CN107898711A - A kind of amino acid pattern moisturizing face cleaning foam - Google Patents
A kind of amino acid pattern moisturizing face cleaning foam Download PDFInfo
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- CN107898711A CN107898711A CN201711462321.3A CN201711462321A CN107898711A CN 107898711 A CN107898711 A CN 107898711A CN 201711462321 A CN201711462321 A CN 201711462321A CN 107898711 A CN107898711 A CN 107898711A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The present invention provides a kind of amino acid pattern moisturizing face cleaning foam, it is characterised in that by weight percentage, composed of the following components：Deionized water 30~45%, amino acid surfactant 20~35%, rose 10~20%, glycerine 2~10%, glycine betaine 2~8%, plant extraction elite 1~3%, 1,2 hexylene glycols 0.1~1%, citric acid 0.1~0.3%, hydroxyethyl cellulose 0.1~0.5%.Compared with prior art, amino acid pattern moisturizing face cleaning foam provided by the invention is free of soap matter and any essence and preservative, and cleaning effect is strong, and moistening effect is lasting, is more suitable for sensitive skin crowd；In faintly acid, close to the pH value of human skin, gentle pro-skin, using it is rear it is smooth, comfortable, without tight feeling, the protection function of quick-recovery skin soon is capable of after clean skin, makes skin acid-base balance, is adapted to overwhelming majority skin quality simultaneously can long-time service.
Description
Technical field
The present invention relates to daily cosmetics field, more particularly to a kind of amino acid pattern moisturizing face cleaning foam of gentle pro-skin.
Background technology
Allergy is also referred to as allergy, is caused immune response behind allergic constitution crowd's contact allergy source.Skin allergy
It is one of common skin problem, and in recent years, with the change of dietary structure, atmosphere pollution, the increasing of live and work pressure
Greatly, autopath sharply increases.Skin sensitivity has become the social concern for influencing human health.According to incompletely statistics, entirely
The crowd that ball feels sensitiveness skin is more and more, and wherein male accounts for 39%, and women accounts for 61%.
It is soap base type face cleaning product that sold face cleaning product is most of on the market at present.Soap base type face cleaning product adds alkalescence
Surfactant, foaming agent, the component such as soap base, its pH is in alkalescence, and the skin of human body is weakly acidic, uses meeting for a long time
Skin is stimulated, influences skin barrier function, severe patient easily causes allergic reaction.Therefore with consumer's skin care realize raising,
How to provide that a kind of cleaning effect is strong, and moistening effect is lasting, while gentle pro-skin again, be more suitable for the face cleaning of sensitive skin crowd
Product is the important research direction in one, daily cosmetics field.
The content of the invention
The defects of in order to overcome the prior art, it is an object of the invention to provide a kind of amino acid pattern moisturizing face cleaning foam,
It is characterized in that, by weight percentage, it is composed of the following components：Deionized water 30~45%, amino acid surfactant 20
~35%, rose 10~20%, glycerine 2~10%, glycine betaine 2~8%, plant extraction elite 1~3%, 1,2- oneself two
Alcohol 0.1~1%, citric acid 0.1~0.3%, hydroxyethyl cellulose 0.1~0.5%.
Preferably, the amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionization
Water 35~40%, amino acid surfactant 25~30%, rose 12~16%, glycerine 3~8%, glycine betaine 3~7%,
1.5~3%, 1,2- hexylene glycol 0.3~0.8% of plant extraction elite, citric acid 0.1~0.2%, hydroxyethyl cellulose 0.1~
0.2%.
Preferably, the amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionization
Water 40%, amino acid surfactant 30%, rose 15%, glycerine 6%, glycine betaine 6%, plant extraction elite 2%, 1,
2- hexylene glycols 0.6%, citric acid 0.2%, hydroxyethyl cellulose 0.2%.
Preferably, the amino acid surfactant is lauroyl Sodium L-alaninate.
Preferably, the plant extraction elite includes tuberose extract and shepherd's purse extract.
Preferably, the mass ratio of the tuberose extract and shepherd's purse extract is 0.5~2:1.
Tuberose, also known as cordate telosma, Amaryllidaceae, belongs to herbaceos perennial.Saponin is be widely present in plant kingdom one
The special glucoside of class, can produce lasting saponiform foam after its aqueous solution shaking, have good cleaning efficacy.It is late fragrant
Contain sapogenin 1.8% or so in beautiful root, be mainly Tigogenin, hecogenin and 9- dehydrohecogenins, can be with
Saponin is extracted from tuberose.After the extracting method of the tuberose extract cleans up segment for (a) tuberose root, crush
After machine crushes, according to 1:10 solid-liquid ratios add deionized water, then add the pectase after dilution, stirring extraction；(b) enzyme deactivation,
Cooling, coarse filtration, refined filtration；(c) decolourize, cool down, filtering, filtrate sterilizing anti-corrosion, obtains tuberose extracting solution.
Shepherd's purse is Cruciferae one, biennial herb plant, is widely distributed in Chinese each province, contains glycosides in shepherd's purse extract
The components such as class, amino acid, organic acid and flavones, there is the effect of cleaning, skin care and anti-inflammatory.Shepherd's purse extract of the present invention
Extracting method is：A certain amount of dry shepherd's purse is taken, is wrapped, is placed in apparatus,Soxhlet's with filter paper, add ethanol.It is heated to reflux a few hours
Afterwards, extracting solution is placed on evaporator and evaporated.Obtained solid matter is poured into separatory funnel, is used petroleum ether with after hot water dissolving
Extraction, until petroleum ether layer is colourless, discards petroleum ether layer, is being evaporated after remaining aqueous solution is repeatedly extracted with ethyl acetate again
It is evaporated to dryness on device, obtains shepherd's purse extract.
Rose (also known as crystal's oil, Hydrolat), refers to the water that essential oil stays during distillation extraction, is essence
A kind of byproduct of oil, is a kind of hydrosol for 100% saturation separated during essential oil is refined, and composition is naturally pure,
Fragrance is light pleasant.The effect of rose can directly penetrate into cell interior from it, near with cell by strengthening
The activity of capillary even come have the function that nutrition supply, toxin exclude, balance blood vessel and fat secretion.It is quick at the same time to mend
The moisture of cell is filled, increases the water content of moisture in cell, fundamentally solves the problems, such as dry skin, product is reached good
Moisture-keeping efficacy.In addition, what is included inside rose is the volatile aromatic component of substantial amounts of fresh rose flower, pleasant aroma, compared with
Essence has the advantages that natural harmless.Preferably Ping Yin Rose of the invention as raw material, Ping Yin Rose be referred to as " Chinese rose it
King ", the environment of its growth is suitable, conveniently situation, the rose aromatic flavour made with it, moisturizing and nourishing effect
More preferably.
Preferably, the plant extraction elite further includes horse chestnut extract, and by weight percentage, the horse chestnut carries
It is 0.5~1.5% to take thing, and the horse chestnut extract can promote blood circulation, so as to provide various nutrition for skin, take away generation
Thank to product, accelerate skin metabolism, reaching improves elastic, the low and deep tarnish of improvement skin, slow down microgroove, improve drying slightly
Rough, reduction fat metabolism Product bulk, improves skin senescence and sub-health state.It can suppress to destroy venous structures integrality
Enzyme, such as the activity of Collagenase, hyaluronidase, gst enzyme and elastoser etc., the blood vessel knot of maintaining healthy
Structure balances and blood circulation, also has certain effect for the pouch produced because of fat accumulation, while have necessarily to Green Tea Extract
Oxidation resistant effect.
1,2- hexylene glycol is as one of indispensable important raw and processed materials component being widely used in cosmetic industry, temperature
Do not stimulate skin, good synergistic effect played to skin moisturizing, substituted traditional irritation preservative be added to it is clean
In papula foam, antibacterial, corrosion-resistant effect can be played.
The preparation method of amino acid moisturizing face cleaning foam of the present invention is：(a) hydroxyethyl cellulose is added into glycerine
In, it is uniformly dispersed, citric acid is previously dissolved in the water of part, spare；(b) add water in emulsification pot, by A phases raw material and glycerine point
The hydroxyethyl cellulose dissipated is added in emulsification pot, and mixing speed 600rpm, is warming up to 80 DEG C~85 DEG C, be evacuated to-
Below 0.05MPa, insulated and stirred 30min；(c) it is slowly introducing cooling water after keeping the temperature to start to cool down, mixing speed is adjusted to
600rpm, cooling rate are 1~1.5 DEG C/min；(d) when temperature is down to 45 DEG C, aqueous citric acid solution is added by filter screen,
1,2- hexylene glycols are stirring evenly and then adding into, as raw material has impurity to be kept stirring speed with being added after the filtering of 200 mesh filter screens in kettle
Degree and cooling rate are constant, continue to cool down；(e) when temperature is down to 35 DEG C, discharge after the assay was approved.
Compared with prior art, amino acid pattern moisturizing face cleaning foam provided by the invention without soap matter and any essence and is prevented
Rotten agent, cleaning effect is strong, and moistening effect is lasting, is more suitable for sensitive skin crowd；In faintly acid, close to the pH of human skin
Value, gentle pro-skin, using it is rear it is smooth, comfortable, without tight feeling, the protection function of quick-recovery skin soon is capable of after clean skin, makes skin
Acid-base balance, is adapted to overwhelming majority skin quality simultaneously can long-time service.
Brief description of the drawings
Fig. 1 is the cleaning capacity evaluation figure of face cleaning foam prepared by embodiment 1.
Fig. 2 is the moisture-retaining capacity evaluation figure of face cleaning foam prepared by embodiment 1.
Fig. 3 is the degreasing ability evaluation figure of face cleaning foam prepared by embodiment 1.
Embodiment
With reference to specific embodiment, the present invention is described further：
Embodiment 1
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 40%,
Lauroyl Sodium L-alaninate 30%, rose 15.5%, glycerine 8%, glycine betaine 3%, tuberose extract 1.5%, shepherd's purse carries
Take thing 1.5%, 1,2- hexylene glycol 0.3%, citric acid 0.1%, hydroxyethyl cellulose 0.1%.
Embodiment 2
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 35%,
Lauroyl Sodium L-alaninate 25%, rose 19.8%, glycerine 9%, glycine betaine 7%, tuberose extract 1%, shepherd's purse extraction
Thing 2%, 1,2- hexylene glycols 0.8%, citric acid 0.2%, hydroxyethyl cellulose 0.2%.
Embodiment 3
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 39%,
Lauroyl Sodium L-alaninate 29%, rose 15%, glycerine 8%, glycine betaine 5%, tuberose extract 1.8%, shepherd's purse extraction
Thing 1.2%, 1,2- hexylene glycols 0.5%, citric acid 0.25%, hydroxyethyl cellulose 0.25%.
Embodiment 4
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 30%,
Lauroyl Sodium L-alaninate 35%, rose 20%, glycerine 10%, glycine betaine 2%, tuberose extract 1%, shepherd's purse extract
1%, horse chestnut extract 0.5%, 1,2- hexylene glycol 0.1%, citric acid 0.1%, hydroxyethyl cellulose 0.3%.
Embodiment 5
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 45%,
Lauroyl Sodium L-alaninate 27%, rose 18%, glycerine 3%, glycine betaine 3%, tuberose extract 2%, shepherd's purse extract
1%, 1,2- hexylene glycol 0.6%, citric acid 0.3%, hydroxyethyl cellulose 0.1%.
Embodiment 6
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 45%,
Lauroyl Sodium L-alaninate 28%, rose 14%, glycerine 2%, glycine betaine 8%, tuberose extract 0.5%, shepherd's purse extraction
Thing 0.5%, horse chestnut extract 1%, 1,2- hexylene glycol 0.6%, citric acid 0.2%, hydroxyethyl cellulose 0.2%.
Embodiment 7
A kind of amino acid pattern moisturizing face cleaning foam, it is by weight percentage, composed of the following components：Deionized water 40%,
Lauroyl Sodium L-alaninate 20%, rose 20%, glycerine 10%, glycine betaine 6%, tuberose extract 1%, shepherd's purse extract
1.5%, 1,2- hexylene glycol 0.7%, citric acid 0.3%, hydroxyethyl cellulose 0.5%.
Following experiments are carried out for face cleaning foam prepared by embodiment 1：
First, safety evaluatio-human body patch experiment
(1) experimental principle：After the skin or mucosal contact sensibiligen of patient produce allergic reaction, if appointing in body surface
What location contacts to and same sensibiligen or structure are similar, have the material of same antigen, contact site will occur quickly
Scytitis reacts, this i.e. allergic contact dermatitis.
(2) skin closure type patch test dermoreaction grade scale, is shown in Table 1：
1 patch of table tests dermoreaction grade scale
(3) experimental procedure：
1. the personnel 30 of experiment are participated in by the selection of subject enrollment standard；
2. this face cleaning foam 0.02mL~0.025mL is taken to be put into the small interior of spot examination device；
3. (No. 1 is blank control, is added without any material for test section；No. 2 be this product solution, No. 3 on the market certain
The solution of amino acid cleansing foam, No. 4 solution for soap base type face cleaning foam on the market)；
4. pass through certain time, according to whether having positive reaction to determine whether for sensitizer.
(4) result and analysis：
Experimental result is shown in Table 2, and as shown in Table 2, in 30 subjects, doubtful small erythema occur in an only people,
Remaining 29 good dermoreaction occurs invariably per capita.According to 2015《Cosmetics safety technical specification》Regulation draws this amino acid
Face cleaning foam does not cause human skin adverse reaction, therefore that is such face cleaning foam does not cause the bad of human skin
Reaction, security are very high.
The safety evaluatio table of face cleaning foam prepared by 2 embodiment 1 of table
2nd, cleaning force is evaluated
On the inside of left arm in the range of 4cm × 5cm, oiliness lipstick and eyebrow pencil are being smeared, is weighing equivalent this product and commercially available amino
Each 0.5g of acid type face cleaning foam, is applied to spot, gently rubs 1min, wash with water respectively.Effect is cleaned in observation, and is shot with camera
Record result.
By Fig. 1 cleaning results as it can be seen that amino acid cleansing foam can effectively remove mouth with commercially available amino acid pattern face cleaning foam
Red and eyebrow pencil dirt, shows that such amino acid cleansing foam has reached the cleaning effect same with commercially available amino acid pattern face cleaning product
Fruit.
3rd, moisture-retaining capacity is evaluated
(1) laboratory apparatus：Moisture of skin tester CM825；
(2) experiment condition：25 DEG C of room temperature, humidity 40~60%, accuracy of instrument ± 3%, 10 people of subject；
(3) experimental method：
1. using warm water arm of cleaning before test, after 30min, start to test；
2. selection subject's left and right arm marks two identical regions (4*4cm) as examination at palm base portion 5cm
Area is tested, is denoted as this product trial zone and commercially available amino acid pattern face cleaning foam test area respectively；
3. tester tests the moisture content of skin numerical value in each region using moisture of skin tester CM825, survey five times,
It is averaged；
4. subject smeared respectively in left and right arm Test sites Liang Ge areas equivalent this product and commercially available amino acid pattern it is clean
Papula foam cleans；
5. after 30min, start to test the water content in different subject's different tests areas；
6. testing procedure 5. after the completion of, per every other hour, then once tested, record data.
By analyzing moisture content of skin, trial zone moisture content of skin is changed over time and changed data result, is surveyed
Numerical quantity is bigger, and moisture content of skin is higher, and it is fewer to illustrate that moisture of skin scatters and disappears, and the moistening effect of product is better.It is tested by detecting
The numerical value of person's moisture content of skin, assesses the moistening effect of product.
Test result is shown in Fig. 2, and as shown in Figure 2 in test period 4h, this product group moisture content of skin is always above commercially available
Amino acid pattern face cleaning foam group；Particularly substantially reduced in 1~4h, commercially available amino acid pattern face cleaning foam group moisture content of skin, and
This product group moisture content of skin slightly reduces.From analysis relatively, this product has more than commercially available amino acid pattern face cleaning foam
Accommodate continuous moistening effect.
4th, degreasing ability is evaluated
1. select 20 volunteers, with MPA580, Sebumeter (oil content test probe) in the environment of 25 DEG C of constant temperature,
Using forehead, left cheek, lower-left jaw as test section, test before face cleaning and contained with the grease of regional after this product face cleaning respectively
Amount.Degreasing ability is evaluated with oil stain removing rate；
2. skin oil and fat before oil stain removing rate=(skin oil and fat content after skin oil and fat content-clean skin before clean skin)/clean skin
Content × 100%；
3. result and analysis
The skin surface of people has one layer of natural sebum film, and the face cleaning product of the strong degreasing power of long-time service can destroy this layer
Sebum film, reduces the self-protection ability of skin, and good face cleaning product can prevent dry skin person's degreasing but also remove oiliness
The excessive grease of skin person.
This experimental subjects totally 20 people, wherein numbering 1-10 subject for Oily subject the skin after using this product
Skin fat content has different degrees of decline, numbering 11-20 subject skin after using this product for dry skin subject
Skin fat content does not have significant change to a certain extent.Due to the difference of different subjects skin's situations so that different tested
The difference of person's skin oil and fat clean rate, but grease cleaning rate is stable in normal scope.Result can (see Fig. 3) according to the experiment
Know, this product can show better degreasing power for different crowds.
The above described is only a preferred embodiment of the present invention, being not the limitation for making other forms to the present invention, appoint
What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc.
Imitate embodiment.But it is every without departing from technical solution of the present invention content, the technical spirit according to the present invention is to above example institute
Any simple modification, equivalent variations and the remodeling made, still fall within the protection domain of technical solution of the present invention.
Claims (6)
1. a kind of amino acid pattern moisturizing face cleaning foam, it is characterised in that by weight percentage, composed of the following components：Go from
Sub- water 30~45%, amino acid surfactant 20~35%, rose 10~20%, glycerine 2~10%, glycine betaine 2~
8%, 1~3%, 1,2- hexylene glycol 0.1~1% of plant extraction elite, citric acid 0.1~0.3%, hydroxyethyl cellulose 0.1~
0.5%.
2. amino acid pattern moisturizing face cleaning foam as claimed in claim 1, it is characterised in that by weight percentage, by following
Component forms：Deionized water 35~40%, amino acid surfactant 25~30%, rose 12~16%, glycerine 3~
8%, glycine betaine 3~7%, 1.5~3%, 1,2- hexylene glycol 0.3~0.8% of plant extraction elite, citric acid 0.1~0.2%,
Hydroxyethyl cellulose 0.1~0.2%.
3. amino acid pattern moisturizing face cleaning foam as claimed in claim 2, it is characterised in that by weight percentage, by following
Component forms：Deionized water 40%, amino acid surfactant 30%, rose 15%, glycerine 6%, glycine betaine 6%, plants
Thing extracts elite 2%, 1,2- hexylene glycol 0.6%, citric acid 0.2%, hydroxyethyl cellulose 0.2%.
4. the amino acid pattern moisturizing face cleaning foam as described in claim 1-3 is any, it is characterised in that the plant extraction elite
Including tuberose extract and shepherd's purse extract.
5. amino acid pattern moisturizing face cleaning foam as claimed in claim 4, it is characterised in that the tuberose extract and shepherd's purse
The mass ratio of extract is 0.5~2:1.
6. amino acid pattern moisturizing face cleaning foam as claimed in claim 5, it is characterised in that the amino acid surfactant is
Lauroyl Sodium L-alaninate.
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| CN201711462321.3A CN107898711A (en) | 2017-12-28 | 2017-12-28 | A kind of amino acid pattern moisturizing face cleaning foam |
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| CN201711462321.3A CN107898711A (en) | 2017-12-28 | 2017-12-28 | A kind of amino acid pattern moisturizing face cleaning foam |
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ID=61871783
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Cited By (1)
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Application publication date: 20180413 |