CN110115691B - Whitening and skin-tendering emulsion containing rice fermentation product and preparation method thereof - Google Patents
Whitening and skin-tendering emulsion containing rice fermentation product and preparation method thereof Download PDFInfo
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- CN110115691B CN110115691B CN201910458979.XA CN201910458979A CN110115691B CN 110115691 B CN110115691 B CN 110115691B CN 201910458979 A CN201910458979 A CN 201910458979A CN 110115691 B CN110115691 B CN 110115691B
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a whitening and skin-tendering emulsion containing a rice fermentation product and a preparation method thereof, belonging to the technical field of daily cosmetics. The whitening and skin-tendering emulsion containing the rice fermentation product comprises a mixture of lactobacillus/rice fermentation product, maltitol and arginine, and the rice fermentation product is a natural component, so that the emulsion is easy to absorb and has no irritation, can obviously moisten skin after being used, and has obvious whitening and skin-tendering effects; in addition, the whitening and skin-tendering emulsion also contains yeast peptide, saussurea involucrate fermentation liquor and rice fermentation product filtrate which are all natural components, is safe and non-irritant, and has good nourishing effect; the invention also provides a method for preparing the mask paste, wherein the mass ratio of the lactobacillus/rice fermentation product, the mixture of maltitol and arginine and the rice fermentation product filtrate is controlled to be 0.1-2: 1, the prepared emulsion has better water locking effect, thereby enabling the skin to be rich in elasticity.
Description
Technical Field
The invention belongs to the technical field of daily cosmetics, and relates to a whitening and skin-tendering emulsion containing a rice fermentation product and a preparation method thereof.
Background
In modern society, people have more and more communications, and people who have beautiful skin want to have the skin, especially women are important. Therefore, the skin care is accompanied with people at any time, and becomes an indispensable thing in daily life. With the aging, the skin function is degraded, the skin is inevitably in a small state, and the skin feels tired and loses moisture and oil due to factors such as ultraviolet irradiation, air pollution, body fatigue and the like, so that the water and oil are unbalanced, the skin is dry and rough, and the oil, the water and the nutrient which are necessary for the skin operation are lacked. When the skin lacks nourishment, a series of problems such as spots, wrinkles, dark yellow complexion, lackluster and the like are caused correspondingly.
The emulsion is the most important step of basic skin care, and effective components in the emulsion, such as moisture retention, whitening, aging resistance and the like, can be better absorbed by the skin, so that the emulsion with a bottle is very important. However, most of the emulsions appearing in the market contain a large amount of chemical substances, and as is well known, many chemical substances have certain toxicity to human beings, and can generate certain side effects on the skin after long-term use, so that the ideal skin care effect cannot be obtained.
Skin care emulsions and methods of preparation have been widely reported in the prior art. For example, chinese patent application 201510713075.9 discloses a nourishing skin care lotion, which comprises the following components by mass percent: 0.0001-0.001% of cell growth factor, 0.5-5% of bearberry leaf extract, 1-5% of glycyrrhetinic acid, 0.1-0.5% of allantoin, 2-5% of horse oil, 5-10% of propylheptyl caprylate, 2-6% of glycosaminoglycans, 6-15% of alcohols, 1-3% of carbomer, 4-6% of diethylhexyl carbonate, 1-5% of surfactant, 0.01-1% of preservative, 0.01-5% of pH regulator and the balance of water; the cell growth factor, the bearberry leaf extract and the glycyrrhetinic acid are reasonably compatible, and cooperatively play a role in moistening skin, enhancing skin elasticity, reducing pigmentation and promoting cell repair and regeneration, so that the purpose of nourishing and rejuvenating skin is achieved; the invention also provides a preparation method of the skin-nourishing cream, so that the activity of effective components in the formula is effectively protected, and the skin-nourishing cream has a more obvious effect, but the problem of improving the skin elasticity is not concerned in the invention.
For another example, chinese patent application 201610209367.3 discloses a blue lotus moisturizing skin care emulsion, which is mainly prepared from the following raw materials in parts by weight: 2-5 parts of shea butter, 5-10 parts of jojoba oil, 2-7 parts of squalane, 1-5 parts of natural emulsifying wax, 8-12 parts of humectant, 50-70 parts of blue lotus hydrolat and 3-15 parts of plant extract. The invention also discloses a preparation method of the blue lotus flower moisturizing and skin-care emulsion. The product is natural, mild and non-irritant, can be used for moisturizing the skin for a long time, has good moisturizing effects on dry skin, sensitive skin and the like, and has the effects of whitening, tendering and whitening the skin. The natural emulsifying wax is added in a certain amount, so that the greasy feeling of the emulsion is easily increased, and the freshness of the emulsion is reduced.
Therefore, it is necessary to develop an emulsion which can effectively whiten and tender skin, make skin have better elasticity and effectively lock water.
Disclosure of Invention
In order to solve the problems and the defects in the prior art, the invention aims to provide the emulsion which can effectively lock water, whiten and tender the skin and enable the skin to be elastic.
One of the technical schemes adopted by the invention for solving the technical problems is as follows: the whitening and skin-tendering emulsion containing the rice fermentation product comprises the following components in percentage by weight: 0.1-2% of mixture of cetearyl olive oleate and sorbitan olive oleate, 0.1-2% of mixture of lactobacillus/rice fermentation product, maltitol and arginine, 0.1-2% of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1-3% of saussurea involucrate fermentation liquor, 1-5% of yeast peptide, 1-5% of rice fermentation product filtrate and the balance of water.
Preferably, the whitening and skin-tendering emulsion comprises the following components in percentage by weight: 0.5-1.5% of mixture of cetearyl olive oleate and sorbitan olive oleate, 0.5-1.5% of mixture of lactobacillus/rice fermentation product, maltitol and arginine, 0.5-1.5% of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1.5-2.5% of saussurea involucrate fermentation liquid, 2-4% of yeast peptide, 2-4% of rice fermentation product filtrate and the balance of water.
The whitening and skin-tendering emulsion also comprises the following components in percentage by weight: 3-10% of butanediol, 2-6% of trehalose, 2-5% of phytosterol/octyldodecanol lauroyl glutamate, 2-5% of betaine, 1-5% of covered yeast fermentation product filtrate, 1-5% of tranexamic acid, 1-3% of nicotinamide, 1-3% of C13-16 isoparaffin, 1-3% of pentaerythritol tetra (ethyl hexanoate), 1-3% of polydimethylsiloxane, 101-3% of methyl glucitol polyether, 0.1-2% of cholesterol hydroxystearate, 0.1-2% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 0.1-2% of 1, 2-pentanediol, 0.1-2% of tocopherol acetate, 0.1-2% of behenyl alcohol, 0.1-2% of medicinal rhubarb (RheuofFicinALE) extract, 0.1-2% of nano-encapsulated ceramide, 0.1-2% of preservative, 0.1-2% of hydrogenated lecithin, 60.1-1% of polyacrylate cross-linked polymer, 0.1-1% of carnosine, 0.01-0.2% of xanthan gum, 0.01-0.2% of carboxymethyl chitosan, 0.01-0.2% of beta-glucan, 0.01-0.2% of sodium hyaluronate, 0.01-0.2% of TREMELLA (Tremella ciformis) fruiting body extract, 0.01-0.2% of disodium EDTA, 0.01-0.2% of sodium polyglutamate and 0.01-0.2% of essence.
Preferably, the whitening and skin-tendering emulsion further comprises the following components in percentage by weight: 5-8% of butanediol, 3-5% of trehalose, 3-5% of phytosterol/octyldodecanol lauroyl glutamate, 3-5% of betaine, 2-4% of covered yeast fermentation product filtrate, 2-4% of tranexamic acid, 1.5-2.5% of nicotinamide, 1.5-2.5% of C13-16 isoparaffin, 1.5-2.5% of pentaerythritol tetra (ethyl hexanoate), 1.5-2.5% of polydimethylsiloxane, 101.5-2.5% of methyl glucitol polyether, 0.5-1.5% of cholesteryl hydroxystearate, 0.5-1.5% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 0.5-1.5% of 1, 2-pentanediol, 0.5-1.5% of tocopherol acetate, 0.5-1.5% of behenyl alcohol, 0.5-1.5% of medicinal rhubarb (EURHM OFFICINALE) extract, 0.5-1.5% of nano-encapsulated ceramide, 0.5-1.5% of preservative, 0.5-1.5% of hydrogenated lecithin, 60.5-0.8% of polyacrylate cross-linked polymer, 0.5-0.8% of carnosine, 0.05-0.15% of xanthan gum, 0.05-0.15% of carboxymethyl chitosan, 0.05-0.15% of beta-glucan, 0.05-0.15% of sodium hyaluronate, 0.05-0.15% of TREMELLA (Tremella FUCIFORMIS) fruiting body extract, 0.05-0.15% of EDTA disodium, 0.05-0.15% of sodium polyglutamate and 0.05-0.15% of essence.
Preferably, the whitening and skin-tendering emulsion containing the rice fermentation product comprises the following components in percentage by weight: 6-7% of butanediol, 4-5% of trehalose, 4-5% of phytosterol/octyldodecanol lauroyl glutamate, 4-5% of betaine, 3-4% of yeast peptide, 3-4% of rice fermentation product filtrate, 3-4% of tectorial membrane yeast fermentation product filtrate, 3-4% of tranexamic acid, 2-2.5% of snow lotus fermentation broth, 2-2.5% of nicotinamide, 2-2.5% of C13-16 isoparaffin, 2-2.5% of pentaerythritol tetra (ethyl hexanoate), 2-2.5% of polydimethylsiloxane, 102-2.5% of methyl glucitol polyether, 1-1.5% of cholesterol hydroxystearate, 1-1.5% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 1-1.5% of 1, 2-pentanediol, 1 to 1.5 percent of mixture of cetearyl olive oleate and sorbitan olive oleate, 1 to 1.5 percent of tocopherol acetate, 1 to 1.5 percent of behenyl alcohol, 1 to 1.5 percent of lactobacillus/rice fermentation product, 1 to 1.5 percent of mixture of maltitol and arginine, 1 to 1.5 percent of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1 to 1.5 percent of rhubarb (Rheum OFFICINALE) extract, 1 to 1.5 percent of nano-encapsulated ceramide, 1 to 1.5 percent of preservative, 1 to 1.5 percent of hydrogenated lecithin, 60.6 to 0.7 percent of polyacrylate cross-linked polymer, 0.6 to 0.7 percent of carnosine, 0.1 to 0.15 percent of xanthan gum, 0.1 to 0.15 percent of carboxymethyl chitosan, 0.1 to 0.15 percent of beta-glucan, 0.1 to 0.15 percent of sodium hyaluronate, 0.1 to 0.15 percent of Tremella (Tremella FUCIFORMIS) fruiting body extract, 0.1-0.15% of EDTA disodium, 0.1-0.15% of sodium polyglutamate, 0.1-0.15% of essence and the balance of water.
In a preferred embodiment, the mass ratio of the mixture of cetearyl olive oleate and sorbitan olive oleate to the mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6 is 1-10: 1;
still preferably, the mass ratio of the mixture of cetearyl olive oleate and sorbitan olive oleate to the mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6 is 3-6: 1.
in another preferred embodiment, the mass ratio of the lactobacillus/rice fermented product, the maltitol and arginine mixture to the rice fermented product filtrate is 0.1-2: 1;
still preferably, the mass ratio of the lactobacillus/rice fermentation product, the mixture of maltitol and arginine to the rice fermentation product filtrate is 0.5-1: 1.
the second technical scheme adopted by the invention for solving the technical problems is as follows: the invention also provides a preparation method of the whitening and skin-tendering emulsion containing the rice fermentation product, which comprises the following steps:
(1) adding butanediol, trehalose, betaine, tranexamic acid, nicotinamide, methyl gluceth-10, 1, 2-pentanediol, a mixture of cetearyl olive oleate and sorbitan olive oleate, a lactobacillus/rice fermentation product, a mixture of maltitol and arginine, hydrogenated lecithin, polyacrylate cross-linked polymer-6, xanthan gum, sodium hyaluronate, a TREMELLA (TREMELLA FUCIFORMIS) fruiting body extract, EDTA disodium and sodium polyglutamate into an emulsifying device according to formula dosage, stirring uniformly, heating and preserving heat to obtain a mixture A;
(2) adding phytosterol/octyldodecanol lauroyl glutamate, C13-16 isoparaffin, pentaerythritol tetra (ethyl hexanoate), polydimethylsiloxane, cholesteryl hydroxystearate, glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water into a dissolving device, heating to dissolve, uniformly stirring, and preserving heat to obtain a mixture B;
(3) adding the mixture B obtained in the step (2) into the mixture A, stirring and homogenizing for 5-10 minutes to obtain a mixture C, then adding the mixture of sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 with formula dosage into the mixture C, continuing homogenizing for 1-5 minutes, keeping the temperature, stirring, and cooling to obtain a mixture D;
(4) adding yeast peptide, rice fermentation product filtrate, membrane-covered yeast fermentation product filtrate, saussurea involucrate fermentation liquid, rhubarb (RHEUM OFFICINALE) extract, nano-encapsulated ceramide, carnosine, carboxymethyl chitosan, beta-glucan, preservative and essence according to the formula dosage after the mixture D is cooled, stirring for 10-30 minutes, and continuously cooling to obtain a mixture E;
(5) and cooling the mixture E, filtering and discharging to obtain a finished product of the whitening and skin-tendering emulsion containing the lactobacillus fermented rice product.
The temperature rise in the step (1) is 85-95 ℃, and the heat preservation and stirring time is 20-40 minutes.
The temperature rise in the step (2) is 80-90 ℃, and the heat preservation time is 5-15 minutes.
The heat preservation stirring time in the step (3) is 10-30 minutes.
The temperature reduction in the step (4) is to reduce the temperature to 40-45 ℃.
The temperature reduction in the step (5) is 35-40 ℃.
The preparation method of the whitening and skin-tendering emulsion containing the rice fermentation product specifically comprises the following steps:
(1) adding butanediol, trehalose, betaine, tranexamic acid, nicotinamide, methyl gluceth-10, 1, 2-pentanediol, a mixture of cetearyl olive oleate and sorbitan olive oleate, a lactobacillus/rice fermentation product, a mixture of maltitol and arginine, hydrogenated lecithin, polyacrylate cross-linked polymer-6, xanthan gum, sodium hyaluronate, a TREMELLA (TREMELLA FUCIFORMIS) fruiting body extract, EDTA disodium and sodium polyglutamate into an emulsifying device according to formula dosage, uniformly stirring, heating to 85-95 ℃, preserving heat and stirring for 20-40 minutes to obtain a mixture A;
(2) adding phytosterol/octyldodecanol lauroyl glutamate, C13-16 isoparaffin, pentaerythritol tetra (ethyl hexanoate), polydimethylsiloxane, cholesteryl hydroxystearate, glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water into a dissolving device, heating to 80-90 ℃, uniformly stirring after dissolving, and preserving heat for 5-15 minutes to obtain a mixture B;
(3) adding the mixture B obtained in the step (2) into the mixture A, stirring and homogenizing for 5-10 minutes to obtain a mixture C, then adding the mixture of sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 with the formula dosage into the mixture C, continuing homogenizing for 1-5 minutes, keeping the temperature and stirring for 10-30 minutes, and cooling to obtain a mixture D;
(4) adding yeast peptide, rice fermentation product filtrate, membrane-covered yeast fermentation product filtrate, herba Saussureae Involueratae fermentation liquid, radix et rhizoma Rhei Palmati (Rheum Officinale) extract, nanometer-coated ceramide, carnosine, carboxymethyl chitosan, beta-dextran, antiseptic and essence according to formula dosage when the temperature of the mixture D is reduced to 40-45 deg.C, stirring for 10-30 min, and continuously cooling to obtain mixture E;
(5) and (3) cooling the mixture E to 35-40 ℃, filtering and discharging to obtain a finished product of the whitening and skin-tendering emulsion containing the lactobacillus fermented rice product.
Compared with the prior art, the invention has the beneficial effects that:
(1) the skin care emulsion prepared by the invention contains rice fermentation products, is natural, easy to absorb, has no irritation, can obviously moisten skin after being used, and has obvious whitening and skin tendering effects;
(2) the emulsion prepared by the invention contains the yeast peptide, the saussurea involucrate fermentation liquor and the rice fermentation product filtrate which are all natural components, is safe and non-irritant, and has good nourishing effect;
(3) in the preparation process of the mask paste prepared by the invention, the mass ratio of the lactobacillus/rice fermentation product, the mixture of maltitol and arginine and the rice fermentation product filtrate is controlled to be 0.1-2: 1, the prepared emulsion has better water locking effect and makes skin elastic.
Detailed Description
The advantageous effects of the present invention are further described by the following examples, which are for illustrative purposes only and do not limit the scope of the present invention, and variations and modifications obvious to those skilled in the art according to the present invention are included in the scope of the present invention, and the following components are calculated in parts by weight unless otherwise specified. The butylene glycol mentioned in the examples below was purchased from OXEA, trehalose from Prolin Chemicals, under the trade name trehalose, phytosterol/octyldodecanol lauroyl glutamate from Japan monosodium glutamate, type ELDEW PS-203, betaine from Dupont, type BP-20, yeast peptide from Yazhi, type TIA, rice fermentation product filtrate from Chongyasu, type holoenzyme, tectorial yeast fermentation product filtrate from Saccharum sachalinensis, type tectorial yeast fermentation product filtrate from Saccharum sinensis, type tectorial yeast fermentation product filtrate, tranexamic acid from Hunan Dongting pharmacy, type tranexamic acid, saussurea involucrate fermentation broth from Saccharum sachalinensis, type FS002, nicotinamide from Disma, type Niacinamide PC, C13-16 isoparaffin from Japan, type X-Light I, pentaerythritol tetra (ethyl hexanoate) from Japan Nissian, SALACOS 5408, dimethicone from Dow Corning USA, model PMX-200, Methylgluceth-10 from Dow Corning USA, model GLUCAM E-10, Cholesterol hydroxystearate from Nippon, model SALACOS HS, Glycerol amide EtOH methacrylate/stearyl alcohol methacrylate copolymer from Nippon, model Ceracute L, 1, 2-pentanediol from Delaware Germany, model Sendiio PG, cetearyl Olive oleate and sorbitan Olive oleate mixture from Italy B & T, model Olive 1000, tocopheryl acetate from Pasteur Germany, trade name vitamin E acetate, netbehenyl alcohol from Pasteur Germany, model number Late 22, Lactobacillus/Rice fermentation product, maltitol and arginine mixture from Nonbao Japan, technolong rice supplement, sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 mixture from Lancefield, model G57, rhubarb for medicinal use (Rheum Officinale) extract from Chongqing essence, under the trade name Dahuang ferment, nano-encapsulated ceramide from Korea fighting mountain, model Hydroceramide5, preservative from Torrel, model MICROCARE PHDG, hydrogenated lecithin from Japan, model Lecinol s-10, polyacrylate crosspolymer-6 from Spirabeck, model Sepimax n, carnosine from Vickera, xanthan gum from SpiboKeldc, model Keldent, carboxymethyl chitosan from Shanghai dew, model MHA micro, beta-dextran from Bobonuo, sodium beta-dextran, hyaluronic acid from Lang 40 HA-20, tremella (Tremella FUCIFORMIS) fruiting body extract is obtained from Ningbo hinooya under the trade name Tremella polysaccharide, disodium EDTA is obtained from Acksonobel, sodium polyglutamate is obtained from Jun' an, Wuhan province under the trade name Poly-gamma-sodium glutamate.
The instrument homogenizer used in the following examples was purchased from IKA, germany, model T25; the stirrer was purchased from IKA, Germany, and the model number is RW 20; the electronic scale is purchased from a normal-maturing Shuangjie, and the model is 1000 g; the pH meter is purchased from Mettler & Toriduo Switzerland and is of the type FE 28; the constant temperature water bath kettle is purchased from Shanghai Bo Xuan with the model number of HHS-11-1; the water purifier is purchased from Qin Yuan Zhejiang and has the model of RO-1851; beaker was purchased from Sichuan glass 500 mL.
The olivem 1000 mentioned in the following examples is in a mass ratio of 60: 40 of cetearyl olive oleate and sorbitan olive oleate; technolong rice fermentation is a mixture of lactobacillus/rice fermentation product, maltitol and arginine in a mass ratio of 79.2:20: 0.8; g57 is a mixture of sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 with the mass ratio of 60:35: 5; the herba Saussureae Involueratae fermentation broth is a mixture of yeast fermentation filtrate and herba Saussureae Involueratae (SAUSSUREA INVOLUCRATA) extract at a mass ratio of 99: 1; the nano-encapsulated ceramide is a mixture of ceramide 3, water, caprylic/capric triglyceride, glycerol, ceteareth-20, polyglycerol-10 stearate and polysorbate-20 in a mass ratio of 5:40:3:25:15:10: 2; the preservative is a mixture of phenoxyethanol, decanediol and caprylyl glycol in a mass ratio of 92:4: 4.
Examples 1 to 5A whitening and skin-tendering emulsion containing a rice fermentation product and a method for preparing the same
The preparation method comprises the following steps: the method specifically comprises the following steps:
(1) adding butanediol, trehalose, betaine, tranexamic acid, nicotinamide, methyl glucitol polyether-10, 1, 2-pentanediol, a mixture of cetearyl olive oleate and sorbitan olive oleate, a lactobacillus/rice fermentation product, a mixture of maltitol and arginine, hydrogenated lecithin, polyacrylate cross-linked polymer-6, xanthan gum, sodium hyaluronate, a TREMELLA (TREMELLA FUCIFORMIS) fruiting body extract, EDTA disodium and sodium polyglutamate into an emulsifying pot according to formula dosage, uniformly stirring, heating to 90 ℃, preserving heat and stirring for 30 minutes to obtain a mixture A;
(2) adding phytosterol/octyldodecanol lauroyl glutamate, C13-16 isoparaffin, pentaerythritol tetra (ethyl hexanoate), polydimethylsiloxane, cholesteryl hydroxystearate, glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water into an oil phase pot according to formula dosage, heating to 85 ℃ to dissolve, uniformly stirring, and keeping the temperature for 10 minutes to obtain a mixture B;
(3) adding the mixture B obtained in the step (2) into the mixture A, stirring and homogenizing for 6 minutes to obtain a mixture C, then adding the mixture of sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 with the formula dosage into the mixture C, continuing homogenizing for 5 minutes, keeping the temperature and stirring for 20 minutes, and cooling to obtain a mixture D;
(4) adding the formula dosage of yeast peptide, rice fermentation product filtrate, membrane covering yeast fermentation product filtrate, snow lotus fermentation liquor, rhubarb (RHEUM OFFICINALE) extract, nano-encapsulated ceramide, carnosine, carboxymethyl chitosan, beta-glucan, preservative and essence when the temperature of the mixture D is reduced to 45 ℃, stirring for 20 minutes, and continuously cooling to obtain a mixture E;
(5) and (3) cooling the mixture E to 38 ℃, filtering and discharging to obtain a finished product of the whitening and skin-tendering emulsion containing the lactobacillus fermented rice product.
Control group 1-5 whitening and skin-tendering emulsion containing rice fermentation product and preparation method thereof
Control 1 differs from example 1 in that: control 1 had no added olivem 1000 and G57.
Control 2 differs from example 1 in that: the mass ratio of olivem 1000 and G57 in control group 2 was 0.5: 1, i.e. 0.5% for olivem 1000 and 1% for G57.
Control 3 differs from example 1 in that: the mass ratio of olivem 1000 and G57 in control group 3 was 14: 1, i.e. 1.4% for olivem 1000 and 0.1% for G57.
Control 4 differs from example 1 in that: the control group 4 is not added with the rice fermentation product filtrate, the snow lotus fermentation liquor and the yeast peptide;
control 5 differs from example 1 in that: control 5 had no Technolong rice comment added.
Control 6 differs from example 1 in that: the mass ratio of Technolong rice conversion to rice fermentation product filtrate in the control group 6 was 0.2: 1, namely the percentage content of the Technolong rice conversion is 0.42 percent, and the percentage content of the rice fermentation product filtrate is 2.08 percent.
Control 7 differs from example 1 in that: the mass ratio of the Technolong rice conversion to the rice fermentation product filtrate in the control group 7 was 5:1, namely the percentage content of the Technolong rice conversion is 2.08 percent, and the percentage content of the rice fermentation product filtrate is 0.42 percent.
And (3) test evaluation:
1. test of whitening and freckle-removing effects
(1) Experimental population
240 female volunteers of 20-50 years old are selected and randomly and evenly divided into 12 groups of 20.
(2) Laboratory apparatus
German CK multi-probe skin test system MPA9, melanin and heme test probe (Mexamter MX 18).
(3) Experimental methods
After cleaning face, the product is applied on face until absorption, and no cleaning is needed; used 3 times per week for 4 weeks; before testing, the test subjects cleaned their faces with clear water, wiped clean with facial tissue, and started to measure after sitting still in a constant temperature and humidity laboratory (temperature 20. + -. 1 ℃ C., humidity 55. + -. 3) for 30 minutes. A4 x 4cm area in the middle of the right face of each human subject was selected and the average melanin content was measured by a probe at the four corners and in the middle for a total of 5 locations in the area. Then respectively testing the average melanin content of each group of people according to the method when trying the whitening and skin-tendering emulsion for 3 rd, 6 th, 9 th and 12 th times.
(4) Evaluation method
The skin melanin content is tested by an instrument, and the content is reduced to indicate effectiveness, and the content is increased or unchanged to indicate ineffectiveness.
(5) Results of the experiment
The results for melanin content are shown in Table 1
TABLE 1 results comparing the effects of examples 1-5 with those of control 1-7
According to the detection data in the table 1, it can be seen that the emulsions prepared in the embodiments of the present invention and the control group have the effects of whitening skin and removing spots, and can reduce melanin of skin. However, the skin melanin is reduced more obviously after the emulsion prepared in the example is used, so that the whitening and freckle removing effects of the emulsion prepared in the example are obvious.
2. Water lock effect detection
(1) Experimental population
240 female volunteers of 20-50 years old are selected and randomly and evenly divided into 12 groups of 20.
(2) Laboratory apparatus
The transdermal water loss rate (g/h/m) was calculated by measuring the difference in the water vapor pressure gradient with the Tewameter TM3002) Skin barrierThe more intact, the lower the TEWL value, the better the skin's ability to lock water.
(3) Experimental methods
After cleaning face, the product is applied on face until absorption, and no cleaning is needed; used 3 times per week for 4 weeks; before testing, the test subjects cleaned their faces with clear water, wiped clean with facial tissue, and started to measure after sitting still in a constant temperature and humidity laboratory (temperature 20. + -. 1 ℃ C., humidity 55. + -. 3) for 30 minutes. A4 x 4cm area in the middle of the right face of each human subject is selected, and the average capacitance values of the four corners and the middle of the area are tested by a probe for 5 positions in total. Then, the average capacitance value of each group of people is respectively tested according to the method on the 7 th, 14 th, 21 th and 28 th days after the whitening and skin-tendering emulsion is tried out.
(4) Evaluation method
The lower the TEWL value, the better the skin's ability to lock water.
(5) Results of the experiment
The water locking effect is shown in Table 2
TABLE 2 comparison of the effects of the products of examples 1-5 with those of the controls 1-7
3. Skin elasticity detection
(1) Experimental population
240 female volunteers of 20-50 years old are selected and randomly and evenly divided into 12 groups of 20.
(2) Laboratory apparatus
Cutomer dual MPA580 host, Germany CK company, skin elasticity probe PVM 600;
the test principle is as follows: based on the principle of suction and stretching, a negative pressure is generated on the skin, which is sucked into a specific probe, and the suction depth is measured by an optical test system. The probe contains a transmitter and a receiver of light, the ratio of which (the ratio of the transmitted light to the received light) is proportional to the depth of inhalation, thus obtaining a curve of the length of the skin stretched versus time, which is then analyzed by the MPA software to determine the elastic properties of the skin.
(3) Experimental methods
After cleaning face, the product is applied on face until absorption, and no cleaning is needed; used 3 times per week for 4 weeks; before testing, the test subjects cleaned their faces with clear water, wiped clean with facial tissue, and started to measure after sitting still in a constant temperature and humidity laboratory (temperature 20. + -. 1 ℃ C., humidity 55. + -. 3) for 30 minutes. A4 x 4cm area in the middle of the right face of each human subject was selected and the average spring force was measured at the upper, middle and lower 3 positions of the area using a probe. Then, when the whitening and skin-tendering emulsion is tried for 3 rd, 6 th, 9 th and 12 th times, the average elasticity value of each group of people is tested according to the method. Setting parameters: negative pressure is-450 mbar; the negative pressure time is-2 s.
(4) Evaluation method
R2 is Ua/Uf, and the ratio of the amount of springback of the skin (Ua) in the absence of negative pressure to the maximum amount of stretch (Uf) in the presence of negative pressure, the closer the R2 data is to 1, the better the skin elasticity.
(5) Results of the experiment
The skin elasticity effect is shown in Table 3
TABLE 3 comparison of the effects of the products of examples 1-5 with those of the controls 1-7
As can be seen from the test data in Table 3 above, the emulsions prepared in the examples of the present invention and the control group have the effect of improving the elasticity. However, the skin elasticity of the emulsion prepared in the example is improved more obviously after the emulsion is used, and when one or more ingredients in the ingredients are reduced, the using effect of the emulsion is obviously influenced, so that the skin elasticity increasing effect is reduced, and therefore, the skin elasticity improving effect of the emulsion prepared in the example is obvious.
The above detailed description is specific to possible embodiments of the present invention, and the embodiments are not intended to limit the scope of the present invention, and all equivalent implementations or modifications that do not depart from the scope of the present invention should be included within the technical scope of the present invention.
Claims (7)
1. A whitening and skin-tendering emulsion containing rice fermentation products is characterized in that: the whitening and skin-tendering emulsion comprises the following components in percentage by weight: 0.1-2% of mixture of cetearyl olive oleate and sorbitan olive oleate, 0.1-2% of mixture of lactobacillus/rice fermentation product, maltitol and arginine, 0.1-2% of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1-3% of saussurea involucrate fermentation liquor, 1-5% of yeast peptide, 1-5% of rice fermentation product filtrate and the balance of water;
the mass ratio of the lactobacillus/rice fermentation product, the mixture of the maltitol and the arginine to the rice fermentation product filtrate is 0.5-2: 1;
the mass ratio of the components in the mixture of the lactobacillus/rice fermentation product, the maltitol and the arginine is 79.2:20: 0.8;
the whitening and skin-tendering emulsion further comprises the following components in percentage by weight: 3-10% of butanediol, 2-6% of trehalose, 2-5% of phytosterol/octyldodecanol lauroyl glutamate, 2-5% of betaine, 1-5% of tectorial membrane yeast fermentation product filtrate, 1-5% of tranexamic acid, 1-3% of nicotinamide, 1-3% of C13-16 isoparaffin, 1-3% of pentaerythritol tetra (ethyl hexanoate), 1-3% of polydimethylsiloxane, 101-3% of methyl glucitol polyether, 0.1-2% of cholesterol hydroxystearate, 0.1-2% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 0.1-2% of 1, 2-pentanediol, 0.1-2% of tocopherol acetate, 0.1-2% of behenyl alcohol, 0.1-2% of medicinal rhubarb extract, 0.1-2% of nano-encapsulated ceramide, 0.1-2% of preservative, 0.1-2% of hydrogenated lecithin, 60.1-1% of polyacrylate cross-linked polymer, 0.1-1% of carnosine, 0.01-0.2% of xanthan gum, 0.01-0.2% of carboxymethyl chitosan, 0.01-0.2% of beta-glucan, 0.01-0.2% of sodium hyaluronate, 0.01-0.2% of tremella entity extract, 0.01-0.2% of disodium EDTA, 0.01-0.2% of sodium polyglutamate and 0.01-0.2% of essence.
2. The whitening and skin-tendering emulsion containing rice fermentation product according to claim 1, characterized in that: the whitening and skin-tendering emulsion comprises the following components in percentage by weight: 0.5-1.5% of mixture of cetearyl olive oleate and sorbitan olive oleate, 0.5-1.5% of mixture of lactobacillus/rice fermentation product, maltitol and arginine, 0.5-1.5% of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1.5-2.5% of saussurea involucrate fermentation liquid, 2-4% of yeast peptide, 2-4% of rice fermentation product filtrate and the balance of water;
the whitening and skin-tendering emulsion further comprises the following components in percentage by weight: 5-8% of butanediol, 3-5% of trehalose, 3-5% of phytosterol/octyldodecanol lauroyl glutamate, 3-5% of betaine, 2-4% of tectorial membrane yeast fermentation product filtrate, 2-4% of tranexamic acid, 1.5-2.5% of nicotinamide, 1.5-2.5% of C13-16 isoparaffin, 1.5-2.5% of pentaerythritol tetra (ethyl hexanoate), 1.5-2.5% of polydimethylsiloxane, 101.5-2.5% of methyl glucitol polyether, 0.5-1.5% of cholesterol hydroxystearate, 0.5-1.5% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 0.5-1.5% of 1, 2-pentanediol, 0.5-1.5% of tocopherol acetate, 0.5-1.5% of behenyl alcohol, 0.5-1.5% of medicinal rhubarb extract, 0.5 to 1.5 percent of nano-encapsulated ceramide, 0.5 to 1.5 percent of preservative, 0.5 to 1.5 percent of hydrogenated lecithin, 60.5 to 0.8 percent of polyacrylate cross-linked polymer, 0.5 to 0.8 percent of carnosine, 0.05 to 0.15 percent of xanthan gum, 0.05 to 0.15 percent of carboxymethyl chitosan, 0.05 to 0.15 percent of beta-glucan, 0.05 to 0.15 percent of sodium hyaluronate, 0.05 to 0.15 percent of tremella entity extract, 0.05 to 0.15 percent of EDTA disodium, 0.05 to 0.15 percent of sodium polyglutamate and 0.05 to 0.15 percent of essence.
3. The whitening and skin-tendering emulsion containing rice fermentation product according to claim 2, characterized in that: the whitening and skin-tendering emulsion containing the rice fermentation product comprises the following components in percentage by weight: 6-7% of butanediol, 4-5% of trehalose, 4-5% of phytosterol/octyldodecanol lauroyl glutamate, 4-5% of betaine, 3-4% of yeast peptide, 3-4% of rice fermentation product filtrate, 3-4% of tectorial membrane yeast fermentation product filtrate, 3-4% of tranexamic acid, 2-2.5% of snow lotus fermentation broth, 2-2.5% of nicotinamide, 2-2.5% of C13-16 isoparaffin, 2-2.5% of pentaerythritol tetra (ethyl hexanoate), 2-2.5% of polydimethylsiloxane, 102-2.5% of methyl glucitol polyether, 1-1.5% of cholesterol hydroxystearate, 1-1.5% of glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, 1-1.5% of 1, 2-pentanediol, 1 to 1.5 percent of mixture of cetearyl alcohol olive oleate and sorbitan olive oleate, 1 to 1.5 percent of tocopherol acetate, 1 to 1.5 percent of behenyl alcohol, 1 to 1.5 percent of lactobacillus/rice fermentation product, 1 to 1.5 percent of mixture of maltitol and arginine, 1 to 1.5 percent of mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6, 1 to 1.5 percent of medicinal rhubarb extract, 1 to 1.5 percent of nano-encapsulated ceramide, 1 to 1.5 percent of preservative, 1 to 1.5 percent of hydrogenated lecithin, 60.6 to 0.7 percent of polyacrylate cross-linked polymer, 0.6 to 0.7 percent of carnosine, 0.1 to 0.15 percent of xanthan gum, 0.1 to 0.15 percent of carboxymethyl chitosan, 0.1 to 0.15 percent of beta-glucan, 0.1 to 0.15 percent of sodium hyaluronate, 0.1 to 0.15 percent of tremella entity extract, 0.1 to 0.15 percent of EDTA disodium, 0.1 to 0.15 percent of sodium polyglutamate and 0.1 to 0.15 percent of essence.
4. The whitening and skin-tendering emulsion containing rice fermentation product according to claim 1, characterized in that: the mass ratio of the mixture of cetearyl olive oleate and sorbitan olive oleate to the mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6 is 1-10: 1.
5. the whitening and skin-tendering emulsion containing rice fermentation product according to claim 4, characterized in that: the mass ratio of the mixture of cetearyl olive oleate and sorbitan olive oleate to the mixture of sodium polyacrylate, C18-21 alkane and isodecyl polyether-6 is 3-6: 1.
6. the whitening and skin-tendering emulsion containing rice fermentation product according to claim 1, characterized in that: the mass ratio of the lactobacillus/rice fermentation product, the mixture of the maltitol and the arginine to the rice fermentation product filtrate is 1-2: 1.
7. a method for preparing a whitening and skin-tendering emulsion containing rice fermentation products according to any one of claims 1 to 6, which is characterized by comprising the following steps: the method comprises the following steps:
(1) adding butanediol, trehalose, betaine, tranexamic acid, nicotinamide, methyl gluceth-10, 1, 2-pentanediol, a mixture of cetearyl olive oleate and sorbitan olive oleate, a lactobacillus/rice fermentation product, a mixture of maltitol and arginine, hydrogenated lecithin, polyacrylate cross-linked polymer-6, xanthan gum, sodium hyaluronate, tremella entity extract, disodium EDTA and sodium polyglutamate into an emulsifying device according to formula dosage, stirring uniformly, heating and preserving heat to obtain a mixture A;
(2) adding phytosterol/octyldodecanol lauroyl glutamate, C13-16 isoparaffin, pentaerythritol tetra (ethyl hexanoate), polydimethylsiloxane, cholesteryl hydroxystearate, glyceramide ethanol methacrylate/stearyl alcohol methacrylate copolymer, tocopherol acetate, behenyl alcohol and water into a dissolving device, heating to dissolve, uniformly stirring, and preserving heat to obtain a mixture B;
(3) adding the mixture B obtained in the step (2) into the mixture A, stirring and homogenizing to obtain a mixture C, then adding a mixture of sodium polyacrylate, C18-21 alkane and isodecyl alcohol polyether-6 with a formula dosage into the mixture C, continuing homogenizing, keeping the temperature, stirring, and cooling to obtain a mixture D;
(4) adding the yeast peptide, the rice fermentation product filtrate, the membrane-covered yeast fermentation product filtrate, the snow lotus fermentation liquid, the medicinal rhubarb extract, the nano-encapsulated ceramide, the carnosine, the carboxymethyl chitosan, the beta-glucan, the preservative and the essence according to the formula dosage after the mixture D is cooled, stirring, and continuously cooling to obtain a mixture E;
(5) and after the mixture E is cooled, filtering and discharging to obtain a finished product of the whitening and skin-tendering emulsion containing the lactobacillus fermented rice product.
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