CN110638685A - Edible lipstick and preparation method thereof - Google Patents
Edible lipstick and preparation method thereof Download PDFInfo
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- CN110638685A CN110638685A CN201910930868.4A CN201910930868A CN110638685A CN 110638685 A CN110638685 A CN 110638685A CN 201910930868 A CN201910930868 A CN 201910930868A CN 110638685 A CN110638685 A CN 110638685A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention relates to the field of cosmetic manufacturing, in particular to an edible lipstick and a manufacturing method thereof, wherein the edible lipstick comprises the following raw materials in parts by weight: 14-26 parts of natural vegetable oil, 4-6 parts of natural farmhouse beewax, 1.5-2 parts of plant natural pigment, 1-2 parts of Chinese date extract, 0.1-0.5 part of vitamin E, 0.05-0.3 part of vitamin B and 0.5-1 part of vitamin C. The lipstick prepared by the invention is safe to use, does not contain toxic and harmful substances, can be eaten, and has a nourishing effect on lips.
Description
Technical Field
The invention relates to the field of cosmetic manufacturing, in particular to an edible lipstick and a manufacturing method thereof.
Background
At present, the lipstick generally existing in the market mainly comprises base raw materials such as oil, wax, softener and the like, and auxiliary materials such as pigment, surfactant, spice and the like. The composition ratio is 20-25% of wax, 65-70% of oil and grease, and less than 15% of pigment, pigment and surfactant. However, the commercially available lipsticks still have certain problems, such as using inferior raw materials containing heavy metals such as lead as coloring agents, using lanolin with complex ingredients as main oil raw materials, using synthetic waxes of unnatural ingredients such as ozokerite, spermaceti, microcrystalline wax and liquid paraffin, adding synthetic essences to adjust the odor, and even adding industrial pigments to perform color matching. Few lipsticks can really achieve the food grade.
Disclosure of Invention
In view of the above, the invention provides an edible lipstick and a preparation method thereof, and the specific technical scheme is as follows:
the edible lipstick comprises the following raw materials in parts by weight:
14-26 parts of natural vegetable oil, 4-6 parts of natural farmhouse beewax, 1.5-2 parts of plant natural pigment, 1-2 parts of Chinese date extract, 0.1-0.5 part of vitamin E, 0.05-0.3 part of vitamin B and 0.5-1 part of vitamin C. Because the absolute ethyl alcohol is both a water-soluble solvent and a fat-soluble solvent, the absolute ethyl alcohol is adopted to carry out continuous reflux extraction on the Chinese dates, the effective components in the Chinese dates are extracted, and the extract is used as one of raw materials for preparing the lipstick so as to improve the anti-oxidation function of the lipstick.
Preferably, the natural vegetable oil is obtained by supercritical extraction, and the supercritical extraction can be performed at room temperature (35-40 ℃) and CO2The gas is extracted under a cover, so that the oxidation and the dissipation of the natural plant oil are effectively prevented, therefore, the effective components of the natural plants are kept in the extract, and the substances with high boiling point, low volatility and easy pyrolysis can be extracted at the temperature far lower than the boiling point of the substances; because no organic solvent is used in the whole process, the extract has no residual solvent substances, thereby preventing the existence of harmful substances to human bodies and the pollution to the environment in the extraction process and ensuring the pure naturalness of 100 percent.
Preferably, the natural vegetable oil comprises 3-5 parts of calamus margaritae oil, 2-4 parts of almond oil, 4-6 parts of olive oil, 3-4 parts of pomegranate seed oil and 2-7 parts of aloe oil.
Preferably, the plant natural pigment is derived from one or more of plant extracts with darker colors such as carrot, dragon fruit, spinach and tomato.
Preferably, the edible lipstick comprises the following raw materials in parts by weight: 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.12 parts of natural farmhouse beewax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
Preferably, the edible lipstick further comprises tea polyphenol, and the added tea polyphenol can block ultraviolet rays, remove free radicals induced by the ultraviolet rays, inhibit lipoxygenase and lipid peroxidation in skin mitochondria, and play roles in effectively preserving, inhibiting bacteria and resisting aging. In addition, the tea polyphenol can promote the absorption of human body to vitamin C, reduce the occurrence of lip skin anaphylactic reaction and enhance the immunity.
Preferably, the edible lipstick comprises the following raw materials in parts by weight: 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.1 parts of natural farmhouse beeswax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
Preferably, the edible lipstick further comprises one or more of coconut oil, jojoba oil and avocado oil.
In addition, lanolin has a complex composition, and is liable to cause allergic reactions such as cracking and peeling of lip mucous membrane, and sometimes itching or slight pain of lips. And because lanolin has strong adsorbability, dust, bacteria, viruses and some heavy metal ions in the air can be adsorbed on lip mucosa, and when people drink water and eat things, lipstick and the substances harmful to health on the lipstick are inevitably brought into the mouth, so that the lipstick enters the body. Therefore, lanolin is not used in the lipstick raw material of the present invention.
The preparation method of the edible lipstick comprises the following steps:
s1, uniformly mixing the natural vegetable oil and the natural plant pigment, and stirring for 5-10 minutes to obtain a mixture, wherein the stirring temperature is 40-70 ℃, and the stirring speed is 1000-2000 r/min;
s2, adding natural farmyard beewax into the mixture, heating in a water bath, stirring until the natural farmyard beewax and the mixture are completely melted, and adding the Chinese date extract, the vitamin E, the vitamin B and the vitamin C to obtain liquid lipstick;
s3, cooling and forming the liquid lipstick at the temperature below room temperature to obtain the edible lipstick.
Preferably, the preparation method of the edible lipstick comprises the following steps:
s1, uniformly mixing 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil and 1.9 parts of plant natural pigment, and stirring for 8 minutes to obtain a mixture, wherein the stirring temperature is 55 ℃, and the stirring speed is 1400 r/min;
s2, adding 6.12 parts of natural farmhouse beewax into the mixture, heating in a water bath at 70 ℃, stirring until the natural farmhouse beewax and the mixture are completely melted, and adding 1.5 parts of Chinese date extract, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C to obtain liquid lipstick;
s3, freezing the liquid lipstick at-8 to-10 ℃ for 30 minutes to obtain the edible lipstick.
Preferably, the preparation method of the edible lipstick comprises the following steps:
s1, uniformly mixing 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil and 1.9 parts of plant natural pigment, and stirring for 8 minutes to obtain a mixture, wherein the stirring temperature is 55 ℃, and the stirring speed is 1400 r/min;
s2, adding 6.1 parts of natural farmhouse beewax into the mixture, heating in a water bath at 70 ℃, stirring until the natural farmhouse beewax and the mixture are completely melted, and adding 1.5 parts of Chinese date extract, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C to obtain liquid lipstick;
s3, freezing the liquid lipstick at-8 to-10 ℃ for 30 minutes to obtain the edible lipstick.
The natural vegetable oil and the plant natural pigment are uniformly mixed firstly in order to color the beeswax more quickly in the later period. The mixture and the beeswax are heated in a water bath, so that the beeswax and the mixture are completely mixed, the color of the lipstick is more uniform, no mixed color is generated, lip wrinkles can be lightened, oxidation resistance is realized, aging is delayed, the texture of the lipstick is more smooth by adding natural functional additives such as Chinese date extract, tea polyphenol and vitamin E, and the lipstick is convenient to apply. Compared with the prior art, the lipstick has the beneficial effects that the prepared lipstick is safe to use, does not contain toxic and harmful substances, can be eaten, and has a nourishing effect on lips.
Detailed Description
The technical solutions in the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The edible lipstick comprises 4.2 parts of mei teng fruit oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.12 parts of natural farmhouse beewax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
Example 2
An edible lipstick comprises 4.2 parts of fig oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.1 parts of natural farmhouse beeswax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
The method of making an edible lipstick as described in example 1, comprising the steps of:
s1, uniformly mixing 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil and 1.9 parts of plant natural pigment, and stirring for 8 minutes to obtain a mixture, wherein the stirring temperature is 55 ℃, and the stirring speed is 1400 r/min;
s2, adding 6.12 parts of natural farmhouse beewax into the mixture, heating in a water bath at 70 ℃, stirring until the natural farmhouse beewax and the mixture are completely melted, and adding 1.5 parts of Chinese date extract, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C to obtain liquid lipstick;
s3, freezing the liquid lipstick at-8 to-10 ℃ for 30 minutes to obtain the edible lipstick.
The method of making an edible lipstick as described in example 2, comprising the steps of:
s1, uniformly mixing 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil and 1.9 parts of plant natural pigment, and stirring for 8 minutes to obtain a mixture, wherein the stirring temperature is 55 ℃, and the stirring speed is 1400 r/min;
s2, adding 6.1 parts of natural farmhouse beewax into the mixture, heating in a water bath at 70 ℃, stirring until the natural farmhouse beewax and the mixture are completely melted, and adding 1.5 parts of Chinese date extract, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C to obtain liquid lipstick;
s3, freezing the liquid lipstick at-8 to-10 ℃ for 30 minutes to obtain the edible lipstick.
Comparative example 1
The edible lipstick comprises 4.2 parts of mei teng fruit oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 7.62 parts of natural farmhouse beewax, 1.9 parts of plant natural pigment, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
Comparative example 2
The edible lipstick comprises 4.2 parts of sweet vine fruit oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 7.6 parts of natural farmhouse beewax, 1.9 parts of plant natural pigment, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
The edible lipsticks prepared in examples 1-2 and comparative examples 1-2 were subjected to a correlation test.
And (3) illumination test: and (3) placing the prepared lipstick in the sunlight, and observing whether the lipstick and the surface of the lipstick have air holes or not.
Heat resistance and cold resistance test: and respectively placing the prepared lipstick in a constant temperature box at 45 ℃ and a constant temperature box at-10 ℃ for 24 hours, and observing whether the lipstick is deformed or seeps water or delaminates.
And (3) centrifugal test: and (3) putting the sample into a centrifuge tube, carrying out centrifugal treatment for 15min, and observing whether the paste is deformed or layered.
The test results are shown in Table 1.
TABLE 1 test results of examples 1-2 and comparative examples 1-2
Weighing 1g of lipstick prepared in example 1, example 2, comparative example 1 and comparative example 2 respectively, adding 9ml of pure water, mixing and grinding for 5min, centrifuging to remove supernatant, preparing into 20mg/ml to-be-detected product, passing through a microporous filter membrane to obtain sterile to-be-detected product solution, and performing antioxidant test.
H2DCF-DA is very sensitive to hydrogen peroxide and can be used to detect the active oxide, H, produced in cells2DCF-DA is not fluorescent, and when added into the culture solution, it can enter cells through cell membrane via diffusion, and enzyme esterase in cells can act on H2DCF-DA undergoes deacetylation to form polar compounds, which in the presence of intracellular peroxides will give rise to H2DCF-DA oxidizes to form a product (DCF) that has fluorescence. H when the amount of intracellular ROS (reactive oxygen species) is larger2The more DCF-DA is oxidized to form fluorescence (DCF), so that the amount of ROS generated in the cell can be known by detecting the fluorescence intensity of DCF.
Taking 1 × 105cells/well cell culture solution to 96wells, and culturing at 37 ℃ for 24 h; addition of 10. mu.M/ml H2DCF-DA, culturing at 37 ℃ for 24 h;adding 1mM H2O2 into 20mg/ml sterile solution to be tested, and culturing at 37 deg.C in dark for 1H; after washing the cells with PBS (phosphate buffered saline), the ROS content was measured with a fluorescence spectrophotometer and 3 replicates were performed, the mean and standard deviation of which are detailed in table 2:
TABLE 2 ROS expression in Oxidation resistance test
Experiments prove that the ROS expression amount of example 1 is 1.76 +/-0.31, the ROS expression amount of example 2 is 1.73 +/-0.29, the ROS expression amount of comparative example 1 is 1.83 +/-0.36, and the ROS expression amount of comparative example 2 is 1.80 +/-0.33. Compared with the comparative example 1, the oxidation reaction of the example 1 is reduced by 3.8 percent, and the oxidation reaction of the example 2 is reduced by 5.5 percent; the oxidation reaction of example 1 decreased by 2.2% and the oxidation reaction of example 2 decreased by 3.9% relative to comparative example 2. In conclusion, the Chinese date and tea polyphenol have oxidation resistance, and the Chinese date and tea polyphenol with certain amount are added into the lipstick material, so that the oxidation resistance is better.
Finally, it should be noted that the above-mentioned preferred embodiments of the present invention are provided merely to help illustrate the present invention. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (10)
1. The edible lipstick is characterized by comprising the following raw materials in parts by weight: 14-26 parts of natural vegetable oil, 4-6 parts of natural farmhouse beewax, 1.5-2 parts of plant natural pigment, 1-2 parts of Chinese date extract, 0.1-0.5 part of vitamin E, 0.05-0.3 part of vitamin B and 0.5-1 part of vitamin C.
2. The edible lipstick according to claim 1 wherein said natural vegetable oil is obtained by supercritical extraction.
3. The edible lipstick according to claim 1, wherein the natural vegetable oil comprises 3-5 parts of calamus fruit oil, 2-4 parts of almond oil, 4-6 parts of olive oil, 3-4 parts of pomegranate seed oil and 2-7 parts of aloe oil.
4. The edible lipstick according to claim 1, wherein said plant natural pigment is derived from one or more of carrot, dragon fruit, spinach and tomato which are darker plant extracts.
5. The edible lipstick according to claim 1, comprising the following raw materials in parts by weight: 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.12 parts of natural farmhouse beewax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
6. The edible lipstick according to claim 1 further comprising tea polyphenols.
7. The edible lipstick according to claim 6, comprising the following raw materials in parts by weight: 4.2 parts of calamus margaritae oil, 3.3 parts of almond oil, 4.5 parts of olive oil, 3.6 parts of pomegranate seed oil, 5.6 parts of aloe oil, 6.1 parts of natural farmhouse beeswax, 1.9 parts of plant natural pigment, 1.5 parts of Chinese date extract, 0.02 part of tea polyphenol, 0.3 part of vitamin E, 0.2 part of vitamin B and 0.8 part of vitamin C.
8. The edible lipstick according to claim 1 further comprising one or more of coconut oil, jojoba oil and avocado oil.
9. The edible lipstick according to claim 1 wherein said edible lipstick is a raw material free of lanolin.
10. The method of claim 1, comprising the steps of:
s1, uniformly mixing the natural vegetable oil and the natural plant pigment, and stirring for 5-10 minutes to obtain a mixture, wherein the stirring temperature is 40-70 ℃, and the stirring speed is 1000-2000 r/min;
s2, adding natural farmyard beewax into the mixture, heating in a water bath, stirring until the natural farmyard beewax and the mixture are completely melted, and adding the Chinese date extract, the vitamin E, the vitamin B and the vitamin C to obtain liquid lipstick;
s3, cooling and forming the liquid lipstick at the temperature below room temperature to obtain the edible lipstick.
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CN115957165A (en) * | 2023-01-17 | 2023-04-14 | 广东茂名健康职业学院 | Edible lipstick and preparation method thereof |
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CN114869806A (en) * | 2022-06-01 | 2022-08-09 | 普洱联众生物资源开发有限公司 | Plukenetia volubilis linneo lipstick |
CN115957165A (en) * | 2023-01-17 | 2023-04-14 | 广东茂名健康职业学院 | Edible lipstick and preparation method thereof |
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