CN108785140A - A kind of carbonic acid face cleaning foam and preparation method thereof - Google Patents

A kind of carbonic acid face cleaning foam and preparation method thereof Download PDF

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Publication number
CN108785140A
CN108785140A CN201810863151.8A CN201810863151A CN108785140A CN 108785140 A CN108785140 A CN 108785140A CN 201810863151 A CN201810863151 A CN 201810863151A CN 108785140 A CN108785140 A CN 108785140A
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Prior art keywords
carbonic acid
face cleaning
cleaning foam
added
acid face
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Pending
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CN201810863151.8A
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Chinese (zh)
Inventor
王跃
王璐
王彦宾
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Shanghai West West Qidong Daily Chemicals Co Ltd
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Shanghai West West Qidong Daily Chemicals Co Ltd
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Priority to CN201810863151.8A priority Critical patent/CN108785140A/en
Publication of CN108785140A publication Critical patent/CN108785140A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/046Aerosols; Foams
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Emergency Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

A kind of carbonic acid face cleaning foam of present invention offer and preparation method thereof, carbonic acid face cleaning foam of the invention including the following raw material measured by mass percentage by being prepared:Rheological agent 0.1~1.8%;Antibacterial moisturizer 0.1~4%;Amino acid surfactant 7.5~17%;Gas component 1.5~17%;Oil phase component 0.5~14%;Essence 0.1~1%;Water phase components surplus;Wherein, include liquefied petroleum gas and carbon dioxide in above-mentioned gas component.The carbonic acid face cleaning foam of the present invention reaches cleaning effect using amino acid surfactant, it does not stimulate mildly, carbon dioxide is added using aerosol form in formula simultaneously, so that foam more satin has texture, it is careful lasting, increase face's blood circulation simultaneously, other active components in formula is promoted to be absorbed by the skin.

Description

A kind of carbonic acid face cleaning foam and preparation method thereof
Technical field
The present invention relates to technical field of skin care of washing one's face, and in particular to a kind of carbonic acid face cleaning foam and preparation method thereof.
Background technology
Face cleaning foam is one of most common face cleaning product, and this kind of product strong cleaning force feels salubrious after washing, most joyous by people It meets.Existing two kinds of foam patterns of face cleaning foam generally use, first, using foam pump, the foam of this method output is coarse not Exquisiteness, cleaning force are relatively low;Second is that using aerosol form, propellant is made using liquefied petroleum gas.But both foaming shapes Formula all only generates foam, without functional effect.
In addition, being usually added with the strong surfactant of irritations and the different thiophenes of methyl such as soap base in current face cleaning foam The preservatives such as oxazoline ketone, methyl hydroxybenzoate, integral formula are not mild enough.
Invention content
The present invention is to carry out to solve the above-mentioned problems, and it is an object of the present invention to provide a kind of carbonic acid face cleaning foam and its preparation Method.
Carbonic acid face cleaning foam provided by the invention, which is characterized in that including the following raw material system measured by mass percentage It is standby to form:
Wherein, include liquefied petroleum gas and carbon dioxide in above-mentioned gas component.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, rheology Agent is one or more of xanthans, hydroxyethyl cellulose, polyquaternium.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, antibacterial Moisturizer is one or more of decoyl hydroximic acid, pungent glycol, Sensiva SC50,1,3- propylene glycol.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, amino Acids surfactant includes cocounut oil acyl disodium glutamate and laruyl alcohol phosphate potassium.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, oil phase Group be divided into docosyl alcohol, myristic acid, Queensland nut seed oil, stearic acid, PEG-10 stearates, thorn A Gan tree benevolence oil in one kind or It is several.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, water phase Component includes glycerine, dipropylene glycol and water.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:Wherein, it liquefies Oil gas is the composition of propane, iso-butane.
Further, it in carbonic acid face cleaning foam provided by the invention, can also have the feature that:By including following The raw material measured by mass percentage is prepared:
The present invention also provides the preparation methods of above-mentioned carbonic acid face cleaning foam, have the feature that, include the following steps:
Step 1, all raw materials are weighed according to mass percent;
Step 2, rheological agent component is added in glycerine and is dispersed with stirring by the glycerine half for taking weighing;
Step 3, oil phase component is heated to 75~80 DEG C, dissolving is complete;
Step 4, water, dipropylene glycol are mixed with the glycerine of remaining half, step 2 is added and handles obtained rheological agent It carrying out prewired, is heated to 75~80 DEG C, stirs evenly, add step 3 and handle obtained oil phase component, homogeneous stirs evenly, 50 DEG C are cooled to, amino acid surfactant is subsequently added into, continues to be cooled to 40 DEG C, antibacterial moisturizer and perfume (or spice) is then added Essence, filtering and discharging obtain stoste;
Step 5, stoste progress step 4 processing obtained is filling, is filled with liquefied petroleum gas and carbon dioxide, then carry out Then water-bath, purging plus nozzle are sprayed through squeezing up to carbonic acid face cleaning foam.
The effect of invention
In the carbonic acid face cleaning foam of the present invention, cleaning effect is reached using amino acid surfactant, does not contain soap base Etc. the strong surfactant of irritations, it is not tight that amino acid cleansing is formulated mild face cleaning, reduces skin stimulation, meanwhile, using gas Carbon dioxide is added in mist dosage form formula in formula so that foam more satin has texture, careful lasting, and carbon dioxide can Increase face blood circulation, other active components in formula not only promoted to be efficiently absorbed, be also beneficial to the water used after face cleaning, The absorption of the products such as essence, lotion.
Particularly, preservative is free of in carbonic acid face cleaning foam of the invention, but the moisturizer with bacteria resistance function is pungent Acyl hydroximic acid, pungent glycol, Sensiva SC50 and 1,3-PD are combined, and have not only played good moistening effect, but also real Antiseptic and inhibiting bacteria function effect is showed, compared to the cleanser that tradition uses preservative, mildness is significantly improved.
In addition, being added to extracted form natural plant ingredient in the carbonic acid face cleaning foam of the present invention:Queensland nut (MACADAMIA TERNIFOLIA) seed oil and thorn A Ganshu (ARGANIASPINOSA) benevolence oil, Queensland nut seed oil boost metabolism, contribute to The effect of nutrition and beautifying skin, generation for reducing wrinkle, thorn A Gan tree benevolence oil plays beauty and skin care.
Each component is added according to specified ratio in carbonic acid face cleaning foam formulation of the present invention, makes more to melt between each component The effect of closing, making each component maximizes, and not only realizes mild face cleaning, but also active constituent in formula is promoted to be efficiently absorbed, and rises To cosmetology effect.
Specific implementation mode
It is real below in order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand Example is applied to be specifically addressed the carbonic acid face cleaning foam and preparation method thereof of the present invention.
<Embodiment 1>
It is formulated (by mass percentage):Xanthans 0.1%;Hydroxyethyl cellulose 0.1%;Polyquaternium -70.3%;Behenyl Alcohol 5%;Myristic acid 0.5%;Queensland nut (MACADAMIATERNIFOLIA) seed oil 0.5%;Stearic acid 2%;PEG-10 is hard Resin acid ester 2.5%;Dry tree (ARGANIA SPINOSA) the benevolence oil 1% of Ci A;Decoyl hydroximic acid 0.1%;Pungent glycol 0.7%;Ethyl Hexyl glycerine 1%;1,3- propylene glycol 0.3%;Iso-butane 6.5%;Propane 1%;Carbon dioxide 1.5%;Cocounut oil acyl glutamic acid two Sodium 12%;Laruyl alcohol phosphate potassium 0.5;Glycerine 5%;Dipropylene glycol 5%;Water 54.4%.
Preparation method:
Step 1, all raw materials are weighed according to mass percent.
Step 2, xanthans, hydroxyethyl cellulose, polyquaternium -7 are added in glycerine the glycerine half for taking weighing It is dispersed with stirring, obtains rheological agent.
Step 3, by the oil phase component of weighing:Docosyl alcohol, myristic acid, Queensland nut seed oil, stearic acid, PEG-10 are stearic Acid esters, thorn A Gan tree benevolence oil are mixed and heated to 75 DEG C, and dissolving is complete.
Step 4, water, dipropylene glycol are mixed with the glycerine of remaining half, step 2 is added and handles obtained rheological agent It carries out prewired, is heated to 77 DEG C, stirs evenly, add step 3 and handle obtained oil phase component, homogeneous stirs evenly, and cools down To 50 DEG C, be subsequently added into cocounut oil acyl disodium glutamate and laruyl alcohol phosphate potassium, continue to be cooled to 40 DEG C, then be added essence, Decoyl hydroximic acid, pungent glycol, Sensiva SC50,1,3-PD, filtering and discharging obtain stoste.
Step 5, stoste progress step 4 processing obtained is filling, is re-filled with propane, iso-butane and carbon dioxide, then Water-bath, purging plus nozzle are carried out, then, is sprayed up to carbonic acid face cleaning foam through squeezing.
<Embodiment 2>
It is formulated (by mass percentage):Xanthans 0.1%;Hydroxyethyl cellulose 0.5%;Polyquaternium -70.2%;Behenyl Alcohol 4%;Myristic acid 2.5%;Queensland nut seed oil 0.1%;Stearic acid 0.5%;PEG-10 stearates 2%;The dry trees of Ci A Benevolence oil 0.8;Decoyl hydroximic acid 0.5%;Pungent glycol 1%;Sensiva SC50 0.6%;1,3- propylene glycol 0.1%;Iso-butane 2%;Propane 0.1%;Carbon dioxide 0.5%;Cocounut oil acyl disodium glutamate 15%;Laruyl alcohol phosphate potassium 1%;Glycerine 14%; Dipropylene glycol 1%;Water 53.5%.
Preparation method:
Step 1, all raw materials are weighed according to mass percent.
Step 2, xanthans, hydroxyethyl cellulose, polyquaternium -7 are added in glycerine the glycerine half for taking weighing It is dispersed with stirring, obtains rheological agent.
Step 3, by the oil phase component of weighing:Docosyl alcohol, myristic acid, Queensland nut seed oil, stearic acid, PEG-10 are stearic Acid esters, thorn A Gan tree benevolence oil are mixed and heated to 80 DEG C, and dissolving is complete.
Step 4, water, dipropylene glycol are mixed with the glycerine of remaining half, step 2 is added and handles obtained rheological agent It carries out prewired, is heated to 80 DEG C, stirs evenly, add step 3 and handle obtained oil phase component, homogeneous stirs evenly, and cools down To 50 DEG C, be subsequently added into cocounut oil acyl disodium glutamate and laruyl alcohol phosphate potassium, continue to be cooled to 40 DEG C, then be added essence, Decoyl hydroximic acid, pungent glycol, Sensiva SC50,1,3-PD, filtering and discharging obtain stoste.
Step 5, stoste progress step 4 processing obtained is filling, is re-filled with propane, iso-butane and carbon dioxide, then Water-bath, purging plus nozzle are carried out, then, is sprayed up to carbonic acid face cleaning foam through squeezing.
<Embodiment 3>
It is formulated (by mass percentage):Xanthans 0.1%;Hydroxyethyl cellulose 0.24%;Polyquaternium -70.1%;Mountain Yu alcohol 1%;Myristic acid 2%;Queensland nut seed oil 1%;Stearic acid 1%;PEG-10 stearates 0.5%;The dry tree benevolence of Ci A Oil 0.1%;Decoyl hydroximic acid 1%;Pungent glycol 0.1%;Sensiva SC50 0.01%;1,3- propylene glycol 1%;Iso-butane 8%; Propane 0.85%;Carbon dioxide 0.8%;Cocounut oil acyl disodium glutamate 7%;Laruyl alcohol phosphate potassium 2%;Glycerine 15%;Double third Glycol 3%;Water 55.2%.
Preparation method:
Step 1, all raw materials are weighed according to mass percent.
Step 2, xanthans, hydroxyethyl cellulose, polyquaternium -7 are added in glycerine the glycerine half for taking weighing It is dispersed with stirring, obtains rheological agent.
Step 3, by the oil phase component of weighing:Docosyl alcohol, myristic acid, Queensland nut seed oil, stearic acid, PEG-10 are stearic Acid esters, thorn A Gan tree benevolence oil are mixed and heated to 78 DEG C, and dissolving is complete.
Step 4, water, dipropylene glycol are mixed with the glycerine of remaining half, step 2 is added and handles obtained rheological agent It carries out prewired, is heated to 75 DEG C, stirs evenly, add step 3 and handle obtained oil phase component, homogeneous stirs evenly, and cools down To 50 DEG C, be subsequently added into cocounut oil acyl disodium glutamate and laruyl alcohol phosphate potassium, continue to be cooled to 40 DEG C, then be added essence, Decoyl hydroximic acid, pungent glycol, Sensiva SC50,1,3-PD, filtering and discharging obtain stoste.
Step 5, stoste progress step 4 processing obtained is filling, is re-filled with propane, iso-butane and carbon dioxide, then Water-bath, purging plus nozzle are carried out, then, is sprayed up to carbonic acid face cleaning foam through squeezing.

Claims (9)

1. a kind of carbonic acid face cleaning foam, which is characterized in that be prepared including the following raw material measured by mass percentage:
Wherein, include liquefied petroleum gas and carbon dioxide in the gas component.
2. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the rheological agent is one or more of xanthans, hydroxyethyl cellulose, polyquaternium.
3. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the antibacterial moisturizer be decoyl hydroximic acid, pungent glycol, Sensiva SC50, one kind in 1,3-PD or It is several.
4. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the amino acid surfactant includes cocounut oil acyl disodium glutamate, laruyl alcohol phosphate potassium.
5. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the oil phase component is docosyl alcohol, myristic acid, Queensland nut seed oil, stearic acid, PEG-10 stearates, thorn It is one or more of in A Gan tree benevolence oil.
6. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the water phase components include glycerine, dipropylene glycol and water.
7. carbonic acid face cleaning foam according to claim 1, it is characterised in that:
Wherein, the liquefied petroleum gas is the composition of propane, iso-butane.
8. the carbonic acid face cleaning foam according to any one of claim 1, which is characterized in that by including below by quality hundred The raw material than metering is divided to be prepared:
9. the preparation method of the carbonic acid face cleaning foam as described in any one of claim 1~8, which is characterized in that including with Lower step:
Step 1, all raw materials are weighed according to mass percent;
Step 2, rheological agent component is added in glycerine and is dispersed with stirring by the glycerine half for taking weighing;
Step 3, oil phase component is heated to 75~80 DEG C, dissolving is complete;
Step 4, water, dipropylene glycol are mixed with the glycerine of remaining half, the rheological agent that step 2 processing obtains is added and carries out It is prewired, 75~80 DEG C are heated to, is stirred evenly, step 3 is added and handles obtained oil phase component, homogeneous stirs evenly, and cools down To 50 DEG C, it is subsequently added into amino acid surfactant, continues to be cooled to 40 DEG C, antibacterial moisturizer and essence is then added, Filtering and discharging obtains stoste;
Step 5, stoste progress step 4 processing obtained is filling, is filled with liquefied petroleum gas and carbon dioxide, then carry out Then water-bath, purging plus nozzle are sprayed through squeezing up to carbonic acid face cleaning foam.
CN201810863151.8A 2018-08-01 2018-08-01 A kind of carbonic acid face cleaning foam and preparation method thereof Pending CN108785140A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528562A (en) * 2018-12-28 2019-03-29 中山市天图精细化工有限公司 A kind of ozone wire drawing cleansing mousse of use in personal care and preparation method thereof
CN110680759A (en) * 2019-11-18 2020-01-14 浙江绿岛科技有限公司 Aerosol type amino acid face-cleaning gel and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105997548A (en) * 2016-08-02 2016-10-12 苏州药基美研医药科技有限公司 Mild cleansing foam based on amino acid derivative surfactant
CN107898711A (en) * 2017-12-28 2018-04-13 齐鲁工业大学 A kind of amino acid pattern moisturizing face cleaning foam

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105997548A (en) * 2016-08-02 2016-10-12 苏州药基美研医药科技有限公司 Mild cleansing foam based on amino acid derivative surfactant
CN107898711A (en) * 2017-12-28 2018-04-13 齐鲁工业大学 A kind of amino acid pattern moisturizing face cleaning foam

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
裘炳毅: "《现代化妆品科学与技术》", 31 March 2016 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528562A (en) * 2018-12-28 2019-03-29 中山市天图精细化工有限公司 A kind of ozone wire drawing cleansing mousse of use in personal care and preparation method thereof
CN110680759A (en) * 2019-11-18 2020-01-14 浙江绿岛科技有限公司 Aerosol type amino acid face-cleaning gel and preparation method thereof

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