CN111467269A - Health product containing Tuber summer fungus extract and its preparation method - Google Patents
Health product containing Tuber summer fungus extract and its preparation method Download PDFInfo
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- CN111467269A CN111467269A CN202010304730.6A CN202010304730A CN111467269A CN 111467269 A CN111467269 A CN 111467269A CN 202010304730 A CN202010304730 A CN 202010304730A CN 111467269 A CN111467269 A CN 111467269A
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- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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Abstract
The invention provides a maintenance product containing a tuber muskmelon extract and a preparation method thereof, and the maintenance product containing the tuber muskmelon extract mainly comprises an orange extract, a tuber muskmelon extract, hydrolyzed collagen, various amino acids, moisturizing, thickening and emulsifying components. According to the invention, three active substances of hydrolyzed collagen, orange extract and summer truffle extract are added into the care product, and components with moisturizing, thickening and emulsifying functions of a specific combination are matched and activated in a mutual cooperation manner, so that the care product can simultaneously exert excellent antioxidant, whitening and moisturizing functions.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a maintenance product containing a tuber muskmelon extract and a preparation method thereof.
Background
With the improvement of living standard, people pay more and more attention to skin care, and various skin care products with the functions of moisturizing, resisting oxidation and the like become essential products for most people. Most skin care products mainly comprise emulsifiers, humectants, emollients, essences, thickeners, preservatives and the like, and various special active substances are also blended into the skin care products in order to endow a certain special effect. The raw materials of the wrinkle-removing and anti-aging cosmetic provided by CN104856928A mainly comprise 1-3% of emulsifier, 5-15% of humectant, 5-15% of emollient, 2-6% of active matter and the balance of water, wherein the active matter is selected from a mixture of trifluoroacetyl tripeptide-2, glycerol and glucan, an echinacea extract and a white truffle extract. CN110575410A discloses a cosmetic, which comprises cetyl alcohol, glycerol stearate, PEG-75 stearate, butylene glycol, propylene glycol, hyaluronic acid and other emulsifiers, thickeners and substances with skin moistening effect, and is matched with certain active extracts such as hydrolytic yeast extract, yeast fermentation product filtrate, millettia leaf/stem extract, camellia extract and the like to obtain certain effects of relieving skin dryness, repairing damaged skin cuticle and the like. However, in actual detection and use, the antioxidant, whitening and moisturizing performances of the cosmetics of CN104856928A and CN110575410A are still weak, and the requirements are difficult to meet.
Disclosure of Invention
The invention aims to provide a maintenance product containing a tuber muskmelon extract and a preparation method thereof, and the maintenance product has excellent antioxidant, whitening and moisturizing functions.
The technical scheme adopted by the invention is as follows:
a health product containing Tuber summer fungus extract comprises A, B, C, D, E, F components;
wherein the raw materials of the component A comprise: glyceryl stearate SE, ceteth-25, PEG-5 glyceryl stearate, ozokerite, cetyl alcohol, stearyl alcohol, stearic acid, hydrogenated coconut oil glycerides, jojoba esters, petrolatum, glyceryl tri (ethylhexanoate), isostearyl isostearate, rice bran oil, propylheptyl caprylate, beeswax;
the component B comprises the following raw materials: water, carbomer;
the raw materials of the component C comprise: water, phenoxyethanol, glycerol, pigment water, EDTA disodium, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, and PEG-60 glyceryl isostearate;
the component D comprises the following raw materials: water, triethanolamine;
the raw materials of the component E comprise: 3-O-ethyl ascorbic acid, hydrolyzed collagen, Citrus junos fruit extract, amino acids and/or amino acid derivatives, hydroxyphenylpropionamide benzoic acid, Tuber Marie extract, water;
the raw materials of the component F comprise: cetyl N-palmitoyl hydroxyproline, retinol and essence.
Preferably, the maintenance product containing the tuber muskmelon extract consists of A, B, C, D, E, F components, wherein the components comprise the following raw materials in parts by mass:
the raw materials of the component A comprise: 2-3 parts of glyceryl stearate SE, 1-2 parts of ceteth-25, 1-2 parts of PEG-5 glyceryl stearate, 0-2 parts of ozokerite, 0-2 parts of cetyl alcohol, 0-2 parts of stearyl alcohol, 0-2 parts of stearic acid, 4-6 parts of hydrogenated coconut oil glyceride, 2-4 parts of jojoba esters, 1-3 parts of petrolatum, 7-9 parts of glycerol tri (ethyl hexanoate), 1-3 parts of isostearyl alcohol isostearate, 1-3 parts of rice bran oil, 5-7 parts of caprylic propyl heptyl ester and 0-2 parts of beeswax;
the component B comprises the following raw materials: 10-20 parts of water and 0-2 parts of carbomer;
the raw materials of the component C comprise: 10-20 parts of water, 8-12 parts of 4% phenoxyethanol, 1-3 parts of glycerol, 0-2 parts of pigment water, 0-2 parts of EDTA disodium, 10-15 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 1-2 parts of PEG-60 glycerol isostearate;
the component D comprises the following raw materials: 1-3 parts of water and 0-2 parts of triethanolamine;
the raw materials of the component E comprise: 0-1 part of 3-O-ethyl ascorbic acid, 0-1 part of hydrolyzed collagen, 0-1 part of orange fruit extract, 0-2 parts of amino acid and/or amino acid derivative, 0-1 part of hydroxyphenylpropionamide benzoic acid, 0.1-2 parts of truffle extract and 1-3 parts of water;
the raw materials of the component F comprise: 0-1 part of N-palmitoyl hydroxyproline cetyl esters, 0-1 part of retinol and 0-1 part of essence.
More preferably, the maintenance product containing the tuber muskmelon extract comprises A, B, C, D, E, F components, wherein the A, B, C, D, E, F components comprise the following raw materials in parts by mass:
the raw materials of the component A comprise: 2-3 parts of glyceryl stearate SE, 1-2 parts of ceteth-25, 1-2 parts of PEG-5 glyceryl stearate, 0-2 parts of ozokerite, 0-2 parts of cetyl alcohol, 0-2 parts of stearyl alcohol, 0-2 parts of stearic acid, 4-6 parts of hydrogenated coconut oil glyceride, 2-4 parts of jojoba esters, 1-3 parts of petrolatum, 7-9 parts of glycerol tri (ethyl hexanoate), 1-3 parts of isostearyl alcohol isostearate, 1-3 parts of rice bran oil, 5-7 parts of caprylic propyl heptyl ester and 0-2 parts of beeswax;
the component B comprises the following raw materials: 10-20 parts of water and 0-2 parts of carbomer;
the raw materials of the component C comprise: 10-20 parts of water, 8-12 parts of 4% phenoxyethanol, 1-3 parts of glycerol, 0-2 parts of pigment water, 0-2 parts of EDTA disodium, 10-15 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 1-2 parts of PEG-60 glycerol isostearate;
the component D comprises the following raw materials: 1-3 parts of water and 0-2 parts of triethanolamine;
the raw materials of the component E comprise: 0-1 part of 3-O-ethyl ascorbic acid, 0.1-0.2 part of hydrolyzed collagen, 0.1-0.2 part of orange fruit extract, 0-2 parts of amino acid and/or amino acid derivative, 0-1 part of hydroxyphenylpropionamide benzoic acid, 1-1.5 parts of tuber pinellia extract and 1-3 parts of water;
the raw materials of the component F comprise: 0-1 part of N-palmitoyl hydroxyproline cetyl esters, 0-1 part of retinol and 0-1 part of essence.
The amino acid is at least one of glycine, alanine, proline, serine, threonine and arginine.
The amino acid derivative is at least one selected from the group consisting of sodium PCA and betaine.
The raw material of the component E also comprises sorbitol.
A method for preparing a health product containing Tuber summer fungus extract comprises the following steps:
(1) mixing the raw materials of the component A, and heating to 70-100 ℃;
(2) dispersing carbomer in the component B into water of the component B;
(3) mixing the raw materials of the component C, and heating to 70-100 ℃;
(4) stirring and dissolving the raw materials of the component D uniformly;
(5) sequentially weighing the raw materials of the component E for later use;
(6) sequentially weighing the raw materials of the component F for later use;
(7) heating the component B to 70-100 ℃ after mixing, then adding the component A and the component C, vacuumizing, and emulsifying; and cooling to 40-50 ℃, adding the component D, the component E and the component F, uniformly stirring, cooling to 30-35 ℃, and discharging.
In the step (7), the vacuum degree in the vacuumizing process is-600 to-400 mPa.
In the step (7), the emulsifying time is 5-10 min.
In the step (7), the stirring speed during emulsification is 3000-3500 r/min.
In the maintenance product, the hydrolyzed collagen contains hydrophilic natural moisturizing factors and triple-helix structures, can strongly lock moisture, protect the skin to maintain a moist and tender state, and can keep the moisture content of the skin so as to keep the skin glossy; the molecules of the hydrolyzed collagen are small and are very easy to be absorbed by the skin, the absorbed hydrolyzed collagen is filled between the dermis of the skin to help increase the tightness of the skin, generate skin tension and reduce pores of the skin, so that the skin becomes tight and elastic, meanwhile, the dermis containing a plump hydrolyzed collagen layer can support skin cells, and the effects of fading fine lines and stretching coarse lines can be achieved by combining the moisture-preserving type of the hydrolyzed collagen. In addition, hydrolyzed collagen can well permeate into the skin bottom layer, has good affinity with surrounding tissues, can assist cells to prepare hydrolyzed collagen, promotes the normal growth of cells in the skin, and has the function of skin repair.
The Citrus junos extract has good cell proliferation activity and high safety. The 3-O-ethyl ascorbic acid ether is a derivative of vitamin C, can inhibit the generation of tyrosinase, thereby inhibiting the generation of melanin, and has effects of whitening skin and removing speckle.
The Prunellae Spica extract, i.e. black truffle extract, has effects of inhibiting tyrosinase activity in melanocyte, inhibiting melanin synthesis, and whitening skin.
Hydroxyphenylpropionamide benzoic acid, having multifunctional anti-inflammatory activity, comprising inhibiting the degradation of keratinized nuclear factor directly associated with inflammation, preventing the phosphorylation of the protein subunit of the nuclear factor, thereby blocking the process of cellular inflammation; reducing the occurrence of inflammatory immune response and the reaction of neurodermatitis in the skin. Has multiple effects of resisting histamine, oxidation, irritation, inflammation, erythema and the like, and has good effects on relieving pruritus, irritation, redness and the like of sensitive skin.
Compared with the prior art, the hydrolyzed collagen, the orange extract and the summer truffle extract are added into the care product, and are matched with the components with the moisturizing, thickening and emulsifying functions in a specific combination to be mutually activated in a synergistic manner, so that the care product can simultaneously exert excellent antioxidant, whitening and moisturizing functions.
Detailed Description
The technical scheme of the invention is further explained by combining the embodiment.
Example 1
The embodiment provides a maintenance product containing a tuber muskmelon extract, which consists of A, B, C, D, E, F components, and the raw materials of the components are shown in the following table 1:
TABLE 1 raw materials and their ratio of health product containing Tuber summer fungus extract
The preparation method of the maintenance product containing the truffle extract comprises the following steps:
(1) sequentially adding the component A into an oil phase pot, stirring and heating to 80 ℃, and preserving heat for 10 min;
(2) scattering carbomer in the component B into water of the component B, and soaking until no white particles exist;
(3) sequentially adding the component C into an emulsifying pot, stirring and heating to 80 ℃, and preserving heat for 10 min;
(4) stirring and dissolving the component D uniformly;
(5) weighing the component E in turn for later use;
(6) sequentially weighing the component F for later use;
(7) adding the component B into an emulsifying pot, stirring and heating to 80 ℃; pumping the component A and the component C into an emulsifying pot, vacuumizing to-500 mPa, uniformly stirring (20r/min), emulsifying (3200r/min) for 5min, starting cooling water to cool, cooling to 45 ℃, adding the component D, uniformly stirring, sequentially adding the component E, F, uniformly stirring, continuously cooling to 35 ℃, and discharging.
Example 2
The embodiment provides a maintenance product containing a tuber muskmelon extract, which consists of A, B, C, D, E, F components, and the raw materials of the components are shown in the following table 2:
TABLE 2 materials and their ratio of health product containing Tuber summer fungus extract
The preparation method of the cosmetic containing the truffle extract of the present example was the same as that of example 1.
Comparative example 1
The comparative example provides a maintenance product, which mainly increases the proportion of hydrolyzed collagen and orange extract compared with the examples 1 and 2, and specifically comprises the following raw materials:
TABLE 3 raw materials of health product and their mixture ratio
The comparative example maintenance article was prepared in the same manner as in example 1.
Comparative example 2
This comparative example differs from example 1 in that hydrolyzed collagen was omitted.
Comparative example 3
This comparative example differs from example 1 in that the orange extract was omitted.
Comparative example 4
This comparative example differs from example 1 in that the tuber summer fungus extract is omitted.
And (3) performance testing:
(1) antioxidant activity
Antioxidant activity [ AOA (antioxidant activity) ] expressed in terms of the coulomb dose titrated to 100g of the material analyzed for the treatments of examples 1 and 2 and comparative examples (kCb/100g), results are shown in Table 4:
TABLE 4 antioxidant Activity of maintenance products
As can be seen from Table 4, the maintenance articles of examples 1 and 2 and the comparative example have higher AOA values, wherein the AOA values of examples 1 and 2 are obviously higher than those of the comparative example and are also significantly higher than those of CN110575410A (265.8 and 266.3) in the prior art, which indicates that the maintenance article of the invention has good antioxidant activity and can effectively scavenge free radicals.
(2) Skin complexion
Skin complexion L values were tested using a Colorimeter C L400 manufactured by Courage Khazaka (CK) of germany, and the effect of the treatment on skin radiance was evaluated by measuring the change in skin L values before and after use of the product.
Specifically, three groups of volunteers having the same average starting L value (skin tone L value before use of the treatment product) were selected for the test, 10 persons per group, the subjects were rubbed twice daily with the treatment products of examples 1 and 2 and comparative example, after four weeks, the skin tone L values of the subjects were tested and the results were averaged and are shown in Table 5:
TABLE 5 Effect of skin Care on skin tone
| Example 1 | Example 2 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
| 0 week | 45.0 | 45.0 | 45.0 | 45.0 | 45.0 | 45.0 |
| 4 weeks | 54.3 | 54.9 | 52.3 | 50.3 | 49.9 | 49.8 |
As is clear from Table 5, the skin color of the skin care products of examples 1 and 2 and the skin care products of comparative examples were clearly highlighted after four weeks of use as compared with the skin color L before use, and among them, the skin color L of the skin care products of examples 1 and 2 was higher, so that the skin color could be more effectively highlighted and the skin whitening effect could be achieved.
(3) Degree of skin hydration
Skin hydration was measured to have the same starting mean for three groups of 10 subjects over a four week period, and the results averaged, as in table 6:
TABLE 6 Effect of skin Care on skin hydration
| Example 1 | Example 2 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
| 0 week | 23.0 | 23.0 | 23.0 | 23.0 | 23.0 | 23.0 |
| 4 weeks | 34.2 | 35.2 | 33.5 | 29.2 | 29.9 | 28.5 |
As can be seen from Table 6, the skin hydration levels were improved in the care products of examples 1 and 2 and the comparative example after four weeks of use, wherein the skin hydration levels were improved more in the care products of examples 1 and 2, and the moisture was locked more effectively, resulting in a better moisturizing effect.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (10)
1. A cosmetic containing a Tuber summer fungus extract, which is characterized in that: consists of A, B, C, D, E, F components;
wherein the raw materials of the component A comprise: glyceryl stearate SE, ceteth-25, PEG-5 glyceryl stearate, ozokerite, cetyl alcohol, stearyl alcohol, stearic acid, hydrogenated coconut oil glycerides, jojoba esters, petrolatum, glyceryl tri (ethylhexanoate), isostearyl isostearate, rice bran oil, propylheptyl caprylate, beeswax;
the component B comprises the following raw materials: water, carbomer;
the raw materials of the component C comprise: water, phenoxyethanol, glycerol, pigment water, EDTA disodium, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, and PEG-60 glyceryl isostearate;
the component D comprises the following raw materials: water, triethanolamine;
the raw materials of the component E comprise: 3-O-ethyl ascorbic acid, hydrolyzed collagen, Citrus junos fruit extract, amino acids and/or amino acid derivatives, hydroxyphenylpropionamide benzoic acid, Tuber Marie extract, water;
the raw materials of the component F comprise: cetyl N-palmitoyl hydroxyproline, retinol and essence.
2. The cosmetic composition according to claim 1, wherein the cosmetic composition comprises: the maintenance product containing the truffle extract comprises A, B, C, D, E, F components, wherein the components comprise the following raw materials in parts by mass:
the raw materials of the component A comprise: 2-3 parts of glyceryl stearate SE, 1-2 parts of ceteth-25, 1-2 parts of PEG-5 glyceryl stearate, 0-2 parts of ozokerite, 0-2 parts of cetyl alcohol, 0-2 parts of stearyl alcohol, 0-2 parts of stearic acid, 4-6 parts of hydrogenated coconut oil glyceride, 2-4 parts of jojoba esters, 1-3 parts of petrolatum, 7-9 parts of glycerol tri (ethyl hexanoate), 1-3 parts of isostearyl alcohol isostearate, 1-3 parts of rice bran oil, 5-7 parts of caprylic propyl heptyl ester and 0-2 parts of beeswax;
the component B comprises the following raw materials: 10-20 parts of water and 0-2 parts of carbomer;
the raw materials of the component C comprise: 10-20 parts of water, 8-12 parts of 4% phenoxyethanol, 1-3 parts of glycerol, 0-2 parts of pigment water, 0-2 parts of EDTA disodium, 10-15 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 1-2 parts of PEG-60 glycerol isostearate;
the component D comprises the following raw materials: 1-3 parts of water and 0-2 parts of triethanolamine;
the raw materials of the component E comprise: 0-1 part of 3-O-ethyl ascorbic acid, 0-1 part of hydrolyzed collagen, 0-1 part of orange fruit extract, 0-2 parts of amino acid and/or amino acid derivative, 0-1 part of hydroxyphenylpropionamide benzoic acid, 0.1-2 parts of truffle extract and 1-3 parts of water;
the raw materials of the component F comprise: 0-1 part of N-palmitoyl hydroxyproline cetyl esters, 0-1 part of retinol and 0-1 part of essence;
the amount of each raw material is different from 0.
3. The cosmetic composition according to claim 2, wherein the extract of truffle is selected from the group consisting of: the maintenance product containing the truffle extract comprises A, B, C, D, E, F components, wherein the components comprise the following raw materials in parts by mass:
the raw materials of the component A comprise: 2-3 parts of glyceryl stearate SE, 1-2 parts of ceteth-25, 1-2 parts of PEG-5 glyceryl stearate, 0-2 parts of ozokerite, 0-2 parts of cetyl alcohol, 0-2 parts of stearyl alcohol, 0-2 parts of stearic acid, 4-6 parts of hydrogenated coconut oil glyceride, 2-4 parts of jojoba esters, 1-3 parts of petrolatum, 7-9 parts of glycerol tri (ethyl hexanoate), 1-3 parts of isostearyl alcohol isostearate, 1-3 parts of rice bran oil, 5-7 parts of caprylic propyl heptyl ester and 0-2 parts of beeswax;
the component B comprises the following raw materials: 10-20 parts of water and 0-2 parts of carbomer;
the raw materials of the component C comprise: 10-20 parts of water, 8-12 parts of 4% phenoxyethanol, 1-3 parts of glycerol, 0-2 parts of pigment water, 0-2 parts of EDTA disodium, 10-15 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 1-2 parts of PEG-60 glycerol isostearate;
the component D comprises the following raw materials: 1-3 parts of water and 0-2 parts of triethanolamine;
the raw materials of the component E comprise: 0-1 part of 3-O-ethyl ascorbic acid, 0.1-0.2 part of hydrolyzed collagen, 0.1-0.2 part of orange fruit extract, 0-2 parts of amino acid and/or amino acid derivative, 0-1 part of hydroxyphenylpropionamide benzoic acid, 1-1.5 parts of tuber pinellia extract and 1-3 parts of water;
the raw materials of the component F comprise: 0-1 part of N-palmitoyl hydroxyproline cetyl esters, 0-1 part of retinol and 0-1 part of essence;
the amount of each raw material is different from 0.
4. The cosmetic composition according to any one of claims 1 to 3, which comprises the extract of Tuber Marie belonging to genus Tuber of summer: the amino acid is at least one of glycine, alanine, proline, serine, threonine and arginine.
5. The cosmetic composition according to claim 4, wherein the cosmetic composition comprises: the amino acid derivative is at least one selected from the group consisting of sodium PCA and betaine.
6. The cosmetic preparation containing a truffle extract according to any one of claims 1 to 3, wherein: the raw material of the component E also comprises sorbitol.
7. A method for producing a cosmetic containing a Tuber summer fungus extract according to any one of claims 1 to 6, wherein the method comprises the steps of: the method comprises the following steps:
(1) mixing the raw materials of the component A, and heating to 70-100 ℃;
(2) dispersing carbomer in the component B into water of the component B;
(3) mixing the raw materials of the component C, and heating to 70-100 ℃;
(4) stirring and dissolving the raw materials of the component D uniformly;
(5) sequentially weighing the raw materials of the component E for later use;
(6) sequentially weighing the raw materials of the component F for later use;
(7) heating the component B to 70-100 ℃ after mixing, then adding the component A and the component C, vacuumizing, and emulsifying; and cooling to 40-50 ℃, adding the component D, the component E and the component F, uniformly stirring, cooling to 30-35 ℃, and discharging.
8. The method according to claim 7, wherein: in the step (7), the vacuum degree in the vacuumizing process is-600 to-400 mPa.
9. The method according to claim 7, wherein: in the step (7), the emulsifying time is 5-10 min.
10. The method according to claim 7, wherein: in the step (7), the stirring speed during emulsification is 3000-3500 r/min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010304730.6A CN111467269A (en) | 2020-04-17 | 2020-04-17 | Health product containing Tuber summer fungus extract and its preparation method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114848542A (en) * | 2022-06-01 | 2022-08-05 | 中森优品(广州)生物科技有限公司 | Black truffle cosmetic composition, black truffle face cream and preparation method thereof |
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2020
- 2020-04-17 CN CN202010304730.6A patent/CN111467269A/en active Pending
Non-Patent Citations (1)
| Title |
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| 安婕妤化妆品科技股份有限公司: "安婕妤臻美金纯赋活霜", 《国产非特殊用途化妆品备案信息服务平台》 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114848542A (en) * | 2022-06-01 | 2022-08-05 | 中森优品(广州)生物科技有限公司 | Black truffle cosmetic composition, black truffle face cream and preparation method thereof |
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Application publication date: 20200731 |