CN112263492A - Formula of jelly-like suspended oil drop high-moisture sleeping mask and preparation process thereof - Google Patents
Formula of jelly-like suspended oil drop high-moisture sleeping mask and preparation process thereof Download PDFInfo
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- CN112263492A CN112263492A CN202011358801.7A CN202011358801A CN112263492A CN 112263492 A CN112263492 A CN 112263492A CN 202011358801 A CN202011358801 A CN 202011358801A CN 112263492 A CN112263492 A CN 112263492A
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- solution
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- moisture
- skin
- hexanediol
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- 238000002360 preparation method Methods 0.000 title abstract description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 54
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims abstract description 26
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims abstract description 22
- 229920002545 silicone oil Polymers 0.000 claims abstract description 22
- 150000004676 glycans Chemical class 0.000 claims abstract description 19
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 19
- 239000005017 polysaccharide Substances 0.000 claims abstract description 19
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 19
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 18
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 18
- 239000013535 sea water Substances 0.000 claims abstract description 17
- 235000001855 Portulaca oleracea Nutrition 0.000 claims abstract description 15
- 235000011187 glycerol Nutrition 0.000 claims abstract description 15
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 14
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229960001631 carbomer Drugs 0.000 claims abstract description 14
- 229940015975 1,2-hexanediol Drugs 0.000 claims abstract description 13
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims abstract description 13
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 13
- DFPAKSUCGFBDDF-ZQBYOMGUSA-N [14c]-nicotinamide Chemical compound N[14C](=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-ZQBYOMGUSA-N 0.000 claims abstract description 13
- 239000001110 calcium chloride Substances 0.000 claims abstract description 13
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 13
- 229920001577 copolymer Polymers 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001509 sodium citrate Substances 0.000 claims abstract description 13
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229920002148 Gellan gum Polymers 0.000 claims abstract description 8
- 239000007853 buffer solution Substances 0.000 claims abstract description 8
- 239000000216 gellan gum Substances 0.000 claims abstract description 8
- 235000010492 gellan gum Nutrition 0.000 claims abstract description 8
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229940072056 alginate Drugs 0.000 claims abstract description 6
- 235000010443 alginic acid Nutrition 0.000 claims abstract description 6
- 229920000615 alginic acid Polymers 0.000 claims abstract description 6
- 239000000243 solution Substances 0.000 claims description 51
- 238000003756 stirring Methods 0.000 claims description 20
- 241000219304 Portulacaceae Species 0.000 claims description 14
- 241000596504 Tamarindus Species 0.000 claims description 12
- 235000004298 Tamarindus indica Nutrition 0.000 claims description 12
- BQMNFPBUAQPINY-UHFFFAOYSA-N azane;2-methyl-2-(prop-2-enoylamino)propane-1-sulfonic acid Chemical compound [NH4+].[O-]S(=O)(=O)CC(C)(C)NC(=O)C=C BQMNFPBUAQPINY-UHFFFAOYSA-N 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 5
- 239000000872 buffer Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- ACCCMOQWYVYDOT-UHFFFAOYSA-N hexane-1,1-diol Chemical compound CCCCCC(O)O ACCCMOQWYVYDOT-UHFFFAOYSA-N 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- FWFUWXVFYKCSQA-UHFFFAOYSA-M sodium;2-methyl-2-(prop-2-enoylamino)propane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(C)(C)NC(=O)C=C FWFUWXVFYKCSQA-UHFFFAOYSA-M 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 3
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 2
- 229940058015 1,3-butylene glycol Drugs 0.000 claims 1
- 239000002537 cosmetic Substances 0.000 abstract description 6
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- 244000234609 Portulaca oleracea Species 0.000 abstract 1
- YLGYACDQVQQZSW-UHFFFAOYSA-N n,n-dimethylprop-2-enamide Chemical compound CN(C)C(=O)C=C YLGYACDQVQQZSW-UHFFFAOYSA-N 0.000 abstract 1
- 229940104261 taurate Drugs 0.000 abstract 1
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 41
- 230000003020 moisturizing effect Effects 0.000 description 24
- 238000012360 testing method Methods 0.000 description 10
- 239000003921 oil Substances 0.000 description 8
- 230000001815 facial effect Effects 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
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- 238000004519 manufacturing process Methods 0.000 description 4
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- 241000227647 Fucus vesiculosus Species 0.000 description 3
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- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
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- QRYRORQUOLYVBU-VBKZILBWSA-N Carnosic acid Natural products CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 description 1
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- CQOVPNPJLQNMDC-UHFFFAOYSA-N N-beta-alanyl-L-histidine Natural products NCCC(=O)NC(C(O)=O)CC1=CN=CN1 CQOVPNPJLQNMDC-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
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- CQOVPNPJLQNMDC-ZETCQYMHSA-N carnosine Chemical compound [NH3+]CCC(=O)N[C@H](C([O-])=O)CC1=CNC=N1 CQOVPNPJLQNMDC-ZETCQYMHSA-N 0.000 description 1
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Images
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Mycology (AREA)
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a jelly-shaped suspended oil-drop high-moisture sleeping mask and a preparation process thereof, wherein the sleeping mask comprises the following components: glycerol, butanediol, seawater, lima bean seed polysaccharide, acryloyl dimethyl ammonium taurate/VP copolymer, nicotinamide, carbomer, p-hydroxyacetophenone, 1, 2-hexanediol, sodium hyaluronate, EDTA-disodium, purslane, alginate gel, gellan gum, calcium chloride, a citric acid and sodium citrate buffer system, phenyl silicone oil and the balance of deionized water. The invention has stable and controllable quality, mild and non-irritant use and simple preparation process, and is suitable for large-scale development.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a jelly-shaped suspended oil-drop high-moisture sleeping mask and a preparation process thereof.
Background
At present, the working pressure of women is large, the sleep quality becomes poor, the poor sleep directly leads to the skin of the next day dull and dull, the skin all can become comparatively dry, except that some fruits and vegetables need to be eaten more at this time, skin care products are also indispensable, so many women's friends all can seek the good product of moisturizing, the water emulsion must be indispensable on moistening and caring the skin, but the dry problem that wants to solve the skin is not enough. In order to enable the skin to absorb sufficient moisture at night and keep the skin in a tender state, a sleep mask with high water locking and moisturizing functions is essential. At present, most of people mainly adopt a relieving mode in the selection of cosmetics, and simultaneously, safe and zero chemical addition is needed, so that good skin care effect can be achieved, and irritation to skin can be reduced.
Disclosure of Invention
In order to effectively solve the problems in the background art, the invention provides a jelly-shaped suspended oil drop high-moisture sleeping mask and a preparation process thereof, and the specific technical scheme is as follows;
a jelly-like suspended oil-drop high-moisture-retention sleeping mask comprises the following components: 4.0-8.0% of glycerin, 2.0-5.0% of butanediol, 1-3% of seawater, 0.1-1.0% of tamarind seed polysaccharide, 0.4-1.0% of ammonium acryloyldimethyl taurate/VP copolymer, 1.0-3.0% of nicotinamide, 0.1-0.4% of carbomer, 0.3-0.6% of p-hydroxyacetophenone, 0.3-0.6% of 1, 2-hexanediol, 0.1-0.2% of sodium hyaluronate, 0.01-0.1% of EDTA-disodium, 0.2-1% of purslane, 0.5-2% of alginate gel, 0.2-0.6% of gellan gum, 0.05-0.2% of calcium chloride, 0.5-2% of citric acid and sodium citrate buffer system, 1-4% of phenyl silicone oil and the balance of deionized water.
Comprises the following components by weight: 5% of glycerol, 4% of butanediol, 2% of seawater, 0.5% of tamarind seed polysaccharide, 0.6% of acryloyl dimethyl taurate/VP copolymer, 1% of nicotinamide, 0.2% of carbomer, 0.2% of p-hydroxyacetophenone, 0.4% of 1, 2-hexanediol, 0.1% of sodium hyaluronate, 0.02% of EDTA-disodium, 1% of purslane, 1% of furcellaran, 0.4% of gellan gum, 0.06% of calcium chloride, a proper buffer amount of citric acid and sodium citrate, 2% of phenyl silicone oil and the balance of deionized water
The butanediol is 1, 3-butanediol.
The invention also comprises a method for preparing the jelly-shaped suspended oil drop high-moisture-retention sleeping mask, which comprises the following steps:
1) mixing p-hydroxyacetophenone, glycerol, nicotinamide, EDTA-disodium, deionized water and butanediol, heating to 85 ℃ to obtain a solution A;
2) adding the soaked ammonium acryloyl dimethyl taurate/VP copolymer into the solution A, and homogenizing for 1 minute to obtain a solution B;
3) adding the prepared citric acid and citric acid buffer solution into the solution B to obtain a solution C, and adding calcium chloride to obtain a solution D; stirring and cooling;
4) after the temperature of the solution D is reduced to 55 ℃, adding seawater, tamarind seed polysaccharide, 1, 2-hexanediol, sodium hyaluronate, purslane and phycocolloid into the solution D, starting stirring, and uniformly stirring to obtain a solution E;
5) and adding carbomer, sodium citrate, phenyl silicone oil and hexanediol into the solution E, stirring at a high speed, and adjusting the pH to 6.0-7.0 to obtain the jelly-like suspended oil-drop high-moisture sleeping mask.
Compared with the prior art, the invention has the beneficial effects that:
the common sleep mask in the prior art usually does not contain oil, or contains less oil after emulsification, and can not achieve the double effects of water replenishing and water locking, the common sleep mask usually adopts glycerin and carbomer to be coated on the surface of the skin to achieve the effect of water replenishing, but can not reduce the loss of water, and in the application, the macromolecular sodium hyaluronate forms a layer of moisturizing and bright breathable film on the surface layer of the skin by adopting phenyl silicone oil and glycerin which are not emulsified, lima bean seed polysaccharide and a moisturizing solvent sodium hyaluronate thereof. And secondly, the sour soybean seed polysaccharide reduces the skin roughness, increases the skin elasticity and endows velvet skin feeling. And finally, the phenyl silicone oil locks water.
After ensuring that the skin does not lose moisture, to bind more moisture. The invention adds the seawater extracted from the natural reservoir with the depth of more than 22 meters, and the seawater passes through the silicate sand bed and the granite, so that richer special active ingredients are obtained, high-content manganese and silicon are contained, and the silicon directly influences the production of collagen and articular cartilage tissues in vivo and participates in polysaccharide metabolism; manganese is a paving factor of various enzyme systems in human bodies; the sea spring water can strengthen the connectivity of keratinocytes and the skin, thereby improving the firmness of the skin by enhancing the lipid barrier of the skin, preventing transepidermal water loss and helping to maintain skin hydration.
The Fucus vesiculosus Gel (Gmoist Sea-Gel) is a novel humectant which takes Sea plant Fucus vesiculosus as a source, and is focused on preventing dry skin by regulating and controlling formation of cornification and envelope and repairing cutin barrier, so that the problem of skin water shortage is fundamentally solved, and meanwhile, the Fucus vesiculosus Gel has excellent skin feeling and enables the skin to be transparent, moist and glossy after being used.
Purslane is also called longevity grass in China, and is rich in a large amount of flavonoids, adrenalines, polysaccharides, various vitamins, amino acids and other compounds. The effect of the purslane extracting solution is as follows: resisting skin allergy, irritation, inflammation and acne.
In addition, in the extracellular matrix, polysaccharides, together with other polysaccharide components in the skin and fibrous proteins, constitute an extracellular matrix containing a large amount of moisture, providing moisture to the skin.
The phenyl silicone oil and the sodium hyaluronate are matched for use, so that the silky feeling of the product can be increased, and the time for drying the skin can be prolonged. Carnosine is a component present in human muscle, has a strong antioxidant aging function, and can eliminate free radicals. The skin aging problem is avoided.
In conclusion, through the synergistic effect of the parts, the skin can penetrate deeply into the skin to reduce skin inflammation and regulate the secretion of skin grease. The barrier function of the skin is enhanced to perfect the moisturizing function of the skin, and then the active matters deeply enter the skin to lock more water to enable the skin to be full, so that the moisturizing effect is achieved. Finally, a breathable moisturizing film is formed on the surface layer of the skin, so that the loss of water is reduced. The internal and external moisturizing interaction and the multiple moisturizing effects act together, and finally the skin care component with the multiple moisturizing effects and the facial mask thereof are prepared. The invention has stable and controllable quality, mild and non-irritant use and simple preparation process, and is suitable for large-scale development.
Drawings
Fig. 1 shows different embodiments and a graph of a scale-resolved long-lasting moisturization effect.
Detailed Description
In order that those skilled in the art will better understand the technical scheme of the invention, the invention is further described in detail in the following with reference to the accompanying drawings and embodiments;
example 1: 5 parts of glycerol, 4 parts of butanediol, 2 parts of seawater, 0.5 part of tamarind seed polysaccharide, 0.6 part of acryloyl dimethyl taurate/VP copolymer, 1 part of nicotinamide, 0.2 part of carbomer, 0.2 part of p-hydroxyacetophenone, 0.4 part of 1, 2-hexanediol, 0.1 part of sodium hyaluronate, 0.02 part of EDTA-disodium, 1 part of purslane, 1 part of alginate jelly, 0.4 part of gellan gum, 0.06 part of calcium chloride, a proper buffer amount of citric acid and sodium citrate, the balance of deionized water and 0.5 part of phenyl silicone oil.
The process for preparing the jelly-shaped suspended oil drop high-moisture sleeping mask comprises the following steps: (1) mixing p-hydroxyacetophenone, glycerol, nicotinamide, EDTA-disodium, deionized water and butanediol, heating to 85 ℃ to obtain a solution A; (2) adding the soaked ammonium acryloyl dimethyl taurate/VP copolymer into the solution A, and homogenizing for 1 minute to obtain a solution B; (3) and adding the prepared citric acid and the buffer solution of the citric acid into the solution B to obtain a solution C, and adding calcium chloride to obtain a solution D. Stirring and cooling. (4) After the temperature of the solution D is reduced to 55 ℃, adding seawater, tamarind seed polysaccharide, 1, 2-hexanediol, sodium hyaluronate, purslane and phycocolloid into the solution D, starting stirring, and uniformly stirring to obtain a solution E; (5) and adding carbomer, sodium citrate, phenyl silicone oil and hexanediol into the solution E, stirring at a high speed, and adjusting the pH to 6.0-7.0 to obtain the jelly-shaped suspended oil-drop high-moisture sleeping mask.
Control group 1: comparative example 1 differs from example 1 only in that no phenyl silicone oil was added.
Control group 2: comparative example 2 differs from example 1 only in that sodium hyaluronate was not added.
Control group 3: comparative example 3 differs from example 1 only in that no seawater was added.
Example 2: example 1: 5 parts of glycerol, 4 parts of butanediol, 2 parts of seawater, 0.5 part of tamarind seed polysaccharide, 0.6 part of acryloyl dimethyl taurate/VP copolymer, 1 part of nicotinamide, 0.2 part of carbomer, 0.2 part of p-hydroxyacetophenone, 0.4 part of 1, 2-hexanediol, 0.1 part of sodium hyaluronate, 0.02 part of EDTA-disodium, 1 part of purslane, 1 part of alginate jelly, 0.4 part of gellan gum, 0.06 part of calcium chloride, a proper buffer amount of citric acid and sodium citrate, the balance of deionized water and 1 part of phenyl silicone oil.
The process for preparing the jelly-like suspended oil drop high-moisture sleeping mask (1) comprises the steps of mixing p-hydroxyacetophenone, glycerol, nicotinamide, EDTA-disodium, deionized water and butanediol, heating, and heating to 85 ℃ to obtain a solution A; (2) adding the soaked ammonium acryloyl dimethyl taurate/VP copolymer into the solution A, and homogenizing for 1 minute to obtain a solution B; (3) and adding the prepared citric acid and the buffer solution of the citric acid into the solution B to obtain a solution C, and adding calcium chloride to obtain a solution D. Stirring and cooling. (4) After the temperature of the solution D is reduced to 55 ℃, adding seawater, tamarind seed polysaccharide, 1, 2-hexanediol, sodium hyaluronate, purslane and phycocolloid into the solution D, starting stirring, and uniformly stirring to obtain a solution E; (5) and adding carbomer, sodium citrate, phenyl silicone oil and hexanediol into the solution E, stirring at a high speed, and adjusting the pH to 6.0-7.0 to obtain the jelly-shaped suspended oil-drop high-moisturizing sleep mask.
Example 3: 5 parts of glycerol, 4 parts of butanediol, 2 parts of seawater, 0.5 part of tamarind seed polysaccharide, 0.6 part of acryloyl dimethyl taurate/VP copolymer, 1 part of nicotinamide, 0.2 part of carbomer, 0.2 part of p-hydroxyacetophenone, 0.4 part of 1, 2-hexanediol, 0.1 part of sodium hyaluronate, 0.02 part of EDTA-disodium, 1 part of purslane, 1 part of alginate jelly, 0.4 part of gellan gum, 0.06 part of calcium chloride, a proper buffer amount of citric acid and sodium citrate, the balance of deionized water and 2 parts of phenyl silicone oil.
The process for preparing the jelly-like suspended oil drop high-moisture sleeping mask (1) comprises the steps of mixing p-hydroxyacetophenone, glycerol, nicotinamide, EDTA-disodium, deionized water and butanediol, heating, and heating to 85 ℃ to obtain a solution A; (2) adding the soaked ammonium acryloyl dimethyl taurate/VP copolymer into the solution A, and homogenizing for 1 minute to obtain a solution B; (3) and adding the prepared citric acid and the buffer solution of the citric acid into the solution B to obtain a solution C, and adding calcium chloride to obtain a solution D. Stirring and cooling. (4) After the temperature of the solution D is reduced to 55 ℃, adding seawater, tamarind seed polysaccharide, 1, 2-hexanediol, sodium hyaluronate, purslane and phycocolloid into the solution D, starting stirring, and uniformly stirring to obtain a solution E; (5) and adding carbomer, sodium citrate, phenyl silicone oil and hexanediol into the solution E, stirring at a high speed, and adjusting the pH to 6.0-7.0 to obtain the jelly-shaped suspended oil-drop high-moisture sleeping mask.
The test population: the total 30 persons, age 30-60 years, meet the volunteer selection standard health condition of the subject.
Selecting a detected part: the area of 3cm multiplied by 3cm inside the left and right front arms is used as the detected area. The test article is randomly stuck on the inner sides of the left and right front arms.
The test conditions are below 20 plus or minus 2 ℃ at room temperature and below 50 plus or minus 5% of Relative Humidity (RH).
Instruments and reagents: one Corneometer and one hygrothermograph.
When the strength of the moisturizing effect of the moisturizing cosmetic is judged, a single application test, i.e., a moisturizing performance test, which is completed in a short time is preferably performed. The moisturizing effect can be analyzed by applying moisturizing mask liquid for 1 time in a short period and adding a water load test of the organism cuticle in the test of measuring the water content of the cuticle. The method is mainly used for determining whether the humectant has moisture retention property when selecting the humectant in the formula, and determining the optimum concentration when comparing the humectant with a matrix. Before the mask is applied, the moisture content of the horny layer of the detected part is measured. Applying the sample by using a latex finger sleeve; measuring the relative increase rate of the skin water content immediately after the test article is applied for 15min, 1h, 2h, 4h, 6h and 8 h; measuring the water content of stratum corneum of each tested part for 5 times to obtain an average value; the results of the measurements are shown in table 1 for the relative rate of increase in skin moisture content at different times.
TABLE 1
| Group of | Before application | 1h | 2h | 4h | 6h | 8h |
| Example 1 | 0 | 50 | 48 | 45 | 35 | 26 |
| Example 2 | 0 | 52 | 49 | 45 | 36 | 26 |
| Example 3 | 0 | 70 | 65 | 60 | 50 | 40 |
| Control group 1 | 0 | 32 | 30 | 26 | 22 | 18 |
| Control group 2 | 0 | 28 | 25 | 23 | 20 | 15 |
| Control group 3 | 0 | 30 | 26 | 25 | 20 | 15 |
When the moisturizing ability of cosmetics is judged, the moisturizing ability is not immediately obtained. Effective moisturizing for a long time is also important for use as a cosmetic. The long-acting moisturizing effect can be analyzed by adding a water load test of the organism cuticle in a test of measuring the water content of the cuticle by using the moisturizing mask liquid for long-term application as shown in figure 1.
As can be seen from Table 1, the relative water content of the facial mask on the skin is obviously improved, and particularly within the time range of 0-1h after the facial mask is used, the moisturizing effect is reduced along with the prolonging of time, but within the test time range, the relative water content of the skin is still obviously improved within 8h and is higher than that of the skin before the facial mask is applied, so that the moisturizing facial mask liquid prepared in the embodiment 3 of the invention has an obvious moisturizing effect. And relatively example 3 is much larger than example 1 and example 2. Example 1 is comparable to example 2. The difference from example 3 is that the content of phenyl silicone oil is higher than that of example 1 and example 2, and reaches 2%. The control group without the phenyl silicone oil had a relatively weak ability to increase the moisture content of the skin relative to the control group after the addition. In conclusion, the phenyl silicone oil has no stimulation at a content of 2 percent, and the performance of the phenyl silicone oil on the active substance is improved by about 52 percent of absorption rate.
And the difference between the control group 2 and the control group 3 compared to example 1 was that sodium hyaluronate was not added and seawater was not added, respectively. The moisturizing effect of example 1 was much greater than control 2 and control 3. And (4) conclusion: the 0.1 percent sodium hyaluronate and the phenyl silicone oil are matched for use, so that the moisture retention rate can be improved by about 42 percent.
The results of figure 1 show that the facial mask can obviously improve the moisture content in the skin, moisturize and moisturize for a long time and improve the dry state of the skin, the moisture content of the skin is increased by 15% after two weeks of use, and the moisture content of the skin is increased by 22% after four weeks of use.
The same example 3 has considerable advantages over examples 1 and 2 with respect to long-term moisturization.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the invention.
Claims (4)
1. The jelly-shaped suspended oil-drop high-moisture-retention sleeping mask is characterized by comprising the following components: 4.0-8.0% of glycerin, 2.0-5.0% of butanediol, 1-3% of seawater, 0.1-1.0% of tamarind seed polysaccharide, 0.4-1.0% of ammonium acryloyldimethyl taurate/VP copolymer, 1.0-3.0% of nicotinamide, 0.1-0.4% of carbomer, 0.3-0.6% of p-hydroxyacetophenone, 0.3-0.6% of 1, 2-hexanediol, 0.1-0.2% of sodium hyaluronate, 0.01-0.1% of EDTA-disodium, 0.2-1% of purslane, 0.5-2% of alginate gel, 0.2-0.6% of gellan gum, 0.05-0.2% of calcium chloride, 0.5-2% of citric acid and sodium citrate buffer system, 1-5% of phenyl silicone oil and the balance of deionized water.
2. The jelly-like suspended oil drop high-moisture-retention sleep mask as claimed in claim 1, which is characterized by comprising the following components by weight: 5% of glycerol, 4% of butanediol, 2% of seawater, 0.5% of tamarind seed polysaccharide, 0.6% of acryloyl dimethyl taurate/VP copolymer, 1% of nicotinamide, 0.2% of carbomer, 0.2% of p-hydroxyacetophenone, 0.4% of 1, 2-hexanediol, 0.1% of sodium hyaluronate, 0.02% of EDTA-disodium, 1% of purslane, 1% of furcellaran, 0.4% of gellan gum, 0.06% of calcium chloride, a proper amount of citric acid and sodium citrate buffer, 2% of phenyl silicone oil and the balance of deionized water.
3. The jelly-like suspended oil drop high moisture sleeping mask as claimed in claim 1, wherein the butylene glycol is 1, 3-butylene glycol.
4. A method for preparing the jelly-like suspended oil drop high moisture sleeping mask according to any one of claims 1 to 3, comprising the steps of:
1) mixing p-hydroxyacetophenone, glycerol, nicotinamide, EDTA-disodium, deionized water and butanediol, heating to 85 ℃ to obtain a solution A;
2) adding the soaked ammonium acryloyl dimethyl taurate/VP copolymer into the solution A, and homogenizing for 1 minute to obtain a solution B;
3) adding the prepared citric acid and citric acid buffer solution into the solution B to obtain a solution C, and adding calcium chloride to obtain a solution D; stirring and cooling;
4) after the temperature of the solution D is reduced to 55 ℃, adding seawater, tamarind seed polysaccharide, 1, 2-hexanediol, sodium hyaluronate, purslane and phycocolloid into the solution D, starting stirring, and uniformly stirring to obtain a solution E;
5) and adding carbomer, sodium citrate, phenyl silicone oil and hexanediol into the solution E, stirring at a high speed, and adjusting the pH to 6.0-7.0 to obtain the jelly-shaped suspended oil drop high-moisturizing sleep mask.
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