CN112156032A - Whitening essence milk and preparation method thereof - Google Patents
Whitening essence milk and preparation method thereof Download PDFInfo
- Publication number
- CN112156032A CN112156032A CN202011161775.9A CN202011161775A CN112156032A CN 112156032 A CN112156032 A CN 112156032A CN 202011161775 A CN202011161775 A CN 202011161775A CN 112156032 A CN112156032 A CN 112156032A
- Authority
- CN
- China
- Prior art keywords
- parts
- extract
- skin
- whitening essence
- percentage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 230000002087 whitening effect Effects 0.000 title claims abstract description 74
- 235000013336 milk Nutrition 0.000 title claims abstract description 53
- 239000008267 milk Substances 0.000 title claims abstract description 53
- 210000004080 milk Anatomy 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- 108090000526 Papain Proteins 0.000 claims abstract description 33
- 239000004365 Protease Substances 0.000 claims abstract description 33
- 229940055729 papain Drugs 0.000 claims abstract description 33
- 235000019834 papain Nutrition 0.000 claims abstract description 33
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 27
- 239000000516 sunscreening agent Substances 0.000 claims abstract description 27
- 108010084695 Pea Proteins Proteins 0.000 claims abstract description 24
- 235000019702 pea protein Nutrition 0.000 claims abstract description 24
- 239000002562 thickening agent Substances 0.000 claims abstract description 23
- MPDGHEJMBKOTSU-YKLVYJNSSA-N 18beta-glycyrrhetic acid Chemical compound C([C@H]1C2=CC(=O)[C@H]34)[C@@](C)(C(O)=O)CC[C@]1(C)CC[C@@]2(C)[C@]4(C)CC[C@@H]1[C@]3(C)CC[C@H](O)C1(C)C MPDGHEJMBKOTSU-YKLVYJNSSA-N 0.000 claims abstract description 22
- 241001673954 Magnolia sieboldii Species 0.000 claims abstract description 22
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 22
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims abstract description 17
- 241001135917 Vitellaria paradoxa Species 0.000 claims abstract description 17
- 229940057910 shea butter Drugs 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 16
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000011347 resin Substances 0.000 claims abstract description 13
- 229920005989 resin Polymers 0.000 claims abstract description 13
- 239000001947 glycyrrhiza glabra rhizome/root Substances 0.000 claims abstract description 12
- MPDGHEJMBKOTSU-UHFFFAOYSA-N Glycyrrhetinsaeure Natural products C12C(=O)C=C3C4CC(C)(C(O)=O)CCC4(C)CCC3(C)C1(C)CCC1C2(C)CCC(O)C1(C)C MPDGHEJMBKOTSU-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract description 11
- 229960003720 enoxolone Drugs 0.000 claims abstract description 11
- 241001078983 Tetradium ruticarpum Species 0.000 claims abstract description 9
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 8
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 8
- 239000003906 humectant Substances 0.000 claims abstract description 8
- 239000004094 surface-active agent Substances 0.000 claims abstract description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 69
- 150000001875 compounds Chemical class 0.000 claims description 47
- 239000000843 powder Substances 0.000 claims description 36
- -1 octyl glycol Chemical compound 0.000 claims description 32
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 28
- 235000011187 glycerol Nutrition 0.000 claims description 24
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 20
- 239000003755 preservative agent Substances 0.000 claims description 17
- 230000002335 preservative effect Effects 0.000 claims description 17
- 239000000230 xanthan gum Substances 0.000 claims description 17
- 229920001285 xanthan gum Polymers 0.000 claims description 17
- 229940082509 xanthan gum Drugs 0.000 claims description 17
- 235000010493 xanthan gum Nutrition 0.000 claims description 17
- JXPHIHWXMBYJAU-UHFFFAOYSA-N 7-methoxy-2,2-dimethyl-3,4-dihydrochromen-6-ol Chemical compound O1C(C)(C)CCC2=C1C=C(OC)C(O)=C2 JXPHIHWXMBYJAU-UHFFFAOYSA-N 0.000 claims description 14
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 14
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- 239000008172 hydrogenated vegetable oil Substances 0.000 claims description 14
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 14
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- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 13
- 229910052582 BN Inorganic materials 0.000 claims description 13
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 13
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- 229960001631 carbomer Drugs 0.000 claims description 13
- 125000001117 oleyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 13
- 230000002829 reductive effect Effects 0.000 claims description 13
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 12
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 12
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 12
- 239000000839 emulsion Substances 0.000 claims description 12
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- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 12
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- RMTFNDVZYPHUEF-XZBKPIIZSA-N 3-O-methyl-D-glucose Chemical compound O=C[C@H](O)[C@@H](OC)[C@H](O)[C@H](O)CO RMTFNDVZYPHUEF-XZBKPIIZSA-N 0.000 claims description 11
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- 239000004721 Polyphenylene oxide Substances 0.000 claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 10
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- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 8
- OEWBEINAQKIQLZ-CMRBMDBWSA-N [(2s)-2-[(2r)-3,4-bis(2-hexyldecanoyloxy)-5-oxo-2h-furan-2-yl]-2-(2-hexyldecanoyloxy)ethyl] 2-hexyldecanoate Chemical compound CCCCCCCCC(CCCCCC)C(=O)OC[C@H](OC(=O)C(CCCCCC)CCCCCCCC)[C@H]1OC(=O)C(OC(=O)C(CCCCCC)CCCCCCCC)=C1OC(=O)C(CCCCCC)CCCCCCCC OEWBEINAQKIQLZ-CMRBMDBWSA-N 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 8
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 8
- 239000003921 oil Substances 0.000 claims description 8
- 235000019198 oils Nutrition 0.000 claims description 8
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims description 8
- HSFQBFMEWSTNOW-UHFFFAOYSA-N sodium;carbanide Chemical group [CH3-].[Na+] HSFQBFMEWSTNOW-UHFFFAOYSA-N 0.000 claims description 8
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims description 8
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 claims description 8
- 229960000281 trometamol Drugs 0.000 claims description 8
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 7
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 7
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 7
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 7
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 claims description 7
- 229920002774 Maltodextrin Polymers 0.000 claims description 7
- 239000005913 Maltodextrin Substances 0.000 claims description 7
- ONIBWKKTOPOVIA-UHFFFAOYSA-N Proline Natural products OC(=O)C1CCCN1 ONIBWKKTOPOVIA-UHFFFAOYSA-N 0.000 claims description 7
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 claims description 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 7
- 235000004279 alanine Nutrition 0.000 claims description 7
- 235000006708 antioxidants Nutrition 0.000 claims description 7
- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical compound [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 claims description 7
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- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 7
- 239000008103 glucose Substances 0.000 claims description 7
- KBDSLGBFQAGHBE-MSGMIQHVSA-N limonin Chemical compound C=1([C@H]2[C@]3(C)CC[C@H]4[C@@]([C@@]53O[C@@H]5C(=O)O2)(C)C(=O)C[C@@H]2[C@]34COC(=O)C[C@@H]3OC2(C)C)C=COC=1 KBDSLGBFQAGHBE-MSGMIQHVSA-N 0.000 claims description 7
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 7
- OVGXLJDWSLQDRT-UHFFFAOYSA-L magnesium lactate Chemical compound [Mg+2].CC(O)C([O-])=O.CC(O)C([O-])=O OVGXLJDWSLQDRT-UHFFFAOYSA-L 0.000 claims description 7
- 239000000626 magnesium lactate Substances 0.000 claims description 7
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- PHZLMBHDXVLRIX-UHFFFAOYSA-M potassium lactate Chemical compound [K+].CC(O)C([O-])=O PHZLMBHDXVLRIX-UHFFFAOYSA-M 0.000 claims description 7
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- UITSPQLTFPTHJZ-UHFFFAOYSA-N 2-[[3,4,5-tris(2-hydroxyethoxy)-6-methoxyoxan-2-yl]methoxy]ethanol Chemical compound COC1OC(COCCO)C(OCCO)C(OCCO)C1OCCO UITSPQLTFPTHJZ-UHFFFAOYSA-N 0.000 claims description 6
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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Abstract
The invention relates to the technical field of cosmetics, and particularly relates to whitening essence milk and a preparation method thereof. The whitening essence milk is mainly prepared from the following raw materials in parts by weight: papain complex, glycyrrhiza glabra root extract, composite evodia rutaecarpa fruit extract, hydrolyzed pea protein complex, shea butter fruit resin extract, composite magnolia sieboldii extract, glycyrrhetinic acid stearate, a skin conditioner, an antioxidant, an emulsifier, a sunscreen agent, a surfactant, a humectant, a thickener and water. The whitening essence cream obtained by the coordination and cooperation of the components mildly peels off cutin, promotes skin microcirculation and enables the skin to be smooth and bright; the skin barrier is effectively repaired, and the capability of the skin for resisting external stimulation is improved; protecting skin from light radiation, improving cell photoadaptability, and reducing photoaging; inhibiting melanin synthesis, delaying aging, and making skin finer and more white.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to whitening essence milk and a preparation method thereof.
Background
With the rapid development of economy, skin care products become daily fast-consumption products, and the expectation value of people for skin care products also rises synchronously. The 'one white and covering three ugly' is the pursuit of skin care products with whitening effect by consumers since ancient times. In recent years, some consumers try to achieve the purpose of quickly whitening skin through modes such as medical and beauty, but the risk is high, and some consumers have the adverse effects that the feedback later period rebounds obviously, the sebum membrane falls off, the cuticle becomes thin and the like. In consideration of safety, more consumers prefer to use daily skin care products to achieve the effect of whitening skin.
With the development of the technology and the improvement of the cognitive level of people, the definition of whitening by consumers is not limited to the existence of color spots, the darkness and the yellow of the face color and the like, but the glossiness, the transparency, the red and moist feeling and the like of the skin are all brought into the indexes for evaluating whitening, and the consumers pay more attention to whether the skin barrier is still intact and whether the skin is kept healthy while achieving the whitening effect.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
The invention aims to provide a whitening essence emulsion which has the effects of brightening skin color, increasing skin permeability, increasing glossiness, lightening spots and the like.
The second object of the present invention is to provide a method for preparing the whitening essence milk, which is simple and easy to implement, and the whitening essence milk obtained by the method has a more excellent whitening effect.
In order to achieve the above purpose of the present invention, the following technical solutions are adopted:
the whitening essence milk is mainly prepared from the following raw materials in parts by weight:
20-30 parts of papain compound, 0.03-0.07 part of glycyrrhiza glabra root extract, 0.5-20 parts of compound evodia rutaecarpa fruit extract, 1.5-2.5 parts of hydrolyzed pea protein compound, 0.2-0.8 part of shea butter extract, 0.05-0.15 part of compound Magnolia sieboldii extract, 0.1-0.3 part of glycyrrhetinic acid stearate, 5.2-19.3 parts of skin conditioner, 3.03-7.07 parts of antioxidant, 2.5-7.0 parts of emulsifier, 0.41-1.85 parts of sun-screening agent, 0.2-0.8 part of surfactant, 4-8 parts of humectant, 2.11-4.35 parts of thickener and 18.14-56.82 parts of water;
preferably, the papain complex mainly comprises the following components in percentage by mass: 57.11-64.91% of water, 21.321-26.059% of glycerol, 6.075-7.425% of maltodextrin, 1.62-1.98% of calcium pantothenate, 1.476-1.804% of xanthan gum, 0.9-1.1% of urea, 0.9-1.1% of octyl glycol, 0.09-0.11% of proline, 0.09-0.11% of alanine, 0.09-0.11% of serine, 0.747-0.913% of magnesium lactate, 0.324-0.396% of potassium lactate, 0.09-0.11% of magnesium chloride, 0.063-0.077% of sodium citrate, 0.675-0.825% of papain and 0.6294-0.7692% of ethylhexylglycerol;
preferably, the composite fructus evodiae extract mainly comprises the following components in percentage by mass: 90-95% of 1, 3-propylene glycol and 5-10% of fructus evodiae extract;
preferably, the hydrolyzed pea protein complex consists essentially of the following components in percentage by mass: glycerol 77.648-81.712%, water 17.9527-21.9421%, hydrolyzed pea protein 0.1059-0.1295%, glucose 0.1336-0.1632%, sodium chloride 0.0888-0.1086% and sodium succinate 0.0070-0.0086%;
preferably, the composite magnolia sieboldii extract mainly comprises the following components in percentage by mass: 0.1 to 0.2 percent of magnolia sieboldii extract, 58 to 62 percent of butanediol and 37.9 to 41.8 percent of water.
Preferably, the skin conditioning agent comprises at least one of squalane, methyl gluceth-10, glycerol tri (ethyl hexanoate) ester, hydrogenated vegetable oil, PPG-10 methyl gluceth, dimethicone, and cyclopentademethicone.
Preferably, the antioxidant comprises ascorbyl tetraisopalmitate and/or dimethylmethoxychromanol.
Preferably, the emulsifier comprises at least one of oleyl polyether-20, sodium methyl stearyl taurate and emulsifier a;
preferably, the emulsifier A mainly comprises the following components in percentage by mass: 50% of behenyl alcohol, 38% of polyglycerol-10 pentastearate and 12% of sodium stearoyl lactylate;
preferably, the humectant comprises butylene glycol and/or glycerin.
Preferably, the thickener comprises at least one of xanthan gum, carbomer and thickener B;
preferably, the thickener B mainly comprises the following components in percentage by mass: 80-90% of cyclopenta dimethyl silicone polymer and 10-20% of dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer.
Preferably, the sunscreen agent comprises at least one of sunscreen agent B and boron nitride;
the sunscreen agent B mainly comprises the following components in percentage by mass: 30-40% of synthetic fluorophlogopite, 20-30% of titanium dioxide, 0-0.5% of tin oxide, 30-40% of polymethyl methacrylate and 0-0.1% of polyvinyl alcohol.
Preferably, the whitening essence milk further comprises 0.2-1 part by weight of a preservative;
preferably, the preservative mainly comprises the following components in percentage by mass: 60 to 70 percent of phenoxyethanol and 30 to 40 percent of caprylyl glycol;
preferably, the whitening essence milk further comprises 0.02-0.1 part by weight of hydrophilic treatment pearl powder;
preferably, the whitening essence milk further comprises 0.03-0.07 part of essence by weight;
preferably, the whitening essence milk further comprises 0.5-2 parts by weight of functional powder;
preferably, the functional powder mainly comprises the following components in percentage by mass: HDI/trihydroxymethyl hexyl lactone cross-linked polymer 97.5-98.5 wt% and silica 1.5-2.5 wt%.
Preferably, the whitening essence milk is mainly prepared from the following raw materials in parts by weight:
20-30 parts of papain complex, 1.5-2.5 parts of hydrolyzed pea protein complex, 0.5-2.0 parts of compound evodia rutaecarpa fruit extract, 0.05-0.15 parts of compound Magnolia sieboldii extract, 0.2-0.8 part of shea butter fruit resin extract, 1.5-2.5 parts of glycerol tri (ethyl hexanoate), 0.03-0.07 part of dimethyl methoxy chromanol, 1-3 parts of ascorbyl tetraisopalmitate, 2-4 parts of squalane, 1.8-3.0 parts of emulsifier A, 0.2-0.8 part of polydimethylsiloxane, 2-4 parts of cyclopenta dimethyl siloxane, 0.1-0.3 part of glycyrrhetinic acid stearate, 0.05-4 parts of organic silicon elastomer dispersion SFE 8392-4 parts, 1.5-4 parts of hydrogenated vegetable oil, 0.05-0.15 part of disodium EDTA, 0.1-0.3 part of glucose syrup, 0.01-0.05 part of carbomer, 2.05-4 parts of glycerol polyether, 2.5-4 parts of 2.07-0.5 parts of methyl polyether, 200.3-1.5 parts of oleyl polyether, 0.1-0.5 part of methyl stearyl sodium taurate, 0.05-0.15 part of tromethamine, 0.2-1 part of preservative, 0.5-2.0 parts of functional powder, 0.02-0.1 part of hydrophilic treatment pearl powder, 0.1-0.3 part of sun-screening agent B, 0.3-1.5 parts of boron nitride, 1.5-2.5 parts of PPG-10 methyl glucose ether, 0.03-0.07 part of essence and 18.14-56.82 parts of water.
The preparation method of the whitening essence milk comprises the following steps:
and uniformly mixing the raw material components of the whitening essence milk.
Preferably, the preparation method of the whitening essence milk comprises the following steps:
(a) heating a mixture of glycerol tri (ethyl hexanoate) ester, dimethyl methoxy chromanol and ascorbic acid tetraisopalmitate, mixing and heating with squalane, emulsifier A, glycyrrhetinic stearate, thickener B, hydrogenated vegetable oil and shea butter fruit resin extract to obtain an oil phase;
(b) heating a mixture of disodium EDTA, xanthan gum, carbomer, butanediol, glycerol, deionized water, methyl gluceth-10, Glycyrrhiza glabra root extract, oleyl polyether-20, and sodium methyl stearyl taurate to obtain a water phase;
(c) mixing the water phase and the oil phase and homogenizing;
(d) adding tromethamine into the mixture obtained in the step (c), uniformly stirring and cooling;
(e) adding a preservative, a papain compound, functional powder, hydrophilic treatment pearl powder, a sun-screening agent B, a compound evodia fruit extract, boron nitride, a hydrolyzed pea protein compound, PPG-10 methyl glucose ether and essence into the emulsion obtained in the step (d), stirring uniformly, and cooling;
preferably, in the step (a), the heating temperature is 75-80 ℃;
preferably, in the step (b), the heating temperature is 75-80 ℃;
preferably, in the step (c), the rotation speed of the homogenizing treatment is 2500-3500 rpm, and the time of the homogenizing treatment is 2.5-3.5 min;
preferably, in the step (d), the temperature is reduced to 35-40 ℃;
preferably, the rotating speed of the stirring is 200-300 r/min.
Compared with the prior art, the invention has the beneficial effects that:
(1) the whitening essence cream obtained by the coordination and coordination of the components is soft in texture, easy to absorb and soft and comfortable in later-period skin feeling; the cutin is peeled off mildly, the skin microcirculation is promoted, and the skin is smooth and bright; effectively repair the skin barrier, improve the capability of the skin to resist external stimulation and ensure that the skin is more healthy. Protecting skin from light radiation, improving cell photoadaptability, and reducing photoaging; inhibiting melanin synthesis, reducing pigmentation, scavenging free radicals, preventing lipid peroxidation, delaying aging, and making skin finer and more white.
(2) The preparation method of the whitening essence milk is simple and easy to implement, and the whitening essence milk obtained by the method has an excellent whitening effect.
Detailed Description
Embodiments of the present invention will be described in detail below with reference to examples, but it will be understood by those skilled in the art that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available.
According to one aspect of the invention, the invention relates to whitening essence milk which is mainly prepared from the following raw materials in parts by weight:
20-30 parts of papain compound, 0.03-0.07 part of glycyrrhiza glabra root extract, 0.5-20 parts of compound evodia rutaecarpa fruit extract, 1.5-2.5 parts of hydrolyzed pea protein compound, 0.2-0.8 part of shea butter extract, 0.05-0.15 part of compound Magnolia sieboldii extract, 0.1-0.3 part of glycyrrhetinic acid stearate, 5.2-19.3 parts of skin conditioner, 3.03-7.07 parts of antioxidant, 2.5-7.0 parts of emulsifier, 0.41-1.85 parts of sun-screening agent, 0.2-0.8 part of surfactant, 4-8 parts of humectant, 2.11-4.35 parts of thickener and 18.14-56.82 parts of water.
In one embodiment, the papain complex is 20 to 30 parts, and may further be selected from 20 parts, 20.1 parts, 20.2 parts, 20.3 parts, 20.4 parts, 20.5 parts, 20.6 parts, 20.7 parts, 20.8 parts, 20.9 parts, 21 parts, 21.1 parts, 21.2 parts, 21.3 parts, 21.4 parts, 21.5 parts, 21.6 parts, 21.7 parts, 21.8 parts, 21.9 parts, 22 parts, 22.1 parts, 22.2 parts, 22.3 parts, 22.4 parts, 22.5 parts, 22.6 parts, 22.7 parts, 22.8 parts, 22.9 parts, 23 parts, 23.1 parts, 23.2 parts, 23.3 parts, 23.4 parts, 23.5 parts, 23.6 parts, 23.7 parts, 23.8 parts, 23.9 parts, 24.5 parts, 24.1 parts, 24.2 parts, 23.3 parts, 23.4 parts, 27.5 parts, 23.6 parts, 23.7 parts, 23.8 parts, 27.9 parts, 24.5 parts, 24.1, 25.2 parts, 26.8 parts, 26.9 parts, 27.9 parts, 26.9.9 parts, 26.8 parts, 26.9 parts, 26.9.9, 26.8.9, 26.8 parts, 26.9, 26.2.8.8.9, 26.9, 26.8.9, 26.9, 26.8, 26.2, 26.8.8.9, 26.9, 26.8, 26.8.8, 26.9, 26.8.1, 26., 28.1 parts, 28.2 parts, 28.3 parts, 28.4 parts, 28.5 parts, 29 parts, 29.1 parts, 29.2 parts, 29.3 parts, 29.4 parts, 29.5 parts, 29.6 parts, 29.7 parts, 29.8 parts, 29.9 parts or 30 parts.
In one embodiment, the glycyrrhiza glabra root extract is 0.03-0.07 part, and optionally 0.03 part, 0.04 part, 0.05 part, 0.06 part or 0.07 part.
In one embodiment, the compound evodia rutaecarpa fruit extract is 0.5-20 parts, and optionally 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts, 9.5 parts, 10 parts, 10.5 parts, 11 parts, 11.5 parts, 12 parts, 12.5 parts, 13 parts, 13.5 parts, 14 parts, 14.5 parts, 15 parts, 16 parts, 16.5 parts, 17 parts, 17.5 parts, 18 parts, 18.5 parts, 19 parts, 19.5 parts or 20 parts.
In one embodiment, the hydrolyzed pea protein complex is 1.5 to 2.5 parts, and optionally 1.5 parts, 1.51 parts, 1.52 parts, 1.53 parts, 1.54 parts, 1.55 parts, 1.56 parts, 1.57 parts, 1.58 parts, 1.59 parts, 1.6 parts, 1.61 parts, 1.62 parts, 1.63 parts, 1.64 parts, 1.65 parts, 1.66 parts, 1.67 parts, 1.68 parts, 1.69 parts, 1.7 parts, 1.71 parts, 1.72 parts, 1.73 parts, 1.74 parts, 1.75 parts, 1.76 parts, 1.77 parts, 1.78 parts, 1.79 parts, 1.8 parts, 1.81 parts, 1.82 parts, 1.83 parts, 1.84 parts, 1.85 parts, 1.86 parts, 1.87 parts, 1.88 parts, 1.79 parts, 1.8 parts, 1.81 parts, 1.82 parts, 1.83 parts, 2.84 parts, 2.85 parts, 2.86 parts, 1.87 parts, 1.88 parts, 1.9.91, 2.9.35 parts, 2.9.9, 2.9, 2.35 parts, 2.9.9, 2.9.8 parts, 2.9.9, 2.9.9.9, 2.9.9, 2.9.3, 2.9.9, 2.9.3.3, 2.3.9, 2.9.9, 2.9, 2.9.9, 2.3, 2.3.3.3.3.3, 2.3, 2.3.3, 2.3, 2.3.3, 2.3.3.3.3, 2.3, 2.3.3, 2.23, 2.36 parts, 2.37 parts, 2.38 parts, 2.39 parts, 2.4 parts, 2.41 parts, 2.42 parts, 2.43 parts, 2.44 parts, 2.45 parts, 2.46 parts, 2.47 parts, 2.48 parts, 2.49 parts or 2.5 parts.
Preferably, the papain complex mainly comprises the following components in percentage by mass: 57.11-64.91% of water, 21.321-26.059% of glycerol, 6.075-7.425% of maltodextrin, 1.62-1.98% of calcium pantothenate, 1.476-1.804% of xanthan gum, 0.9-1.1% of urea, 0.9-1.1% of octyl glycol, 0.09-0.11% of proline, 0.09-0.11% of alanine, 0.09-0.11% of serine, 0.747-0.913% of magnesium lactate, 0.324-0.396% of potassium lactate, 0.09-0.11% of magnesium chloride, 0.063-0.077% of sodium citrate, 0.675-0.825% of papain and 0.6294-0.7692% of ethylhexylglycerol.
Preferably, the papain complex mainly comprises the following components in percentage by mass: 60 to 63.25 percent of water, 21 to 25.33 percent of glycerol, 6.5 to 7 percent of maltodextrin, 1.7 to 1.9 percent of calcium pantothenate, 1.5 to 1.6 percent of xanthan gum, 1 to 1.1 percent of urea, 1 to 1.1 percent of caprylyl glycol, 0.09 to 0.1 percent of proline, 0.1 to 0.11 percent of alanine, 0.09 to 0.1 percent of serine, 0.75 to 0.8 percent of magnesium lactate, 0.3 to 0.35 percent of potassium lactate, 0.09 to 0.1 percent of magnesium chloride, 0.065 to 0.07 percent of sodium citrate, 0.7 to 0.805 percent of papain and 0.65 to 0.75 percent of ethylhexylglycerol.
In one embodiment, the papain complex consists essentially of the following components in mass percent: water 60%, glycerol 25.33%, maltodextrin 6.5%, calcium pantothenate 1.7%, xanthan gum 1.5%, urea 1%, caprylyl glycol 1%, proline 0.1%, alanine 0.1%, serine 0.1%, magnesium lactate 0.8%, potassium lactate 0.35%, magnesium chloride 0.1%, sodium citrate 0.07%, papain 0.7%, and ethylhexylglycerol 0.65%.
In one embodiment, the papain complex consists essentially of the following components in mass percent: water 63.25%, glycerol 21%, maltodextrin 7%, calcium pantothenate 1.9%, xanthan gum 1.6%, urea 1.1%, caprylyl glycol 1.1%, proline 0.09%, alanine 0.11%, serine 0.09%, magnesium lactate 0.75%, potassium lactate 0.3%, magnesium chloride 0.09%, sodium citrate 0.065%, papain 0.805%, and ethylhexylglycerol 0.75%.
Preferably, the composite fructus evodiae extract mainly comprises the following components in percentage by mass: 90-95% of 1, 3-propylene glycol and 5-10% of fructus evodiae extract;
preferably, the hydrolyzed pea protein complex consists essentially of the following components in percentage by mass: glycerol 77.648-81.712%, water 17.9527-21.9421%, hydrolyzed pea protein 0.1059-0.1295%, glucose 0.1336-0.1632%, sodium chloride 0.0888-0.1086% and sodium succinate 0.0070-0.0086%.
Preferably, the composite magnolia sieboldii extract mainly comprises the following components in percentage by mass: 0.1 to 0.2 percent of magnolia sieboldii extract, 58 to 62 percent of butanediol and 37.9 to 41.8 percent of water.
Preferably, the composite magnolia sieboldii extract mainly comprises the following components in percentage by mass: 0.1 percent of magnolia sieboldii extract, 60 percent of butanediol and 39.9 percent of water.
The addition of a proper amount of the shea butter extract can stimulate epidermal barrier repair and slow down ossein decomposition, and has the effects of relieving and health skin and restoring the skin to a young state.
The liquorice root extract with a proper amount is added in the invention, so that the effects of whitening, removing freckles, brightening skin color, isolating ultraviolet rays, inhibiting melanin and the like are achieved.
The papain complex added in the invention is a high-pressure micro-flow precisely controlled molecular membrane with optimized papain transmission effect and enhanced moisturizing effect, and natural moisturizing factor components contained in the membrane can help maintain the natural barrier function of epidermis. Meanwhile, the papain has the capability of mildly peeling off dead keratinocytes on the outer layer of the epidermis, so that the skin is smooth and bright.
The added appropriate amount of the fructus evodiae extract can effectively inhibit melanin synthesis, improve darkness, brighten skin color, promote skin microcirculation and oxygenation, and improve skin glossiness and transparency.
The magnolia sieboldii extract with a proper amount is added, so that the melanin formation can be obviously inhibited by inhibiting inflammatory factors, and the pigmentation induced by UV can be effectively inhibited. In addition, the Magnolia sieboldii extract has good oxidation resistance and the ability to reduce 1L-1 alpha and NO.
According to the invention, the obtained essence milk has an excellent whitening effect through the specific matching effect of the papain complex, the glycyrrhiza glabra root extract, the evodia rutaecarpa fruit extract, the hydrolyzed pea protein complex, the shea butter fruit resin extract, the skin conditioner, the antioxidant, the emulsifier, the humectant and the water.
Preferably, the skin conditioning agent comprises at least one of squalane, methyl gluceth-10, glycerol tri (ethyl hexanoate) ester, hydrogenated vegetable oil, PPG-10 methyl gluceth, dimethicone, and cyclopentademethicone.
The addition of the specific skin conditioning agent of the present invention can lubricate the skin in the stratum corneum, usually fill the space on the skin surface, replace the lipid lost in the stratum corneum, reduce the scaly skin, and improve the skin appearance.
Preferably, the antioxidant comprises ascorbyl tetraisopalmitate and/or dimethylmethoxychromanol.
Preferably, the emulsifier comprises at least one of oleyl polyether-20, sodium methyl stearyl taurate and emulsifier a.
Preferably, the emulsifier A mainly comprises the following components in percentage by mass: behenyl alcohol 50%, polyglycerol-10 pentastearate 38% and sodium stearoyl lactylate 12%.
The specific emulsifier of the invention can improve the surface tension between various constituent phases in the essence emulsion to form a uniform dispersion or emulsion.
Preferably, the humectant comprises butylene glycol and/or glycerin.
The proper amount of the moisturizer of the invention can better maintain the skin barrier function while maintaining the skin hydration.
Preferably, the thickener comprises at least one of xanthan gum, carbomer and thickener B.
Preferably, the thickener B mainly comprises the following components in percentage by mass: 80-90% of cyclopenta dimethyl silicone polymer and 10-20% of dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer.
The proper amount of the thickening agent can improve the viscosity of a system and keep the system in a uniform and stable suspension state or an emulsion state.
Preferably, the sunscreen agent comprises at least one of sunscreen agent B and boron nitride.
The sunscreen agent B mainly comprises the following components in percentage by mass: 30-40% of synthetic fluorophlogopite, 20-30% of titanium dioxide, 0-0.5% of tin oxide, 30-40% of polymethyl methacrylate and 0-0.1% of polyvinyl alcohol.
The specific sun-screening agent is more beneficial to improving skin and whitening effect.
Preferably, the whitening essence milk further comprises 0.2-1 part by weight of a preservative;
preferably, the preservative mainly comprises the following components in percentage by mass: 60 to 70 percent of phenoxyethanol and 30 to 40 percent of caprylyl glycol.
The special preservative is added, so that the growth and the propagation of microorganisms can be better inhibited, the property stability of the cosmetic is kept, the cosmetic is not easy to deteriorate after being uncovered, and the storage time is prolonged.
Preferably, the whitening essence milk further comprises 0.02-0.1 part by weight of hydrophilic treatment pearl powder.
Preferably, the whitening essence milk further comprises 0.03-0.07 part of essence by weight.
The invention can also add a proper amount of essence to provide pleasant smell and cover the smell of the product matrix.
Preferably, the whitening essence milk further comprises 0.5-2 parts by weight of functional powder.
Preferably, the functional powder mainly comprises the following components in percentage by mass: HDI/trihydroxymethyl hexyl lactone cross-linked polymer 97.5-98.5 wt% and silica 1.5-2.5 wt%.
The functional powder, namely [ HDI/trihydroxymethyl hexyl lactone crosslinked polymer (and) silica ], is added to serve as a slipping agent and is matched with other components to improve the skin quality, so that the whitening effect is achieved.
Preferably, the whitening essence milk is mainly prepared from the following raw materials in parts by weight:
20-30 parts of papain complex, 1.5-2.5 parts of hydrolyzed pea protein complex, 0.5-2.0 parts of compound evodia rutaecarpa fruit extract, 0.05-0.15 parts of compound Magnolia sieboldii extract, 0.2-0.8 part of shea butter fruit resin extract, 1.5-2.5 parts of glycerol tri (ethyl hexanoate), 0.03-0.07 part of dimethyl methoxy chromanol, 1-3 parts of ascorbyl tetraisopalmitate, 2-4 parts of squalane, 1.8-3.0 parts of emulsifier A, 0.2-0.8 part of polydimethylsiloxane, 2-4 parts of cyclopenta dimethyl siloxane, 0.1-0.3 part of glycyrrhetinic acid stearate, 0.05-4 parts of organic silicon elastomer dispersion SFE 8392-4 parts, 1.5-4 parts of hydrogenated vegetable oil, 0.05-0.15 part of disodium EDTA, 0.1-0.3 part of glucose syrup, 0.01-0.05 part of carbomer, 2.05-4 parts of glycerol polyether, 2.5-4 parts of 2.07-0.5 parts of methyl polyether, 200.3-1.5 parts of oleyl polyether, 0.1-0.5 part of methyl stearyl sodium taurate, 0.05-0.15 part of tromethamine, 0.2-1 part of preservative, 0.5-2.0 parts of functional powder, 0.02-0.1 part of hydrophilic treatment pearl powder, 0.1-0.3 part of sun-screening agent B, 0.3-1.5 parts of boron nitride, 1.5-2.5 parts of PPG-10 methyl glucose ether, 0.03-0.07 part of essence and 18.14-56.82 parts of water.
The whitening essence emulsion obtained by the specific raw materials has the appearance of a glittering pearly-lustre dilute emulsion, has a more excellent whitening effect, is soft in texture and easy to absorb, and is soft and comfortable in later-period skin feel; the cutin is peeled off mildly, the skin microcirculation is promoted, and the skin is smooth and bright; effectively repair the skin barrier, improve the capability of the skin to resist external stimulation and ensure that the skin is more healthy. Protecting skin from light radiation, improving cell photoadaptability, and reducing photoaging; inhibiting melanin synthesis, reducing pigmentation, scavenging free radicals, preventing lipid peroxidation, delaying aging, and making skin finer and more white.
The preparation method of the whitening essence milk comprises the following steps:
and uniformly mixing the raw material components of the whitening essence milk.
Preferably, the preparation method of the whitening essence milk comprises the following steps:
(a) heating a mixture of glycerol tri (ethyl hexanoate) ester, dimethyl methoxy chromanol and ascorbic acid tetraisopalmitate, mixing and heating with squalane, emulsifier A, glycyrrhetinic stearate, thickener B, hydrogenated vegetable oil and shea butter fruit resin extract to obtain an oil phase;
(b) heating a mixture of disodium EDTA, xanthan gum, carbomer, butanediol, glycerol, deionized water, methyl gluceth-10, Glycyrrhiza glabra root extract, oleyl polyether-20, and sodium methyl stearyl taurate to obtain a water phase;
(c) mixing the water phase and the oil phase and homogenizing;
(d) adding tromethamine into the mixture obtained in the step (c), uniformly stirring and cooling;
(e) adding a preservative, a papain compound, functional powder, hydrophilic treatment pearl powder, a sun-screening agent B, a compound evodia fruit extract, boron nitride, a hydrolyzed pea protein compound, PPG-10 methyl glucose ether and essence into the emulsion obtained in the step (d), stirring uniformly, and cooling.
The whitening essence milk prepared by the specific feeding sequence has a more excellent whitening effect.
Preferably, in the step (a), the heating temperature is 75-80 ℃.
In one embodiment, in the step (a), the heating temperature is 75-80 ℃, and 75 ℃, 76 ℃, 77 ℃, 78 ℃, 79 ℃ or 80 ℃ can be selected.
Preferably, in the step (b), the heating temperature is 75-80 ℃.
In an embodiment, in the step (b), the heating temperature is 75-80 ℃, and the heating temperature can be selected from 75 ℃, 75.1 ℃, 75.2 ℃, 75.3 ℃, 75.4 ℃, 75.5 ℃, 75.6 ℃, 75.7 ℃, 75.8 ℃, 75.9 ℃, 76 ℃, 76.1 ℃, 76.2 ℃, 76.3 ℃, 76.4 ℃, 76.5 ℃, 76.6 ℃, 76.7 ℃, 76.8 ℃, 76.9 ℃, 77 ℃, 77.1 ℃, 77.2 ℃, 77.3 ℃, 77.4 ℃, 77.5 ℃, 77.6 ℃, 77.7 ℃, 77.8 ℃, 77.9 ℃, 78, 78.1 ℃, 78.2 ℃, 78.4 ℃, 77.5 ℃, 77.6 ℃, 77.7 ℃, 78.8 ℃, 77.9 ℃, 78, 3.5 ℃, 78, 9, 78, 9, 78, 3.2, 3, 3.4, 78, 9, 79, 9, 79, 9, 79, 9, 79, 2, 79, 79.4 degrees Celsius, 79.5 degrees Celsius, 79.6 degrees Celsius, 79.7 degrees Celsius, 79.8 degrees Celsius, 79.9 degrees Celsius, or 80 degrees Celsius.
Preferably, in the step (c), the rotation speed of the homogenization treatment is 2500-3500 rpm, and the time of the homogenization treatment is 2.5-3.5 min.
In one embodiment, in step (c), the rotation speed of the homogenization treatment is 2500-3500 rpm, and 2600rpm, 2700rpm, 2800rpm, 2900rpm, 3000rpm, 3100rpm, 3200rpm, 3300rpm, or 3400rpm may also be selected.
Preferably, in the step (d), the temperature is reduced to 35-40 ℃.
Preferably, the rotating speed of the stirring is 200-300 r/min.
The stirring rotation in the step (d) and the step (e) is respectively 200-300 r/min, and 200r/min, 210r/min, 220r/min, 230r/min, 240r/min, 250r/min, 260r/min or 270r/min can be selected.
The invention will be further explained with reference to specific examples.
Example 1
The whitening essence milk is mainly prepared from the following raw materials in parts by weight:
25 parts of papain compound, 2 parts of hydrolyzed pea protein compound, 1 part of compound evodia fruit extract, 0.1 part of compound Magnolia sieboldii extract, 0.5 part of shea butter fruit resin extract, 2 parts of glycerol tri (ethyl hexanoate), 0.05 part of dimethyl methoxy chromanol, 2 parts of ascorbyl tetraisopalmitate, 3 parts of squalane, 2.4 parts of emulsifier A, 0.5 part of polydimethylsiloxane, 3 parts of cyclopenta dimethyl siloxane, 0.2 part of glycyrrhetinic acid stearate, 3 parts of thickening agent B, 2.7 parts of hydrogenated vegetable oil, 0.1 part of EDTA disodium, 0.2 part of xanthan gum, 0.03 part of carbomer, 3 parts of butanediol, 3 parts of glycerol, 1 part of methyl glucitol polyether-102, 0.05 part of glycyrrhiza glabra extract, 200.8 parts of oleyl polyether, 0.3 part of sodium methyl stearyl taurate, 0.6 part of preservative, 0.3 part of caprylyl glycol, 1 part of functional powder, 0.06 part of pearl light treated powder, 0.06 part of hydrophilic powder, 0.2 part of sun-screening agent B, 0.85 part of boron nitride, 2 parts of PPG-10 methyl glucose ether, 0.05 part of essence and 38.24 parts of water;
the papain compound mainly comprises the following components in percentage by mass: water 60%, glycerol 25.33%, maltodextrin 6.5%, calcium pantothenate 1.7%, xanthan gum 1.5%, urea 1%, caprylyl glycol 1%, proline 0.1%, alanine 0.1%, serine 0.1%, magnesium lactate 0.8%, potassium lactate 0.35%, magnesium chloride 0.1%, sodium citrate 0.07%, papain 0.7%, and ethylhexylglycerol 0.65%;
the composite fructus evodiae extract mainly comprises the following components in percentage by mass: 90% of 1, 3-propylene glycol and 10% of fructus evodiae extract;
the hydrolyzed pea protein compound mainly comprises the following components in percentage by mass: 79% of glycerol, 20.623% of water, 0.12% of hydrolyzed pea protein, 0.15% of glucose, 0.1% of sodium chloride and 0.0070% of sodium succinate;
the composite Magnolia sieboldii extract mainly comprises the following components in percentage by mass: 0.1% of magnolia sieboldii extract, 60% of butanediol and 39.9% of water;
the emulsifier A mainly comprises the following components in percentage by mass: 50% of behenyl alcohol, 38% of polyglycerol-10 pentastearate and 12% of sodium stearoyl lactylate;
the thickener B mainly comprises the following components in percentage by mass: cyclopenta dimethicone 90% and dimethicone/vinyl dimethicone crosspolymer 10%;
the functional powder mainly comprises the following components in percentage by mass: HDI/trimethylol hexyl lactone crosspolymer 98.5% and silica 1.5%.
The preservative mainly comprises the following components in percentage by mass: 70% of phenoxyethanol and 30% of caprylyl glycol;
the sunscreen agent B mainly comprises the following components in percentage by mass: 35% of synthetic fluorophlogopite, 29.4% of titanium dioxide, 0.5% of tin oxide, 35% of polymethyl methacrylate and 0.1% of polyvinyl alcohol.
The preparation method of the whitening essence milk comprises the following steps:
(a) weighing glycerol tri (ethyl hexanoate) ester, dimethyl methoxy chromanol and ascorbic acid tetraisopalmitate in proportion, mixing and heating to completely dissolve the glycerol tri (ethyl hexanoate) ester, the dimethyl methoxy chromanol and the ascorbic acid tetraisopalmitate, weighing squalane, an emulsifier A, glycyrrhetinic acid stearate, a thickening agent B, hydrogenated vegetable oil and shea butter fruit resin extract in proportion, adding the squalane, the emulsifier A, the glycyrrhetinic acid stearate, the thickening agent B, the hydrogenated vegetable oil and the shea butter fruit resin extract into the completely dissolved solution, heating to 80 ℃, and preparing an oil phase after the dissolution is finished;
(b) weighing disodium EDTA, xanthan gum, carbomer, butanediol, glycerol, deionized water, methyl glucitol polyether-10, Glycyrrhiza glabra root extract, oleyl polyether-20 and sodium methyl stearyl taurate according to a proportion, mixing and relieving heat to 80 ℃, and preparing a water phase after complete dissolution;
(c) adding the water phase into the oil phase, and homogenizing at 3000rpm for 3 min;
(d) weighing tromethamine according to a proportion, adding the tromethamine into the emulsion prepared in the step (c), uniformly stirring at 250r/min, and cooling to 40 ℃;
(e) weighing phenoxyethanol, caprylyl glycol, a papain compound, functional powder, hydrophilic treatment pearl powder, a sun-screening agent B, a compound evodia fruit extract, water-dispersed boron nitride, a hydrolyzed pea protein compound, PPG-10 methyl glucose ether and essence according to a proportion, adding the mixture into the emulsion prepared in the step (d), uniformly stirring at 250r/min, and cooling to obtain the whitening essence emulsion.
Example 2
The whitening essence milk is mainly prepared from the following raw materials in parts by weight:
20 parts of papain compound, 2.5 parts of hydrolyzed pea protein compound, 0.5 part of compound evodia fruit extract, 0.15 part of compound Magnolia sieboldii extract, 0.2 part of shea butter fruit resin extract, 2.5 parts of glycerol tri (ethyl hexanoate) ester, 0.03 part of dimethyl methoxy chromanol, 3 parts of ascorbic acid tetraisopalmitate, 2 parts of squalane, 3.0 parts of emulsifier A, 0.2 part of polydimethylsiloxane, 4 parts of cyclopenta dimethyl siloxane, 0.1 part of glycyrrhetinic acid stearate, 1.5 parts of thickening agent B, hydrogenated vegetable oil, 0.15 part of EDTA disodium, 0.1 part of xanthan gum, 0.05 part of carbomer, 2 parts of butanediol, 4 parts of glycerol, 101.5 parts of methyl glucitol polyether-101.5 parts, 0.07 part of glycyrrhiza glabra root extract, 200.3 parts of oleyl polyether-200.3 parts of methyl stearyl taurate, 0.5 part of preservative, 2.0.0 part of functional powder, 2.02 parts of hydrophilic powder treatment powder, 0.3 part of sun-screening agent B, 0.3 part of boron nitride, 2.5 parts of PPG-10 methyl glucose ether, 0.03 part of essence and 49.82 parts of water.
The specific composition of the components such as the compound fructus evodiae extract, the functional powder, the sun-screening agent and the like in the raw materials of the whitening essence milk is the same as that in example 1.
The preparation method of the whitening essence milk is the same as that of example 1.
Example 3
The whitening essence milk is mainly prepared from the following raw materials in parts by weight:
30 parts of papain compound, 1.5 parts of hydrolyzed pea protein compound, 2.0 parts of compound evodia fruit extract, 0.05 part of compound Magnolia sieboldii extract, 0.8 part of shea butter fruit resin extract, 1.5 parts of glycerol tri (ethyl hexanoate) ester, 0.07 part of dimethyl methoxy chromanol, 1 part of ascorbyl tetraisopalmitate, 4 parts of squalane, 1.8 parts of emulsifier A, 0.8 part of polydimethylsiloxane, 2 parts of cyclopenta dimethyl siloxane, 0.3 part of glycyrrhetinic stearate, 2 parts of thickening agent B, 4 parts of hydrogenated vegetable oil, 0.05 part of EDTA disodium, 0.3 part of xanthan gum, 0.01 part of carbomer, 4 parts of butanediol, 2 parts of glycerol, methyl glucitol polyether-102.5 parts, 0.03 part of glycyrrhiza glabra root extract, oleyl polyether-201.5 parts, 0.1 part of methyl stearyl sodium taurate, 1 part of preservative, 0.5 part of glycerol octylene glycol powder, 0.5 part of functional powder treatment powder, 0.1.1 part of pearl light, 0.1 part of sun-screening agent B, 1.5 parts of boron nitride, 1.5 parts of PPG-10 methyl glucose ether, 0.07 part of essence and 50 parts of water.
The specific composition of the components such as the compound fructus evodiae extract, the functional powder, the sun-screening agent and the like in the raw materials of the whitening essence milk is the same as that in example 1.
The preparation method of the whitening essence milk is the same as that of example 1.
Examples of the experiments
The whitening effect is tested by adopting the whitening essence milk in the embodiment 1 of the invention, and the method comprises the following steps:
after a tested person cleans the face in the morning, moisturizing the skin by using toner, uniformly smearing the skin-whitening essence milk on the whole face, and massaging until the skin-whitening essence milk is absorbed, wherein the dosage is 1.8-2.2 ml; after the sun block is smeared, the sun block is well performed when the sun block is out. Removing makeup before sleeping at night, cleaning the face, moistening the skin with toner, applying 1.8-2.2 ml of whitening essence milk to the pigmented areas (such as spots and acne marks) of the face skin, and massaging until the whitening essence milk is absorbed.
VISIA detector records every seven days, comparing data of skin surface patches and uv patches after two weeks of use, and comparing with records from earlier untested products. The results are as follows:
(1) ultraviolet ray color spot characteristic change:
face on front: the ultraviolet color spot special evidence count is reduced from 447 to 424, and is reduced by 5.1%;
left side face: the ultraviolet color spot special certificate count is reduced from 307 to 297, which is reduced by 3.3%;
right side face: the uv stain signature count was reduced from 309 to 284, a reduction of 8.1%.
(3) Surface mottle characterization changes:
face on front: the surface color spot special certificate count is reduced from 172 to 161, and is reduced by 6.4%;
left side face: the surface stain characteristic count is reduced from 129 to 124, which is reduced by 3.9%;
right side face: the surface mottle characterization count was reduced from 115 to 109 by 5.2%.
The whitening essence cream obtained by the coordination and cooperation of the components mildly peels off cutin, promotes skin microcirculation and enables the skin to be smooth and bright; the skin barrier is effectively repaired, and the capability of the skin for resisting external stimulation is improved; protecting skin from light radiation, improving cell photoadaptability, and reducing photoaging; inhibiting melanin synthesis, delaying aging, and making skin finer and more white.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.
Claims (10)
1. The whitening essence milk is characterized by being mainly prepared from the following raw materials in parts by weight:
20-30 parts of papain compound, 0.03-0.07 part of glycyrrhiza glabra root extract, 0.5-20 parts of compound evodia rutaecarpa fruit extract, 1.5-2.5 parts of hydrolyzed pea protein compound, 0.2-0.8 part of shea butter extract, 0.05-0.15 part of compound Magnolia sieboldii extract, 0.1-0.3 part of glycyrrhetinic acid stearate, 5.2-19.3 parts of skin conditioner, 3.03-7.07 parts of antioxidant, 2.5-7.0 parts of emulsifier, 0.41-1.85 parts of sun-screening agent, 0.2-0.8 part of surfactant, 4-8 parts of humectant, 2.11-4.35 parts of thickener and 18.14-56.82 parts of water;
preferably, the papain complex mainly comprises the following components in percentage by mass: 57.11-64.91% of water, 21.321-26.059% of glycerol, 6.075-7.425% of maltodextrin, 1.62-1.98% of calcium pantothenate, 1.476-1.804% of xanthan gum, 0.9-1.1% of urea, 0.9-1.1% of octyl glycol, 0.09-0.11% of proline, 0.09-0.11% of alanine, 0.09-0.11% of serine, 0.747-0.913% of magnesium lactate, 0.324-0.396% of potassium lactate, 0.09-0.11% of magnesium chloride, 0.063-0.077% of sodium citrate, 0.675-0.825% of papain and 0.6294-0.7692% of ethylhexylglycerol;
preferably, the composite fructus evodiae extract mainly comprises the following components in percentage by mass: 90-95% of 1, 3-propylene glycol and 5-10% of fructus evodiae extract;
preferably, the hydrolyzed pea protein complex consists essentially of the following components in percentage by mass: glycerol 77.648-81.712%, water 17.9527-21.9421%, hydrolyzed pea protein 0.1059-0.1295%, glucose 0.1336-0.1632%, sodium chloride 0.0888-0.1086% and sodium succinate 0.0070-0.0086%;
preferably, the composite magnolia sieboldii extract mainly comprises the following components in percentage by mass: 0.1 to 0.2 percent of magnolia sieboldii extract, 58 to 62 percent of butanediol and 37.9 to 41.8 percent of water.
2. The whitening essence of claim 1, wherein the skin conditioner comprises at least one of squalane, methyl gluceth-10, glycerol tri (ethyl hexanoate) ester, hydrogenated vegetable oil, PPG-10 methyl glucose ether, polydimethylsiloxane, and cyclopentadimethylsiloxane.
3. The whitening essence of claim 1, wherein the antioxidant comprises ascorbyl tetraisopalmitate and/or dimethylmethoxychromanol.
4. The whitening essence of claim 1, wherein the emulsifier comprises at least one of oleyl polyether-20, sodium methyl stearyl taurate and emulsifier a;
preferably, the emulsifier A mainly comprises the following components in percentage by mass: 50% of behenyl alcohol, 38% of polyglycerol-10 pentastearate and 12% of sodium stearoyl lactylate;
preferably, the humectant comprises butylene glycol and/or glycerin.
5. The whitening essence milk according to claim 1, wherein the thickener comprises at least one of xanthan gum, carbomer and thickener B;
preferably, the thickener B mainly comprises the following components in percentage by mass: 80-90% of cyclopenta dimethyl silicone polymer and 10-20% of dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer.
6. The whitening essence milk according to claim 1, wherein the sunscreen agent comprises at least one of sunscreen agent B and boron nitride;
the sunscreen agent B mainly comprises the following components in percentage by mass: 30-40% of synthetic fluorophlogopite, 20-30% of titanium dioxide, 0-0.5% of tin oxide, 30-40% of polymethyl methacrylate and 0-0.1% of polyvinyl alcohol.
7. The whitening essence milk according to claim 1, further comprising 0.2-1 part by weight of a preservative;
preferably, the preservative mainly comprises the following components in percentage by mass: 60 to 70 percent of phenoxyethanol and 30 to 40 percent of caprylyl glycol;
preferably, the whitening essence milk further comprises 0.02-0.1 part by weight of hydrophilic treatment pearl powder;
preferably, the whitening essence milk further comprises 0.03-0.07 part of essence by weight;
preferably, the whitening essence milk further comprises 0.5-2 parts by weight of functional powder;
preferably, the functional powder mainly comprises the following components in percentage by mass: HDI/trihydroxymethyl hexyl lactone cross-linked polymer 97.5-98.5 wt% and silica 1.5-2.5 wt%.
8. The whitening essence milk according to claim 7, which is prepared from the following raw materials in parts by weight:
20-30 parts of papain complex, 1.5-2.5 parts of hydrolyzed pea protein complex, 0.5-2.0 parts of compound evodia rutaecarpa fruit extract, 0.05-0.15 parts of compound Magnolia sieboldii extract, 0.2-0.8 part of shea butter fruit resin extract, 1.5-2.5 parts of glycerol tri (ethyl hexanoate), 0.03-0.07 part of dimethyl methoxy chromanol, 1-3 parts of ascorbyl tetraisopalmitate, 2-4 parts of squalane, 1.8-3.0 parts of emulsifier A, 0.2-0.8 part of polydimethylsiloxane, 2-4 parts of cyclopenta dimethyl siloxane, 0.1-0.3 part of glycyrrhetinic acid stearate, 0.05-4 parts of organic silicon elastomer dispersion SFE 8392-4 parts, 1.5-4 parts of hydrogenated vegetable oil, 0.05-0.15 part of disodium EDTA, 0.1-0.3 part of glucose syrup, 0.01-0.05 part of carbomer, 2.05-4 parts of glycerol polyether, 2.5-4 parts of 2.07-0.5 parts of methyl polyether, 200.3-1.5 parts of oleyl polyether, 0.1-0.5 part of methyl stearyl sodium taurate, 0.05-0.15 part of tromethamine, 0.2-1 part of preservative, 0.5-2.0 parts of functional powder, 0.02-0.1 part of hydrophilic treatment pearl powder, 0.1-0.3 part of sun-screening agent B, 0.3-1.5 parts of boron nitride, 1.5-2.5 parts of PPG-10 methyl glucose ether, 0.03-0.07 part of essence and 18.14-56.82 parts of water.
9. The preparation method of the whitening essence milk according to any one of claims 1 to 8, characterized by comprising the following steps:
and uniformly mixing the raw material components of the whitening essence milk.
10. The preparation method of the whitening essence milk according to claim 9, comprising the steps of:
(a) heating a mixture of glycerol tri (ethyl hexanoate) ester, dimethyl methoxy chromanol and ascorbic acid tetraisopalmitate, mixing and heating with squalane, emulsifier A, glycyrrhetinic stearate, thickener B, hydrogenated vegetable oil and shea butter fruit resin extract to obtain an oil phase;
(b) heating a mixture of disodium EDTA, xanthan gum, carbomer, butanediol, glycerol, deionized water, methyl gluceth-10, Glycyrrhiza glabra root extract, oleyl polyether-20, and sodium methyl stearyl taurate to obtain a water phase;
(c) mixing the water phase and the oil phase and homogenizing;
(d) adding tromethamine into the mixture obtained in the step (c), uniformly stirring and cooling;
(e) adding a preservative, a papain compound, functional powder, hydrophilic treatment pearl powder, a sun-screening agent B, a compound evodia fruit extract, boron nitride, a hydrolyzed pea protein compound, PPG-10 methyl glucose ether and essence into the emulsion obtained in the step (d), stirring uniformly, and cooling;
preferably, in the step (a), the heating temperature is 75-80 ℃;
preferably, in the step (b), the heating temperature is 75-80 ℃;
preferably, in the step (c), the rotation speed of the homogenizing treatment is 2500-3500 rpm, and the time of the homogenizing treatment is 2.5-3.5 min;
preferably, in the step (d), the temperature is reduced to 35-40 ℃;
preferably, the rotating speed of the stirring is 200-300 r/min.
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|---|---|---|---|---|
| CN112675076A (en) * | 2021-01-04 | 2021-04-20 | 上海新高姿化妆品有限公司 | Cosmetic composition for brightening skin color and preparation method and application thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112675076A (en) * | 2021-01-04 | 2021-04-20 | 上海新高姿化妆品有限公司 | Cosmetic composition for brightening skin color and preparation method and application thereof |
| CN113041174A (en) * | 2021-02-20 | 2021-06-29 | 仲恺农业工程学院 | Camellia seed oil essence containing hydrolyzed vegetable protein and preparation method and application thereof |
| CN113041174B (en) * | 2021-02-20 | 2023-05-30 | 仲恺农业工程学院 | Oil tea seed oil essence containing hydrolyzed vegetable protein and preparation method and application thereof |
| CN115300443A (en) * | 2022-08-02 | 2022-11-08 | 银川凤仪堂生物工程有限公司 | Sheep placenta extract extraction method and application thereof in cosmetics |
| CN115300443B (en) * | 2022-08-02 | 2023-12-08 | 银川凤仪堂生物工程有限公司 | Sheep embryo extract extraction method and application thereof in cosmetics |
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