CN109528564B - Skin care composition and cosmetic preparation - Google Patents

Skin care composition and cosmetic preparation Download PDF

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CN109528564B
CN109528564B CN201910045397.9A CN201910045397A CN109528564B CN 109528564 B CN109528564 B CN 109528564B CN 201910045397 A CN201910045397 A CN 201910045397A CN 109528564 B CN109528564 B CN 109528564B
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composition
camellia
extract
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skin
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CN109528564A (en
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何泽剑
孙云起
孙怀庆
裴运林
聂艳峰
胡露
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Guangdong Marubi Biological Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18

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  • Cosmetics (AREA)

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a skin care composition and a cosmetic preparation. The skin care composition comprises the following components in parts by weight: 1-10 parts of camellia seed oil, 1-10 parts of camellia extract, 1-10 parts of camellia leaf extract and 1-10 parts of camellia seed extract. The skin care composition provided by the invention comprises camellia seed oil, camellia extract, camellia leaf extract, camellia seed extract and hibiscus flower vinegar extract, and all the components are matched with each other to play a synergistic effect, so that the composition has excellent effects of removing various wrinkles and repairing after pregnancy, enhancing skin elasticity and whitening skin.

Description

Skin care composition and cosmetic preparation
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a skin care composition and a cosmetic preparation.
Background
With the rapid development of Chinese economy, the rapid expansion of the domestic salary level and the increasing working pressure, many people, especially women, begin to pay attention to the state of their skin, and the pursuit of skin care products is higher and higher. People are not satisfied with moisturizing gradually, but have started to have higher pursuit and exploration in the aspect of maintaining skin elasticity, removing wrinkles, brightening and smoothing skin and the like, which can enable the appearance of the people to obtain certain improvement effect. The appearance of skin care products with more excellent wrinkle-removing, skin elasticity-enhancing and brightening effects is urgently needed.
The camellia seed oil is prepared from camellia seeds by low-temperature squeezing or low-temperature extraction, and contains 83% of oleic acid, 10% of saturated fatty acid and 3% of unsaturated fatty acid. Which is added to make-up removal products more in the future to give the make-up removal products a certain skin care effect.
The camellia extract is a concentrate obtained by extracting camellia, and has certain oxidation resistance, ethanol absorption inhibition effect, sugar absorption inhibition effect, gastric mucosa protection effect and platelet aggregation effect.
The camellia leaf extract is an extract of camellia leaves, and studies have been disclosed to show that the camellia leaf extract has excellent antioxidation and skin saccharification prevention effects, but the effects of the camellia leaf extract on preventing various wrinkles and striae gravidarum, repairing after delivery, enhancing skin elasticity and whitening skin are unknown.
The camellia seed extract is extracted from camellia seeds, and camellia saponin contained in the camellia seed extract can promote the proliferation of fibroblasts, so that the yield of collagen and hyaluronic acid is increased, and the effects of promoting blood circulation and resisting saccharification are achieved.
The hibiscus syriacus extract has certain effects of repairing skin, resisting bacteria and enhancing immunity.
At present, reports of the application of the extract in wrinkle removal, skin elasticity enhancement and facial skin brightness improvement do not appear.
Disclosure of Invention
The invention aims to provide a skin care composition and a cosmetic preparation, and the skin care composition has the remarkable effects of whitening skin, removing wrinkles and striae gravidarum, repairing after delivery and enhancing skin elasticity.
In order to achieve the purpose, the invention adopts the following technical scheme: a skin care composition comprises the following components in parts by weight: 1-10 parts of camellia seed oil, 1-10 parts of camellia extract, 1-10 parts of camellia leaf extract and 1-10 parts of camellia seed extract.
Further, the hibiscus flower vinegar beverage also comprises 1-5 parts of hibiscus flower vinegar extract.
The CAMELLIA (Camellia JAPONICA) seed oil is prepared from CAMELLIA seeds by low temperature squeezing or low temperature extraction, and contains 83% oleic acid, 10% saturated fatty acid and 3% unsaturated fatty acid. It is added into makeup removing products more at day time, and endows the makeup removing products with certain skin care effect. But the efficacy of the Chinese medicinal preparation in removing wrinkles and striae gravidarum after postpartum repair is not involved. The CAMELLIA (Camellia JAPONICA) seed oil is obtained from Xiamen republic chemical industry.
The CAMELLIA (CAMELLIA JAPONICA) flower extract has certain inoxidizability, ethanol absorption inhibition effect, sugar absorption inhibition effect, gastric mucosa protection effect and platelet aggregation effect, but does not relate to the effects of removing wrinkles and striae gravidarum after postpartum repair, enhancing skin elasticity and whitening skin. The "Camellia JAPONICA (Camellia JAPONICA) flower extract" as described herein was obtained from Siam Biotech limited.
The "CAMELLIA (CAMELLIA JAPONICA) leaf extract" described herein has been disclosed to have an excellent antioxidant effect, an effect of preventing skin glycation, but it is not known how it has an effect of preventing postpartum repair of various wrinkles and stretch marks. The "Camellia JAPONICA (Camellia JAPONICA) leaf extract" as described herein was purchased from Seisano Biotechnology Ltd.
The CAMELLIA saponin extracted from the seeds of the CAMELLIA (Camellia JAPONICA) is capable of promoting the proliferation of fibroblasts, increasing the yield of collagen and hyaluronic acid, and promoting blood circulation and resisting saccharification. But does not know how it will work in post-partum repair of stretch marks. The "Camellia JAPONICA (Camellia JAPONICA) seed extract" as described herein was obtained from Western safe Olympic Biotech, Inc.
The 'hibiscus syriacus vinegar extract' is prepared by the following steps:
s1, preparing vinasse: cleaning hibiscus syriacus buds, mixing the hibiscus syriacus buds with soaked sticky rice according to the ratio of 1: 2-5, cooking for 10-20 min, cooling to room temperature, adding malt flour for saccharification for 12h, adding malt, saccharifying at 25-32 ℃ for 36-48 h, adding purified water into the obtained wine rice, and sealing at 25 ℃ for 36-72 h to obtain vinasse;
s2, fermentation: adding purified water into the vinasse obtained in the step, carrying out aerobic acetic acid fermentation at 25-28 ℃ until the pH of the detected supernatant is 4.2, separating the supernatant, curing and filtering to obtain the finished product.
The invention also aims to provide a cosmetic preparation which comprises 3-10% of the composition.
Further, the water-based paint also comprises 0.1-0.3% of thickening agent, 0.01-0.06% of antioxidant, 1-6% of surfactant and 0.1-0.5% of preservative. .
The "thickener" as used herein includes, but is not limited to, one or more of carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer and xanthan gum, preferably carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer and xanthan gum in a mass ratio of (0.1-0.14): (0.01-0.03): (0.02-0.07), and the content of the composition in the cosmetic is preferably 0.1-0.3%.
The antioxidant is selected from tocopherol acetate, and the content of the tocopherol acetate in the cosmetic is preferably 0.01-0.06%; the "surfactant" is selected from one or two of PEG-60 hydrogenated castor oil and PEG-5 glyceryl stearate, and preferably, the surfactant is prepared from PEG-60 hydrogenated castor oil and PEG-5 glyceryl stearate according to the mass ratio of (1-4): (0.2-1.5), and the content of the composition in the cosmetic is preferably 1-6%.
The preservative is phenoxyethanol, and the content of the preservative in the cosmetic is preferably 0.1-0.5%.
Further, the cosmetic preparation may further comprise a pH regulator, preferably aminomethyl propanol, which is preferably contained in the cosmetic in an amount of 0.066-0.102%.
Further, the cosmetic preparation may further comprise a metal chelating agent, preferably ED TA disodium, which is preferably contained in the cosmetic in an amount of 0.01-0.04%.
Furthermore, the cosmetic preparation can also comprise a humectant which is prepared from sodium hyaluronate, glycerin, butanediol, polyethylene glycol-32 and polyethylene glycol-6 according to the mass ratio of (0.01-0.07): (1-7): (4-10): (0.5-2): (0.5-2), and the content of the composition in the cosmetic is preferably 5-20%.
Further, in order to impart anti-inflammatory effect to the cosmetic, an anti-inflammatory agent, preferably dipotassium glycyrrhizinate, which is preferably contained in the cosmetic in an amount of 0.01-0.07%, may be further included.
Further, the cosmetic preparation can also comprise an oil and fat, wherein the oil and fat is selected from one of hydrogenated polydecene, polydimethylsiloxane, glycerol tri (ethyl hexanoate), behenyl alcohol and stearyl alcohol, and preferably the oil and fat is prepared from hydrogenated polydecene, polydimethylsiloxane, glycerol tri (ethyl hexanoate), behenyl alcohol, stearyl alcohol and petrolatum according to the mass ratio of (2-6): (1-7): (1-4): (0.1-1.2): (0.05-0.4): (1-5).
The invention has the following advantages:
the invention provides a skin care composition, which comprises camellia seed oil, a camellia extract, a camellia leaf extract, a camellia seed extract and a hibiscus syriacus vinegar extract, wherein the components are matched with each other to play a synergistic effect, so that the composition has excellent effects of removing various wrinkles, repairing after pregnancy striae, enhancing skin elasticity and whitening skin.
Detailed Description
The present invention will be described in further detail with reference to the following examples. It should not be understood that the scope of the above-described subject matter of the present invention is limited to the following examples.
Example 1 preparation of Hibiscus syriacus Vinegar extract
S1, preparing vinasse: cleaning hibiscus syriacus bud, mixing with soaked sticky rice according to a ratio of 1:3, steaming for 20min, cooling to room temperature, adding malt powder for saccharifying for 12h, adding malt yeast, saccharifying for 48h at 27 ℃, adding purified water with the weight of 3 times of that of the wine rice into the obtained wine rice, and sealing for 48h at 25 ℃ to obtain wine lees;
s2, fermentation: adding 3 times of purified water into the distiller's grains, performing aerobic acetic acid fermentation at 26 deg.C until pH is 4.2, separating supernatant, aging, and filtering.
Example 2 skin care compositions 1 to 7
Figure BDA0001948980790000051
Examples 3 to 5 cosmetic preparations
Figure BDA0001948980790000052
Figure BDA0001948980790000061
The preparation method comprises the following steps:
A) dissolving carbomer and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water at room temperature, adding EDTA disodium, sodium hyaluronate, glycerol, butanediol, polyethylene glycol-32 and polyethylene glycol-6, heating, stirring and dissolving to obtain a mixture A;
B) dispersing phenoxyethanol, dipotassium glycyrrhizinate, tocopheryl acetate and xanthan gum in butanediol to obtain a mixture B;
C) mixing the mixture A and the mixture B, and adding an aminomethyl propanol solution to obtain a water phase;
D) mixing hydrogenated polydecene, polydimethylsiloxane, glycerol tri (ethyl hexanoate), docosyl alcohol, stearyl alcohol, petrolatum, PEG-60 hydrogenated castor oil, PEG-5 glyceryl stearate and essence to obtain an oil phase, adding the oil phase into the water phase while homogenizing, cooling after homogenizing, adding the composition 2, and stirring uniformly to obtain the composition.
Comparative example 1
The difference from example 3 is that composition 1 is used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Comparative example 2
The difference from example 3 is that composition 3 was used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Comparative example 3
The difference from example 3 is that composition 4 was used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Comparative example 4
The difference from example 3 is that composition 5 was used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Comparative example 5
The difference from example 3 is that composition 6 was used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Comparative example 6
The difference from example 3 is that composition 7 was used instead of composition 2, and the remaining parameters and operation are as shown in example 3.
Test example one, wrinkle removal and skin elasticity enhancement test
140 volunteers aged 30 to 40 were recruited and randomly divided into 7 groups of 20 persons, each group was treated with the cosmetics of example 3 and comparative examples 1 to 6, and the appropriate amount of the cosmetics was applied to the left face and the right face of the face was applied with the cosmetics without the skin care composition after the face was cleaned every morning and evening, and the measurement and analysis were performed on their faces using an instrument after 28 consecutive days.
Using an instrument: skin moisture detector (CM2.1-
Figure BDA0001948980790000073
CM825), skin elasticity tester (Cutometer; courage + Khazaka), VISIA-CR (Canfield corporation). The moisture condition of the skin was measured with a skin moisture meter, and the skin elasticity was measured with a skin elasticity tester to obtain table 1. Facial brightness using VISIA-CR table 2, and facial wrinkles using VISIA-CR (which evaluates the depth and length of wrinkles for reduction) are shown in table 3.
TABLE 1 skin moisture and skin elasticity enhancement test results
Figure BDA0001948980790000071
Figure BDA0001948980790000072
Figure BDA0001948980790000081
Note: in comparison with the example 3, the method of the present invention,*P＜0.05，**P＜0.01。
table 2 facial skin brightness test results
Figure BDA0001948980790000082
Group of Skin brightness change rate (%)
Example 3 6.53±2.24
Comparative example 1 4.86±0.78*
Comparative example 2 3.05±1.35*
Comparative example 3 1.58±0.93**
Comparative example 4 4.32±1.03*
Comparative example 5 3.15±1.15*
Comparative example 6 4.21±1.62*
Note: in comparison with the example 3, the method of the present invention,*P＜0.05，**P＜0.01。
TABLE 3 skin texture test results
Figure BDA0001948980790000083
Group of Average surface wrinkle reduction amount (%) Mean wrinkle volume reduction (%)
Example 3 32.01±8.25 28.11±5.43
Comparative example 1 24.64±5.18* 21.46±4.25*
Comparative example 2 15.33±3.08** 16.47±3.39**
Comparative example 3 2.21±8.25** 1.61±1.18**
Comparative example 4 18.48±6.35** 15.16±4.26**
Comparative example 5 16.76±5.38** 13.27±3.55**
Comparative example 6 1.35±1.44** 1.89±0.35*
Note: in comparison with the example 3, the method of the present invention,*P＜0.05，**P＜0.01。
as can be seen from tables 1 to 3 above, the camellia seed oil, the camellia extract, the camellia leaf extract, the camellia seed extract and the hibiscus vinegar extract are combined to achieve a synergistic effect, the cosmetic of embodiment 3 of the invention containing the five active ingredients has the remarkable effects of removing wrinkles, enhancing skin elasticity and moisture and improving facial skin brightness, and compared with the single use of various ingredients, the cosmetic has remarkable differences (P is less than 0.05).
Test example II postpartum repair test of striae gravidarum
140 women with striae gravidarum and other healthy body indexes in the ages of 25-35 are randomly divided into 7 groups, 20 people in each group use the cosmetics in the embodiment 3 and the comparative examples 1-6 respectively, the abdomen of a subject is divided into a left area and a right area by taking the midline of the abdomen as a boundary, one striae gravidarum with similar lines and colors is selected in each area, a proper amount of cosmetics is applied to the left side in the morning and evening every day, the cosmetics without a skin care composition is applied to the right side to serve as a control group, after the cosmetic is used for 32 days, the striae gravidarum repair effect is evaluated according to evaluation criteria, the effective rate is calculated, and the results are shown in the following.
Evaluation indexes are as follows: the effect is shown: the striae gravidarum of the abdomen disappears or is obviously improved, and the range is narrowed to more than 60 percent (inclusive); the method has the following advantages: improving abdominal striae gravidarum, and reducing the range to more than 30 percent (inclusive); and (4) invalidation: the improvement of abdominal stretch marks is not significant and the reduction in range does not meet the above requirements or is not reduced.
The total effective rate (%) - (number of effective cases + number of effective cases)/number of total test cases × 100%
TABLE 4 striae gravidarum repair in the groups of subjects
Group of Number of effective cases Effective number of cases Number of invalid cases Total effective rate (%)
Example 3 13 6 1 95.0％
Comparative example 1 5 6 9 55.0％
Comparative example 2 1 3 16 20.0％
Comparative example 3 0 3 17 15.0％
Comparative example 4 2 4 14 30.0％
Comparative example 5 1 4 15 25.0％
Comparative example 6 3 1 16 20.0％
As can be seen from table 4 above, the combined use of camellia seed oil, camellia extract, camellia leaf extract, camellia seed extract and hibiscus vinegar extract has a synergistic effect on repairing postpartum striae gravidarum, the cosmetic disclosed in embodiment 3 of the invention has a repair rate of 95% for postpartum striae gravidarum, and compared with the single use of each component, the difference is large, and a significant progress is made.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Any person skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.

Claims (8)

1. The skin care composition is characterized by comprising the following components in parts by weight: 1-10 parts of camellia seed oil, 1-10 parts of camellia extract, 1-10 parts of camellia leaf extract and 1-10 parts of camellia seed extract;
the composition also comprises 1-5 parts of hibiscus syriacus vinegar extract;
the hibiscus syriacus vinegar extract is prepared by the following steps:
s1, preparing vinasse: cleaning hibiscus syriacus buds, mixing the hibiscus syriacus buds with soaked sticky rice according to the ratio of 1: 2-5, cooking for 10-20 min, cooling to room temperature, adding malt flour for saccharification for 12h, adding malt, continuing to saccharify for 36-48 h at the temperature of 25-32 ℃, adding purified water into the obtained wine rice, and sealing for 36-72 h at the temperature of 25 ℃ to obtain vinasse;
s2, fermentation: adding purified water into the vinasse obtained in the step, carrying out aerobic acetic acid fermentation at 25-28 ℃ until the pH of the detected supernatant is 4.2, separating the supernatant, curing and filtering to obtain the finished product.
2. The composition of claim 1, wherein the composition is for the removal of wrinkles.
3. The composition of claim 1, wherein the composition is used for post-pregnancy repair of stretch marks.
4. The composition of claim 1, wherein the composition is for whitening skin.
5. The composition of claim 1, wherein the composition is for enhancing skin elasticity.
6. A cosmetic preparation comprising 3 to 10% of the composition according to any one of claims 1 to 5.
7. The cosmetic preparation according to claim 6, further comprising 0.1 to 0.3% of a thickener, 0.01 to 0.06% of an antioxidant, 1 to 6% of a surfactant, and 0.1 to 0.5% of a preservative.
8. The cosmetic preparation according to claim 6 or 7, wherein the cosmetic preparation is used for removing wrinkles, postpartum repair of stretch marks, whitening the skin and enhancing skin elasticity.
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CN110559243B (en) * 2019-09-26 2022-06-28 上海清轩生物科技有限公司 Repairing and whitening composition containing camellia extract and microcapsule prepared from repairing and whitening composition
CN110804509B (en) * 2019-12-13 2021-09-21 上海清轩生物科技有限公司 Makeup-removing handmade soap and preparation method thereof
CN113509408A (en) * 2021-04-23 2021-10-19 施政宏 Skin-care composite essential oil
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