
Alcohol 0.1-2%, Rheum officinale extract 0.1-2%, nano-encapsulated ceramide 0.1-2%, preservative 0.1-2% hydrogenate ovum
Phosphatidase 0 .1-2%, polyacrylate cross-linked polymer -6 0.1-1%, carnosine 0.1-1%, xanthan gum 0.01-0.2%, carboxylic first
Base chitosan 0.01-0.2%, beta glucan 0.01-0.2%, Sodium Hyaluronate 0.01-0.2%, Tremella fructification mention
Take object 0.01-0.2%, EDETATE SODIUM 0.01-0.2%, polyglutamic acid sodium 0.01-0.2% and essence 0.01-0.2%.
4. the whitening and softening skin lotion of the product according to claim 2 containing rice fermentation, it is characterised in that: the whitening is tender
Skin lotion further includes following components by weight percentage: butanediol 5-8%, trehalose 3-5%, phytosterol/octyl 12
Alcohol lauroyl glutamate ester 3-5%, glycine betaine 3-5%, overlay film saccharomycetes to make fermentation Product filtrate 2-4%, tranexamic acid 2-4%, cigarette
Amide 1.5-2.5%, C13-16 isoparaffin 1.5-2.5%, (thylhexoic acid) the ester 1.5-2.5% of pentaerythrite four, poly- diformazan
Radical siloxane 1.5-2.5%, -10 1.5-2.5% of methyl gluceth, Cholesteryl hydroxystearate 0.5-1.5% are sweet
Oleyl alcohol methacrylate/stearyl alcohol methacrylate copolymer 0.5-1.5%, 1,2- pentanediol 0.5-1.5%,
Tocopherol acetate 0.5-1.5%, docosyl alcohol 0.5-1.5%, Rheum officinale extract 0.5-1.5%, nano-encapsulated nerve acyl
Amine 0.5-1.5%, preservative 0.5-1.5%, hydrolecithin 0.5-1.5%, polyacrylate cross-linked polymer -60.5-
0.8%, carnosine 0.5-0.8%, xanthan gum 0.05-0.15%, carboxymethylchitosan 0.05-0.15%, beta glucan
0.05-0.15%, Sodium Hyaluronate 0.05-0.15%, Tremella fructification extract 0.05-0.15%, EDETATE SODIUM 0.05-
0.15%, polyglutamic acid sodium 0.05-0.15% and essence 0.05-0.15%.
5. the whitening and softening skin lotion of the product according to claim 4 containing rice fermentation, it is characterised in that: described contains rice
The whitening and softening skin lotion of tunning includes following components by weight percentage: butanediol 6-7%, trehalose 4-5%, plant
Sterol/octyl dodecanol lauroyl glutamate ester 4-5%, glycine betaine 4-5%, yeast peptide 3-4%, rice tunning filtrate 3-
4%, overlay film saccharomycetes to make fermentation Product filtrate 3-4%, tranexamic acid 3-4%, saussurea involucrata fermentation liquid 2-2.5%, niacinamide 2-2.5%,
C13-16 isoparaffin 2-2.5%, pentaerythrite four (thylhexoic acid) ester 2-2.5%, dimethyl silicone polymer 2-2.5%, first
Base glucitol polyethers -10 2-2.5%, Cholesteryl hydroxystearate 1-1.5%, glycerol amide ethanol methyl acrylate/hard
Lipidol methacrylate copolymer 1-1.5%, 1,2- pentanediol 1-1.5%, cetostearyl alcohol olive oleate and sorb are smooth
The mixture 1-1.5% of olive oleate, tocopherol acetate 1-1.5%, docosyl alcohol 1-1.5%, Bacillus acidi lactici/rice fermentation
Product, maltitol and arginic mixture 1-1.5%, the mixing of Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6
Object 1-1.5%, Rheum officinale extract 1-1.5%, nano-encapsulated Cer EOS -1.5%, preservative 1-1.5% hydrogenate ovum
Phosphatidase 1-1.5%, polyacrylate cross-linked polymer-6 0.6-0.7%, carnosine 0.6-0.7%, xanthan gum 0.1-0.15%,
Carboxymethylchitosan 0.1-0.15%, beta glucan 0.1-0.15%, Sodium Hyaluronate 0.1-0.15%, tremella are real
Body extract 0.1-0.15%, EDETATE SODIUM 0.1-0.15%, polyglutamic acid sodium 0.1-0.15%, essence 0.1-0.15% and water
Surplus.
6. the whitening and softening skin lotion of the product according to claim 1 containing rice fermentation, it is characterised in that: the spermaceti is hard
Lipidol olive oleate and the smooth olive oil acid ester mixtures of sorb and Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6 it is mixed
The mass ratio for closing object is 1-10:1.
7. the whitening and softening skin lotion of the product according to claim 6 containing rice fermentation, it is characterised in that: the spermaceti is hard
Lipidol olive oleate and the smooth olive oil acid ester mixtures of sorb and Sodium Polyacrylate, C18-21 alkane and isodecanol polyethers -6 it is mixed
The mass ratio for closing object is 3-6:1.
8. the whitening and softening skin lotion of the product according to claim 1 containing rice fermentation, it is characterised in that: the lactic acid bar
Bacterium/rice fermentation product, maltitol and ar-ginine mixtures and the mass ratio of rice tunning filtrate are 0.1-2:1.
9. the whitening and softening skin lotion of the product according to claim 8 containing rice fermentation, it is characterised in that: the lactic acid bar
Bacterium/rice fermentation product, maltitol and ar-ginine mixtures and the mass ratio of rice tunning filtrate are 0.5-1:1.
10. a kind of preparation method of the whitening and softening skin lotion of the described in any item products containing rice fermentation of claim 1-9, special
Sign is: the following steps are included:
(1) by the butanediol of formulation dosage, trehalose, glycine betaine, tranexamic acid, niacinamide, methyl gluceth -10,1,2-
Pentanediol, the mixture of cetostearyl alcohol olive oleate and the smooth olive oleate of sorb, Bacillus acidi lactici/rice fermentation product,
Maltitol and arginic mixture, hydrolecithin, polyacrylate cross-linked polymer -6, xanthan gum, Sodium Hyaluronate,
Tremella fructification extract, EDETATE SODIUM and polyglutamic acid sodium heating emulsification after mixing, obtain mixture A；
(2) by the phytosterol of formulation dosage/octyl dodecanol lauroyl glutamate ester, C13-16 isoparaffin, pentaerythrite
Four (thylhexoic acid) esters, dimethyl silicone polymer, Cholesteryl hydroxystearate, glycerol amide ethanol methyl acrylate/hard
After mixing, heating stirring is obtained to dissolving for lipidol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water
Mixture B；
(3) mixture B obtained in step (2) is added in mixture A and is uniformly mixed, obtain mixture C, then use formula
The mixture of the Sodium Polyacrylate of amount, C18-21 alkane and isodecanol polyethers -6 is added in mixture C after mixing, insulated and stirred
To dissolution, mixture D is obtained；
(4) yeast peptide, rice tunning filtrate, the overlay film saccharomycetes to make fermentation that formulation dosage is added after object D cooling to be mixed produce
Object filtrate, saussurea involucrata fermentation liquid, Rheum officinale extract, nano-encapsulated ceramide, carnosine, carboxymethylchitosan, β-
Glucan, preservative and essence obtain mixture E after mixing evenly；
(5) to get the whitening and softening skin lotion finished product for arriving the product of rice containing lactobacillus fermentation after object E cooling to be mixed.
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| CN112691065A (en) * | 2021-02-08 | 2021-04-23 | 福建片仔癀化妆品有限公司 | Moisturizing emulsion and preparation method thereof |
| CN116440051A (en) * | 2022-12-29 | 2023-07-18 | 华熙生物科技股份有限公司 | Composition with moisturizing effect and application of composition in cosmetics |
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