CN110200872A - A kind of body care composition of water phase and an oil phase and preparation method thereof - Google Patents

A kind of body care composition of water phase and an oil phase and preparation method thereof Download PDF

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Publication number
CN110200872A
CN110200872A CN201910598445.7A CN201910598445A CN110200872A CN 110200872 A CN110200872 A CN 110200872A CN 201910598445 A CN201910598445 A CN 201910598445A CN 110200872 A CN110200872 A CN 110200872A
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oil
phase
water phase
parts
care composition
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王文扬
姜春鹏
成浩楠
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Shanghai Lurui Biotechnology Co Ltd
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Shanghai Lurui Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/03Liquid compositions with two or more distinct layers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/007Preparations for dry skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
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  • Microbiology (AREA)
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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to skin care fields, and in particular to a kind of body care composition and preparation method thereof of water phase and an oil phase.It includes oil phase and water phase that the body care composition of the water phase and an oil phase, which prepares raw material,;The oil mutually includes the base oil of 10~60 parts by weight and the vegetable oil of 10~50 parts by weight;The oil is mutually and the weight ratio of water phase is 1:(0.1~9).The composition is compared with prior art during the preparation process without heating, and the operation such as emulsifying, simple process, low energy consumption, environmentally protective;One spray one brush, it is easy to use;A kind of new skin-protection product form, two layers of water oil shake up and are used in mixed way, and restore double-deck after standing, can be more fully by percutaneous absorption;Without adding emulsifier, grease can be atomized into droplet, skin is made to be easier to absorb;Help adjusts that skin water and oil balance, skin sense is not clearly sticky, infiltration rate is fast, and oil residue is low;Long-acting moisturizing persistently moistens, dry skin peeling, fine and smooth pore etc. is effectively relieved.

Description

A kind of body care composition of water phase and an oil phase and preparation method thereof
Technical field
The present invention relates to skin care fields, and in particular to body care composition and its preparation side to a kind of water phase and an oil phase Method.
Background technique
Common body care product generally has essential oil and two kinds of lotion/frost on the market, for moistening dry skin, moisturizing Moisturizing.And all there is respective shortcoming in two kinds of body care products.Body care essential oil, moisturizing effect is good, but using upper There is also some problems, such as nursing essential oil to belong to oily mater, and surface tension is big, can form a tunic in skin surface, inhale Receive situations such as speed is slow not to be absorbed even, and fat residue sense is strong, and skin sense is greasy, easily contamination clothing, some even result in bored acne;It is right In body lotion, for opposite essential oil, oil residue is relatively smaller, more preferable to absorb, but body lotion is in use, and spreadability can poor one Point, it is not easy to apply, it is easy to produce glutinous soapy feeling, and the production technology of most of lotion requires to heat, the processes such as emulsifying are numerous It is trivial and energy consumption is high;For the people vigorous for chaeta, essential oil and body lotion are all easy to cause hair to paste on skin, cause flesh Skin is uncomfortable.
For example, patent CN103340802A is a kind of by water phase and the oil mutually face cream body that is formed of reconciliation, including A agent and B agent, A agent is individually present before use with B agent, and when use mixes.Wherein: A agent includes Essence, and B agent includes several essential oil and table Face activating agent;The surfactant includes one or both of isosteareth and Avocado Oil;When A agent and B agent are according to one Certainty ratio is placed in vessel, and is cooperated uniform stirring to generate emulsification and answered, and about 1~2min forms a kind of cream that light is stable Body.The technological invention patent, although can solve essential oil is not easy absorbed problem, needed in system addition emulsifier, and Also needing to be mixed emulsify before use uniformly just can be used, and product uses cumbersome and inconvenient.In addition, absorbing emulsions are fast Degree is slow, and hair is easy to cause to paste on skin.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of body care composition with water phase and an oil phase, Preparing raw material includes oil phase and water phase;The oil mutually includes the base oil of 10~60 parts by weight and the plant of 10~50 parts by weight Oil;The oil is mutually and the weight ratio of water phase is 1:(0.1~9).
As a kind of perferred technical scheme, the base oil is in alkanes, lightweight silicone oil, aliphatic ester/ethers At least one.
As a kind of perferred technical scheme, the base oil is selected from lauric alcohol-caprylate/decylate, C11~C19 alkane Hydro carbons and its isomers, saualane, isononyl isononanoate, carbonic acid dioctyl ester, dicaprylyl ether, pentaerythrite (thylhexoic acid) ester, Two heptanoate of neopentyl glycol, diethyl hexylcarbonate, sad Propylheptyl, dipropylene, octyl dodecanol nutmeg One of acid esters, Parleam, white oil, dimethyl silicone polymer, octyl dimethyl silicone polymer are a variety of.
As a kind of perferred technical scheme, the base oil is the mixing of lauric alcohol-caprylate/decylate and saualane Object, weight ratio are (2~4): 1.
As a kind of perferred technical scheme, the vegetable oil is selected from sunflower seed oil, jojoba oil, macadamia nut oil, camellia One of seed oil, apricot kernel oil, grape seed oil, apple oil, hippophae rhamnoides fruit oil, soybean oil, Tujue's rose caul-fat are a variety of.
As a kind of perferred technical scheme, the vegetable oil is the mixture of sunflower seed oil and jojoba oil;It is described The weight ratio of jojoba oil and sunflower seed oil is 1:(6~9).
As a kind of perferred technical scheme, the water phase, by percentage to the quality, including moisturizer 0.5~20%, chlorine Change sodium 0.1~1.0%, preservative 0.5~5.0%, balance deionized water;The viscosity of the water phase is no more than 1000cst.
As a kind of perferred technical scheme, the moisturizer be selected from glycerol, Sodium Hyaluronate, trehalose, tremella polysaccharides, Ethoxy urea, glycine betaine, allantoin, tamarind seed polysaccharide, diglycerol, potentilla anserina extract, hippophae rhamnoides, the leaf of bamboo extract One of object, Radix et Caulis Opuntiae Dillenii extract, Mi Luomu extract, arginine are a variety of.
As a kind of perferred technical scheme, the moisturizer is Sodium Hyaluronate, glycerol, glycine betaine, cactus extraction The mixture of object, wherein the weight ratio of the glycine betaine, Radix et Caulis Opuntiae Dillenii extract and glycerol is 1:(0.8~1.5): (1.5~ 3)。
As a kind of perferred technical scheme, the raw material of the oily phase further includes the auxiliary agent of 0.05~5 parts by weight;It is described to help Agent is selected from one of antioxidant, ultraviolet absorbing agent, stabilizer, pH adjusting agent or a variety of.
Body care composition provided in the present invention with water phase and an oil phase has many merits compared with the prior art. For example, the operation such as emulsifying, simple process, low energy consumption, environmentally protective without heating in preparation process;One spray one brush, It is easy to use;A kind of new skin-protection product form, two layers of water oil shake up and are used in mixed way, and restore double-deck after standing, can be more comprehensively By percutaneous absorption;Without adding emulsifier, grease can be atomized into droplet, skin is made to be easier to absorb;Help adjuster Skin water and oil balance, skin sense is not clearly sticky, infiltration rate is fast, and oil residue is low;Long-acting moisturizing is persistently moistened, is effectively relieved Dry skin peeling, fine and smooth pore etc..
Detailed description of the invention
Fig. 1 is dermatoglyph figure of the composition in the embodiment of the present invention 6 using preceding subject.
Fig. 2 is dermatoglyph figure of the composition in the embodiment of the present invention 6 using rear subject.
Specific embodiment
It is further clear, complete that the technical characteristic work in technical solution is provided to the present invention With reference to embodiment Description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this Embodiment in invention, every other reality obtained by those of ordinary skill in the art without making creative efforts Example is applied, shall fall within the protection scope of the present invention.
Those skilled in the art of the present technique are appreciated that unless otherwise defined, all terms used herein (including technology art Language and scientific term) there is meaning identical with the general understanding of those of ordinary skill in fields of the present invention.Should also Understand, those terms such as defined in the general dictionary, which should be understood that, to be had and the meaning in the context of the prior art The consistent meaning of justice, and unless defined as here, it will not be explained in an idealized or overly formal meaning.
Word " preferred ", " preferably ", " preferred " in the present invention etc. refer to, can provide certain in some cases The embodiment of the present invention of a little beneficial effects.However, other embodiments may also under identical circumstances or in the case of other It is preferred.In addition, not implying that other embodiments are unavailable to the statement of one or more preferred embodiments, it is not yet It is intended to exclude other embodiments except the scope of the present invention.
In order to solve the above-mentioned technical problems, the present invention provides a kind of body care compositions with water phase and an oil phase, should Composition is stood two layers of the time-division, and upper oil phase, lower layer's water phase, interface is clear, and when use shakes up mixing, usable spraying pump head into Row atomization, forms small drop, is sprayed on skin surface, easy to use, is easy to absorb, and non-greasy is not sticky, persistently protects It is wet, simple process, without heating and emulsifying, low energy consumption, environmental protection.
The raw material for preparing of the composition includes oil phase and water phase;The oil mutually includes the base oil and 10 of 10~60 parts by weight The vegetable oil of~50 parts by weight;The oil is mutually and the weight ratio of water phase is 1:(0.1~9).
It can be rapidly absorbed to make product when in use, it is necessary to assure Material can be atomized into very tiny drop, To which the ratio of water phase and an oil phase is also required to control in certain range, and it cannot contain or can only contain on a small quantity macromolecule in system Otherwise weight polymers will lead to stifled pump or be atomized bad.
Preferably, the oil is mutually and the weight ratio of water phase is 1:(0.8~2).
The body care composition in the present invention can pass through method system well-known to those skilled in the art It is standby to obtain, such as can be carried out according to following operation:
1. successively adding oily phase each component to be uniformly mixed;
2. successively addition water phase each component is uniformly mixed;
3. grease mutually carries out in filling to same packaging material by a certain percentage.
It is found by the applicant that needing to guarantee that water phase and oil can mutually form apparent layering to improve synthesis effect of composition Interface, and after shaking up mixing, it can continue to restore two layer interface in a short time, two-phase is independent of each other;And shake up mixing after can It is atomized into very tiny liquid pearl by pump head, is rapidly absorbed when to guaranteeing use, salubrious non-greasy;Composition at the same time Guarantee that there is certain moisture feeling and moistening effect, it is therefore desirable to the phase in base oil, vegetable oil and the water phase in oily phase Ingredient is answered to carry out particular determination.
In some embodiments, the base oil in alkanes, lightweight silicone oil, aliphatic ester/ethers at least It is a kind of.
Do not do particular determination as alkanes base oil, including but not limited to C10~C30 alkanes and its isomers, Saualane, monocycle alkane, bicyclic alkane, polycyoalkane, Parleam, white oil etc..
Particular determination, including but not limited to dimethicone, methyl-silicone oil, second are not done as lightweight silicone oil base oil Base silicone oil, phenyl silicone oil, Methyl Hydrogen Polysiloxane Fluid, methyl phenyl silicone oil, methylchlorophenyl silicone oil, MethylethoxylsiliconFluid Fluid, methyl Trifluoro propyl silicone oil, methyl vinyl silicon oil, methylhydroxy silicone oil, ethyl containing hydrogen silicone oil, hydroxyl hydrogen silicone oil, containing nitrile silicone, Dimethyl silicone polymer, X 2-1401, octyl dimethyl silicone polymer etc..
Particular determination is not done as aliphatic ester/ethers base oil, including but not limited to lauric alcohol-caprylate/capric acid Ester, isononyl isononanoate, carbonic acid dioctyl ester, dicaprylyl ether, pentaerythrite (thylhexoic acid) ester, two heptanoate of neopentyl glycol, carbon It is sour ethylhexyl, sad Propylheptyl, dipropylene, octyl dodecanol myristinate, stearine, sweet Oily oleate, stearic lauryl ester, behenyl alcohol behenic acid ester, C10-18 resin acid triglyceride, diisopropyl sebacate etc..
Preferably, the base oil is selected from lauric alcohol-caprylate/decylate, C11~C19 alkanes and its isomers, angle Shark alkane, isononyl isononanoate, carbonic acid dioctyl ester, dicaprylyl ether, pentaerythrite (thylhexoic acid) ester, two heptanoate of neopentyl glycol, Diethyl hexylcarbonate, sad Propylheptyl, dipropylene, octyl dodecanol myristinate, Parleam, One of white oil, dimethyl silicone polymer (< 100cst), octyl dimethyl silicone polymer are a variety of.
It is further preferred that the base oil is lauric alcohol-caprylate/decylate and saualane mixture, weight Ratio is (2~4): 1.
Heretofore described lauric alcohol-caprylate/decylate is lauric alcohol, octanoic acid, capric acid as monomer and passes through esterification instead The compound that should be obtained, wherein being not particularly limited to the molar ratio between each monomer.Lauric alcohol-octanoic acid in the present invention Ester/decylate can be obtained from purchase on the market, can also be obtained by oneself synthesis.It is commercially available to transport Chemical trade from Shanghai ancient cooking vessel Co., Ltd, the trade mark are the product of 810 C of DUB.
Saualane also known as isotriacontane, shark alkane in the present invention are to be made after being hydrogenated by squalene, can be used as face cream, battalion Support the basic cosmetics oiliness raw materials such as lotion.Squalene is from blue shark (Centrophorus) or other deepwater shark class liver oils It obtains, initially as the by-product by dogfish oil production vitamin A.Saualane iodine number 0~5, saponification number 0~5, acid value 0~ 0.2, -38 DEG C of freezing point, 350 DEG C of boiling point.It is stable in the air, it will be slow oxidation under effect of sunlight.Sebaceous glands can synthesize spiny dogfish Alkene, sebum contain squalene, and adult sebum is 10% up to mass fraction;Sebum mass fraction containing saualane is about 2%.This hair Saualane in bright can be from being commercially available, without limitation to purchase producer on the market.
Still more preferably, the base oil is lauric alcohol-caprylate/decylate and saualane mixture, heavy Amount ratio is 3:1.
Due to the ingredient that care composition is water phase and oily phase stratification state in the present invention, so needing to guarantee between two-phase It is able to maintain layering, and the selection of base oil and ratio are the key that guarantee to form two-phase interface, the selected best right and wrong of grease Polarity or low pole grease have high spreadability, the property of low viscosity.It is found by the applicant that when using lauric alcohol-caprylate/capric acid It is oily based on the mixture of ester and saualane, and when weight ratio between the two is 3:1, base oil has paving well Malleability and lower viscosity, while can guarantee and being layered well between water phase and oily phase again, two-phase is independent of each other.It may be cocounut oil The parameters such as length, the polarity of alcohol-caprylate/decylate and saualane strand reach certain balance, Effective Regulation oil phase Surface tension, strand can unfold comprehensively, sprawl oily phase preferably in water phase, obtain stable biphase equilibrium.
Particular determination is not done to the vegetable oil in the present invention, sunflower seed oil, jojoba oil, nut can be selected Oil, camellia seed oil, apricot kernel oil, grape seed oil, apple oil, hippophae rhamnoides fruit oil, soybean oil, rapeseed oil, peanut oil, sesame oil, Tujue One of rose caul-fat, shea butter, shorea double tree seed oil, evening primrose oil are a variety of.
Preferably, the vegetable oil is the mixture of sunflower seed oil and jojoba oil;The jojoba oil and sunflower The weight ratio of seed oil is 1:(6~9).
It is further preferred that the weight ratio of the jojoba oil and sunflower seed oil is 2:15.
The acid value of jojoba oil in the present invention: 0.1~5.2mgKOH/g, iodine number: 81.8~85.7gI2/ (100g), soap Change value: 90.1~101.3mgKOH/g, unsaponifiable matter: 48%~51%.Sunflower seed oil saponification number (mgKOH/g): 188- 194, iodine number (gI2/100g):120-136。
It is found by the applicant that the selection and ratio of vegetable oil, and the reason of influence the interface of two-phase, but main influence It is the moist degree and moistening effect of product.Vegetable oil itself is difficult to maintain compared with water stable two-phase interface, needs base oil Help stable equilibrium, and base oil moisture retention and moisten degree on it is weaker, the two must in the combination under certain proportion range, It just can guarantee the use feeling and effect of product.It is found by the applicant that using the mixture of sunflower seed oil and jojoba oil as plant Oil, especially when weight ratio between the two is 1:(6~9) in range when, cooperateed with well between vegetable oil and base oil Effect plays balance water phase and an oil phase well, and does not influence the use feeling and effect of product.
In some embodiments, the raw material of the oily phase further includes the auxiliary agent of 0.05~5 parts by weight;The auxiliary agent is selected from One of antioxidant, ultraviolet absorbing agent, stabilizer, pH adjusting agent are a variety of.
Particular determination do not carried out to the antioxidant, including but not limited to BHT, tocopherol, rosemary leaf extract, Pentaerythrite four (double-relax butylhydroxy hydrocinnamic acid) ester etc..Preferably tocopherol.
It is further preferred that the oil phase, in parts by weight, including lauric alcohol -15 parts of caprylate/decylate, sunflower Seed oil 15 parts, 5 parts of saualane, 2 parts of jojoba oil, 0.5 part of tocopherol.
In some embodiments, the water phase, by percentage to the quality, including moisturizer 0.5~20%, sodium chloride 0.1~1.0%, preservative 0.5~5.0%, balance deionized water;The viscosity of the water phase is no more than 1000cst.
The test of the water phase viscosity can be surveyed according to method well-known to those skilled in the art in the present invention Examination can also be tested according to GB/T 10247-2008 " Viscosity Measurement Methods " standard.
In order to enable product to have the function that long-acting moisturizing, need to be added a certain amount of moisturizer in water phase, it is right in the present invention The moisturizer does not carry out particular determination, can be using the guarantor that can be added in cosmetics well-known to those skilled in the art Wet ingredient is as moisturizer.Applicant have discovered that and not all moisturizer can use, need to guarantee the molecule of moisturizer Molecular weight cannot be excessive, and system viscosity controls within 1000cst.
In some embodiments, the moisturizer is selected from glycerol, Sodium Hyaluronate, trehalose, tremella polysaccharides, ethoxy Urea, glycine betaine, allantoin, tamarind seed polysaccharide, diglycerol, potentilla anserina extract, hippophae rhamnoides, bamboo extractive, celestial being People slaps one of extract, Mi Luomu extract, arginine or a variety of.
Preferably, the moisturizer be Sodium Hyaluronate, glycerol, glycine betaine, Radix et Caulis Opuntiae Dillenii extract mixture, wherein institute The weight ratio for stating glycine betaine, Radix et Caulis Opuntiae Dillenii extract and glycerol is 1:(0.8~1.5): (1.5~3).
It is further preferred that the weight ratio of the glycine betaine, Radix et Caulis Opuntiae Dillenii extract and glycerol is 1:1:2.
It is further preferred that the water phase, in parts by weight, including 0.1 part of Sodium Hyaluronate, 2 parts of glycerol, glycine betaine 1 part, 1 part of Radix et Caulis Opuntiae Dillenii extract, 0.5 part of preservative, 57.9 parts of water.
The present invention is specifically described below by embodiment.It is necessarily pointed out that following embodiment is only used In the invention will be further described, it should not be understood as limiting the scope of the invention, professional and technical personnel in the field The some nonessential modifications and adaptations made according to the content of aforementioned present invention, still fall within protection scope of the present invention.
In addition, if without other explanations, it is raw materials used to be all commercially available, and the body care with water phase and an oil phase Composition is to be prepared via a method which to obtain:
1. successively adding oily phase each component to be uniformly mixed;
2. successively addition water phase each component is uniformly mixed;
3. grease mutually carries out in filling to same packaging material by a certain percentage.
Embodiment
Embodiment 1A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 8 parts of C15-19 alkane (CAS:64741-76-0), 1.5 parts of apple oil, 0.5 part of tocopherol;
Water phase: 0.5 part of glycerol, 0.5 part of trehalose, 0.2 part of sodium chloride, 1.0 parts of bamboo extractive, 0.5 part of preservative, water 87.3 parts.
Embodiment 2A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 88 parts of C15-19 alkane (CAS:64741-76-0), 1.5 parts of apple oil, 0.5 part of tocopherol;
Water phase: 0.5 part of glycerol, 0.5 part of trehalose, 0.2 part of sodium chloride, 1.0 parts of bamboo extractive, 0.5 part of preservative, water 7.3 part.
Embodiment 3A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 48 parts of C15-19 alkane, 1.5 parts of apple oil, 0.5 part of tocopherol;
Water phase: 0.5 part of glycerol, 0.5 part of trehalose, 0.2 part of sodium chloride, 1.0 parts of bamboo extractive, 0.5 part of preservative, water 47.3 parts.
Embodiment 4A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -5 parts of caprylate/decylate, 15 parts of macadamia nut oil, 15 parts of camellia seed oil, 10 parts of jojoba oil, fan Repeatedly 0.2 part of Herba Pelargonii Graveolentis extract, (double-easypro 0.1 part of the butylhydroxy hydrogenated cinnamates of pentaerythrite four;
Water phase: 2 parts of 1,3 butylene glycol, 0.1 part of Sodium Hyaluronate, 0.3 part of sodium chloride, 0.5 part of Radix Gentianae extract, preservative 0.5 part, 51.3 parts of water.
Embodiment 5A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 20 parts of dimethyl silicone polymer, 2 parts of saualane, 6 parts of C15-19 alkane, 1.5 parts of apple oil, tocopherol 0.5 Part;
Water phase: 1 part of ethoxy urea, 1 part of glycine betaine, 0.3 part of sodium chloride, 0.5 part of camomile extract, 0.5 part of preservative, 66.7 parts of water.
Embodiment 6A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -15 parts of caprylate/decylate, 15 parts of sunflower seed oil, 5 parts of saualane, 2 parts of jojoba oil, life Educate 0.5 part of phenol;
Water phase: 0.1 part of Sodium Hyaluronate, 2 parts of glycerol, 1 part of glycine betaine, 1 part of Radix et Caulis Opuntiae Dillenii extract, is prevented 0.2 part of sodium chloride 0.5 part of rotten agent, 57.9 parts of water.
Embodiment 7A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 17 parts of C15-19 alkane, 13 parts of dimethyl silicone polymer, 2 parts of macadimia nut oil, 5 parts of saualane, rosemary leave 0.5 part of extract, 0.2 part of tocopherol;
Water phase: 1 part of ethoxy urea, 1 part of trehalose, 0.5 part of sodium chloride, 2 parts of hippophae rhamnoides, 0.5 part of preservative, water 57.3 parts.
Embodiment 8A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 7 parts of octyl dimethyl silicone polymer, 5 parts of white oil, 2.5 parts of macadimia nut oil, 13 parts of sunflower seed oil, life Educate 0.5 part of phenol;
Water phase: 0.1 part of Sodium Hyaluronate, 1.5 parts of ethoxy urea, 0.3 part of sodium chloride, 0.5 part of Mi Luomu extract, anti-corrosion 0.5 part of agent, 69.1 parts of water.
Embodiment 9A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -15 parts of caprylate/decylate, 5 parts of saualane, 2 parts of jojoba oil, 0.5 part of tocopherol;
Water phase: 0.1 part of Sodium Hyaluronate, 2 parts of glycerol, 1 part of glycine betaine, 1 part of Radix et Caulis Opuntiae Dillenii extract, is prevented 0.2 part of sodium chloride 0.5 part of rotten agent, 57.9 parts of water.
Embodiment 10A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -15 parts of caprylate/decylate, 15 parts of sunflower seed oil, 5 parts of saualane, 0.5 part of tocopherol;
Water phase: 0.1 part of Sodium Hyaluronate, 2 parts of glycerol, 1 part of glycine betaine, 1 part of Radix et Caulis Opuntiae Dillenii extract, is prevented 0.2 part of sodium chloride 0.5 part of rotten agent, 57.9 parts of water.
Embodiment 11A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: 15 parts of sunflower seed oil, 5 parts of saualane, 2 parts of jojoba oil, 0.5 part of tocopherol;
Water phase: 0.1 part of Sodium Hyaluronate, 2 parts of glycerol, 1 part of glycine betaine, 1 part of Radix et Caulis Opuntiae Dillenii extract, is prevented 0.2 part of sodium chloride 0.5 part of rotten agent, 57.9 parts of water.
Embodiment 12A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -15 parts of caprylate/decylate, 15 parts of sunflower seed oil, 5 parts of saualane, 2 parts of jojoba oil, life Educate 0.5 part of phenol;
Water phase: 0.1 part of Sodium Hyaluronate, 0.2 part of sodium chloride, 2 parts of glycerol, 1 part of glycine betaine, 0.5 part of preservative, water 57.9 Part.
Embodiment 13A kind of body care composition with water phase and an oil phase is provided, preparing raw material includes oil phase and water Phase;One parts by weight meter, are as follows:
Oily phase: lauric alcohol -15 parts of caprylate/decylate, 15 parts of sunflower seed oil, 5 parts of saualane, 2 parts of jojoba oil, life Educate 0.5 part of phenol;
Water phase: 0.1 part of Sodium Hyaluronate, 0.2 part of sodium chloride, 0.1 part of glycerol, 3 parts of glycine betaine, 2 parts of Radix et Caulis Opuntiae Dillenii extract, 0.5 part of preservative, 57.9 parts of water.
Performance test
1. layered effect: after being shaken up with single concussion, whether water phase and an oil phase can form clearly layering interfaces and be used as layering The judgement of effect, from difference to be followed successively by well+, ++, +++, ++++, +++ ++.
2. recovery time: after being shaken up with single concussion, standing to the time required for complete be layered.
3. atomizing effect: a commercially available common spraying pump head of selection, about 60 ° of jet angle, single pump amount about 0.5ml, with water Spray effect is defined as 1.0 points as reference standard, the > 1 better than water spray effect, than the < 1 of water spray effect difference.
4. moisture feeling: using supervisor's impression of at least ten subject as reference, indicating moisture feeling quality, " * " with " * " Amount is more, and moisture feelings are better, and vice versa.
5. oil residue: being applied to 3min after absorption, tested with Delfin sebumeter.
6. moisture content of skin: under the conditions of constant temperature and humidity (relative humidity 50,20 DEG C of temperature), first testing recipient site basis It is worth (generally hand inner forearm), 0min, 15min, 30min, 1h, 2h, 6h period after using product distinguish re-test skin The value of skin water content, 15 people of sample size use Delfin instrument, model MOISTURE METER SC.
1 the performance test results of table
The test of 2 water content of table
Embodiment Basic value 0min 15min 30min 1h 2h 6h
Embodiment 1 11.6 79.9 53.9 42.1 32.3 29.9 20.1
Embodiment 2 11.9 45.8 40.1 36.7 34.4 33.9 29.8
Embodiment 3 12.5 58.7 45.5 40.9 38.8 30.6 27.1
Embodiment 4 11.2 64.5 48.5 43.4 42.1 40.1 39.1
Embodiment 5 12.0 75.4 53.4 40.9 35.9 30.1 21.6
Embodiment 6 11.6 72.3 57.8 46.5 44.4 43.3 38.9
Embodiment 7 11.8 74.5 54.5 43.6 40.1 39.8 35.6
Embodiment 8 10.9 78.3 60.1 45.6 41.1 37.9 34.5
Embodiment 9 11.2 64.1 49.1 41.7 35.5 32.7 30.9
Embodiment 10 11.9 70.5 52.3 43.2 39.5 35.2 32.1
Embodiment 11 11.4 64.2 53.5 42.0 38.4 34.6 31.6
Embodiment 12 11.9 64.1 51.0 40.1 35.9 30.1 27.7
Embodiment 13 11.3 61.8 49.8 39.9 34.2 29.8 26.2
It is found by the applicant that working as the oil residue of the composition in embodiment 6 and the FURTERER 5 bought on the market SENS (the refined five weights multiple-effect nursing oil of the green moral of fragrance) compares, and the refined five weights multiple-effect nursing oil of the green moral of fragrance has used grease on the skin residual Allowance is 5.4 times of the Example formulations sample, it will be seen that the composition in the present invention has good comprehensive performance.
The above is only presently preferred embodiments of the present invention, is not the limitation for making other forms to invention, any Those skilled in the art are changed or are changed to the equivalent of equivalent variations possibly also with the technology contents of the disclosure above Embodiment, but without departing from the technical solutions of the present invention, it is to the above embodiments according to the technical essence of the invention Any simple modification, equivalent variations and remodeling, still fall within the protection scope of technical solution of the present invention.

Claims (10)

1. a kind of body care composition with water phase and an oil phase, which is characterized in that it includes oil phase and water phase that it, which prepares raw material,;Institute Stating oily mutually includes the base oil of 10~60 parts by weight and the vegetable oil of 10~50 parts by weight;The weight ratio of the oil phase and water phase For 1:(0.1~9).
2. as described in claim 1 with the body care composition of water phase and an oil phase, which is characterized in that the base oil is selected from At least one of alkanes, lightweight silicone oil, aliphatic ester/ethers.
3. as claimed in claim 2 with the body care composition of water phase and an oil phase, which is characterized in that the base oil is selected from Lauric alcohol-caprylate/decylate, C11~C19 alkanes and its isomers, saualane, isononyl isononanoate, carbonic acid dioctyl ester, Dicaprylyl ether, pentaerythrite (thylhexoic acid) ester, two heptanoate of neopentyl glycol, diethyl hexylcarbonate, sad Propylheptyl, third The poly- diformazan of glycol dibenzoic acid, octyl dodecanol myristinate, Parleam, white oil, dimethyl silicone polymer, octyl One of radical siloxane is a variety of.
4. as described in claim 1 with the body care composition of water phase and an oil phase, which is characterized in that the base oil is coconut palm Oleyl alcohol-caprylate/decylate and saualane mixture, weight ratio are (2~4): 1.
5. as described in claim 1 with the body care composition of water phase and an oil phase, which is characterized in that the vegetable oil is selected from Sunflower seed oil, macadamia nut oil, camellia seed oil, apricot kernel oil, grape seed oil, apple oil, hippophae rhamnoides fruit oil, soybean oil, is dashed forward at jojoba oil It faints one of rose caul-fat or a variety of.
6. as claimed in claim 5 with water phase and an oil phase body care composition, which is characterized in that the vegetable oil be to The mixture of day seed oil of sunflower and jojoba oil;The weight ratio of the jojoba oil and sunflower seed oil is 1:(6~9).
7. as described in claim 1 with the body care composition of water phase and an oil phase, which is characterized in that the water phase, with matter Measure percentages, including moisturizer 0.5~20%, sodium chloride 0.1~1.0%, preservative 0.5~5.0%, surplus deionization Water;The viscosity of the water phase is no more than 1000cst.
8. as claimed in claim 7 with the body care composition of water phase and an oil phase, which is characterized in that the moisturizer is selected from Glycerol, Sodium Hyaluronate, trehalose, tremella polysaccharides, ethoxy urea, glycine betaine, allantoin, tamarind seed polysaccharide, diglycerol, goose down One of Herba Potentillae Chinensis extract, hippophae rhamnoides, bamboo extractive, Radix et Caulis Opuntiae Dillenii extract, Mi Luomu extract, arginine or It is a variety of.
9. as claimed in claim 8 with the body care composition of water phase and an oil phase, which is characterized in that the moisturizer is Bright matter acid sodium, glycerol, glycine betaine, Radix et Caulis Opuntiae Dillenii extract mixture, wherein the glycine betaine, Radix et Caulis Opuntiae Dillenii extract and glycerol Weight ratio is 1:(0.8~1.5): (1.5~3).
10. as described in claim 1 with the body care composition of water phase and an oil phase, which is characterized in that the original of the oil phase Material further includes the auxiliary agent of 0.05~5 parts by weight;The auxiliary agent is selected from antioxidant, ultraviolet absorbing agent, stabilizer, pH adjusting agent One of or it is a variety of.
CN201910598445.7A 2019-07-04 2019-07-04 A kind of body care composition of water phase and an oil phase and preparation method thereof Withdrawn CN110200872A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111358734A (en) * 2020-04-10 2020-07-03 上海新高姿化妆品有限公司 A warehouse-separated anti-aging cosmetic composition
CN111759781A (en) * 2020-07-25 2020-10-13 高洋 Skin care product of shaking milk
CN112263492A (en) * 2020-11-27 2021-01-26 天津郁美净集团有限公司 Formula of jelly-like suspended oil drop high-moisture sleeping mask and preparation process thereof
CN115252450A (en) * 2022-08-30 2022-11-01 时垠(上海)生物科技有限公司 Oily composition carrying water-soluble components and application thereof
CN115300422A (en) * 2021-09-29 2022-11-08 糖果(上海)化妆品有限公司 Fragrance yeast composition, body essence and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111358734A (en) * 2020-04-10 2020-07-03 上海新高姿化妆品有限公司 A warehouse-separated anti-aging cosmetic composition
CN111759781A (en) * 2020-07-25 2020-10-13 高洋 Skin care product of shaking milk
CN112263492A (en) * 2020-11-27 2021-01-26 天津郁美净集团有限公司 Formula of jelly-like suspended oil drop high-moisture sleeping mask and preparation process thereof
CN115300422A (en) * 2021-09-29 2022-11-08 糖果(上海)化妆品有限公司 Fragrance yeast composition, body essence and preparation method thereof
CN115252450A (en) * 2022-08-30 2022-11-01 时垠(上海)生物科技有限公司 Oily composition carrying water-soluble components and application thereof
CN115252450B (en) * 2022-08-30 2024-05-17 时垠(上海)生物科技有限公司 Oily composition carrying water-soluble components and application thereof

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Application publication date: 20190906