CN108125859A - A kind of multi-functional amino acid cleansing cream and preparation method thereof - Google Patents

A kind of multi-functional amino acid cleansing cream and preparation method thereof Download PDF

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Publication number
CN108125859A
CN108125859A CN201810036192.XA CN201810036192A CN108125859A CN 108125859 A CN108125859 A CN 108125859A CN 201810036192 A CN201810036192 A CN 201810036192A CN 108125859 A CN108125859 A CN 108125859A
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sodium
amino acid
extract
functional amino
plant
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汪丽
李莹
崔逢起
方永培
孙剑
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Shaanxi HuiKang Bio Tech Co Ltd
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Shaanxi HuiKang Bio Tech Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

Abstract

The invention discloses a kind of multi-functional amino acid cleansing creams, and by weight percentage, the face cleaning cream includes the following raw material:Glycerine 20 25%, amino acid type surfactant 7.5 22.5%, 1,3 propylene glycol 5 15%, xanthans 0.1 0.3%, EDETATE SODIUM 0.05 0.1%, lauryl glucoside 1 2%, anti-acne ingredient 0.01 0.02%, grease 1 6%, Sodium Hyaluronate 0.01 0.05%, Sodium Polyacrylate 0.005 0.01%, plant desensitizer 2 3%, plant antiseptic agent 0.1 0.3%, essence 0.1 0.2%, surplus is deionized water, wherein, the amino acid type surfactant includes myristoyl glutamate sodium, sodium cocoyl glutamate, sodium lauroyl glutamate.Under the synergistic effect of each raw material, face cleaning cream provided by the invention can safely and effectively removal eye, lip heavy make-up, wash unload it is thorough, mild it is non-stimulated, moisten it is not tight;Acne and a small number of small poxs can be effectively removed, improves sensitive skin, reduces allergy rate;Essence smell can be extended, effectively cover peculiar smell.The invention also discloses a kind of preparation methods of multi-functional amino acid cleansing cream.

Description

A kind of multi-functional amino acid cleansing cream and preparation method thereof
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of multi-functional amino acid cleansing cream and preparation method thereof.
Background technology
With people's living standards continue to improve, the continuous development of cosmetics development technique, Cosmetic Market day crescent It is different, wherein all kinds of color make-up skin care item enable many people seeking beauties please heartily and enjoy beautiful dressing particularly by consumers, however, Foundation cream, color make-up have considerable degree of adhesive force on the skin, it is difficult to which thoroughly cleaning, the color make-up meeting blocked pore of attachment cause skin Lipid metaboli is difficult.Meanwhile atmosphere pollution, haze take place frequently, the dust, dirt in air increase, and are easily attached to skin, and the time is long Skin of face can be caused to have difficulty in breathing long, lead to the problem of the skin such as acne, small pox, allergy.In addition, the sebum of oily skin crowd Secrete vigorous, dirt cleans not in time is easily oxidized to form keratotic plug, and the time can block pore for a long time, so as to cause small pox, mistake The skin problem for making us puzzlement such as quick.Part population is tormented often by the embarrassment that abnormal smell of body is brought, in life For the people of clean skin not skin care, abnormal smell of body problem is more prominent.It can be seen that skin care process starts from clean skin, facial cleansing ring It saves particularly important.
At present, Cosmetic Market facial cleansing is presented with " makeup removing+cleaning " dual mode, is not easy to consumer in fast pace Living environment under use.In addition, in place of the equal Shortcomings of the common makeup removal products such as makeup remover, makeup remover, makeup remover by " with The mode of the molten oil of oil " is removed ornaments and formal dress, and makeup removing ability is strong, but skin sense is greasy, flushing capacity is poor, residual soil is more, particularly oiliness Skin crowd should more use with caution;Makeup remover contains emulsifier, meets the cleanable excess oil of water emulsification, but ability of removing ornaments and formal dress is weak, and residual is dirty Dirt is more, can also cause the skin problem such as clogging of pores, small pox, allergy.
Face cleaning cream (breast) decontamination mechanism is that the surface tension of dirt is reduced using surfactant, by soaking, disperseing, sending out The effects that bubble, emulsification, removes dirt.Two class of soap base type and non-soap fundamental mode can be divided into, wherein, soap base type face cleaning cream is that ester is made with alkali With and generate the reaction of corresponding sour (or salt) and alcohol, because containing fatty acid soaps ingredient, strong detergency is easy to rinse, but stimulation Property is big, and washing rear skin has tight feeling, easily makes skin dry and astringent.Non-soap fundamental mode, such as SLES (laureth sulfuric ester sodium salt, ten Dialkyl ether sodium sulphate, laureth sodium sulfovinate), SLS (sodium lauryl sulfate, alkyl sulfate, dodecyl sulphate Sodium, laruyl alcohol sodium sulfovinate) surfactant-based face cleaning product cleaning force and degreasing power it is very strong, but when it for being in direct contact During skin product, the moisture of skin surface is easily taken away, irritation is larger, and sensitive skin and dry skin should not make for a long time With.The existing non-soap fundamental mode face cleaning cream based on amino acid type surfactant can be adjusted to faintly acid, close to the pH of human skin, It does not stimulate mildly, but effect is relatively simple and cleaning capacity is general.In addition, since cleaning products on the market are mostly washing-off type, So product fragrance general persistence is very short, it is impossible to meet the demand of liking to be beautiful of consumers in general.
Therefore, facial cleansing gradually tends to the multi-C stereo pattern of " makeup removing+cleaning+other effects ", exploitation safety, height Matter multiple-effect, convenient, healthy face cleaning product are the active demands in market, and with very wide application prospect.
Invention content
The purpose of the present invention is to provide a kind of makeup removing ability it is strong, wash and unload one, moisten moisturizing;Can effectively remove acne and A small number of small poxs improve sensitive skin, reduce allergy rate;Essence smell can be extended, the multi-functional amino acid for effectively covering peculiar smell is clean Face cream, it is of the existing technology to solve the problems, such as.
The present invention also provides the preparation methods of above-mentioned multi-functional amino acid cleansing cream.
To achieve the above object, the first aspect of the present invention provides a kind of multi-functional amino acid cleansing cream, and by weight hundred Divide ratio, the face cleaning cream includes the following raw material:Glycerine 20-25%, amino acid type surfactant 7.5-22.5%, 1,3- the third two Alcohol 5-15%, xanthans 0.1-0.3%, EDETATE SODIUM 0.05-0.1%, lauryl glucoside 1-2%, anti-acne ingredient 0.01- 0.02%th, grease 1-6%, Sodium Hyaluronate 0.01-0.05%, Sodium Polyacrylate 0.005-0.01%, plant desensitizer 2- 3%th, plant antiseptic agent 0.1-0.3%, essence 0.1-0.2%, surplus are deionized water, wherein, the amino acid pattern surface is lived Property agent include myristoyl glutamate sodium, sodium cocoyl glutamate, sodium lauroyl glutamate.
Wherein, glycerine, 1,3-PD have dispersion, moisture-keeping function as solvent;Xanthans has thickening, improves skin Sense acts on;Amino acid type surfactant is as decontamination core component, with wetting power is strong, detergency is notable, foaming abundancy is thin The characteristics of greasy, nontoxic, harmless, non-stimulated to skin;Lauryl glucoside is new non-ionic surfactants, is generally also claimed For green surfactant, other than the feature with above-mentioned amino acid type surfactant, can also live with any types surface Property agent compounding, and synergistic effect is apparent, and thickening effect is notable, is easy to dilute, no gelatin phenomenon;Anti-acne ingredient can effectively inhibit, Remove small pox;Selected grease is arranged in pairs or groups with essence science, can effectively be covered abnormal smell of body, be extended essence smell, while have moisturizing Effect;Sodium Hyaluronate is efficient moisture-retention agent;Sodium Polyacrylate has thickening power, can also improve lotion appearance, skin sense;Plant Anti-sensitizer, plant antiseptic agent are respectively provided with releive skin discomfort, antisepsis, to skin without any stimulation.
Further, by weight percentage, the face cleaning cream includes the following raw material:Glycerine 22-25%, amino acid pattern surface Activating agent 14-20.5%, 1,3- propylene glycol 10-15%, xanthans 0.1-0.3%, EDETATE SODIUM 0.05-0.1%, lauryl Portugal Glucosides 1-2%, anti-acne ingredient 0.01-0.02%, grease 1-4%, Sodium Hyaluronate 0.01-0.03%, Sodium Polyacrylate 0.005-0.008%, plant desensitizer 2-3%, plant antiseptic agent 0.1-0.3%, essence 0.1-0.2%, surplus are deionization Water.
Further, by weight percentage, the amino acid type surfactant includes myristoyl glutamate sodium 5- 15%th, sodium cocoyl glutamate 1.5-2.5%, sodium lauroyl glutamate 1-3%.Preferably, by weight percentage, the amino Acid type surfactant includes myristoyl glutamate sodium 10-15%, sodium cocoyl glutamate 2-2.5%, lauroyl glutamate Sodium 2-3%.
Further, the grease be selected from Queensland nut seed oil, jojoba oil, olive oil, palm oil, coconut oil, octanoic acid/ Triglyceride DDD, ethylhexyl palmitate, isopropyl myristate, isopropyl palmitate, isononyl isononanoate, C12-15 alcohol It is one or more in benzoic ether, dimethyl silicone polymer, ring five dimethyl silicone polymer, cyclohexasiloxane.
Further, the anti-acne ingredient selected from tea oil, accutane, azelaic acid, salicylic acid, skin it is proud it is peaceful in It is one or more.
Further, the plant desensitizer is selected from Gotu Kola P.E, licorice root extract, giant knotweed root extract, Huang A kind of reed mentioned in ancient books root extract, the sweet root extract of light fruit, german chamomile flower extract, rough gentian root extract, peony root extractive, Sage extract In it is one or more.
Further, the plant antiseptic agent be selected from Cortex Moutan extract, grapefruit seed extract, Flos Lonicerae extractive solution, It is one or more in vine of multiflower knotweed extracting solution, Chinese prickly ash berry extract, Folium Artemisiae Argyi extract, Fructus Citri grandis extract.
The second aspect of the present invention provides a kind of preparation method of above-mentioned multi-functional amino acid cleansing cream, including walking as follows Suddenly:
(1) each raw material for standby is weighed by weight percentage;
(2) breast is added in after 1,3- propylene glycol, xanthans, anti-acne ingredient, Sodium Hyaluronate, Sodium Polyacrylate being uniformly dispersed Change pot, then sequentially add glycerine, EDETATE SODIUM and deionized water, under stirring condition, warming-in-water is to keeping the temperature after 80-85 DEG C 15-20min, then it is cooled to 60 DEG C;
(3) amino acid type surfactant after mixing, under the conditions of mixing slowly, is slowly added to above-mentioned system, At a temperature of 60 DEG C, 30-40min is at the uniform velocity stirred, after observation material body is uniform, is cooled to 50 DEG C;
(4) lauryl glucoside, grease, essence are added in into above-mentioned system after mixing, at a temperature of 50 DEG C, at the uniform velocity 10-15min is stirred, after observation material body is uniform, is cooled to 40 DEG C;
(5) plant desensitizer, plant antiseptic agent are sequentially added, stirs 10-15min, after observation material body is uniform, it is qualified to examine It can discharge.
The invention has the advantages that:
1st, in multi-functional amino acid cleansing cream provided by the invention amino acid type surfactant with myristoyl glutamate Based on sodium, sodium cocoyl glutamate and sodium lauroyl glutamate are compounded, in other surfaces activating agent, moisturizer, thickener and oil Under the collective effect of fat, synergistic function is played between each raw material, face cleaning cream obtained is made to remove ornaments and formal dress, and ability is strong, washes and unloads one; The pH=5-6 of face cleaning lotion system, approaches with skin ph value, does not stimulate mildly, reduces skin allergy rate;Skin sense water profit is not done It is puckery, not tight;
2nd, multi-functional amino acid cleansing cream selection anti-acne ingredient provided by the invention, plant desensitizer, plant antiseptic agent etc. Ingredient, property is mild, and irritation is small, the effect of releiving to skin, can improve sensitive skin, effectively removes acne and a small number of acnes Acne washes while unload two-in-one, can solve the problems, such as the skin such as sensitivity, small pox;
3rd, selected lubricant component in multi-functional amino acid cleansing cream provided by the invention, ingenious jointly perfume ingredient, can prolong Long essence smell, can effectively cover peculiar smell.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
Embodiment 1
A kind of multi-functional amino acid cleansing cream, by weight percentage, including the following raw material:Glycerine 24%, myristoyl paddy Propylhomoserin sodium 12%, sodium cocoyl glutamate 2.5%, sodium lauroyl glutamate 2.3%, 1,3- propylene glycol 12%, xanthans 0.2%th, EDETATE SODIUM 0.05%, lauryl glucoside 1.5%, skin be proud peaceful 0.01%, Queensland nut seed oil 2%, olive oil 2%th, Sodium Hyaluronate 0.02%, Sodium Polyacrylate 0.005%, plant desensitizer 2%, plant antiseptic agent 0.3%, essence 0.15%, surplus is deionized water.
The preparation method of the multi-functional amino acid cleansing cream of the present embodiment, includes the following steps:
(1) each raw material for standby is weighed by weight percentage;
(2) emulsification is added in after 1,3- propylene glycol, xanthans, Pi Aoning, Sodium Hyaluronate, Sodium Polyacrylate being uniformly dispersed Pot, then sequentially adds glycerine, EDETATE SODIUM and deionized water, under stirring condition, warming-in-water to keeping the temperature 15min after 80 DEG C, It is cooled to 60 DEG C again;
(3) amino acid type surfactant after mixing, under the conditions of mixing slowly, is slowly added to above-mentioned system, At a temperature of 60 DEG C, 40min is at the uniform velocity stirred, after observation material body is uniform, is cooled to 50 DEG C;
(4) lauryl glucoside, Queensland nut seed oil, olive oil, essence are added in into above-mentioned system after mixing, 50 At a temperature of DEG C, 12min is at the uniform velocity stirred, after observation material body is uniform, is cooled to 40 DEG C;
(5) plant desensitizer, plant antiseptic agent are sequentially added, stirs 10min, after observation material body is uniform, inspection qualification is It can discharge.
Embodiment 2
A kind of multi-functional amino acid cleansing cream, by weight percentage, including the following raw material:Glycerine 20%, myristoyl paddy Propylhomoserin sodium 15%, sodium cocoyl glutamate 1.5%, sodium lauroyl glutamate 1.5%, 1,3- propylene glycol 8%, xanthans 0.25%th, EDETATE SODIUM 0.08%, lauryl glucoside 1.8%, accutane 0.02%, olive oil 2%, coconut oil 1%th, Sodium Hyaluronate 0.01%, Sodium Polyacrylate 0.008%, plant desensitizer 2%, plant antiseptic agent 0.15%, essence 0.1%, surplus is deionized water.
The preparation method is the same as that of Example 1 for the multi-functional amino acid cleansing cream of the present embodiment.
Embodiment 3
A kind of multi-functional amino acid cleansing cream, by weight percentage, including the following raw material:Glycerine 25%, myristoyl paddy Propylhomoserin sodium 8%, sodium cocoyl glutamate 2.2%, sodium lauroyl glutamate 2%, 1,3- propylene glycol 5%, xanthans 0.15%, EDETATE SODIUM 0.1%, tea oil 0.01%, jojoba oil 2%, Sodium Hyaluronate 0.04%, gathers lauryl glucoside 1.3% Sodium acrylate 0.01%, plant desensitizer 3%, plant antiseptic agent 0.25%, essence 0.12%, surplus are deionized water.
The preparation method is the same as that of Example 1 for the multi-functional amino acid cleansing cream of the present embodiment.
Embodiment 4
A kind of multi-functional amino acid cleansing cream, by weight percentage, including the following raw material:Glycerine 20%, myristoyl paddy Propylhomoserin sodium 10%, sodium cocoyl glutamate 2%, sodium lauroyl glutamate 3%, 1,3- propylene glycol 10%, xanthans 0.1%, EDETATE SODIUM 0.06%, lauryl glucoside 1%, skin are proud peaceful 0.01%, Queensland nut seed oil 2%, jojoba oil 4%, transparent Matter acid sodium 0.02%, Sodium Polyacrylate 0.01%, plant desensitizer 2%, plant antiseptic agent 0.3%, essence 0.1%, surplus are Deionized water.
The preparation method is the same as that of Example 1 for the multi-functional amino acid cleansing cream of the present embodiment.
Embodiment 5
A kind of multi-functional amino acid cleansing cream, by weight percentage, including the following raw material:Glycerine 22%, myristoyl paddy Propylhomoserin sodium 5%, sodium cocoyl glutamate 1.8%, sodium lauroyl glutamate 1%, 1,3- propylene glycol 15%, xanthans 0.3%, EDETATE SODIUM 0.09%, lauryl glucoside 2%, salicylic acid 0.02%, Sodium Hyaluronate 0.03%, Sodium Polyacrylate 0.006%th, plant desensitizer 3%, plant antiseptic agent 0.2%, essence 0.2%, surplus are deionized water.
The preparation method is the same as that of Example 1 for the multi-functional amino acid cleansing cream of the present embodiment.
Comparative example 1
The raw material components of the face cleaning cream of this comparative example are substantially the same manner as Example 1, the difference lies in:Percentage by weight Than the amino acid type surfactant of this comparative example includes myristoyl glutamate sodium 2.5%, sodium cocoyl glutamate 12%.
The preparation method is the same as that of Example 1 for the face cleaning cream of this comparative example.
Comparative example 2
The raw material components of the face cleaning cream of this comparative example are substantially the same manner as Example 1, the difference lies in:Percentage by weight Than the raw material components of this comparative example do not include grease.
The preparation method is the same as that of Example 1 for the face cleaning cream of this comparative example.
Comparative example 3
The raw material components of the face cleaning cream of this comparative example are substantially the same manner as Example 1, the difference lies in:The original of this comparative example Expect that component does not include anti-acne ingredient.
The preparation method is the same as that of Example 1 for the face cleaning cream of this comparative example.
Comparative example 4
This comparative example is common amino acid pattern face cleaning cream, by weight percentage, including the following raw material:Lauroyl paddy ammonia Sour sodium 21.5%, glycerine 3.5%, 1,3 butylene glycol 13.5%, hydroxyethyl cellulose 0.05%, caprylic/capric triglyceride 2%th, PCA-Na 2.25%, EDETATE SODIUM 0.05%, essence 0.15%, preservative 0.2%, surplus are deionized water.
The preparation method of the amino acid cleansing cream of this comparative example, includes the following steps:
(1) each raw material for standby is weighed by weight percentage;
(2) glycerine, 1,3 butylene glycol, hydroxyethyl cellulose, EDETATE SODIUM, preservative, deionized water are sequentially added into breast Change pot, under stirring condition, warming-in-water is to keeping the temperature 20min, then be cooled to 60 DEG C after 80 DEG C;
(3) under the conditions of mixing slowly, sodium lauroyl glutamate is slowly added to above-mentioned system, constant temperature at the uniform velocity stirs 35min after observation material body is uniform, is cooled to 50 DEG C;
(4) caprylic/capric triglyceride, PCA-Na, essence are sequentially added into above-mentioned system, it is even at a temperature of 50 DEG C Speed stirring 15min, after observation material body is uniform, is cooled to 35 DEG C, examines qualification that can discharge.
Comparative example 5
This comparative example is common soap base type face cleaning cream, by weight percentage, including the following raw material:Stearic acid 15%, meat Myristic acid 8%, lauric acid 6%, beeswax 1%, glycerin monostearate 1%, glycerine 22%, glycol distearate 4%, hydrogen Potassium oxide 4.9%, polyquaternium -7 2%, tetra- sodium 0.05% of EDTA, essence 0.15%, is prevented laureth sodium sulfovinate 3% Rotten agent 0.2%, surplus are deionized water.
The preparation method of the soap base type face cleaning cream of this comparative example, includes the following steps:
(1) each raw material for standby is weighed by weight percentage;
(2) glycerine, potassium hydroxide, tetra- sodium of EDTA, preservative, deionized water are sequentially added into water phase pot, are heated to 70 DEG C, Insulated and stirred, it is ensured that material body is completely dissolved;By stearic acid, myristic acid, lauric acid, beeswax, glycerin monostearate, ethylene glycol Distearate, laureth sodium sulfovinate add in oil phase pot, are heated to 80 DEG C, insulated and stirred, it is ensured that material body is completely dissolved;
(3) under the conditions of insulated and stirred, water phase material is slowly added to oil phase pot, 20min is added, stirring 40min to neat soap It is completely dispersed uniformly, slow cooling is to 50 DEG C.
(4) polyquaternium -7, essence are added in into above-mentioned system, stir 15min, after observation material body is uniform, be cooled to 35 DEG C, Examine qualification that can discharge.
Test example
1st, the sense organ and physical and chemical index of the face cleaning cream of the present invention are tested
Organoleptic indicator's assessment method:Appropriate product is squeezed on flat glass, back to light from the color and luster of product, density, State etc. is tested and assessed.
Heat-resisting cold-resistant indication test method:Outturn sample is respectively placed in 40 DEG C of constant incubator and -15 DEG C of refrigerator In, it takes out afterwards restore whether have layering or apparent Traits change to room temperature observation sample for 24 hours.
Acid-base value test method:Using dilution method, it is 10% that sample is diluted to mass percent with deionized water, uses pH Meter is tested.
It centrifuges:It is fitted into the centrifuge tube of 5mL by product, 2000r/min centrifugation 30min, it is existing that observation whether there is layering As.
The organoleptic indicator of cleansing cream made from the embodiment of the present invention 1 and physical and chemical index test result are shown in Table 1.
Table 1
The organoleptic indicator of embodiment 2~5 and physical and chemical index test result and embodiment 1 are without significant difference.
The sense organ and physical and chemical index of the face cleaning cream of the present invention meet China's facial cleanser, cleansing cream professional standard GB/T The requirement of 29680-2013, product are stablized, and pH=5~6 in faintly acid, approach with skin ph value, do not stimulate mildly.
2nd, evaluation on probation is carried out to face cleaning cream the effect of property of the present invention
2.1 both effectiveness experiment I
Appraisal procedure:30 heavy make-up volunteers are selected, wherein, Oily, neutral skin and each 10 of dry skin, examination User carries out facial cleansing using the product of Examples 1 to 5 and comparative example 1~5 respectively using identical method, and each sample is each After 1 week on probation, questionnaire survey is carried out, evaluation index includes product cleaning force, water humidity, antiallergy power, goes peculiar smell effect, extends Fragrance time, final appraisal results use arithmetic average Data-Statistics, and statistical test the results are shown in Table 2, and test result is made using 5 points, From 5 to 1 points, it is fine, good, general, poor, very poor to be followed successively by.
Table 2
Test result shows:The present invention is arranged in pairs or groups by the science to selected amino acid type surfactant, cleans dynamics It is better than common soap base type face cleaning cream, hence it is evident that better than common amino acid type face cleaning cream.
Grease influences significantly the water humidity of face cleaning cream, and moisturizing star's ingredient Sodium Hyaluronate can also influence water humidity, this The water humidity of the face cleaning cream of invention is far superior to common face cleaning cream.
Decontamination core component amino acid type surfactant and green surfactant lauryl glucose selected by the present invention Glycosides, have the characteristics that it is nontoxic, harmless, non-stimulated to skin, with reference to pure natural components plant desensitizer, plant antiseptic agent, mildly It does not stimulate, can releive skin discomfort, improve sensitive skin, reduce allergy rate.
Selected fat type and content can significantly affect the using effect of essence in the present invention, and of the invention goes peculiar smell to imitate Fruit, extension fragrance time are superior to comparative example.
2.2 both effectiveness experiments II
Appraisal procedure:30 small pox skin volunteers are selected, wherein, Oily, neutral skin and dry skin each 10 Name, trier carry out facial cleansing using the product of Examples 1 to 5 and comparative example 1~5 respectively using identical method, each After each 2 weeks on probation of sample, questionnaire survey is carried out, evaluation index is anti-acne effect, and final appraisal results use arithmetic average primary system Meter, statistical test the results are shown in Table 3.Wherein, statistical test result using 5 points system, from 5 to 1 points, be followed successively by it is fine, good, general, It is poor, very poor.Anti-acne effect experimental result is shown in Table 3.
Table 3
As shown in Table 3, anti-acne ingredient is especially added in face cleaning cream of the invention, anti-acne effect is apparent.
It can be seen that amino acid type surfactant is multiple based on myristoyl glutamate sodium in the face cleaning cream of the present invention With sodium cocoyl glutamate and sodium lauroyl glutamate, in the common work of other surfaces activating agent, moisturizer, thickener and grease Under, make to play synergistic function between each raw material, making face cleaning cream obtained, most of tester thinks it after on probation Strong cleaning force, can wash unload one, skin sense water profit it is not dry and astringent, not tight, do not stimulate mildly, can improve sensitive skin, reduction allergy Rate can effectively cover peculiar smell, and extend and cover the peculiar smell time.
Although above having used general explanation and specific embodiment, the present invention is described in detail, at this On the basis of invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Therefore, These modifications or improvements without departing from theon the basis of the spirit of the present invention belong to the scope of protection of present invention.

Claims (8)

1. a kind of multi-functional amino acid cleansing cream, which is characterized in that by weight percentage, the face cleaning cream includes the following raw material: Glycerine 20-25%, amino acid type surfactant 7.5-22.5%, 1,3- propylene glycol 5-15%, xanthans 0.1-0.3%, EDETATE SODIUM 0.05-0.1%, lauryl glucoside 1-2%, anti-acne ingredient 0.01-0.02%, grease 1-6%, Sodium Hyaluronate 0.01-0.05%, Sodium Polyacrylate 0.005-0.01%, plant desensitizer 2-3%, plant antiseptic agent 0.1-0.3%, essence 0.1-0.2%, surplus are deionized water, wherein, the amino acid type surfactant includes myristoyl glutamate sodium, cocounut oil Acyl sodium glutamate and sodium lauroyl glutamate.
2. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that by weight percentage, the face cleaning Cream includes the following raw material:Glycerine 22-25%, amino acid type surfactant 14-20.5%, 1,3- propylene glycol 10-15%, xanthan Glue 0.1-0.3%, EDETATE SODIUM 0.05-0.1%, lauryl glucoside 1-2%, anti-acne ingredient 0.01-0.02%, grease 1- 4%th, Sodium Hyaluronate 0.01-0.03%, Sodium Polyacrylate 0.005-0.008%, plant desensitizer 2-3%, plant antiseptic agent 0.1-0.3%, essence 0.1-0.2%, surplus are deionized water.
3. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that by weight percentage, the amino Acid type surfactant includes myristoyl glutamate sodium 5-15%, sodium cocoyl glutamate 1.5-2.5%, lauroyl glutamate Sodium 1-3%.
4. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that the grease is selected from Queensland nut seed Oil, jojoba oil, olive oil, palm oil, coconut oil, caprylic/capric triglyceride, ethylhexyl palmitate, myristic acid are different Propyl ester, isopropyl palmitate, isononyl isononanoate, C12-15 alcohol benzoic ethers, dimethyl silicone polymer, five poly dimethyl silicon of ring It is one or more in oxygen alkane, cyclohexasiloxane.
5. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that the anti-acne ingredient is selected from tea tree Oil, accutane, azelaic acid, salicylic acid, skin it is proud it is peaceful in it is one or more.
6. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that the plant desensitizer is selected from accumulated snow Careless extract, licorice root extract, giant knotweed root extract, radix scutellariae root extract, the sweet root extract of light fruit, german chamomile flower extract, It is one or more in rough gentian root extract, peony root extractive, Sage extract.
7. multi-functional amino acid cleansing cream according to claim 1, which is characterized in that the plant antiseptic agent is selected from tree peony Bark extract, grapefruit seed extract, Flos Lonicerae extractive solution, vine of multiflower knotweed extracting solution, Chinese prickly ash berry extract, Folium Artemisiae Argyi extract, shaddock It is one or more in berry extract.
8. a kind of preparation method of multi-functional amino acid cleansing cream described in claim 1, which is characterized in that including walking as follows Suddenly:
(1) each raw material for standby is weighed by weight percentage;
(2) emulsification is added in after 1,3- propylene glycol, xanthans, anti-acne ingredient, Sodium Hyaluronate, Sodium Polyacrylate being uniformly dispersed Pot, then sequentially adds glycerine, EDETATE SODIUM and deionized water, and under stirring condition, warming-in-water is to keeping the temperature 15- after 80-85 DEG C 20min, then it is cooled to 60 DEG C;
(3) amino acid type surfactant after mixing, under the conditions of mixing slowly, is slowly added to above-mentioned system, at 60 DEG C At a temperature of, 30-40min is at the uniform velocity stirred, after observation material body is uniform, is cooled to 50 DEG C;
(4) lauryl glucoside, grease, essence are added in into above-mentioned system after mixing, at a temperature of 50 DEG C, at the uniform velocity stirred 10-15min after observation material body is uniform, is cooled to 40 DEG C;
(5) plant desensitizer, plant antiseptic agent are sequentially added, stirs 10-15min, after observation material body is uniform, it is qualified to examine Discharging.
CN201810036192.XA 2018-01-15 2018-01-15 A kind of multi-functional amino acid cleansing cream and preparation method thereof Pending CN108125859A (en)

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CN108685760A (en) * 2018-08-01 2018-10-23 湘南学院 A kind of composition for soap base product
CN109234085A (en) * 2018-08-16 2019-01-18 惠州兆婷化妆品有限公司 A kind of floating soap and preparation method thereof
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