CN114632028B - Lifting and tightening cream and preparation method thereof - Google Patents

Lifting and tightening cream and preparation method thereof Download PDF

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Publication number
CN114632028B
CN114632028B CN202210325912.0A CN202210325912A CN114632028B CN 114632028 B CN114632028 B CN 114632028B CN 202210325912 A CN202210325912 A CN 202210325912A CN 114632028 B CN114632028 B CN 114632028B
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phase
stirring
combination
skin
filler
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CN114632028A (en
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叶晓纯
杜万锋
黄振振
曹波
杨菊
李金印
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Guangzhou Youjiyuan Cosmetics Co ltd
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Guangzhou Youjiyuan Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention discloses a lifting and tightening cream, which comprises the following components: the phase A comprises a solvent, a humectant, a thickener and a skin conditioning agent, wherein the thickener in the phase A consists of carbomer, sodium polyacrylate grafted starch and xanthan gum; the B1 phase comprises an emulsifier, a thickener, a cleanser, an emollient and a filler; the filler in the B1 phase consists of polydimethylsiloxane and polysiloxane-11; b2 phase comprises filler mica, titanium dioxide and bismuth oxychloride; the C1 phase comprises a stabilizer; the C2 phase comprises an emollient and a filler, and the filler in the C2 phase is polymethyl silsesquioxane; the C3 phase comprises a pH regulator and a solvent; phase D includes antioxidant and humectant; phase E includes moisturizers and skin conditioners. The lifting and tightening face cream has strong moisturizing capability, can form lifting effect on skin, ensures that the skin is compact and full, is slightly waterproof, soft, glutinous and fine in texture, and has the advantages of simple preparation method, simple process and easily controlled quality.

Description

Lifting and tightening cream and preparation method thereof
Technical Field
The invention relates to the technical field of skin care products, in particular to a lifting and tightening cream and a preparation method thereof.
Background
With economic development, people have increasingly pursued life, including morphological demands. However, the skin care varieties in the market are various, and the forms of the skin care varieties are liquid, emulsion and solid; the types of the skin-softening lotion, the skin-refreshing lotion, the essence, the emulsion, the face cream, the facial mask and the like are classified; the Chinese medicinal composition has effects of keeping moisture, whitening skin, removing acne, eliminating yellow, removing wrinkle, and resisting allergy. The choice of a suitable skin care product is critical to skin care. On the other hand, as women age, more and more skin problems such as skin sagging, etc., have occurred, which have long plagued the average consumer. For high-end consumers, they can choose to lift the skin by injecting an anti-wrinkle needle, etc., but the anti-wrinkle needle is expensive and also has a certain risk, and the anti-wrinkle needle is not a routine choice for the average consumer. The average consumer also tends to apply skin care products to skin. In order to meet the high-end skin care requirements of common consumers, the research and development of the high-end skin care product has good market prospect.
Disclosure of Invention
In order to overcome the defects of the prior art, one of the purposes of the invention is to provide a lifting and tightening face cream which has strong moisturizing capability, can form lifting effect on skin, enables the skin to be compact and full, has a micro-waterproof effect, prevents a skin care layer from being easily taken away by water, sweat and the like, is suitable for long-time maintenance of the skin, has soft, glutinous and fine texture, and is a high-end upgrade face cream.
The second purpose of the invention is to provide a preparation method of the lifting tension face cream, which has simple process and easily controlled quality.
One of the purposes of the invention is realized by adopting the following technical scheme:
a lift-tensioning face cream comprising a phase a, B, C, D, E, F and G phases, in weight percent in the face cream:
the phase A comprises a solvent and the balance; 5-11% of humectant; 0.2-0.8% of thickener; 0.1-0.3% of skin conditioning agent; the thickener in the phase A consists of carbomer, sodium polyacrylate grafted starch and xanthan gum;
the B phase comprises a B1 phase and a B2 phase; the B1 phase comprises 1.4-3.5% of emulsifying agent; 1.5 to 4.2 percent of thickener; 2-5% of a cleaning agent; 5-18.5% of an emollient; 5-15% of filler; the filler in the B1 phase consists of polydimethylsiloxane and polysiloxane-11; the B2 phase comprises 1-2.9% of filler, and the filler in the B2 phase comprises mica, titanium dioxide and bismuth oxychloride;
the C phase comprises a C1 phase, a C2 phase and a C3 phase; the C1 phase comprises 0.8-1.2% of stabilizer; the C2 phase comprises 0.8-1.5% of an emollient and 0.8-1.5% of a filler, and the filler in the C2 phase is polymethylsilsesquioxane; the C3 phase comprises 0.15-0.5% of pH regulator and 0.5-2% of solvent;
the phase D comprises 0.3-0.6% of antioxidant and 1-5.6% of humectant;
the E phase comprises 0.5-2% of humectant and 0.6-4.5% of skin conditioner;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% colorant.
The tightening and thickening cream provided by the invention comprises a plurality of components, each component is accurately blended into different phases, and a plurality of components such as a humectant, an emulsifier, a thickener, a filler, an emollient, a skin conditioner, a cleanser and the like are skillfully matched, so that the formed cream is soft, waxy and dense in texture, excellent in moisturizing capability, has a micro-waterproof effect, is moist and not greasy, can enable skin to be full and compact, and meets the high-end skin care requirements of common mass consumers. Wherein, the addition of the sodium polyacrylate grafted starch can not only improve the endless feel of the product. More importantly, the sodium polyacrylate grafted starch can lift and tighten skin, takes hydrophilic and semi-rigid starch macromolecules as a framework, and has polysaccharide compounds, intermolecular acting force and reactivity by introducing different functional groups and adjusting the proportion of hydrophilic and lipophilic chain segment structures. Based on this property, sodium polyacrylate grafted starch, when spread on the skin, immobilizes the skin just like a rigid structure, giving a taut feel. Meanwhile, the sodium polyacrylate grafted starch is an amphoteric compound, namely hydrophilic and oleophylic, and can be closely attached to a water-based end, so that the water-holding effect is more excellent, and the sodium polyacrylate grafted starch can be well filled in a skin cell gap, so that the skin is plump and compact. In addition, the invention adopts the specific filler and the sodium polyacrylate grafted starch to compound, so that the skin is more compact and full, the filler can lighten the skin color, adjust the skin color, enable the skin to be in a healthy state, and simultaneously endow the product with natural use feeling, and is ductile and easy to paint. On the other hand, the filler has a hydrophobic function, can block moisture to a certain extent, and has a micro-waterproof function. The product of the invention realizes the effect of tightening the skin, and the skin does not feel tight and uncomfortable, because the invention also adds a proper amount of humectant, emollient and skin conditioner, the components can ease the skin and soften the skin. In addition, a large amount of grease (mainly an emollient in B1 phase and C2 phase) is added into the formula, and the grease further improves the waterproof function of the product.
Further, in the a phase, the solvent is water; the humectant is a combination of glycerin, butylene glycol and sodium hyaluronate; the skin conditioning agent is allantoin.
The face cream has excellent moisturizing effect, glycerin, butanediol and sodium hyaluronate in phase A are easily absorbed by skin, and hyaluronic acid is a linear polysaccharide structure composed of repeated structures of N-caproamide glucose and D-glucuronic acid. The reduction and destruction of the HA content of hyaluronic acid (hyaluronic acid) in the skin can cause the skin to lose elasticity due to wrinkling during water loss, and the human epidermis is aged. The humectant disclosed by the invention comprises sodium hyaluronate as a high-efficiency humectant, and can delay skin aging.
Further, in the B1 phase, the emulsifier is a combination of lauryl PEG-10 tris (trisilyloxy) silylethyl polydimethylsiloxane, PEG-20 methylglucsesquistearate and glycerol stearate and PEG-100 stearate; the thickening agent is a composition of cetostearyl alcohol and behenyl alcohol; the cleaning agent is a composition of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; the emollient is a combination of dimethicone, C12-15 alcohol benzoate, isohexadecane, dimethicone, dimethiconol, cyclohexasiloxane, cyclopentadimethicone, and octylpolymethylsiloxane.
The face cream of the present invention incorporates a cleansing ingredient in which lauric acid is capable of imparting a finer skin feel.
Further, in the C1 phase, the stabilizer is a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate; in the C2 phase, the emollient is a combination of cyclohexasiloxane and cyclopentadimethicone; the filler is polymethylsilsesquioxane; in the C3 phase, the pH adjuster is aminomethylpropanol; the solvent is water.
Further, in the D phase, the antioxidant is p-hydroxyacetophenone, and the p-hydroxyacetophenone has the effects of resisting oxidization and relieving skin. In the invention, the p-hydroxyacetophenone can be used as a substitute of the traditional preservative, has the functions of corrosion prevention and synergism, and has excellent stability in high and low pH and temperature ranges. Further, in the D phase, the humectant is a combination of butylene glycol and 1, 2-hexanediol.
Further, in the E phase, the humectant is trimethylpentanediol/adipic acid/glycerin crosslinked polymer; the skin conditioning agents include lactobacillus/soy milk fermentation product filtrate, butylene glycol, 1, 2-pentanediol, hydroxypropyl tetrahydropyran triol, 1, 2-hexanediol, hexapeptide-9, and arginine/lysine polypeptides. Arginine/lysine polypeptide and hexapeptide-9 have synergistic effects, and the addition of lysine makes the skin more compact.
Further, in the F phase, the fragrance is a perfume; in the G phase, the colorant is a caramel color.
Further, the lift tension cream comprises an A phase, a B phase, a C phase, a D phase, an E phase, an F phase and a G phase, according to the weight percentage in the cream:
the phase a includes: water, the balance; humectant: 3-5% of glycerol, 2-5% of butanediol and 0.01-0.05% of sodium hyaluronate; and (3) a thickening agent: 0.1 to 0.5 percent of carbomer, 0.05 to 0.15 percent of sodium polyacrylate grafted starch and 0.05 to 0.15 percent of xanthan gum; allantoin as skin conditioner 0.1-0.3%;
the B1 phase comprises: emulsifying agent: lauryl PEG-10 tris (trissilyloxy) silylethyl polydimethylsiloxane 0.1-0.5%, PEG-20 methyl glucose sesquistearate 0.8-1.5%, and a combination of glyceryl stearate and PEG-100 stearate 0.5-1.5%; and (3) a thickening agent: 0.5-1.2% of cetostearyl alcohol and 1-3% of behenyl alcohol; cleaning agent: 2-5% of a combination of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; an emollient: 1-3% of simethicone, 0.5-2% of C12-15 alcohol benzoate, 2-6% of isohexadecane, 0.3-0.6% of a composition of polydimethylsiloxane and dimethiconol, 1-5% of a composition of cyclohexasiloxane and cyclopenta-dimethicone, and 0.5-1.5% of octyl-polymethylsiloxane; filler: 5-15% of a composition of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filler: 0.5 to 1.5 percent of a composition of mica, titanium dioxide and triethoxy octyl silane, 0.5 to 1.2 percent of a composition of mica and titanium dioxide, and 0.05 to 0.15 percent of a composition of bismuth oxychloride and ethylhexyl hydroxystearate;
the C1 phase includes: stabilizing agent: 0.8-1.2% of a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: an emollient: 0.8-1.5% of a composition of cyclohexasiloxane and cyclopentadimethicone, filler: 0.8 to 1.5 percent of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: aminomethylpropanol 0.15-0.5%, solvent: 0.5-2% of water;
the D phase comprises: antioxidant: 0.3-0.6% of p-hydroxyacetophenone, humectant: 1-5% of butanediol and 0.1-0.6% of 1, 2-hexanediol;
the E phase comprises: humectant: trimethylpentanediol/adipic acid/glycerin crosslinked polymer 0.5-2%, skin conditioner: lactobacillus/soy milk fermentation product filtrate, 0.5-2% of a combination of butanediol and 1, 2-pentanediol, 0.1-0.8% of a combination of hydroxypropyl tetrahydropyran triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.05-1.5% of a combination of butanediol and hexapeptide-9, and 0.005-0.015% of arginine/lysine polypeptide;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% colorant.
The second purpose of the invention is realized by adopting the following technical scheme:
a preparation method of a lifting and tightening cream comprises the following steps:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 85-88 ℃, homogenizing for 3-5 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 80-85 ℃, homogenizing until no particles are completely dissolved (stirring for 3-5 min) for later use;
adding the B2 phase raw material into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under rapid stirring, and homogenizing and uniformly stirring;
adding the C1 phase raw material, uniformly stirring, and continuously homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding phase C3, stirring uniformly, preserving heat for 20 minutes, and stirring and cooling;
heating the phase D to 60-65 ℃ independently, stirring and dissolving until the phase D is completely transparent and has no particles, adding the phase D into the emulsifying pot when the temperature of the material in the emulsifying pot is reduced to 65 ℃, and stirring uniformly;
continuously stirring and cooling to below 45 ℃, sequentially adding the E phase, and uniformly stirring;
adding phase F, and stirring uniformly;
adding phase G for mixing, and stirring.
In the preparation process, the temperature, the stirring time and the heat preservation time are very critical, and improper operation can influence the molding of the product, influence the skin feel of the product and even generate peculiar smell. Particularly, the preparation of the B1 phase is particularly important, the B1 phase contains esters, and the esters can deteriorate after being heated and stirred for a long time to generate peculiar smell; too short a time, uneven stirring of the particles, insufficient stirring, and influence the sense.
Compared with the prior art, the invention has the beneficial effects that:
(1) The lifting and tightening cream provided by the invention is an upgrade version of common cream, each component and the component dosage are precisely blended, and the cream is soft, glutinous and fine in texture and skin feel. The cream can lighten skin color, enable skin to be full and compact, provide rich and nourishing natural grease for skin, provide continuous moistening for dry skin, enable a user to feel continuous plump feel and comfortable skin feel in smearing, moisten and moisturize, soft and non-greasy, and have certain waterproof effect and soft and glutinous and fine-moist.
(2) The preparation method of the lifting tension face cream provided by the invention is simple to operate and easy to control the quality.
Drawings
FIG. 1 is a product diagram of a lift tension cream according to example 1 of the present invention;
fig. 2 is a graph showing the effect of lifting tension on a face cream according to example 1 of the present invention.
Detailed Description
The present invention will be further described with reference to the accompanying drawings and detailed description, wherein it is to be understood that, on the premise of no conflict, the following embodiments or technical features may be arbitrarily combined to form new embodiments. The raw materials, equipment, etc. used in the following examples are available in a purchase manner except for special restrictions.
A lift-tensioning face cream is prepared from phase A, phase B, phase C, phase D, phase E, phase F and phase G, and has the specific formula shown in Table 1.
Table 1 Table of formulations of lifting and tightening creams of examples 1-3
The lift tightening cream of examples 1-3 was prepared as follows:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 87 ℃, homogenizing for 4 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 82 ℃, stirring for 4min, wherein the B1 phase raw material is in a homogeneous state, and completely dissolves without particles for later use;
adding the B2 phase raw material into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under rapid stirring, and homogenizing and uniformly stirring;
adding the C1 phase raw material, uniformly stirring, and continuously homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding phase C3, stirring uniformly, preserving heat for 20 minutes, and stirring and cooling;
heating the phase D to 62 ℃ independently, stirring and dissolving until the phase D is completely transparent and has no particles, and adding the phase D into an emulsifying pot when the temperature of the material in the emulsifying pot is reduced to 65 ℃ and stirring uniformly;
continuously stirring and cooling to below 45 ℃, sequentially adding the E phase, and uniformly stirring;
adding phase F, and stirring uniformly;
adding phase G for mixing, and stirring.
Comparative example 1
Comparative example 1 differs from example 1 in that "sodium polyacrylate grafted starch" in phase a was replaced with "polyacrylate crosslinked polymer-6", the amount of polyacrylate crosslinked polymer-6 was 0.08%, and the remainder was the same as in example 1.
Comparative example 2
Comparative example 1 is different from example 1 in that the filler in the B2 phase is omitted and the remainder is the same as example 1.
Comparative example 3
Comparative example 1 is different from example 1 in that the filler in the B1 phase and the C2 phase is omitted, and the rest is the same as example 1.
Comparative example 4
Comparative example 4 was different from example 1 in that the emulsifier "lauryl PEG-10 tris (trisilyloxy) silylethyl polydimethylsiloxane" in the B1 phase was omitted, and the amount of "PEG-20 methylglucsesquistearate" was adjusted to 1.5%, and the remainder was the same as in example 1.
Comparative example 5
Comparative example 5 is different from example 1 in that the cleaning agent in the B1 phase is omitted, and the rest is the same as example 1.
Comparative example 6
Comparative example 6 differs from example 1 in that the emollients "dimethicone" and "isohexadecane" in the B1 phase were omitted, the amounts of the emollients "cyclohexasiloxane, cyclopentadimethicone" in the B1 phase were adjusted to 8%, and the remainder was the same as in example 1.
Evaluation of Effect
90 subjects aged 45-55 were selected and equally divided into 9 groups of 10 subjects each, and the cream samples of examples 1-3 and comparative examples 1-9 were tested, respectively. The facial skin of these subjects had varying degrees of fine lines and had poor skin elasticity. After the human subjects cleaned the facial skin with the same cleanser every day, 2g of the cream samples of examples 1 to 3 and comparative examples 1 to 9 were uniformly applied to the facial skin, and the results were counted for use for 7 days, 14 days, and 28 days, and are shown in Table 2 below.
Evaluation criteria: the tested person self-describes the use feeling and compares the skin texture map through a computer to identify the skin tightening and pulling effect.
The method is effective: the skin becomes compact, the elasticity is better than that before trial, and the fine lines are reduced.
Invalidation: no change in skin was observed before the experiment.
Table 2 usage effect recording table
As can be seen from the records in Table 2, the lifting tension cream provided by the embodiment of the invention has an effective rate of over 80% after being used for 28 days, and can enable skin to become full and compact, restore elasticity, lighten fine lines, and reduce effects to different degrees when the formula of the comparative example is changed. Moreover, the tested personnel evaluate the cream of the embodiment of the invention more highly, and the cream has good skin feel and is willing to be used for a long time. FIGS. 1-2 are diagrams showing the products of examples 1-2 of the present invention, showing that the cream of example 1 is soft, waxy and soft.
The above embodiments are only preferred embodiments of the present invention, and the scope of the present invention is not limited thereto, but any insubstantial changes and substitutions made by those skilled in the art on the basis of the present invention are intended to be within the scope of the present invention as claimed.

Claims (3)

1. A lift tightening cream characterized by comprising an a phase, a B phase, a C phase, a D phase, an E phase, an F phase and a G phase, in weight percent in the cream:
the phase a includes: water, the balance; humectant: 3-5% of glycerol, 2-5% of butanediol and 0.01-0.05% of sodium hyaluronate; and (3) a thickening agent: 0.1 to 0.5 percent of carbomer, 0.05 to 0.15 percent of sodium polyacrylate grafted starch and 0.05 to 0.15 percent of xanthan gum; allantoin as skin conditioner 0.1-0.3%;
the B phase comprises a B1 phase and a B2 phase;
the B1 phase comprises: emulsifying agent: lauryl PEG-10 tris (trissilyloxy) silylethyl polydimethylsiloxane 0.1-0.5%, PEG-20 methyl glucose sesquistearate 0.8-1.5%, and a combination of glyceryl stearate and PEG-100 stearate 0.5-1.5%; and (3) a thickening agent: 0.5-1.2% of cetostearyl alcohol and 1-3% of behenyl alcohol; cleaning agent: 2-5% of a combination of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; an emollient: 1-3% of simethicone, 0.5-2% of C12-15 alcohol benzoate, 2-6% of isohexadecane, 0.3-0.6% of a composition of polydimethylsiloxane and dimethiconol, 1-5% of a composition of cyclohexasiloxane and cyclopenta-dimethicone, and 0.5-1.5% of octyl-polymethylsiloxane; filler: 5-15% of a composition of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filler: 0.5 to 1.5 percent of a composition of mica, titanium dioxide and triethoxy octyl silane, 0.5 to 1.2 percent of a composition of mica and titanium dioxide, and 0.05 to 0.15 percent of a composition of bismuth oxychloride and ethylhexyl hydroxystearate;
the C phase comprises a C1 phase, a C2 phase and a C3 phase;
the C1 phase includes: stabilizing agent: 0.8-1.2% of a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: an emollient: 0.8-1.5% of a composition of cyclohexasiloxane and cyclopentadimethicone, filler: 0.8 to 1.5 percent of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: aminomethylpropanol 0.15-0.5%, solvent: 0.5-2% of water;
the D phase comprises: antioxidant: 0.3-0.6% of p-hydroxyacetophenone, humectant: 1-5% of butanediol and 0.1-0.6% of 1, 2-hexanediol;
the E phase comprises: humectant: trimethylpentanediol/adipic acid/glycerin crosslinked polymer 0.5-2%, skin conditioner: lactobacillus/soy milk fermentation product filtrate, 0.5-2% of a combination of butanediol and 1, 2-pentanediol, 0.1-0.8% of a combination of hydroxypropyl tetrahydropyran triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.05-1.5% of a combination of butanediol and hexapeptide-9, and 0.005-0.015% of arginine/lysine polypeptide;
the F phase comprises 0.02-0.06% of aromatic;
the G phase comprises 0.001-0.006% colorant.
2. The lift-tensioning cream of claim 1, comprising a phase a, B, C, D, E, F and G phases, in weight percent in the cream:
the phase a includes: water, the balance; humectant: 4% of glycerol, 3% of butanediol and 0.03% of sodium hyaluronate; and (3) a thickening agent: 0.3% of carbomer, 0.08% of sodium polyacrylate grafted starch and 0.05% of xanthan gum; 0.2% of allantoin as a skin conditioner;
the B phase comprises a B1 phase and a B2 phase;
the B1 phase comprises: emulsifying agent: lauryl PEG-10 tris (trissilyloxy) silylethyl polydimethylsiloxane 0.3%, PEG-20 methyl glucal sesquistearate 1.2%, a combination of glyceryl stearate and PEG-100 stearate 0.8%; and (3) a thickening agent: cetostearyl alcohol 0.8%, behenyl alcohol 2%; cleaning agent: 2.5% of a combination of lauric acid, myristic acid, palmitic acid, stearic acid and arachidic acid; an emollient: 2% of simethicone, 0.5% of C12-15 alcohol benzoate, 4% of isohexadecane, 0.5% of a combination of polydimethylsiloxane and dimethiconol, 2% of a combination of cyclohexasiloxane and cyclopentadimethicone, and 1% of octyl polymethylsiloxane; filler: 12% of a composition of polydimethylsiloxane and polysiloxane-11;
the B2 phase comprises: filler: 1% of a combination of mica, titanium dioxide and triethoxyoctylsilane, 0.8% of a combination of mica and titanium dioxide, and 0.08% of a combination of bismuth oxychloride and ethylhexyl hydroxystearate;
the C phase comprises a C1 phase, a C2 phase and a C3 phase;
the C1 phase includes: stabilizing agent: 1% of a combination of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80 and sorbitan oleate;
the C2 phase includes: an emollient: composition 1% of cyclohexasiloxane and cyclopentadimethicone, filler: 1% of polymethylsilsesquioxane;
the C3 phase includes: pH regulator: aminomethylpropanol 0.33%, solvent: 0.5-2% of water;
the D phase comprises: antioxidant: p-hydroxyacetophenone 0.5%, humectant: 2% of butanediol and 0.5% of 1, 2-hexanediol;
the E phase comprises: humectant: trimethylpentanediol/adipic acid/glycerin crosslinked polymer 1%, skin conditioning agent: lactobacillus/soy milk fermentation product filtrate, 0.5% of a combination of butanediol and 1, 2-pentanediol, 0.5% of a combination of hydroxypropyl tetrahydropyran triol, 1, 2-hexanediol and 1, 2-pentanediol, 0.1% of a combination of butanediol and hexapeptide-9, 0.01% of arginine/lysine polypeptide;
the F phase includes 0.04% fragrance;
the G phase included colorant 0.00429%.
3. A method of preparing a lift tightening cream as claimed in any one of claims 1 to 2, comprising the steps of:
adding the phase A raw material into an emulsifying pot, uniformly dispersing, stirring and heating to 85-88 ℃, homogenizing for 3-5 minutes until the raw material is completely and uniformly dissolved and has no particles;
adding the B1 phase raw material into an oil pan, stirring and heating to 80-85 ℃, and stirring for 3-5min;
adding the B2 phase raw material into the B1 phase, and uniformly stirring to form a B phase;
slowly pumping the phase B into an emulsifying pot under rapid stirring, and homogenizing and uniformly stirring;
adding the C1 phase raw material, uniformly stirring, and continuously homogenizing;
adding the uniformly dispersed C2 phase, and continuously homogenizing and uniformly stirring;
adding phase C3, stirring uniformly, preserving heat for 20 minutes, and stirring and cooling;
heating the phase D to 60-65 ℃ independently, stirring and dissolving until the phase D is completely transparent and has no particles, adding the phase D into the emulsifying pot when the temperature of the material in the emulsifying pot is reduced to 65 ℃, and stirring uniformly;
continuously stirring and cooling to below 45 ℃, sequentially adding the E phase, and uniformly stirring;
adding phase F, and stirring uniformly;
adding phase G for mixing, and stirring.
CN202210325912.0A 2022-03-30 2022-03-30 Lifting and tightening cream and preparation method thereof Active CN114632028B (en)

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WO2013076238A1 (en) * 2011-11-25 2013-05-30 L'oreal Composition comprising a superabsorbent polymer and a nonsuperabsorbent acrylic acid homopolymer or copolymer which is at least partially neutralized
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