CN102762190A

CN102762190A - Flat cellulose powder processed with amphiphilic substance, and cosmetic preparation containing same

Info

Publication number: CN102762190A
Application number: CN2011800052922A
Authority: CN
Inventors: 村田东吾; 村田哲雄; 饭田亚美; 增渕祐二; 五十岚启二
Original assignee: Kose Corp; Ohken Co Ltd
Current assignee: Kose Corp; Ohken Co Ltd
Priority date: 2010-02-25
Filing date: 2011-02-25
Publication date: 2012-10-31
Anticipated expiration: 2031-02-25
Also published as: TW201143808A; WO2011105535A1; TWI495484B; HK1176304A1; JPWO2011105535A1; KR101626582B1; JP5932633B2; CN102762190B; KR20120135277A

Abstract

Disclosed are: a powder which exhibits good adhesion to the skin and has excellent dispersibility in an oil component or water; and a long-lasting cosmetic preparation which glides excellently smoothly during application and forms an excellently uniform cosmetic film. Specifically disclosed are: a flat cellulose powder processed with an amphiphilic substance, which is obtained by mechanically pulverizing a cellulose-based substance and one or more amphiphilic substances that are selected from the group consisting of phospholipids, ceramides, cholesterol and derivatives thereof, and phytosterols and derivative thereof; and a cosmetic preparation which contains the powder.

Description

Amphiphilic agent is handled plain powder body of flat fiber and the cosmetic material that contains it

[technical field]

The present invention relates to amphiphilic agent and handle plain powder body of flat fiber and the powder cosmetic that contains it; More particularly, relate to the cosmetic material that the amphiphilic agent that has flat shape and utilize amphiphilic agent that its surface has been carried out handling is handled the plain powder body of flat fiber and contained it.

[background technology]

Contain the powder body composition and be widely used at cosmetic field,, can enumerate foundation cream, eye shadow, face powder, rouge etc. as its example with the powder cosmetic that oiliness becomes to grade.

This powder cosmetic normally is filled in the ware shape container through the powder mixture with powder body compositions such as extender pigment, pigment and oiliness composition and is pressed and makes.

As employed powder body composition in this powder cosmetic, in order to make its spreadability, tack on skin good, use the laminal mica sheet that derives from natural materials, sericite, Talcum etc. or its surface treatment thing as extender pigment.And,, together used spherical organic powder body etc. with above-mentioned extender pigment in order to improve the suitable sliding or sense of touch of extender pigment on skin.Further, as pigment, colour lustre pigments such as painted pigment such as Chinese white, iron oxide red, mica titanium such as titanium dioxide have been used.

Among the above-mentioned powder body composition; As laminar composition, the mica sheet that is widely used, sericite, Talcum etc. are inorganic to be powder body, but these to be alumina silicate be mineral; And; According to the difference in the place of production, character is also slightly different, thereby has the problem that pick up the oil property for example is low, can not get the target rerum natura.On the other hand, do not see almost that for flat Organic substance powder body report is arranged, for example, the only known flat fiber crude granule (patent documentation 1) that afterwards it is carried out the mechanicalness pulverizing and obtain that cellulose-based material is mixed with fatty acid.

Yet, in this patent documentation 1,, its concrete use form is not had openly although disclose the flat fiber crude granule, also only have very simply open about the application in cosmetics.

Also known in addition have utilize hydrolecithin that Treatment Technology (patent documentation 2) is carried out on the surface of crystalline cellulose.But the major diameter of this crystalline cellulose is below 3 with the ratio (L/D) of minor axis, can't say that it is flat; In fact wherein disclose, when comparing with the thing that is untreated, although variant aspect the formedness that make up to keep, at usability---there is not very difference aspect " picking property ", " spreadability ", " accomplishing (Ga り on the bodyguard) property ".

[prior art document]

[patent documentation]

Patent documentation 1: TOHKEMY 2004-230719 communique

Patent documentation 2: TOHKEMY 2003-146829 communique

[summary of the invention]

[inventing problem to be solved]

Although multiple cosmetic material powder body is provided, consumer for usability more the demand of good cosmetic material be the trend of nature; Problem of the present invention is to provide a kind of cosmetic material powder body and the cosmetic material that uses it that such cosmetic material is provided.

[being used to solve the means of problem]

It is plain that the inventor is conceived to flat flat fiber; Flat fiber element and autofrettage thereof for rerum natura is more excellent are studied; Discovery prepares the flat fiber element through using specific amphiphilic agent through specific method; Can obtain having the plain powder body of surface-treated fiber of the rerum natura of failing so far to reach, and through utilizing the plain powder of this surface-treated fiber can greatly improve the commodity of material of making up such as powder cosmetic, thereby the present invention accomplished.

Promptly the present invention relates to a kind of amphiphilic agent and handle the plain powder body of flat fiber, it is through cellulose-based material and the amphiphilic agent in the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof of being selected from more than a kind or 2 kinds are carried out the mechanicalness pulverization process and obtain.

The invention still further relates to a kind of cosmetic material, this cosmetic material is characterised in that it contains above-mentioned amphiphilic agent handles the plain powder body of flat fiber.

The invention further relates to a kind of amphiphilic agent and handle the manufacturing approach of the plain powder body of flat fiber; It is characterized in that, cellulose-based material and the amphiphilic agent that is selected from the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof more than a kind or 2 kinds are carried out the mechanicalness pulverization process.

[invention effect]

It is good that amphiphilic agent of the present invention is handled the tack of the plain powder body of flat fiber on skin, and the cosmetic material that is combined with this powder body has smooth sense when coating, the excellent in uniformity of cosmetic film, and also cosmetic retentivity (change make-up and hold Chi) is good.

Thereby the cosmetic material that has utilized amphiphilic agent of the present invention to handle the plain powder body of flat fiber can suitably be used as foundation cream, eye shadow, face powder, rouge etc.

And, among above-mentioned amphiphilic agent is handled the plain powder body of flat fiber, in processing, used the dispersibility of powder body in general oil solution and water of phospholipid excellent especially.Therefore can be suitably as beauty and make-up material (メイ Network アップization make-up material) such as liquid foundation.And the tack of this powder body is good, and the cosmetic retentivity is excellent.Therefore, also can be suitably as beauty and make-up material such as foundation creams.

Further, above-mentioned amphiphilic agent is handled among the plain powder body of flat fiber, and the powder body that in processing, has used ceramide is at the moisture maintenance dose and suppress that moisture evapotranspires and wait aspect the moisture retention excellence especially.Therefore can suitably be used as cosmetic skin-care material, beauty and make-up material.

[specific embodiment]

It is through cellulose-based material and the amphiphilic agent in the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof of being selected from more than a kind or 2 kinds are carried out the mechanicalness pulverization process and make that amphiphilic agent of the present invention is handled the plain powder body of flat fiber.

Specifically; Amphiphilic agent is handled the plain powder body of flat fiber and can be made through following method: add being selected from more than a kind or 2 kinds of amphiphilic agent in the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof with respect to cellulose-based material; Mix as required etc., afterwards it is carried out the mechanicalness pulverization process.In this method,, can carry out according to the method that [0020]～[0041] is put down in writing of patent documentation 1 basically except grinding aid is become the amphiphilic agent.

As amphiphilic agents for treatment of the oblate cellulose starting material powder of the cellulose-based substance is not particularly limited, but preferably used, for example, from the wood of the fibrous or powdered wood flour or wood pulp derived from cotton (cotton flower ) fibrous or powdery kapok (cotton) or cotton linters (ri nn center have fiber), they are refined fibrous or powdered cellulose substances, and these substances can be cellulose acid hydrolysis.Need to prove, as the cellulose-based material that derives from Cotton Gossypii, can be the material in source for the Cotton Gossypii with the authentication of acquisition organic products.And, owing to be easy to absorption or absorb moisture as the cellulose-based material of raw material, thereby have the adsorption moisture about 3～10 quality % (hereafter is " % ") under the state usually.In order to obtain the plain powder body of flat fiber effectively, preferably, cellulose-based material carries out drying in advance before being carried out pulverization process through hot air drying, vacuum drying, drying under reduced pressure etc.

Phospholipid, ceramide, cholesterol and plant sterol that above-mentioned cellulose-based material is handled are the lipid in the organism, perhaps for having the structure close with it, promptly having a such amphiphilic agent with common character of chain alkyl structure and hydrophilic group.

Among the above-mentioned amphiphilic agent, phospholipid is the general name that has the lipid at phosphate ester position in the structure.As concrete phospholipid, can enumerate natural phosphatidyl cholines such as yolk lecithin, soybean lecithin are carried out the material that derives from natural goods that hydrogenation forms; LYSOLECITHIN SUNLECITHIN A, phosphatidylcholine, PHOSPHATIDYL ETHANOLAMINE, Phosphatidylserine, phosphatidyl glycerol, phosphatidylinositols, sphingomyelins etc. are carried out material that hydrogenation forms etc.Among these phospholipid, preferred hydrolecithin, phosphatidylcholine, PHOSPHATIDYL ETHANOLAMINE, hydrogenated phospholipid acyl glycerol.

In addition, ceramide in molecule, have long-chain straight chain and/or branched alkyl or alkenyl more than 1, further have the hydroxyl more than at least 2, the nonionic of the amide groups more than 1 (and/or amino) is the general name of amphiphilic agent.As concrete ceramide, can enumerate the long-chain fat amide of sphingosine, phytosphingosine---natural ceramide types such as ceramide 1, ceramide 2, ceramide 3, ceramide 3 B, ceramide 4, ceramide 5, ceramide 6, ceramide 6I, ceramide 6II etc.Among these ceramides, preferred ceramide 2, ceramide 3.And these ceramides can also can be synthetic for deriving from the material of natural goods.

Further, cholesterol is for the higher alcohol composition that animal oil carried out saponification and form or be the white or the yellowish solid that the fraction that is obtained by fish oil are extracted, crystallization, drying are made with extra care out, and its molecular formula is C ₂₇H ₄₆O.In addition, as the derivant of cholesterol, can enumerate Cholesteryl hydroxystearate, polyoxyethylene cholesteryl ether etc.Among these cholesterol or derivatives thereofs, preferred cholesterol.

In addition, further, plant sterol is the general name of the sterol compound that obtained by plant.As concrete plant sterol, can enumerate sitosterol, stigmasterol, 24-ethylidenecholest-5-en-3.beta.-ol., chondrillasterol, brassicasterol etc.And,, can enumerate plant sterol hydroxy stearic acid ester, polyoxyethylene plant sterol, polyoxyethylene phytostanol etc. as the plant sterol derivant.In these plant sterol or derivatives thereofs, the preferred plant sterol.

Above-mentioned amphiphilic agent and cellulose-based material are carried out in the processing that mechanicalness pulverizes, and pressure or shearing force due to the pulverizing need apply certain hour continuously.Therefore; In the pulverization process; Reducing mechanisms such as the super mixer of preferred use vibrator, screw grinding machine, planet-shaped ball mill, edge runner, medium grinding machine, disc mill, use high speed rotational blade, homomixer, preferred especially planet-shaped ball mill.Crushing treatment method is preferably the dry type pulverization process of not using solvent.Need to prove that the size reduction energy that is applied under the situation of the broken processing of conducting powder is 3G～20G, be preferably 5G～15G is suitable.

When carrying out above-mentioned pulverization process, with respect to cellulose-based material 100 mass parts, add about 0.1 mass parts～12 mass parts, the amphiphilic agent about preferred 1 mass parts～4 mass parts gets final product.And can the combination of the amphiphilic agent more than a kind or 2 kinds be used.Further, about adding the period of amphiphilic agent, as long as before pulverization process; Can add a period in office, and, about its adding method; Can amphiphilic agent be added directly in the cellulose-based material, also can amphiphilic agent be dissolved in appropriate solvent, join afterwards in the cellulose-based material.As the used solvent of the dissolving of amphiphilic agent, can enumerate for example aromatic hydrocarbons such as ethers such as ketone such as alcohol, acetone, oxolane, toluene such as alkane, ethanol such as hexane etc. here.

Next, show the optimal way that is used to obtain the plain powder body of amphiphilic agent processing flat fiber of the present invention below.At first, carry out drying under reduced pressure at 30 ℃～50 ℃, fully remove adsorption moisture, until being below 0.1% for the cellulose powder that derives from wood pulp after refining.This cellulose powder and oxidation aluminum or zirconium oxide system crushing ball are together put in sealable oxidation aluminum or the broken container of zirconium oxide powder process, further added amphiphilic agent to above-mentioned amount with respect to cellulose powder., above-mentioned crushing container be located at planet-shaped ball mill, carry out pulverization process with rotating speed 100rpm～250rpm thereafter.For pulverization process, can be 1 circulation in 5 minutes～15 minutes to pulverize 5 minutes～15 minutes-time-out, carry out 2～72 pulverization process about circulation continuously repeatedly; Also can not suspend and carry out pulverization process about 5 minutes～120 minutes continuously.

Need to prove, after pulverization process, can further utilize known dry means such as air-dry, hot air drying, vacuum drying, drying under reduced pressure to remove to be attached to amphiphilic agent to handle moisture in the plain powder body of flat fiber etc.

Handle the plain powder body of flat fiber for the amphiphilic agent that obtains as stated; For example its mean diameter is 1～100 μ m, is preferably 1 μ m～50 μ m; Average thickness is 0.1 μ m～10 μ m, is preferably the sheet-like article of 0.1～2 μ m, and flatness be 4～200, be preferably 6～150, further more preferably 10～100.

Need to prove; Said here mean diameter refers to; Use laser diffraction and scattering formula particle size distribution device equigranular measure of spread device, the meansigma methods (particle size values of integration volume 50%) on the width of the flat fiber crude granule of measuring with dispersity in the water and the device of length.And so-called average thickness refers to, and selects a plurality of sizes and the equal granule of the above-mentioned mean diameter of obtaining, and utilizes ultramicroscope such as scanning electron microscope that its thickness is measured, and their thickness is averaged and the meansigma methods that obtains.Further, the mean diameter/average thickness of flatness for trying to achieve as stated.

The amphiphilic agent that so obtains is handled the plain powder body of flat fiber and can be used in the various cosmetic material such as powder cosmetic, basis (skin protection) cosmetic material, beauty and make-up material, hair cosmetic material.

Specifically; Handle the cosmetic material of the plain powder body of flat fiber as amphiphilic agent capable of using; Owing to compare with Talcum, the sericite of the existing extender pigment of conduct; It is laminar for what approach that this amphiphilic agent is handled the plain powder body of flat fiber, has excellent characteristic at aspects such as transparent feel, soft feeling, spreadability, natural gloss, and excellent with the affinity of used oil preparation; Thereby can enumerate powder cosmetics such as the existing cosmetic material, particularly foundation cream that contains the powder body composition, eye shadow, rouge, face powder especially.

Amphiphilic agent of the present invention is handled the plain powder body of flat fiber be matched with under the situation in the powder cosmetic, its combined amount is 1%～90%, is preferably 5%～90%, is preferably 5%～70% especially.

In the above-mentioned powder cosmetic, the preferred oiliness composition that further cooperates.Oiliness composition as being engaged in the powder cosmetic does not have special restriction, for example can enumerate: hydro carbons such as hard paraffin, hard wax (セレシ Application ワッ Network ス), ceresine, microwax, montan wax, Fischer-Tropsch wax, Tissuemat E, liquid paraffin, squalane, vaseline, polyisobutylene, polybutene; Natural waxes such as Brazil wax, Cera Flava, lanolin wax, candelilla wax; Esters such as three Compritol 888 ATOs, rosin acid pentaerythritol ester, jojoba oil (jojoba oil), isooctyl acid cetyl ester, isopropyl myristate, tricaprylin, three isostearic acids, two glyceride, dipentaerythritol fatty acid ester; Fatty acids such as stearic acid, mountain Yu acid, 12-hydroxy stearic acid; Higher alcohols such as spermol, stearyl alcohol, behenyl alcohol; Oils such as olive oil, Oleum Ricini, ermine oil, Japan wax; Lanolin derivative classes such as lanolin fatty acid isopropyl ester, lanolin alcohol; Amino acid derivativges classes such as N-lauroyl-L-glutamic acid two (cholesterol ester docosyl ester octyl group dodecyl) ester; Fluorine class oil preparation classes such as PFPE, perfluoro decane, PFO etc.These oiliness compositions can use more than a kind or 2 kinds.Combined amount in powder cosmetic of the present invention under the situation of these oiliness compositions of cooperation is not special to be limited, and is preferably 0.1%～25%.

Above-mentioned powder cosmetic can likewise be made with existing powder cosmetic.Specifically, in the manufacturing approach of the existing cosmetic material that contains powder body composition and oiliness composition, use amphiphilic agent to handle that the plain powder body of flat fiber is replaced a part or all existing powder body gets final product.And; In above-mentioned powder cosmetic, cooperate under the situation of organic dusts such as inorganic powder such as Talcum or nylon; Handle the plain powder body of flat fiber with amphiphilic agent of the present invention and add organic dusts such as inorganic powder such as Talcum or nylon simultaneously; Disperse, add oil content manufacturing as required and get final product.

Need to prove; In above-mentioned powder cosmetic; Except that the above-mentioned plain powder of amphiphilic agent processing flat fiber with the oiliness composition; The composition that also can use with the cosmetic amount usually in proper fit in the scope of effect of the present invention, for example water soluble ingredients such as surfactant, oily gellant, polyalcohols or wetting agent; Powder body, UV absorbent, antiseptic, beauty treatment composition, spice etc.

In addition, specifically,,, thereby can enumerate foundation make up material, beauty and make-up material etc. because this amphiphilic agent is handled the tack height of the plain powder body of flat fiber to skin as the cosmetic material of the plain powder body of amphiphilic agent processing flat fiber capable of using.

Need to prove; It is that ceramide is handled under the situation of the plain powder body of flat fiber that amphiphilic agent is handled the plain powder body of flat fiber; Because moisture maintenance dose and suppress that moisture evapotranspires and wait moisture retention excellence especially, thereby can suitably be used for the cosmetic skin-care material of foundation make up material, particularly beautifying liquid or emulsion, cream and so on.

And it is that phospholipid is handled under the situation of the plain powder body of flat fiber that amphiphilic agent is handled the plain powder body of flat fiber, because the dispersibility in general oil solution and water is excellent especially, thereby can be suitably as beauty and make-up material such as liquid foundation.And, because the tack of this powder body is good, the cosmetic retentivity is excellent, thereby also can be suitably as beauty and make-up material such as foundation creams.

Amphiphilic agent of the present invention is handled the plain powder body of flat fiber be engaged under the situation in the foundation make up material, its combined amount is 0.1%～10%; Be engaged under the situation in the beauty and make-up material, its combined amount is 0.5%～50%.

Above-mentioned foundation make up material can likewise be made with existing foundation make up material.Specifically, can make water, oil, glycol, surfactant etc., under heating or room temperature, oil content can be dissolved or dispersion, emulsifying, make amphiphilic agent of the present invention handle the plain powder body of flat fiber afterwards and disperse, make thus.

Above-mentioned beauty and make-up material also can likewise be made with existing beauty and make-up material.Specifically, can make water, oil, glycol, surfactant etc., under heating or room temperature, oil content can be dissolved or disperse to carry out emulsifying, carry out the dispersion that amphiphilic agent of the present invention is handled flat fiber element powder body afterwards, make thus; Conversely, also can make amphiphilic agent of the present invention handle the plain powder body of flat fiber and be dispersed in the oil content, add water system composition or surfactant afterwards and carry out emulsifying, make thus.

[embodiment]

Enumerate embodiment below and specify the present invention, but the present invention does not receive any qualification of these embodiment.

Embodiment 1

Phospholipid is handled the manufacturing (1) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Drying under reduced pressure through under 40 ℃ is fully removed below the adsorption moisture to 0.1%; Gained cellulose powder (48.5g) and zirconium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable zirconium oxide powder process (volume 500ml); Further add hydrolecithin (manufacturing of Retinol S-10/Nikkol Chemicals society) 1.5g, making hydrolecithin is 3% with respect to cellulose powder, prepares.

Thereafter; Use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), pulverized 10 minutes, time-out 10 minutes with rotating speed 200rpm (size reduction energy of about 10G (acceleration of gravity)), with it as 1 circulation; Carry out 36 circulations, obtain phospholipid and handle the plain powder body (goods 1) of flat fiber.

Use laser diffraction and scattering formula particle size distribution device (LMS-24 type/pure and fresh society makes), utilize flow cell (flow cell) to obtain gained powder body mean diameter under the dispersity (meansigma methods on the device of width and length) in water.Mean diameter is used the particle size values of integration volume 50% here.

For particle size distribution, the 50mg in the gained powder body is dispersed among the distilled water 10ml, what the gained hanging drop was added to particle size distribution device is in the sample cycle groove of medium with water, reach suitable concentration after, measure.Its result, the mean diameter of powder body are 17 μ m.

In addition; For the particulate average thickness of gained; Use scanning electron microscope (manufacturing of S-2450/ Hitachi society) that granule is directly observed, select a plurality of sizes and the equal granule of the above-mentioned mean diameter of obtaining, thickness is measured; They are averaged, thereby obtain this average thickness.

In the observation that utilizes scanning electron microscope to carry out, the few loading gage in the gained powder body is placed on the sample bench of scanning electron microscope, behind the drying under reduced pressure, carry out the vapor deposition of metals such as gold or platinum, process the microscopy sample.For this microscopy sample, under accelerating potential 20～25kV,, observe for 000 times with amplification 500～10, by the equal particulate thickness of the mean diameter of resulting determining image size and said determination, obtain the thickness average thickness by them.Its result, average thickness is 2 μ m.

The goods 1 that obtain thus are that mean diameter is that 17 μ m, average thickness are that 2 μ m, flatness (mean diameter/average thickness) are 8.5 flat cellulose grain (through the plain powder body of the flat fiber of phospholipid processing).

And; As comparing; To the plain powder material of flat fiber---the cellulose powder that derives from wood pulp (W-400G/Nippon Paper Chemicals society makes (being designated hereinafter simply as " cellulose powder ")) after making with extra care and mean diameter, the average thickness of the plain powder of flaxen fiber (the plain powder of Tosco flaxen fiber/Tosco society makes) are measured, and obtain flatness (mean diameter/average thickness).The shape of cellulose powder is not flat but fuel wood shape, and trying to achieve mean diameter is that 28 μ m, average thickness are 10 μ m, and flatness is 2.8.On the other hand, the plain powder of flaxen fiber is not that flat neither the fuel wood shape and be granular, although determining its mean diameter is 7.7 μ m, fails to obtain its average thickness and flatness.

Embodiment 2

Phospholipid is handled the manufacturing (2) of the plain powder body of flat fiber:

Except the amount that makes hydrolecithin is 0.1% and 10%, likewise obtains phospholipid respectively with embodiment 1 and handle the plain powder body of flat fiber (goods 2 and goods 3).Their mean diameter, average thickness and flatness are following.

[table 1]

	Mean diameter (μ m)	Average thickness (μ m)	Flatness
				Goods 1	17	2	8.5
Goods 2	18	3	6
				Goods 3	17	1.5	11.3

Embodiment 3

Phospholipid is handled the manufacturing (3) of the plain powder body of flat fiber:

As phospholipid; Do not use the hydrolecithin of embodiment 1 and use the hydrogenation LYSOLECITHIN SUNLECITHIN A (the Japan society that refines makes: LP-70H), PHOSPHATIDYL ETHANOLAMINE (making with the pure medicine of light society) and sphingomyelins (making with the pure medicine of light society), below likewise obtain phospholipid respectively with embodiment 1 and handle flat fiber element powder body (goods 4～goods 6).Their mean diameter, average thickness and flatness are following.

[table 2]

	Mean diameter (μ m)	Average thickness (μ m)	Flatness
				Goods 1	17	2	8.5
Goods 4	18	2	9
				Goods 5	19	2.5	7.6
Goods 6	17	2.5	6.8

Embodiment 4

Phospholipid is handled the manufacturing (4) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.It is put in the broken container of sealable aluminium oxide powder process with aluminium oxide system crushing ball, and (コット Application cotton) is 5% hydrolecithin (manufacturing of Retinol S-10/Nikkol Chemicals society) with respect to Cotton Gossypii to wherein adding., use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 60 minutes with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.The mean diameter that resulting phospholipid is handled the plain powder body of flat fiber is that 20 μ m, average thickness are that 1.2 μ m, flatness are 16.7 (goods 7).

Embodiment 5

Phospholipid is handled the manufacturing (5) of the plain powder body of flat fiber:

Using organic Cotton Gossypii (No. 7 (kind) comb and parallel cotton fibers prior to spinning line to generate color/AVANTI society as raw material makes).It is utilized pulverizer (the wild industry system of Omaki: after the RC100 type) meticulous cut-out is pulverized; Together putting in the broken container of sealable aluminium oxide powder process with aluminium oxide system crushing ball, is 1% hydrolecithin (manufacturing of Retinol S-10/Nikkol Chemicals society) to wherein adding with respect to Cotton Gossypii., use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 60 minutes with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.The mean diameter that resulting phospholipid is handled the plain powder body of flat fiber is that 20 μ m, average thickness are that 1.6 μ m, flatness are 12.5 (goods 8).

Embodiment 6

Phospholipid is handled the manufacturing (6) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material; It is put in the broken container of sealable aluminium oxide powder process with aluminium oxide system crushing ball, is 2% hydrolecithin (manufacturing of Retinol S-10/Nikkol Chemicals society) to wherein adding with respect to Cotton Gossypii., use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 50 minutes with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.The mean diameter that resulting phospholipid is handled the plain powder body of flat fiber is that 17.8 μ m, average thickness are that 0.2 μ m, flatness are 89.0 (goods 9).

Reference example 1

Stearic acid is handled the manufacturing of the plain powder of flat fiber:

Do not use the stearic acid except not using hydrolecithin, likewise handle, obtain stearic acid and handle the plain powder of flat fiber (relatively goods 1) with embodiment 1.

Handle the plain powder of flat fiber for resulting stearic acid, likewise carry out particle size distribution with embodiment 1, its mean diameter is 16 μ m as a result.

And, likewise resulting relatively the average thickness and the flatness (mean diameter/average thickness) of goods 1 are measured with embodiment 1, average thickness is that 3 μ m, flatness are 5.3 as a result.

Reference example 2

Phospholipid is handled the manufacturing of sericite:

Using soybean phospholipid (lecithin; manufactured by Ajinomoto) 1% of sericite (Oh イ Suites bread ー Hikaru 300S; angle eight fish scale foil manufactured) 99% for the coating treatment, to obtain phospholipid Sericite treated (Comparative product 2).

Reference example 3

Phospholipid is handled the manufacturing of cellulose powder (non-flat):

The cellulose powder that derives from wood pulp (manufacturing of W-100G/Nippon Paper Chemicals society) is put in the blender, will be to add after 3% hydrolecithin (Retinol S-10/Nikkol Chemicals manufacturing) is dissolved in the hexane with respect to cellulose powder., with rotating speed 40rpm carry out 5 minute stir, pulverize behind the drying under reduced pressure, obtain phospholipid and handle cellulose powder (non-flat) (relatively goods 3) thereafter.

Embodiment 7

Dispersivity test:

Study the phospholipid that obtains among the embodiment 1 by following dispersivity test method and handle the dispersibility of the plain powder body (goods 1) of flat fiber in all kinds of solvents.As comparison and contrast, use the stearic acid of reference example 1 to handle flat fiber plain (relatively goods 1) and raw cellulose powder (reference substance).And,, use liquid paraffin (KLEAROL), three (acid of 2-ethyl hexane) glyceride (T.I.O), silicone oil (10cs) (KF-96) and water as disperse medium (solvent).Its result lists in table 3.

(test method)

In No. 6 specification bottles, each sample 0.5g is mixed (2wt%) with disperse medium 24.5g, utilize ultrasound wave to carry out disperseing in 1 hour after, move in the sedimentation pipe dispersity observed.Yet the discrete volume after the scheduled time (volume of the part that powder body is still suspending) is estimated, obtained dispersion rate (%) by following formula.

Dispersion rate (%)=discrete volume (ml)/cumulative volume (ml) * 100

[table 3]

Embodiment 8

The tack test:

Use artificial skin, study the phospholipid that obtains among the embodiment 1 through following tack test method and handle the tack of the plain powder body of flat fiber (goods 1) skin.As relatively, that uses that the stearic acid of reference example 1 handles flat fiber plain (relatively goods 1) and reference example 3 carries out that phospholipid is handled and the goods (comparing goods 3) that obtain to cellulose powder.Its result lists in table 4.

(test method)

Each sample 60mg is coated polyurethane system artificial skin (25cm ²), afterwards Ai Liankou (アレ Application コ) paper is placed on the face after this coating, use hydraulic press to apply 10 seconds of load of 100kg from top.Thereafter, the powder body amount of adhering on the pan paper calculates the adhesion amount of powder body on artificial skin.

[table 4]

Sample	Powder body remaining quantity (g) on the skin
		Goods 1	26
Compare goods 1	18
		Compare goods 3	14

Embodiment 9

Pressed powder type foundation cream:

According to conventional method, prepare the pressed powder foundation cream with the composition shown in the below table 5.For resulting pressed powder foundation cream, estimate its " uniformity of cosmetic film ", " cosmetic retentivity " and " usability (the smooth sense during coating) " according to following evaluation methodology.Its result also gathers and lists in table 5.

(evaluation methodology)

Please the cosmetic evaluation panel 20 use the present invention's article 1～3 and the pressed powder type foundation cream of article 1～4 relatively; By following metewand; Respectively 7 grades of evaluations are carried out in " uniformity of cosmetic film ", " cosmetic retentivity ", " usability (the smooth sense during coating) ", to each sample scoring.Next, each goods is judged by following determinating reference by the meansigma methods of whole group scoring.

Metewand;

(evaluation): (content)

6: very good

5: good

4: good slightly

3: common

2: poor slightly

1: poor

0: non-constant

Determinating reference;

(average mark of scoring): (judgement)

5.0 more than: ◎ (very good)

More than or equal to 3.5 less than 5.0: zero (well)

More than or equal to 1.5 less than 3.5: △ (bad slightly)

Less than 1.5: * (bad)

The result;

[table 5]

Embodiment 10

Two laminar astringent:

Prepare the two laminar astringent of forming shown in following as follows.

Annotate 1) Nikkol DDP-8 (manufacturing of Nihon surfactant kogyo society)

Annotate 2) Emalex RWIS-150 (Nihon Emulsion Co., Ltd. society makes)

(method for making)

(1) composition 1～3 is mixed.

(2) adding ingredient 4～9 in (1) evenly stirs, and obtains two laminar astringent.

Resulting two laminar astringent are excellent, the soft and smooth usability of powder dispersity, two excellent laminar astringent of cosmetic lasting effect.

Embodiment 11

Emulsion:

Make the emulsion of forming shown in following as follows.

Annotate 3) KF-96 (10CS) (manufacturing of chemical industry society of SHIN-ETSU HANTOTAI)

Annotate 4) CARBOPOL1342 (manufacturing of LUBRIZOL ADVANCED MATERIALS society)

(method for making)

(1) composition 1～7 is carried out uniform mixing at 80 ℃.

(2) with composition 8～14 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) when (3) are stirred, make it cooling, adding ingredient 15 back uniform mixing obtain emulsion.

Resulting emulsion is the excellent and soft and smooth usability of emulsion stability, the excellent emulsion of cosmetic lasting effect.

Embodiment 12

Cream:

Prepare the cream of forming shown in following as follows.

(method for making)

(1) with composition 1～7 at 80 ℃ of uniform mixing.

(2) with composition 8～13 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) when (3) are stirred, make it cooling, obtain cream.

Resulting cream is the excellent and soft and smooth usability of emulsion stability, the excellent cream of cosmetic lasting effect.

Embodiment 13

Beautifying liquid:

Prepare the beautifying liquid of forming shown in following as follows.

(method for making)

(1) with composition 1～10 mixed dissolution at normal temperatures, stirs and obtain beautifying liquid simultaneously.

Resulting beautifying liquid is excellent in stability and soft and smooth usability, the excellent beautifying liquid of cosmetic lasting effect.

Embodiment 14

Facial film:

Prepare the facial film of forming shown in following as follows.

(method for making)

(1) with composition 1～4 at 80 ℃ of uniform mixing.

(2) with composition 5～12 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) when (3) are stirred, make it cooling, obtain facial film.

Resulting facial film is the excellent and soft and smooth usability of emulsion stability, the excellent facial film of cosmetic lasting effect.

Embodiment 15

Cleansing Foam:

Prepare the Cleansing Foam of forming shown in following as follows.

(method for making)

(1) with composition 1～7 at 80 ℃ of uniform mixing.

(2) with composition 8～11 at 80 ℃ of uniform mixing.

(3) in (1), add (2), neutralize.

(4) adding ingredient 12 in (3), uniform mixing.

(5) (4) are stirred make its cooling simultaneously, obtain Cleansing Foam.

Resulting Cleansing Foam is the soft and smooth excellent Cleansing Foam of usability.

Embodiment 16

Cleansing cream:

Prepare the cleansing cream of forming shown in following as follows.

(method for making)

(1) with composition 1～8 at 80 ℃ of uniform mixing.

(2) with composition 9～14 at 80 ℃ of uniform mixing.

(3) in (2), add (1), carry out emulsifying.

(4) when (3) are stirred, make it cooling, obtain cleansing cream.

Resulting cleansing cream is the excellent cleansing cream of the excellent and soft and smooth usability of emulsion stability.

Embodiment 17

Pomade:

Prepare the pomade of forming shown in following as follows.

Annotate 5) Nikkol MYS-40V (manufacturing of Nihon surfactant kogyo society)

(method for making)

(1) with composition 1～3 at 80 ℃ of uniform mixing.

(2) with composition 4～8 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) in (3), behind the adding ingredient 9～16, under stirring condition, cool off, obtain pomade.

Resulting pomade is the excellent pomade of the excellent and soft and smooth usability of haircuting property.

Embodiment 18

Oiliness eyeliner (アイライナー):

Prepare the oiliness eyeliner of forming shown in following as follows.

Annotate 6) SA-Black BL-100 (100%) (three change into society well makes)

Annotate 7) SA-Talc JA-13R (three change into society well makes)

(method for making)

(1) composition 1～4 is heated to 100 ℃, uniform mixing.

(2) composition 5～9 is heated to 80 ℃, uniform mixing.

(3) in (1), add (2), uniform mixing.

(4) utilize roller! ローラー, roller) handle (3), obtain the oiliness eyeliner.

Resulting oiliness eyeliner is soft and smooth usability, the excellent oiliness eyeliner of cosmetic lasting effect.

Embodiment 19

The aqueous eyeliner:

Prepare the aqueous eyeliner of forming shown in following as follows.

Annotate 8) Nikkol DDP-6 (manufacturing of Nihon surfactant kogyo society)

Annotate 9) Nikkol BC-20TX (manufacturing of Nihon surfactant kogyo society)

Annotate 10) ヨドゾー Le 32A707 (45% solid constituent) (Japanese NSC society make)

(method for making)

(1) composition 1～6 is utilized the roller homodisperse.

(2) with composition 6～10 uniform mixing.

(3) in (2), add (1), uniform mixing obtains the aqueous eyeliner.

Resulting aqueous eyeliner is soft and smooth usability, the excellent aqueous eyeliner of cosmetic lasting effect.

Embodiment 20

Eyebrow pencil (アイ Block ロウ):

Prepare the eyebrow pencil of forming shown in following as follows.

(method for making)

(1) with composition 1～4 uniform mixing.

(2) utilize roller that composition 5～10 is handled.

(3) in (1), add (2), composition 11,12 after, uniform mixing obtains eyebrow pencil.

Resulting eyebrow pencil is soft and smooth usability, the excellent eyebrow pencil of cosmetic lasting effect.

Embodiment 21

O/W type mascara:

Prepare the O/W type mascara of forming shown in following as follows.

(method for making)

(1) with composition 1～8 at 80 ℃ of uniform mixing, carry out roller and handle.

(2) with composition 9～14 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) with (3) cooling, obtain mascara (O/W).

Resulting O/W type mascara is the excellent and soft and smooth usability of powder dispersity, the excellent O/W type mascara of cosmetic lasting effect.

Embodiment 22

Non-water system mascara:

Prepare the non-water system mascara of forming shown in following as follows.

Annotate 11) BENTONE38V BC (manufacturing of Elementis society)

(method for making)

(1) composition 1～5 is heated to 110 ℃.

(2) adding ingredient 6～9 mixes in (1).

(3) adding ingredient 10～13 mixes in (2).

(4) utilize roller that (3) are handled, obtain non-water system mascara.

Resulting non-water system mascara is soft and smooth usability, the excellent non-water system mascara of cosmetic lasting effect.

Embodiment 23

The strip lipstick:

Prepare the strip lipstick of forming shown in following as follows.

Annotate 12) KF-96 (10CS) (manufacturing of chemical industry society of SHIN-ETSU HANTOTAI)

(method for making)

(1) composition 1～7 being carried out uniform dissolution at 100 ℃ mixes.

(2) adding ingredient 8～14 in (1) carries out uniform mixing.

(3) (2) are poured in the container, cool off, obtain the strip lipstick.

Resulting strip lipstick is soft and smooth usability, the excellent lipstick of cosmetic lasting effect.

Embodiment 24

Liquid rouge (リキッドルージュ):

Prepare the liquid rouge of forming shown in following as follows.

(method for making)

(1) composition 1～5 is mixed 100 ℃ of uniform dissolution.

(2) adding ingredient 6～13 in (1), uniform mixing.

(3) (2) are poured in the container, cool off, obtain liquid rouge.

Resulting liquid rouge is soft and smooth usability, the excellent liquid rouge of cosmetic lasting effect.

Embodiment 25

O/W type foundation cream:

Prepare the O/W type foundation cream of forming shown in following as follows.

Annotate 13) SA-titanium CR-50 (three change into society well makes)

Annotate 14) SA-iron oxide red Sapporo (ベ Application ガラ Sapporo, three change into society well makes)

Annotate 15) the yellow Fructus Citri Limoniae of SA-(イエローレモ Application, three change into society well makes)

(method for making)

(1) composition 1～8 is utilized the roller homodisperse.

(2) with composition 9～12 uniform mixing.

(3) in (2), add (1), uniform mixing.

(4) with composition 13～19 at 80 ℃ of mixed dissolutions.

(5) in (3), add (4) at 80 ℃, carry out emulsifying.

(6) (5) are cooled off, adding ingredient 20 obtains O/W type foundation cream.

Resulting O/W type foundation cream is the excellent and soft and smooth usability of powder dispersity, the excellent O/W type foundation cream of cosmetic lasting effect.

Embodiment 26

The w/o type foundation cream:

Prepare the w/o type foundation cream of forming shown in following as follows.

Annotate 16) KF-6026 (manufacturing of chemical industry society of SHIN-ETSU HANTOTAI)

Annotate 17) KF-6015 (manufacturing of chemical industry society of SHIN-ETSU HANTOTAI)

(method for making)

(1) with composition 1～3 uniform mixing.

(2) utilize roller to carry out homodisperse composition 4～11.

(3) in (1), add (2), uniform mixing.

(4) adding ingredient 12～15 in (3) carries out emulsifying, obtains the w/o type foundation cream.

Resulting w/o type foundation cream is the excellent and soft and smooth usability of powder dispersity, the excellent w/o type foundation cream of cosmetic lasting effect.

Embodiment 27

O/W type eye is color:

It is color to prepare the O/W type eye of forming shown in following as follows.

Annotate 18) SA-Off ラメ Application コゴー Le De (three change into society well makes)

(method for making)

(1) with composition 1～5 at 80 ℃ of uniform mixing.

(2) adding ingredient 6,7 in (1) carries out emulsifying.

(3) composition 8～14 is utilized the roller homodisperse.

(4) in (2), add (3), composition 15, it is color to obtain O/W type eye.

Resulting O/W type eye coloured silk is that the excellent O/W type eye of the excellent and soft and smooth usability of powder dispersity, cosmetic lasting effect is color.

Embodiment 28

The solid type foundation cream of oiliness:

Prepare the solid type foundation cream of forming shown in following of oiliness as follows.

Annotate 19) KF-6026 (manufacturing of chemical industry society of SHIN-ETSU HANTOTAI)

(method for making)

(1) with composition 7～13 90 ℃ of heating for dissolving.

(2) in (1) adding ingredient 1～6, utilize the roller homodisperse.

(3) adding ingredient 14 in (2), 80 ℃ dissolve after, be filled in the metal dish, obtain the solid type foundation cream of oiliness.

The solid type foundation cream of resulting oiliness is the solid type foundation cream of the also excellent oiliness of the excellent and soft and smooth usability of powder dispersity, cosmetic lasting effect.

Embodiment 29

Strip concealer (コンシーラー):

Prepare the strip concealer of forming shown in following as follows.

(method for making)

(1) with composition 1～5 90 ℃ of heating for dissolving.

(2) adding ingredient 6～12 in (1) utilizes the roller homodisperse.

(3) adding ingredient 13 in (2) after 80 ℃ of dissolvings, is filled in the container, obtains the strip concealer.

Resulting strip concealer is the excellent and soft and smooth usability of powder dispersity, the excellent strip concealer of cosmetic lasting effect.

Embodiment 30

The health breast:

Prepare the health breast of forming shown in following as follows.

(method for making)

(1) with composition 1～7 80 ℃ of uniform dissolution.

(2) with composition 8～16 80 ℃ of uniform dissolution.

(3) in (2), add (1), carry out emulsifying.

(4) in (3), behind adding ingredient 17 uniform mixing, stir cooling, obtain the health breast.

Resulting health breast is the excellent health breast of the excellent and soft and smooth usability of emulsion stability, cosmetic lasting effect.

Embodiment 31

Hair conditioner (コ Application ディショナー, conditioner):

Prepare the hair conditioner of forming shown in following as follows.

Annotate 20) アーカー De 22-80 (manufacturing of LIONAKZO society)

(method for making)

(1) with composition 1～5 at 80 ℃ of uniform mixing.

(2) with composition 6～9 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) adding ingredient 10 in (3) stirs cooling behind the uniform mixing, obtains hair conditioner.

Resulting hair conditioner is the excellent hair conditioner of the excellent and soft and smooth usability of emulsion stability.

Embodiment 32

Send out film:

Prepare the film of forming shown in following of sending out as follows.

Annotate 21) BY22-050A (manufacturing of TorayDow Corning society)

(method for making)

(1) with composition 1～6 at 80 ℃ of uniform mixing.

(2) with composition 7～9 at 80 ℃ of uniform mixing.

(3) in (1), add (2), carry out emulsifying.

(4) in (3), behind adding ingredient 10 uniform mixing, stir cooling, obtain sending out film.

Resulting film is the excellent film of the excellent and soft and smooth usability of emulsion stability.

Embodiment 33

W/o type sunscreen cream (a day baked け ends the め material):

Prepare the sunscreen cream of forming shown in following as follows.

Annotate 22) ABIL EM90 (manufacturing of EVONIC GOLDSCHMIDT GMBH society)

(method for making)

(1) composition 1～5 is utilized the roller homodisperse.

(2) adding ingredient 6～9 in (1), uniform mixing.

(3) adding ingredient 10～14 in (2) carries out emulsifying, obtains the w/o type sunscreen cream.

Resulting w/o type sunscreen cream is the excellent and soft and smooth usability of powder dispersity, the excellent sunscreen cream of cosmetic lasting effect.

Embodiment 34

Nial polish (マニキュア, minicure):

Prepare the nial polish of forming shown in following as follows.

(method for making)

(1) with composition 1～9 uniform mixing, obtains nial polish.

Resulting nial polish is the excellent and soft and smooth usability of powder dispersity, the excellent nial polish of cosmetic lasting effect.

Embodiment 35

Sun screen (changing make-up ground down):

Prepare the sun screen of forming shown in following as follows.

Annotate 23) CARBOPOL 940 (manufacturing of LUBRIZOL ADVANCED MATERIALS society)

(method for making)

(1) with composition 1～4 80 ℃ of uniform dissolution.

(2) with composition 5～12 80 ℃ of uniform dissolution.

(3) in (2), add (1), carry out emulsifying.

(4) in (3), add blending constituent 13～14, cool off, obtain sun screen.

Resulting sun screen is the excellent and soft and smooth usability of emulsion stability, the excellent sun screen of cosmetic lasting effect.

Embodiment 36

White lead:

Prepare the white lead of forming shown in following as follows.

(method for making)

(1) with composition 1～5, composition 8～10 uniform mixing.

(2) adding ingredient 6,7 in (1), uniform mixing.

(3) utilize pulverizer to pulverize with (2), obtain white lead.

Resulting white lead is the excellent and soft and smooth usability of powder dispersity, the excellent white lead of cosmetic lasting effect.

Embodiment 37

Pressed powder type foundation cream:

Prepare the pressed powder type foundation cream of forming shown in following as follows.

(method for making)

(1) with composition 1～7, composition 11～13 uniform mixing.

(2) adding ingredient 8～10 in (1), uniform mixing.

(3) utilize pulverizer (パ Le ベライザー) to pulverize with (2).

(4) (3) are filled in the metal dish, obtain pressed powder type foundation cream.

Resulting pressed powder type foundation cream is the excellent and soft and smooth usability of powder dispersity, the excellent foundation cream of cosmetic lasting effect.

Embodiment 38

A pressed powder type kermes! チー Network):

Prepare the pressed powder type kermes of forming shown in following as follows.

(method for making)

(1) with composition 1～4, composition 7～9 uniform mixing.

(2) adding ingredient 5,6 in (1), uniform mixing.

(3) utilize pulverizer to pulverize with (2).

(4) (3) are filled in the metal dish, obtain pressed powder type kermes.

Resulting pressed powder type kermes is the excellent and soft and smooth usability of powder dispersity, the excellent kermes of cosmetic lasting effect.

Embodiment 39

Pressed powder type eye shadow:

Prepare the pressed powder type eye shadow of forming shown in following as follows.

(method for making)

(1) with composition 1～6, composition 10～12 uniform mixing.

(2) adding ingredient 7～9 in (1), uniform mixing.

(3) utilize pulverizer that (2) are pulverized.

(4) (3) are filled in the metal dish, obtain pressed powder type eye shadow.

Resulting pressed powder type eye shadow is the excellent and soft and smooth usability of powder dispersity, the excellent eye shadow of cosmetic lasting effect.

Embodiment 40

Ceramide is handled the manufacturing (1) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), further added ceramide 2 (manufacturing of the high sand spice of TIC-001/ society) by amount with respect to cellulose powder 2%.

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 40 minutes, obtain ceramide and handle the plain powder body (goods 10) of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this ceramide processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 18 μ m, average thickness are that 0.6 μ m, flatness are 30.

Embodiment 41

Ceramide is handled the manufacturing (2) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), and further adding ceramide 6 (manufacturing of Ceramide VI/COSMOFARM society), to make it be 2% with respect to cellulose powder.

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 50 minutes, obtain ceramide and handle the plain powder body of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this ceramide processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 20 μ m, average thickness are that 1.5 μ m, flatness are 13.3.

Embodiment 42

Ceramide is handled the manufacturing (3) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), further added ceramide 1 (manufacturing of Ceramide I/Evonik Goldschmidt GmbH society) and add octyltri-ethoxysilane (octyltri-ethoxysilane/Tokyo changes into industrial society and makes) by the amount that with respect to cellulose powder is 1% by the amount that with respect to cellulose powder is 1%.

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 20 minutes, obtain ceramide and handle the plain powder body of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this ceramide processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 30 μ m, average thickness are that 1.5 μ m, flatness are 20.0.

Embodiment 43

Ceramide is handled the manufacturing (4) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), further added with respect to cellulose powder and be 1% ceramide 3 (manufacturings of Ceramide III/Evonik Goldschmidt GmbH society) and be single terminal carboxyl group modified silicone (manufacturing of chemical society of X-22-3710/ SHIN-ETSU HANTOTAI) of 1% with respect to cellulose powder.

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 30 minutes, obtain ceramide and handle the plain powder body of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this ceramide processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 25 μ m, average thickness are that 1.6 μ m, flatness are 15.6.

Embodiment 44

Cholesterol is handled the manufacturing (1) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), and further adding with respect to cellulose powder is 2% cholesterol (Cholesterol/ Japan refine society's manufacturing).

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 40 minutes, obtain cholesterol and handle the plain powder body (goods 11) of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this cholesterol processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 22 μ m, average thickness are that 0.8 μ m, flatness are 27.5.

Embodiment 45

Cholesterol is handled the manufacturing (2) of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), further added with respect to cellulose powder and be 3% cholesterol (Cholesterol/ Japan refine society's manufacturing) and be 2% perfluoralkyl phosphate with respect to cellulose powder.

, use planet-shaped ball mill (P-5 type/German FRITSCH manufactured), carry out continuously pulverizing in 60 minutes, obtain cholesterol and handle the plain powder body of flat fiber with 200rpm rotating speed (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this cholesterol processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 27 μ m, average thickness are that 1.8 μ m, flatness are 15.0.

Embodiment 46

Plant sterol is handled the manufacturing of the plain powder body of flat fiber:

Use the cellulose powder that derives from wood pulp (manufacturing of W-400G/Nippon Paper Chemicals society) after making with extra care as raw material.At first; Utilize the drying under reduced pressure under 40 ℃ fully to remove below the adsorption moisture to 0.1%; Dried cellulose powder (48g) and aluminium oxide system crushing ball (diameter 20mm) are together put in the broken container of sealable aluminium oxide powder process (volume 500ml), and further interpolation is 2% plant sterol (plant sterol/Eisai Food Chemical) with respect to cellulose powder.

, use planet-shaped ball mill (P-5 type/German FRITSCH company), carry out continuously pulverizing in 40 minutes, obtain plant sterol and handle flat fiber element powder body (goods 12) with rotating speed 200rpm (size reduction energy of about 10G (acceleration of gravity)) thereafter.

Likewise mean diameter, average thickness and the flatness of the plain powder body of this plant sterol processing flat fiber are measured with embodiment 1, mean diameter, average thickness and flatness are respectively as follows as a result: mean diameter is that 24 μ m, average thickness are that 1.0 μ m, flatness are 24.0.

Reference example 4

Ceramide is handled the manufacturing of sericite:

Use grinder (ミルサー (millser); Rock paddy industry society makes) utilize 2% pair of sericite of ceramide 2 (manufacturings of the high sand spices of TIC-001/ society) (manufacturings of エイトパー Le 300S/ angle eight fish phosphorus paper tinsel societies) 98% processing that is covered, obtain ceramide processing sericite (comparison goods 4).

Reference example 5

Ceramide is handled the preparation of cellulose powder (non-flat):

To put in the blender as the cellulose powder that derives from wood pulp (manufacturing of W-100G/Nippon Paper Chemicals society) of raw material, will be to add after 2% ceramide 2 (manufacturing of the high sand spice of TIC-001/ society) is dissolved in the hexane with respect to cellulose powder., with rotating speed 40rpm carry out 5 minute stir, pulverize behind the drying under reduced pressure, obtain ceramide and handle cellulose powder (non-flat) (relatively goods 5) thereafter.

Embodiment 47

The tack test:

Likewise study the plain powder body of ceramide processing flat fiber, the plain powder body of cholesterol processing flat fiber, the plant sterol that obtain in embodiment 40,44 and 46 with embodiment 8 and handle the tack of flat fiber element powder body (goods 10～12) skin.As relatively, use the stearic acid of reference example 1 to handle flat fiber plain (relatively goods 1).Their result lists in table 6.

[table 6]

Embodiment 48

Pressed powder type foundation cream:

Prepare the pressed powder foundation cream according to conventional method with the composition shown in the below table 7.For resulting pressed powder foundation cream, likewise its " uniformity of cosmetic film ", " cosmetic retentivity " and " usability (the smooth sense during coating) " are estimated with embodiment 9.Its result also gathered list in table 7.

[table 7]

Need to prove; Handle the foundation cream (the present invention's article 4～6) of the plain powder body of flat fiber, the plain powder body of cholesterol processing flat fiber, the plain powder body of plant sterol processing flat fiber for having used ceramide; With replace with stearic acid handle the relatively article 5 of the plain powder body of flat fiber, replace with ceramide handle the relatively article 6 of sericite, respectively be combined with cellulose and ceramide relatively article 7, replace with that ceramide is handled the relatively article 8 of cellulose powder, is combined with the relatively article 9 of cellulose and cholesterol respectively, the relatively article 10 that are combined with cellulose and plant sterol are respectively compared; Even experienced long-time; The cosmetic film also can be kept, make up through the time excellent aspect the retentivity.And; For the foundation cream of the present invention's article 4, with the use of embodiment 9 the phospholipid foundation cream (the present invention's article 1～3) of handling the plain powder body of flat fiber compare, even experienced long-time; Also can keep the skin texture fineness of cosmetic film, make up through the time retentivity aspect more excellent.

Embodiment 49

Emulsion:

Make emulsion with the composition shown in the below table 8 as follows.As follows for resulting emulsion is coated water content behind the skin through the time change (after being coated with 5 hours) and study.Its result also gathered list in table 8.

(manufacturing approach)

After following compositions (1)～(10), (23) are heated to 70 ℃ of dissolvings, (11)～(14) are likewise heated, add afterwards, stir.After at room temperature carrying out natural cooling, add a part swollen (15), (16) of mixing with (14).Further disperse to add mixing behind (17)～(22).

(test method)

< water content through time change >

At first utilize the predetermined material that cleans that the coating position is cleaned; Thereafter in the environmental test chamber's (22 ℃ of temperature, relative humidity 50%) that gets into certain condition through after more than 20 minutes; " SKICON200EX " that uses IBS society to make carries out 4 times and measures, and uses its meansigma methods.The wrist medial part marks the cubic frame of 2cm on each measured, and each sample is coated on wherein with each 200ml.To measuring with the water content of coating after 5 hours before each position coating, calculate its ratio with respect to initial value.

< emulsion stability >

With each sample in 50 ℃ down preserve 1 month after, confirm to have or not the generation of crystallization precipitate, with the situation of no crystallization precipitate be judged to be zero, will have crystalline situation be judged to be *.

(result)

[table 8]

Need to prove; Handle the emulsion of the plain powder body of flat fiber for the ceramide that has used the present invention's article 7; With do not add ceramide handle the relatively article 11 of the plain powder body of flat fiber, replace with stearic acid handle the relatively article 12 of the plain powder body of flat fiber, use the plain powder body of untreated fibers relatively article 13, cooperated cellulose to compare respectively with the relatively article 14 of ceramide; Even passed through long-time; The water content of skin also can be kept, and is more excellent aspect moistening effect by the time.

Embodiment 50

Cosmetic gel liquid:

Make cosmetic gel liquid with the composition shown in the below table 9 as follows.As follows for resulting cosmetic gel liquid is coated moisture evapotranspiration behind the skin through the time change (after being coated with 5 hours) and study.Its result also gathered list in table 9.

(manufacturing approach)

After following compositions (1)～(4) uniform dissolution, uniform dissolution is likewise carried out in (5)～(10), add afterwards, stir.Add to mix and carry out swollen (16), (17) with (18).Further (11)～(15) are disperseed, add mixing afterwards.

(test method)

At first utilize the predetermined material that cleans that the coating position is cleaned; Thereafter in the environmental test chamber's (22 ℃ of temperature, relative humidity 50%) that gets into certain condition through after more than 20 minutes; The Vapometer model SWL2 that uses Delfin Technologies society to make carries out the mensuration of 4 moisture evapotranspirations (TEWL), uses its meansigma methods.The wrist medial part marks the cubic frame of 2cm on each measured, and each sample is coated wherein with each 200ml.To measuring with the moisture evapotranspiration of coating after 5 hours before each position coating, calculate its ratio with respect to initial value.

(result)

[table 9]

Need to prove; Handle the beautifying liquid of the plain powder body of flat fiber for the ceramide that has used the present invention's article 8; With do not add ceramide handle the relatively article 15 of the plain powder body of flat fiber, used the plain powder body of untreated fibers relatively article 16, replace with stearic acid and handle the relatively article 17 of the plain powder body of flat fiber and compare; Even passed through for a long time, the moisture evapotranspiration of skin has also obtained inhibition, and is more excellent aspect moistening effect by the time.And; Even the such dosage form of beautifying liquid that crystallization few for oil preparation, that be difficult to suppress ceramide is separated out; The beautifying liquid that has used the ceramide of the present invention's article 8 to handle the plain powder body of flat fiber also can suppress the crystallization of ceramide separates out, and also is excellent can easily cooperating the ceramide this respect.

Embodiment 51

Two laminar astringent:

In the two laminar astringent of embodiment 10, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 40 of ceramide processing flat fiber, in addition, likewise make two laminar astringent.

Resulting two laminar astringent are excellent aspect soft and smooth usability, than embodiment 10, suppress two more excellent laminar astringent of effect for moisture evapotranspires.

Embodiment 52

Emulsion:

In the emulsion of embodiment 11; Phospholipid is handled flat fiber element powder body (goods 1) replace with the cholesterol processing cellulose powder body 1.0% that the ceramide of making among the embodiment 41 is handled manufacturing among plain powder body 1.0% of flat fiber and the embodiment 42, likewise make emulsion in addition.

Resulting emulsion is excellent aspect emulsion stability, and soft and smooth usability is arranged, and compares with embodiment 11, evapotranspires for the moisture maintenance and suppresses the more excellent emulsion of effect.

Embodiment 53

Cream:

In the cream of embodiment 12, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 42 of ceramide processing flat fiber, likewise make cream in addition.

Resulting cream is excellent aspect emulsion stability, soft and smooth usability is arranged, and compares with embodiment 12, suppresses the more excellent cream of effect for moisture keeps evapotranspiring.

Embodiment 54

Beautifying liquid:

In the beautifying liquid of embodiment 13, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 46 of plant sterol processing flat fiber, likewise make beautifying liquid in addition.

Resulting beautifying liquid is excellent aspect stable, with embodiment 13 likewise be soft and smooth usability, the excellent beautifying liquid of cosmetic lasting effect.

Embodiment 55

Facial film:

In the facial film of embodiment 14, phospholipid is handled the plain powder body of flat fiber (goods 5) replace with the plain powder body of making among the embodiment 43 of ceramide processing flat fiber, likewise make facial film in addition.

Resulting facial film is excellent aspect emulsion stability, soft and smooth usability is arranged, and than embodiment 14, suppresses the more excellent facial film of effect for moisture keeps evapotranspiring.

Embodiment 56

Cleansing Foam:

In the Cleansing Foam of embodiment 15, phospholipid is handled the plain powder body of flat fiber (goods 6) replace with the plain powder body of making among the embodiment 45 of cholesterol processing flat fiber, likewise make Cleansing Foam in addition.

Resulting Cleansing Foam and embodiment 15 likewise are the soft and smooth excellent Cleansing Foam of usability.

Embodiment 57

Cleansing cream:

In the cleansing cream of embodiment 16, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 42 of ceramide processing flat fiber, likewise make cleansing cream in addition.

Resulting cleansing cream is excellent aspect emulsion stability, with embodiment 16 likewise be the cleansing cream of soft and smooth usability excellence.

Embodiment 58

Pomade:

In the pomade of embodiment 17, phospholipid is handled the plain powder body of flat fiber (goods 4) replace with the plain powder body of making among the embodiment 40 of ceramide processing flat fiber, likewise make pomade in addition.

Resulting pomade is excellent aspect haircuting property, with embodiment 17 likewise be the pomade of soft and smooth usability excellence.

Embodiment 59

The oiliness eyeliner:

In the oiliness eyeliner of embodiment 18, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 43 of ceramide processing flat fiber, likewise make the oiliness eyeliner in addition.

Resulting oiliness eyeliner and embodiment 18 likewise are soft and smooth usability, the excellent oiliness eyeliners of cosmetic lasting effect.

Embodiment 60

The aqueous eyeliner:

In the aqueous eyeliner of embodiment 19, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 46 of plant sterol processing flat fiber, likewise make the aqueous eyeliner in addition.

Resulting aqueous eyeliner and embodiment 19 likewise are soft and smooth usability, the excellent aqueous eyeliners of cosmetic lasting effect.

Embodiment 61

Eyebrow pencil:

In the eyebrow pencil of embodiment 20, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 44 of cholesterol processing flat fiber, likewise make eyebrow pencil in addition.

Resulting eyebrow pencil and embodiment 20 likewise are soft and smooth usability, the excellent eyebrow pencils of cosmetic lasting effect.

Embodiment 62

O/W type mascara:

In the O/W of embodiment 21 type mascara, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 42 of ceramide processing flat fiber, likewise make O/W type mascara in addition.

Resulting O/W type mascara and embodiment 21 likewise are excellent, the soft and smooth usability of tack, the excellent O/W type mascara of cosmetic lasting effect.

Embodiment 63

Non-water system mascara:

In the non-water system mascara of embodiment 22, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 42 of ceramide processing flat fiber, likewise make non-water system mascara in addition.

Resulting non-water system mascara and embodiment 22 likewise are soft and smooth usability, the excellent non-water system mascaras of cosmetic lasting effect.

Embodiment 64

The strip lipstick:

In the strip lipstick of embodiment 23, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 41 of ceramide processing flat fiber, likewise make the strip lipstick in addition.

Resulting strip lipstick and embodiment 23 likewise are soft and smooth usability, the excellent lipsticks of cosmetic lasting effect.

Embodiment 65

Liquid rouge:

In the liquid rouge of embodiment 24, phospholipid is handled the plain powder body of flat fiber (goods 4) replace with the plain powder body of making among the embodiment 46 0.5% of plant sterol processing flat fiber, likewise make liquid rouge in addition.

Resulting liquid rouge and embodiment 24 likewise are soft and smooth usability, the excellent liquid rouges of cosmetic lasting effect.

Embodiment 66

O/W type foundation cream:

In the O/W of embodiment 25 type foundation cream, phospholipid is handled the plain powder body of flat fiber (goods 5) replace with the plain powder body of making among the embodiment 43 of ceramide processing flat fiber, likewise make O/W type foundation cream in addition.

Resulting O/W type foundation cream and embodiment 25 likewise are soft and smooth usability, the excellent O/W type foundation creams of cosmetic lasting effect.

Embodiment 67

The w/o type foundation cream:

In the w/o type foundation cream of embodiment 26, phospholipid is handled the plain powder body of flat fiber (goods 6) replace with the plain powder body of making among the embodiment 45 3.0% of cholesterol processing flat fiber, likewise make the w/o type foundation cream in addition.

Resulting w/o type foundation cream and embodiment 26 likewise are soft and smooth usability, the excellent w/o type foundation creams of cosmetic lasting effect.

Embodiment 68

O/W type eye is color:

In the O/W of embodiment 27 type eye coloured silk, phospholipid is handled the plain powder body of flat fiber (goods 5) replace with the plain powder body of making among the embodiment 44 of cholesterol processing flat fiber, it is color likewise to make O/W type eye in addition.

Resulting O/W type eye coloured silk likewise is the soft and smooth excellent O/W type eye coloured silk of usability, cosmetic lasting effect with embodiment 27.

Embodiment 69

The solid type foundation cream of oiliness:

In the solid type foundation cream of the oiliness of embodiment 28, phospholipid is handled the plain powder body of flat fiber (goods 4) replace with the plain powder body of making among the embodiment 42 of ceramide processing flat fiber, likewise make the solid type foundation cream of oiliness in addition.

Solid type foundation cream of resulting oiliness and embodiment 28 have the solid type foundation cream of the also excellent oiliness of soft and smooth usability, cosmetic lasting effect.

Embodiment 70

The strip concealer:

In the strip concealer of embodiment 29, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 40 of ceramide processing flat fiber, likewise make the strip concealer in addition.

Resulting strip concealer and embodiment 29 likewise are soft and smooth usability, the excellent strip concealers of cosmetic lasting effect.

Embodiment 71

The health breast:

In the health Ruzhong of embodiment 30, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 45 of cholesterol processing flat fiber, likewise make the health breast in addition.

Resulting health breast is excellent aspect emulsion stability, with embodiment 30 likewise be the soft and smooth excellent health breast of usability, cosmetic lasting effect.

Embodiment 72

Hair conditioner:

In the hair conditioner of embodiment 31, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 41 of ceramide processing flat fiber, likewise make hair conditioner in addition.

Resulting hair conditioner is excellent aspect emulsion stability, with embodiment 31 likewise be the hair conditioner of soft and smooth usability excellence.

Embodiment 73

Send out film:

Sending out in the film of embodiment 32, phospholipid is handled the plain powder body of flat fiber (goods 1) replace with the plain powder body of making among the embodiment 44 of cholesterol processing flat fiber, likewise make in addition and send out film.

Resulting film is excellent aspect emulsion stability, with embodiment 32 likewise be the soft and smooth excellent film of usability.

Embodiment 74

The w/o type sunscreen cream:

In the w/o type sunscreen cream of embodiment 33, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 43 of ceramide processing flat fiber, likewise make the w/o type sunscreen cream in addition.

Resulting w/o type sunscreen cream and embodiment 33 likewise are soft and smooth usability, the excellent sunscreen cream of cosmetic lasting effect.

Embodiment 75

Nial polish:

In the nial polish of embodiment 34, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 45 of cholesterol processing flat fiber, likewise make nial polish in addition.

Resulting nial polish and embodiment 34 likewise are soft and smooth usability, the excellent nial polishs of cosmetic lasting effect.

Embodiment 76

Sun screen:

In the sun screen of embodiment 35, phospholipid is handled the plain powder body of flat fiber (goods 4) replace with the plain powder body of making among the embodiment 46 of plant sterol processing flat fiber, likewise make sun screen in addition.

Resulting sun screen is excellent aspect emulsion stability, with embodiment 35 likewise be the soft and smooth excellent following ground of usability, cosmetic lasting effect.

Embodiment 77

White lead:

In the white lead of embodiment 36, phospholipid is handled the plain powder body of flat fiber (goods 8) replace with the plain powder body of making among the embodiment 40 of ceramide processing flat fiber, likewise make white lead in addition.

Resulting white lead and embodiment 36 likewise are excellent, the soft and smooth usability of tack, the excellent white lead of cosmetic lasting effect.

Embodiment 78

Pressed powder type foundation cream:

In the pressed powder type foundation cream of embodiment 37, phospholipid is handled the plain powder body of flat fiber (goods 9) replace with the plain powder body of making among the embodiment 41 of ceramide processing flat fiber, likewise make pressed powder type foundation cream in addition.

Resulting pressed powder type foundation cream and embodiment 37 are likewise excellent aspect tack, soft and smooth usability, compare with embodiment 35, are the more excellent foundation cream of cosmetic lasting effect.

Embodiment 79

Pressed powder type kermes (Gu shape powder-type チー Network):

In the pressed powder type kermes of embodiment 38, phospholipid is handled the plain powder body of flat fiber (goods 3) replace with the plain powder body of making among the embodiment 46 of plant sterol processing flat fiber, likewise make pressed powder type kermes in addition.

Resulting pressed powder type kermes and embodiment 38 likewise are excellent, the soft and smooth usability of tack, the excellent kermes of cosmetic lasting effect.

Embodiment 80

Pressed powder type eye shadow:

In the pressed powder type eye shadow of embodiment 39, phospholipid is handled the plain powder body of flat fiber (goods 2) replace with the plain powder body of making among the embodiment 44 of cholesterol processing flat fiber, likewise make pressed powder type eye shadow in addition.

Resulting pressed powder type eye shadow and embodiment 39 likewise are soft and smooth usability, the excellent eye shadows of cosmetic lasting effect.

[industrial applicibility]

Amphiphilic agent of the present invention is handled in the plain powder body of flat fiber, substrate fiber plain this as Organic substance, and be flat, thus with compare the usability that tack is high, have excellence as Talcum, the sericite of existing flat inorganic matter.Further, handle the plain powder body of flat fiber for amphiphilic agent, handle through amphiphilic agent on its surface, thereby tack, the soft and smooth sense when in being engaged to the material of making up, being coated with, the excellent in uniformity of cosmetic film, and cosmetic persistence etc. is improved.

Thereby; Amphiphilic agent of the present invention is handled the plain powder body of flat fiber and can be used in the multiple cosmetic material; As the cosmetic material that is easy to show its effect especially; The excellent powder body of moisture retention such as inhibition that evapotranspires for moisture maintenance dose, moisture can suitably be used for the cosmetic skin-care material of foundation make up material, particularly beautifying liquid, emulsion, cream and so on; For the powder body of the excellent dispersion in general oil solution, water, can be suitably as beauty and make-up material such as liquid foundation.And the tack of these powder body is good, the cosmetic retentivity is excellent, thereby also can be suitably as beauty and make-up material such as foundation creams.

Claims

1. an amphiphilic agent is handled the plain powder body of flat fiber; It obtains through cellulose-based material and amphiphilic agent are carried out the mechanicalness pulverization process, and said amphiphilic agent is selected from more than a kind or 2 kinds of amphiphilic agent in the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof.

2. amphiphilic agent as claimed in claim 1 is handled the plain powder body of flat fiber, and its mean diameter is that 1 μ m～50 μ m, average thickness are that 0.1 μ m～10 μ m and flatness are 4～200.

3. according to claim 1 or claim 2 amphiphilic agent is handled the plain powder body of flat fiber, wherein, uses 0.1 mass parts～12 mass parts amphiphilic agents with respect to cellulose-based material 100 mass parts.

4. handle the plain powder body of flat fiber like each described amphiphilic agent of claim 1 to 3, wherein, utilize the planet-shaped ball mill to carry out the mechanicalness pulverization process.

5. handle the plain powder body of flat fiber like each described amphiphilic agent of claim 1 to 4; Wherein, cellulose-based material is fibrous or pulverous wood powder or the wood pulp that derives from timber, the fibrous or pulverous kapok that derives from Cotton Gossypii or linter, they is made with extra care the fibrous or powdered substance that forms.

6. a cosmetic is expected, its each described amphiphilic agent that contains claim 1 to 5 is handled the plain powder body of flat fiber.

7. cosmetic material as claimed in claim 6, it is foundation cream, eye shadow, rouge, face powder.

8. an amphiphilic agent is handled the manufacturing approach of the plain powder body of flat fiber; It is characterized in that; Cellulose-based material and amphiphilic agent are carried out the mechanicalness pulverization process, and said amphiphilic agent is selected from more than a kind or 2 kinds of amphiphilic agent in the group of being made up of phospholipid, ceramide, cholesterol or derivatives thereof, plant sterol or derivatives thereof.

9. amphiphilic agent as claimed in claim 8 is handled the manufacturing approach of the plain powder body of flat fiber, wherein, adds 0.1 mass parts～12 mass parts amphiphilic agents with respect to cellulose-based material 100 mass parts.

10. like the manufacturing approach of claim 8 or the plain powder body of 9 described amphiphilic agents processing flat fibers, wherein, utilize the planet-shaped ball mill to carry out the mechanicalness pulverization process.