CN108969438B - Anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract and preparation method thereof - Google Patents
Anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract and preparation method thereof Download PDFInfo
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Abstract
The invention discloses anti-wrinkle cream containing bletilla striata extract, white-flowered flowering quince extract and hairyvein agrimony extract and a preparation method thereof. The addition amounts of the bletilla striata extract, the white flower common floweringquince fruit extract and the hairyvein agrimonia herb and bud extract in the anti-wrinkle cream are respectively 1.0-10 percent; the preferred content is 3% to 8.0% each, and the most preferred content is 4% to 6% each. According to the invention, the bletilla striata extract, the white flowered quince extract and the hairyvein agrimony extract are compounded and applied to the anti-wrinkle cream, the bletilla striata polysaccharide of the bletilla striata extract keeps skin moistening, the flavonoid substance of the white flowered quince extract promotes skin metabolism and the oxidation effect of the hairyvein agrimony extract on external free radicals are combined, and the anti-wrinkle cream acts on the skin in an all-round and three-dimensional manner, so that the skin is comprehensively improved, and the anti-wrinkle effect of the product is improved.
Description
Technical Field
The invention relates to a beauty skin care product, belongs to the technical field of cosmetics, and particularly relates to anti-wrinkle cream containing extracts of bletilla striata, white-flowered papaya and hairyvein agrimony and a preparation method thereof.
Background
The skin is positioned at the outermost side of the human body and consists of epidermis, dermis and subcutaneous tissues, the main function is to protect the body from being harmed by the adverse external environment, the function of the skin is weakened due to the influence of various factors such as the external environment, heredity and the like, and the aging symptom is shown, so the anti-aging cosmetic becomes one of the products urgently needed by the majority of female consumers.
Skin aging is mainly in the form of natural aging (i.e., intrinsic aging) and photoaging (i.e., extrinsic aging), which is mainly caused by body genetic factors, is limited to the whole body, and is apparently characterized by wrinkles and sagging, and pigmentation, etc. Skin aging resistance is always paid great attention by people, and related aging mechanisms and aging resistance ways are also hot spots of research of people. Skin aging is a complex multi-factor process with multiple mechanisms simultaneously participating, and aiming at the problem that an anti-aging substance generated by a single mechanism can only solve a certain link of aging, the efficient anti-aging cosmetic can be developed from multiple angles and multiple levels.
Along with the advocation of nature, environmental protection and mild concept, various natural active extracts with special characteristics are more and more favored by people.
The existing anti-aging cosmetics mainly delay aging by eliminating excessive free radicals, defending ultraviolet rays, promoting metabolism of skin cells, moisturizing and repairing barrier functions of skin, and supplementing collagen and elastin. However, the existing anti-wrinkle products have the problems of relatively single anti-aging way, unobvious efficacy, poor product stability and the like.
At present, reports on the obvious anti-wrinkle effect of the synergistic effect of the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimony extract on skin are not found.
Disclosure of Invention
The invention aims to provide anti-wrinkle cream containing bletilla striata extract, white-flowered papaya extract and hairyvein agrimonia herb extract, wherein the bletilla striata extract, the white-flowered papaya extract and the hairyvein agrimonia herb extract act on skin synergistically and can generate obvious anti-wrinkle effect.
The invention also aims to provide a preparation method of the anti-wrinkle cream containing the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimony extract, which combines the effects of keeping the bletilla striata polysaccharide of the bletilla striata extract moist and promoting the skin metabolism of flavonoid substances of the chaenomeles speciosa extract and resisting the oxidation of external free radicals of the hairyvein agrimony extract, so that the anti-wrinkle cream can be acted on the skin in a omnibearing and three-dimensional manner, the skin can be comprehensively improved, and the anti-wrinkle effect of the product can be improved.
In order to achieve the above purpose of the present invention, the present invention provides the following technical solutions:
an anti-wrinkle cream containing bletilla striata extract, a chaenomeles speciosa extract and a hairyvein agrimony extract, wherein the addition amount of the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimony extract in the anti-wrinkle cream is 1.0-10 percent respectively;
the anti-wrinkle cream comprises bletilla striata extract, a white-flowered papaya extract and a hairyvein agrimonia herb extract, wherein the addition amount of the bletilla striata extract, the white-flowered papaya extract and the hairyvein agrimonia herb extract in the anti-wrinkle cream is 3% -8.0%, and the preferable content of the bletilla striata extract, the white-flowered papaya extract and the hairyvein agrimonia herb extract is 4% -6%.
The invention relates to anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract, wherein the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimony extract can be extracting solutions; the extraction method comprises the following steps: supercritical CO2Extraction method, ultrasonic extraction method.
An anti-wrinkle cream containing bletilla striata extract, white-flowered papaya extract and hairyvein agrimonia herb and bud extract comprises the following raw material components in percentage by weight:
1-5% of glycerol, 1-5% of butanediol, 0.1-0.2% of EDTA-2Na, 0.01-0.1% of hyaluronic acid, 0.1-5% of trehalose, 0.1-3% of cetearyl glucoside, 0.1-3% of a mixture of glyceryl stearate and PEG-100 stearate, 0.1-1% of tocopheryl acetate, 0.5-3% of polydimethylsiloxane, 0.5-5% of cetearyl alcohol, 1-5% of shea butter tree, 1-10% of hydrogenated polyisobutene, 1-10% of isononyl isononanoate, 0.1-2% of a mixture of polyacrylamide C13-14 isoalkane and lauryl alcohol ether-7, 1-10% of a white flower papaya extract, 1-10% of hairyvein agrimony extract, 1-10% of bletilla striata extract, 0.01-0.1% of propyl hydroxybenzoate, 0.05-0.2% of methyl hydroxybenzoate, 0.01-0.2% of diazolidinyl urea, 0.01-0.2% of essence and the balance of deionized water.
In addition, the anti-wrinkle cream comprises bletilla striata extract, a white floweringquince extract and a hairyvein agrimony extract, and is composed of the following raw material components in percentage by weight:
5% of glycerin, 5% of butanediol, 0.1% of EDTA-2Na, 0.05% of hyaluronic acid, 1% of trehalose, 2% of cetearyl glucoside, 1% of a mixture of glyceryl stearate and PEG-100 stearate, 0.5% of tocopherol acetate, 2% of polydimethylsiloxane, 3% of cetearyl alcohol, 3% of Butyrospermum parkii, 8% of hydrogenated polyisobutene, 5% of isononyl isononanoate, 0.8% of a mixture of polyacrylamide C13-14 isoalkane and lauryl alcohol ether-7, 5% of a Cleomis quince extract, 5% of a hairyvein agrimony extract, 5% of a bletilla striata extract, 0.1% of propylhydroxybenzoate, 0.2% of methylparaben, 0.2% of diazolidinyl urea, 0.02% of essence, and the balance of deionized water.
Further, the preparation method of the anti-wrinkle cream containing the extracts of bletilla striata, chaenomeles speciosa and agrimony comprises the following steps:
1) adding water into a water phase pot, adding glycerol, butanediol, EDTA disodium, hyaluronic acid and trehalose, stirring uniformly, and heating to 80-85 deg.C;
2) adding cetearyl glucoside, glyceryl stearate, PEG-100 stearate, tocopherol acetate, polydimethylsiloxane, cetearyl alcohol, Butyrospermum parkii, hydrogenated polyisobutene, isononyl isononanoate, methylparaben and propylparaben into an oil phase pot, stirring and heating to 80-85 ℃;
3) pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, stirring uniformly, and adding polyacrylamide C13-14The isoalkane and the lauryl alcohol ether-7 are evenly stirred for 3 to 5 minutes;
4) cooling to below 45 deg.C under stirring, adding rhizoma Bletillae extract, herba Hedyotidis Diffusae extract, herba et Gemma Agrimoniae extract, diazolidinyl urea, and essence;
5) continuously stirring and cooling, discharging and filling after the inspection is qualified.
By means of the technical scheme, the invention has the following advantages and beneficial effects:
1) the invention is based on the breakthrough research of the technical level of the application of the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimonia herb extract in cosmetics, the bletilla striata extract, the chaenomeles speciosa extract and the hairyvein agrimonia herb extract are compounded and applied to anti-wrinkle cream, and the anti-wrinkle cream acts on skin in a omnibearing and three-dimensional manner, so that the skin is comprehensively improved, and the anti-wrinkle effect of the product is improved;
2) according to the invention, the bletilla striata extract, the white flowered quince extract and the hairyvein agrimony extract are compounded and applied to the anti-wrinkle cream, the bletilla striata polysaccharide of the bletilla striata extract keeps skin moistening, the flavonoid substance of the white flowered quince extract promotes skin metabolism and the oxidation effect of the hairyvein agrimony extract on external free radicals are combined, and the three-dimensional action is carried out on the skin in all directions, so that the skin is comprehensively improved, and the anti-wrinkle effect of the product is improved;
3) the invention aims to research a natural anti-wrinkle cream which can effectively delay aging, is safe and mild, and has no stimulation and side effects on skin.
Drawings
Figure 1 is a graph showing the rate of change of wrinkles after 4 weeks of continuous use.
Detailed Description
The invention discloses anti-wrinkle cream containing bletilla striata extract, white-flowered flowering quince extract and hairyvein agrimony extract and a preparation method thereof. The addition amounts of the bletilla striata extract, the white flower common floweringquince fruit extract and the hairyvein agrimonia herb and bud extract in the anti-wrinkle cream are respectively 1.0-10 percent; the preferred content is 3% to 8.0% each, and the most preferred content is 4% to 6% each.
According to the invention, the bletilla striata extract, the white flowered quince extract and the hairyvein agrimony extract are compounded and applied to the anti-wrinkle cream, the bletilla striata polysaccharide of the bletilla striata extract keeps skin moistening, the flavonoid substance of the white flowered quince extract promotes skin metabolism and the oxidation effect of the hairyvein agrimony extract on external free radicals are combined, and the anti-wrinkle cream acts on the skin in an all-round and three-dimensional manner, so that the skin is comprehensively improved, and the anti-wrinkle effect of the product is improved.
Compared with the prior art, the anti-wrinkle cream disclosed by the invention resists aging and slows down the formation of wrinkles through three different modes. Clinical experiments prove that the anti-wrinkle facial mask has obvious anti-wrinkle performance, can increase the elasticity of skin and improve the skin firmness, and is very suitable for being prepared with facial mask essence, anti-wrinkle essence and various anti-aging facial or eye cosmetics.
In addition, the anti-wrinkle cream has more obvious effects on firming, resisting wrinkles, smoothing skin and the like compared with the traditional anti-wrinkle product, and has higher market popularization value.
The anti-wrinkle cream comprises three bletilla striata extracts, a white flowered papaya extract and a hairyvein agrimony extract as effective components, and the following extraction processes are respectively adopted:
1. bletilla striata extract:
the extraction method of the bletilla striata extract comprises the following steps: pulverizing dried rhizoma bletilla into powder of about 100 meshes, and mixing the powder with a liquid-solid ratio of 1: extracting with 70% ethanol with pH of 7 at 90 deg.C under reflux for 70 min, distilling the extractive solution under reduced pressure, recovering ethanol, concentrating, and spray drying to obtain powder extract.
2. White flowered papaya extract:
the extraction method of the white flowered papaya extract comprises the following steps: crushing the dried white papaya into powder of about 100 meshes, and mixing the powder with the liquid-solid ratio of 1: 10 mass ratio, adding 70% ethanol, soaking for 12 hr, filtering to remove residue to obtain crude extractive solution, vacuum distilling at 60 deg.C, recovering ethanol, concentrating, and spray drying to obtain powder extract.
3. Extract of hairyvein agrimony:
the extraction method of the hairyvein agrimony extract comprises the following steps: pulverizing dried herba et Gemma Agrimoniae into powder of about 100 meshes, and mixing at a ratio of 1: extracting with 70% ethanol with pH of 7 at 90 deg.C under reflux for 70 min, distilling the extractive solution under reduced pressure, recovering ethanol, concentrating, and spray drying to obtain powder extract.
The anti-wrinkle cream of the present invention will be described in more detail with reference to the following specific preferred embodiments, but the present invention is not limited to the following embodiments.
The following raw material components in the following table 1 are all in the following percentages by weight.
Table 1 compositions of raw materials of examples 1 to 3 and comparative example 1 (% by weight)
The formula and the composition of the anti-wrinkle cream containing the extracts of bletilla striata, chaenomeles speciosa and agrimony shown in the table 1 are as follows:
1) adding water into a water phase pot, adding glycerol, butanediol, EDTA disodium, hyaluronic acid and trehalose, stirring uniformly, and heating to 80-85 deg.C;
2) adding cetearyl glucoside, glyceryl stearate, PEG-100 stearate, tocopherol acetate, polydimethylsiloxane, cetearyl alcohol, Butyrospermum PARKII (Butyrrospermum PARKII), hydrogenated polyisobutene, isononyl isononanoate, methylparaben, and propylparaben into an oil phase pot, stirring and heating to 80-85 deg.C;
3) firstly pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, uniformly stirring, adding polyacrylamide C13-14 isoalkane and lauryl alcohol ether-7, and uniformly stirring for 3-5 minutes;
4) stirring and cooling to below 45 deg.C, adding rhizoma Bletillae extract, fructus Chaenomelis extract, herba et Gemma Agrimoniae extract, diazolidinyl urea, and essence;
5) continuously stirring and cooling, discharging and filling after the inspection is qualified.
Examples of Effect test
The method comprises the following steps: face smoothness test.
Smoothness is one of indexes for showing skin aging, and the skin friction is tested by using a German CK (MPA 9) skin tester, and the health condition of the skin is observed through the change rate of the skin friction, as shown in figure 1.
Test samples: example 1, example 2, example 3, and comparative example.
Subject: age 45 or so, female, 20 people.
Testing parts: the face.
The scheme is as follows:
1. one week before the study began, any one of the tightening or anti-aging products was discontinued. On day 0 of study initiation, the face was cleaned, left to rest in a constant temperature and humidity environment for 20 minutes, and skin friction was measured using a german CK (MPA 9) skin tester as an initial value.
2. The 20 volunteers were divided into 4 groups of 5 persons, using the samples of examples 1, 2, 3 in groups 1, 2, 3, respectively, and the control sample (placebo without added active) in group 4. After the study began, the test samples were applied evenly to the face after cleansing the face in the morning and evening each day.
3. The skin friction was measured on days 7, 14, 21 and 28 using a german CK (MPA 9) skin tester. Before testing, the face is cleaned, and the data is tested after 20 minutes of rest in a constant-temperature and constant-humidity environment.
The test data was compared with the initial data and the rate of change of skin friction was calculated as shown in table 2 below:
TABLE 2 face smoothness test (weeks 1-4)
| Day 7 | Day 14 | Day 21 | Day 28 | |
| Group 1 | -1.25％ | -2.83％ | -4.47％ | -5.12％ |
| Group 2 | -5.21％ | -9.85％ | -13.52％ | -18.63％ |
| Group 3 | -6.36％ | -11.68％ | -18.33％ | -20.52％ |
| Group 4 | -0.32％ | -0.26％ | -0.37％ | -0.14％ |
As shown in fig. 1 and table 2, the facial friction of the test subjects in groups 1, 2, and 3 who used the product containing the added active was significantly reduced and varied more and more from the rate of change of facial skin friction, while the facial friction of the test subjects in group 4 who used the placebo without the added active was substantially unchanged.
And (4) conclusion: in the anti-wrinkle cream containing the bletilla striata extract, the white flowered papaya extract and the hairyvein agrimony extract, the skin is kept moist by virtue of the bletilla striata polysaccharide of the bletilla striata extract, the skin metabolism is promoted by virtue of flavonoids of the white flowered papaya extract, and the external free radical oxidation resistance effect of the hairyvein agrimony extract is combined, so that the anti-wrinkle cream can act on the skin in an all-round and three-dimensional manner, and can effectively delay skin aging.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (6)
1. An anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract is characterized in that:
the addition amounts of the bletilla striata extract, the white flower common floweringquince fruit extract and the hairyvein agrimonia herb and bud extract in the anti-wrinkle cream are respectively 1.0-10 percent;
the bletilla striata extract, the white flower papaya extract and the hairyvein agrimonia herb extract are extracting solutions or extracting powder; the extraction method of the bletilla striata extract comprises the following steps: pulverizing dried rhizoma bletilla into 100 mesh powder, and mixing with the following materials at a ratio of 1: 10, heating and refluxing 70% ethanol with pH of 7 at 90 deg.C for 70 min, distilling the obtained extractive solution under reduced pressure, recovering ethanol, concentrating, and spray drying to obtain powder extract;
the extraction method of the white flowered papaya extract comprises the following steps: crushing dried white papaya into powder of 100 meshes, and mixing the powder with a feed-liquid ratio of 1: 10, adding 70% ethanol, soaking for 12 hours, filtering to remove residues to obtain a crude extract, distilling under reduced pressure at 60 ℃, recovering ethanol, and finally concentrating and spray drying to obtain a powdery extract;
the extraction method of the hairyvein agrimony extract comprises the following steps: crushing dried agrimony into powder of 100 meshes, and mixing the powder and the powder according to a material-liquid ratio of 1: extracting with 70% ethanol with pH of 7 at 90 deg.C under reflux for 70 min, distilling the extractive solution under reduced pressure, recovering ethanol, concentrating, and spray drying to obtain powder extract.
2. The anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and agrimonia pilosa extract according to claim 1, characterized in that: the addition amount of the bletilla striata extract, the white flower common floweringquince fruit extract and the hairyvein agrimonia herb and bud extract in the anti-wrinkle cream is 3-8.0 percent respectively.
3. The anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and agrimonia pilosa extract according to claim 1, characterized in that: the addition amount of the bletilla striata extract, the white flower common floweringquince fruit extract and the hairyvein agrimonia herb and bud extract in the anti-wrinkle cream is respectively 4.0-6%.
4. The anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and agrimony extract as claimed in any one of claims 1-3, characterized in that the anti-wrinkle cream is composed of the following raw material components in percentage by weight:
1-5% of glycerol, 1-5% of butanediol, 0.1-0.2% of EDTA-2Na, 0.01-0.1% of hyaluronic acid, 0.1-5% of trehalose, 0.1-3% of cetearyl glucoside, 0.1-3% of a mixture of glyceryl stearate and PEG-100 stearate, 0.1-1% of tocopheryl acetate, 0.5-3% of polydimethylsiloxane, 0.5-5% of cetearyl alcohol, 1-5% of shea butter tree, 1-10% of hydrogenated polyisobutene, 1-10% of isononyl isononanoate, 0.1-2% of a mixture of polyacrylamide C13-14 isoalkane and lauryl alcohol ether-7, 1-10% of a white flower papaya extract, 1-10% of hairyvein agrimony extract, 1-10% of bletilla striata extract, 0.01-0.1% of propyl hydroxybenzoate, 0.05-0.2% of methyl hydroxybenzoate, 0.01-0.2% of diazolidinyl urea, 0.01-0.2% of essence and the balance of deionized water.
5. The anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract according to claim 4, characterized in that the anti-wrinkle cream is composed of the following raw material components in percentage by weight:
5% of glycerin, 5% of butanediol, 0.1% of EDTA-2Na, 0.05% of hyaluronic acid, 1% of trehalose, 2% of cetearyl glucoside, 1% of a mixture of glyceryl stearate and PEG-100 stearate, 0.5% of tocopherol acetate, 2% of polydimethylsiloxane, 3% of cetearyl alcohol, 3% of Butyrospermum parkii, 8% of hydrogenated polyisobutene, 5% of isononyl isononanoate, 0.8% of a mixture of polyacrylamide C13-14 isoalkane and lauryl alcohol ether-7, 5% of a Cleomis quince extract, 5% of a hairyvein agrimony extract, 5% of a bletilla striata extract, 0.1% of propylhydroxybenzoate, 0.2% of methylparaben, 0.2% of diazolidinyl urea, 0.02% of essence, and the balance of deionized water.
6. The method for preparing anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and agrimonia pilosa extract according to claim 4, comprising the steps of:
1) adding water into a water phase pot, adding glycerol, butanediol, EDTA disodium, hyaluronic acid and trehalose, stirring uniformly, and heating to 80-85 deg.C;
2) adding cetearyl glucoside, glyceryl stearate, PEG-100 stearate, tocopherol acetate, polydimethylsiloxane, cetearyl alcohol, Butyrospermum parkii, hydrogenated polyisobutene, isononyl isononanoate, methylparaben and propylparaben into an oil phase pot, stirring and heating to 80-85 ℃;
3) pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, stirring uniformly, and adding polyacrylamide C13-14The isoalkane and the lauryl alcohol ether-7 are evenly stirred for 3 to 5 minutes;
4) cooling to below 45 deg.C under stirring, adding rhizoma Bletillae extract, herba Hedyotidis Diffusae extract, herba et Gemma Agrimoniae extract, diazolidinyl urea, and essence;
5) continuously stirring and cooling, discharging and filling after the inspection is qualified.
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| CN103735659A (en) * | 2014-01-09 | 2014-04-23 | 广东幸美化妆品股份有限公司 | Preparation method and use of hairyvein agrimony effective ingredient |
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| CN103948523A (en) * | 2014-04-04 | 2014-07-30 | 广东幸美化妆品股份有限公司 | Preparation method and application of papaya effective composition |
| CN106667857A (en) * | 2017-03-08 | 2017-05-17 | 张仕英 | Preparation method of white Chinese floweringquince extract for facial mask through microwave-assisted extraction |
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