CN106619183A - Washing-free powdery shampoo and preparation method thereof - Google Patents
Washing-free powdery shampoo and preparation method thereof Download PDFInfo
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- CN106619183A CN106619183A CN201710149935.XA CN201710149935A CN106619183A CN 106619183 A CN106619183 A CN 106619183A CN 201710149935 A CN201710149935 A CN 201710149935A CN 106619183 A CN106619183 A CN 106619183A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Birds (AREA)
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Abstract
The invention provides powdery shampoo which is free from a surfactant and free from washing. The powdery shampoo consists of the following components in percentage by weight: 5-50% of cellulose porous particles, 5-50% of starch, 5-20% of polymethyl methacrylate, 0.5-2.0% of capryloyl glycine and 0.5-2.0% of xylitylglucoside, wherein particle size of the cellulose porous particles is 4-70 [mu]M, particle size of the starch is 2-70 [mu]M and particle size of the polymethyl methacrylate is 5-20 [mu]M. The washing-free powdery shampoo provided by the invention is simple in formula and convenient to use; grease and dirt on hair and scalp can be completely removed as the powdery shampoo gets into full contact with the hair, the hair is lightly massaged for 1-2min and then the hair is lightly flipped or blown, so that the hair is kept refreshing and smooth, without feeling of being greasy, and the scalp is prevented from getting itchy; the powdery shampoo can achieve a same effect as that of washing shampoo; and the powdery shampoo is especially suitable for areas in lack of a water resource or people that washing is unsuitable. The invention also provides a preparation method of the washing-free shampoo.
Description
Technical field
The present invention relates to a kind of cleaning nursing article, more particularly to a kind of shampoo for cleaning and maintaining hair, more
Body is to be related to a kind of powdery shampoo without surfactant and without the need for washing.The invention further relates to a kind of above-mentioned Non-water washing powdery
The preparation method of shampoo.
Background technology
Shampoo is the transliteration of foreign word " Shampoo ", can be construed to clean and maintain hair and skin from broad sense, simply
Say to be exactly shampoo.Shampoo is mainly made up of detergent, aucillary detergent and additive, and shampoo can clean hair and head
Dirt on skin, reduces or suppresses the growth of antibacterial, makes hair non-greasy and easily combing, therefore is in people's daily life
Requisite articles for use.Traditional shampoo all contains surfactant, and it is to reduce oils and fatss, the table of dirt using surfactant
Face tension force, subsequently into water phase, therefore in use must could oils and fatss, Fouling Cleaning is clean by washing；But
Where some conditions are limited, such as out on tours or field work, often cannot Jing often wash hair, and for weakly disease
Patient or women have given birth to the date of child's " being confined in childbirth ", to avoid having a cold, also tend to dare not to be cleaned with water hair, therefore only
Hair can by force be born and stick the discomforts such as greasy, scalp itch, this not only affects appearance phenomenon, also affects mood；With living standard not
Disconnected to improve, people increasingly focus on the dressing of oneself, and salubrious, the clean and tidy impact to dressing of hair is very big, therefore
Seek it is a kind of can rapid cleaning hair dirt, allow hair to keep cleaning dry and comfortable, while and the shampoo that need not wash, be this area
Technical staff endeavours the problem studied.
The content of the invention
To solve the problem with present on, it is an object of the invention to provide a kind of good, the easy to use Non-water washing of cleaning force
Powdery shampoo.
It is a further object of the present invention to provide a kind of preparation method of above-mentioned Non-water washing powdery shampoo.
To realize object above, the Non-water washing powdery shampoo of the present invention includes cellulose porous grain by weight percentage
Sub- 5-50%, starch 5-50%, polymethyl methacrylate 5-20%, decoyl glycine 0.5-2.0%, xylitol glucoside 0.5-
2.0%；The wherein particle diameter of cellulose porous granule is 4-70um, and the particle diameter of starch is 2-70um, the grain of polymethyl methacrylate
Footpath is 5-20um.
Above-mentioned particle diameter auspicious steps on Mel father and son company for the preferred Germany of cellulose porous granule of 4-70um（Abbreviation JRS）Production
Model Vivapur CS 4FM, Vivapur CS 9FM, VITACEL CS 20FC or Vivapur CS 70FM in it is a kind of
Or it is various.
One or more in the preferred tapioca of above-mentioned starch or corn starch, the preferred 15-20 um of particle diameter.
The preferred 5.8-8.5um of particle diameter of above-mentioned polymethyl methacrylate.
In order to more preferably remove the oils and fatss on hair and dirt, the shampoo of above-mentioned Non-water washing powdery also includes the ring paste of 5-10%
Essence.
The preferred beta-schardinger dextrin-of above-mentioned cyclodextrin.
In order that Non-water washing powdery shampoo has pleasant abnormal smells from the patient, the shampoo of above-mentioned Non-water washing powdery also includes 0.1-0.5%
Spice, one or more in the preferred Fructus Citri Limoniae quintessence oil of spice, chamomile essential oil, rosemary ethereal oil.
Present invention also offers a kind of preparation method of above-mentioned Non-water washing powdery shampoo, the method is successively including following step
Suddenly：
（1）The soft powder of cellulose porous, starch, polymethyl methacrylate and decoyl glycine are placed in Spray Grain-make Drier
Mixing 2-3 minutes；
（2）Xylitol glucoside is put in grinder, step is taken（1）The amount of the powder 8-10% for mixing point adds for 8-10 time
Enter in grinder, every time grinding 1-2 minutes；
（3）By step（2）The powder for obtaining insert in Spray Grain-make Drier with step（1）The powder mixing 4-6 minutes for obtaining,
Can take the dish out of the pot after mix homogeneously.
In above-mentioned preparation method, step（3）Mixing be first not use fly cutter to carry out mixing 2-3 minutes, reuse fly cutter
Mixing 2-3 minutes.
In above-mentioned preparation method, step（1）Cyclodextrin has been additionally added while cellulose porous granule is added；Step
（2）Spice has been additionally added while xylitol glucoside is added.
The Non-water washing powdery shampoo of the present invention, using the native cellulose porous granule of specified particle diameter as carrier, Yi Dian
Powder is first adsorbed and is absorbed as filler to hair excess oil, makes hair keep dry and comfortable, is recycled and is had fine antibacterial effect
The decoyl glycine of fruit can both prevent scalp itch as conditioner, and the superfluous of sebum can be suppressed to secrete again, and poly- methyl-prop
The addition of e pioic acid methyl ester and xylitol glucoside, is in order that hair after cleaning is smooth and prevent the withered tarnish of hair.
The powdery shampoo of the present invention, formula is simple, easy to use, only need to be fully contacted the very little powdery shampoo of particle diameter with hair
Afterwards, gently massage 1-2 minutes, then gently brush off or blow off, just can be clean by the oils and fatss on hair and scalp and soil cleaning, make
Hair keeps salubrious submissive non-greasy, scalp not to itch, and with the effect same with washing, is particularly suitable for the ground that water resource lacks
Area or the crowd for being not suitable for washing use.The preparation method of powdery shampoo of the present invention, process is simple, the properties of product for obtaining are steady
It is fixed, and have safely and efficiently cleaning effect.
Specific embodiment
Technical scheme is described further below by specific embodiment, but these embodiments are not used
Equivalent replacement or each component in limiting the scope of the invention, on the premise of without departing from theory of the present invention, to each component
The adjustment of proportioning, all should belong to protection scope of the present invention.
First, embodiment
Embodiment 1
1st, formula（By weight percentage）
Vivapur CS 9FM 18.0%
VITACEL CS 20FC 30.0%
Tapioca（15-20 um） 30.0%
Polymethyl methacrylate（5.8-8.5um） 15.0%
Beta-schardinger dextrin -5.0%
Decoyl glycine 0.8%
Xylitol glucoside 1.0%
Chamomile essential oil 0.2%
2nd, preparation technology（Experiment is based on 2kg yield）
（1）Each component has been weighed by said ratio；
（2）By Vivapur CS 9FM, VITACEL CS 20FC, tapioca, polymethyl methacrylate, beta-schardinger dextrin-,
Decoyl glycine etc. is placed in Spray Grain-make Drier and mixes 2 minutes；
（3）Xylitol glucoside and chamomile essential oil are put in grinder, 20g steps are added every time（2）The powder for mixing
End is ground 1 minute into grinder, and till being added to 160g powder, powder now has adsorbed completely wetting agent and spice；
（4）By step（3）Powder after absorption is good is inserted in Spray Grain-make Drier and mixed, and does not first use fly cutter to be mixed
Close 2 minutes, reuse fly cutter and mix 2 minutes, can take the dish out of the pot after mix homogeneously.
Embodiment 2
1st, formula（By weight percentage）
Vivapur CS 4FM 5.0%
VITACEL CS 20FC 27.0%
Tapioca 50.0%
Polymethyl methacrylate（5.8-8.5um） 10.0%
Beta-schardinger dextrin -5.0%
Decoyl glycine 1.8%
Xylitol glucoside 1.0%
Chamomile essential oil 0.2%
2nd, preparation technology（Experiment is based on 2kg yield）
（1）Each component has been weighed by said ratio；
（2）By Vivapur CS 4FM, VITACEL CS 20FC, tapioca, polymethyl methacrylate, beta-schardinger dextrin-,
Decoyl glycine etc. is placed in Spray Grain-make Drier and mixes 2 minutes；
（3）Xylitol glucoside and chamomile essential oil are put in grinder, 20g steps are added every time（2）The powder for mixing
End is ground 1 minute into grinder, and till being added to 160g powder, powder now has adsorbed completely wetting agent and spice；
（4）By step（3）Powder after absorption is good is inserted in Spray Grain-make Drier and mixed, and does not first use fly cutter to be mixed
Close 2 minutes, reuse fly cutter and mix 2 minutes, can take the dish out of the pot after mix homogeneously.
Embodiment 3
1st, formula（By weight percentage）
Vivapur CS 9FM 5.0%
VITACEL CS 20FC 30.0%
Corn starch 45.0%
Polymethyl methacrylate（5.8-8.5um） 10.0%
Beta-schardinger dextrin -7.6%
Decoyl glycine 1.2%
Xylitol glucoside 1.0%
Fructus Citri Limoniae quintessence oil 0.2%
2nd, preparation technology（Experiment is based on 2kg yield）
（1）Each component has been weighed by said ratio；
（2）By Vivapur CS 9FM, VITACEL CS 20FC, corn starch, polymethyl methacrylate compound, β-ring
Dextrin, decoyl glycine etc. are placed in Spray Grain-make Drier and mix 2 minutes；
（3）Xylitol glucoside and chamomile essential oil are put in grinder, 20g steps are added every time（2）The powder for mixing
End is ground 1 minute into grinder, and till being added to 160g powder, powder now has fully absorbed wetting agent and spice；
（4）By step（3）Powder after absorption is good is inserted in Spray Grain-make Drier and mixed, and does not first use fly cutter to be mixed
Close 2 minutes, reuse fly cutter and mix 2 minutes, can take the dish out of the pot after mix homogeneously.
2nd, product stability detection
Relevant criterion is found because the shampoo of powder dose-type there is presently no, temporarily according to cosmetics QB/T 1859-2004【It is fragrant
Powder, talcum powder, prickly-heat powder】Standard, the product that embodiment 1-3 is obtained is detected, it is as a result as follows：
1st, sanitary index：
2nd, sense organ, physical and chemical index
As can be seen from the above table, Non-water washing powdery shampoo of the invention items sanitary index, organoleptic indicator, physical and chemical index are complete
Meet cosmetics QB/T 1859-2004 standards.
3rd, using effect test
Use for convenience of consumer, the product of the present invention can be fitted in flat Bottle ＆ Can or inhalator jar.By taking flat Bottle ＆ Can as an example, water will be exempted from
Powdery shampoo is washed in right amount on the palm of the hand, itself and hair uniform contact is allowed, both hands are slightly massaged makes the abundant cleaning head of anhydrous shampoo
Send out and scalp, the powder for being adsorbed with hair oils and fatss and dirt is gently brushed off after 1-2min.
30 volunteers are selected, is tested with the sample obtained by embodiment 1-3, observe Non-water washing powdery of the present invention fragrant
Cleaning effect and antipruritic effect of the ripple to hair, effect is as follows：
It is above-mentioned test result indicate that：Non-water washing powdery shampoo obtained by embodiment 1-3 has preferable cleaning effect to hair,
And smooth effect has certain relation with the particle diameter of cellulose porous granule and the addition of starch for adopting.
Claims (10)
1. a kind of Non-water washing powdery shampoo, including cellulose porous granule 5-50% by weight percentage, starch 5-50%, gathers
Methyl methacrylate 5-20%, decoyl glycine 0.5-2.0% and xylitol glucoside 0.5-2.0%, wherein cellulose porous
The particle diameter of particle is 4-70um, and the particle diameter of starch is 2-70um, and the particle diameter of polymethyl methacrylate is 5-20um.
2. Non-water washing powdery shampoo according to claim 1, it is characterised in that：The particle diameter is the fibrination of 4-70um
Hole particle steps on Mel father and son company for Germany is auspicious（Abbreviation JRS）The model Vivapur CS 4FM of production, Vivapur CS
One or more in 9FM, VITACEL CS 20FC or Vivapur CS 70FM.
3. Non-water washing powdery shampoo according to claim 1 and 2, it is characterised in that：The starch is tapioca or jade
One or more in rice starch, particle diameter is 15-20 um.
4. Non-water washing powdery shampoo according to claim 3, it is characterised in that：The particle diameter of the polymethyl methacrylate
For 5.8-8.5um.
5. Non-water washing powdery shampoo according to claim 4, it is characterised in that：The Non-water washing powdery shampoo is also included
The cyclodextrin of 5-10%.
6. Non-water washing powdery shampoo according to claim 5, it is characterised in that：The cyclodextrin is beta-schardinger dextrin-.
7. Non-water washing powdery shampoo according to claim 6, it is characterised in that：The Non-water washing powdery shampoo is also included
The spice of 0.1-0.5%, spice is one or more in Fructus Citri Limoniae quintessence oil, chamomile essential oil, rosemary ethereal oil.
8. a kind of preparation method of Non-water washing powdery shampoo described in claim 1, the method in turn includes the following steps：
（1）The soft powder of cellulose porous, starch, polymethyl methacrylate and decoyl glycine are placed in Spray Grain-make Drier
Mixing 2-3 minutes；
（2）Xylitol glucoside is put in grinder, step is taken（1）The amount of the powder 8-10% for mixing point adds for 8-10 time
Enter in grinder, every time grinding 1-2 minutes；
（3）By step（2）The powder for obtaining insert in Spray Grain-make Drier with step（1）The powder mixing 4-6 minutes for obtaining,
Can take the dish out of the pot after mix homogeneously.
9. the preparation method of Non-water washing powdery shampoo according to claim 8, it is characterised in that：In the preparation method,
Step（3）Mixing be first not use fly cutter to carry out mixing 2-3 minutes, reuse fly cutter mixing 2-3 minutes.
10. the preparation method of Non-water washing powdery shampoo according to claim 8, it is characterised in that：In the preparation method,
Step（1）Also it is added with cyclodextrin to be mixed；Step（2）Spice has been additionally added while xylitol glucoside is added.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710149935.XA CN106619183A (en) | 2017-03-14 | 2017-03-14 | Washing-free powdery shampoo and preparation method thereof |
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| CN201710149935.XA CN106619183A (en) | 2017-03-14 | 2017-03-14 | Washing-free powdery shampoo and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
| CN109498494A (en) * | 2018-12-26 | 2019-03-22 | 广州蜜妆生物科技有限公司 | A kind of salubrious oil-control is without silicone oil shampoo and preparation method thereof |
| CN109875918A (en) * | 2019-04-23 | 2019-06-14 | 清远市立道精细化工有限公司 | A kind of Non-water washing hair spray composite and preparation method thereof |
| CN110063900A (en) * | 2019-05-06 | 2019-07-30 | 上海绿瑞生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN111317682A (en) * | 2020-04-15 | 2020-06-23 | 惠州兆婷化妆品有限公司 | Hair styling powder and preparation method thereof |
| CN111557865A (en) * | 2020-05-28 | 2020-08-21 | 上海应用技术大学 | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof |
| WO2023152113A1 (en) * | 2022-02-08 | 2023-08-17 | Unilever Ip Holdings B.V. | Dry compositions and methods for forming stable liquid cleansing formulations |
| WO2023152112A1 (en) * | 2022-02-08 | 2023-08-17 | Unilever Ip Holdings B.V. | Dry compositions and methods for forming stable liquid cleansing formulations |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
| CN109498494A (en) * | 2018-12-26 | 2019-03-22 | 广州蜜妆生物科技有限公司 | A kind of salubrious oil-control is without silicone oil shampoo and preparation method thereof |
| CN109498494B (en) * | 2018-12-26 | 2021-11-30 | 广州蜜妆生物科技有限公司 | Refreshing oil-control silicone-oil-free shampoo and preparation method thereof |
| CN109875918A (en) * | 2019-04-23 | 2019-06-14 | 清远市立道精细化工有限公司 | A kind of Non-water washing hair spray composite and preparation method thereof |
| CN110063900A (en) * | 2019-05-06 | 2019-07-30 | 上海绿瑞生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN111317682A (en) * | 2020-04-15 | 2020-06-23 | 惠州兆婷化妆品有限公司 | Hair styling powder and preparation method thereof |
| CN111557865A (en) * | 2020-05-28 | 2020-08-21 | 上海应用技术大学 | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof |
| WO2023152113A1 (en) * | 2022-02-08 | 2023-08-17 | Unilever Ip Holdings B.V. | Dry compositions and methods for forming stable liquid cleansing formulations |
| WO2023152112A1 (en) * | 2022-02-08 | 2023-08-17 | Unilever Ip Holdings B.V. | Dry compositions and methods for forming stable liquid cleansing formulations |
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