CN109966166A - Healthy and safe effective amino acid cleansing product of one kind and preparation method thereof - Google Patents

Healthy and safe effective amino acid cleansing product of one kind and preparation method thereof Download PDF

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Publication number
CN109966166A
CN109966166A CN201910272497.5A CN201910272497A CN109966166A CN 109966166 A CN109966166 A CN 109966166A CN 201910272497 A CN201910272497 A CN 201910272497A CN 109966166 A CN109966166 A CN 109966166A
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amino acid
cleansing product
acid cleansing
emulsion pot
healthy
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CN201910272497.5A
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Chinese (zh)
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CN109966166B (en
Inventor
张娇
韩志东
吴柳杏
刘露
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Quanhou (shenzhen) Investment Development Co Ltd
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Quanhou (shenzhen) Investment Development Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to cosmetic fields, more particularly to a kind of healthy and safe effective amino acid cleansing product and preparation method thereof.It include surfactant 3%-45% in amino acid cleansing products material ingredient provided by the invention, moisturizer 1%-15%, 3-O- ethylascorbyl ether 0.05%-3%, MG-60 0.1%-5%, PEG-60 rilanit special 0.02%-1%, pH blender 0.05%-2%, chelating agent 0.01%-0.3%, preservative 0.02%-1%, essence 0.02%-1%, surplus are deionized water.Experiment shows that present invention offer amino acid cleansing product cleaning effect is strong, and moistening effect is good after face cleaning, and antioxidant effect is obvious, being capable of bright color.

Description

Healthy and safe effective amino acid cleansing product of one kind and preparation method thereof
Technical field
The present invention relates to cosmetic fields, more particularly to a kind of healthy and safe effective amino acid cleansing product and its preparation Method.
Background technique
The first element for wanting to possess healthy skin is exactly the sebum film for needing to possess health.The sebum film of health is in weak acid Property, pH maintain 4.5~6.5 weakly acidic states, and sebum film can inhibit and kill the bacterium of skin surface, to keep skin Health.The purpose of face cleaning is the sebum and dust for cleaning skin surface and being oxidized, unabsorbed skin care products and color make-up etc.. And incorrect face cleaning mode and face cleaning product can hurt this layer of healthy sebum film, keep sebum film more and more thinner, skin Immunity degradation and water lock function weaken, and form various skin problems: drying, pigment, sensitivity or even long acne etc..So healthy The skin first step is exactly correct face cleaning and selection face cleaning product.
Face's cleaning products are many kinds of currently on the market, and portioned product is using soap base as main detergent, such face cleaning What product was focused on is high-efficiency cleaning, pore cleanser, deoils, and in order to improve decontamination, oil removing ability, joined the extremely strong surface of alkalinity The ingredients such as activating agent, foaming agent, soap base are felt to tighten after use, have ignored stimulation of the product itself to skin.And our skin Skin be it is weakly acidic, long-time service will be injured;More seriously, the sebum film of skin can be also destroyed, once it loses Sebum film, skin are highly susceptible to external injury, and particularly with sensitive skin, this injury is even more to be difficult to imagine.
In the market other than the face cleaning of soap base type, there are also part emulsifying products, such product property is mild, but decontamination Power effect is poor, is difficult to make foam abundant, feels greasy after washing.The amino acids face cleaning product occurred recently is to a certain degree On mitigated above-mentioned contradiction, such as amino acid cleansing mousse, while high-efficiency cleaning, mild, low stimulation is suitable for this kind of product Various types of skins.But based on this kind of product mainly cleans, effect is single, such as patent CN106236613B is disclosed One kind moistening clear bubble mildy wash only, which includes two section mustard seed oil of deep-sea, emulsifier, foaming agent, two phase stratification Regulator, pH adjusting agent, chelating agent, preservative, oil mutually and deionized water, novel appearance, with preceding presentation upper layer and lower layer, after shake It can produce a large amount of foams, there is obvious cleaning effect.But the mildy wash is only capable of providing cleaning effect, has no other function.This Invention is intended to provide one kind, and to be finished rear skin wet not tight, it is healthy and safe effectively, and can be anti-oxidant, the amino of bright color Sour face cleaning product.
Summary of the invention
The technical problem to be solved in the present invention is that provide it is a kind of it is healthy and safe effectively, comprising amino acid surfactant and It is added to the face cleaning product of moisturizing antioxidant content.Face cleaning product provided by the invention can mildly clean various dirts, and clean Moistening effect is good behind face, and bright color effect is obvious.
The present invention provides a kind of healthy and safe effective amino acid cleansing product, its raw material by weight percentage is formed Are as follows:
Surfactant 3%-45%
Moisturizer 1%-15%
3-O- ethylascorbyl ether 0.05%-3%
MG-60 0.1%-5%
PEG-60 rilanit special 0.02%-1%
PH blender 0.05%-2%
Chelating agent 0.01%-0.3%
Preservative 0.02%-1%
Essence 0.02%-1%
Deionized water Surplus
Wherein, MG-60 is the mixture of glycosyl trehalose and hydrogenated starch hydrolysate, has protection cell, inhibits skin It is coarse and other effects, while can also act synergistically with surfactant, enhance sophistication, generous sense and the bullet of cleansing mousse foam Property.
Wherein, 3-O- ethylascorbyl ether is vitamin C derivatives, not only highly stable in chemical property, but also It is the amphiprotic substance of hydrophilic and oleophilic, it is easy to be entered skin corium by cuticula, act on the Cu of tyrosinase2+Inhibit its work Property, the formation of melanin is blocked, has the function of very effective whitening and nti-freckle.
In some embodiments of the present invention, the surfactant is one or more combinations in following substance: coconut palm Oleoyl both sexes base diethyl acid disodium, Plantacare 818, lauryl hydroxyl sulfo betaine, cocounut oil acyl disodium glutamate, cocounut oil acyl Sodium glutamate and sodium methyl cocoyl taurate;The moisturizer is one or more combinations in following substance: glycerol, sorb Sugar alcohol, dipotassium glycyrrhizinate and panthenol.
In some embodiments of the present invention, the amino acid cleansing product is amino acid cleansing mousse.
In some embodiments of the present invention, the pH blender is citric acid.
In some embodiments of the present invention, the chelating agent is EDETATE SODIUM.
In some embodiments of the present invention, the amino acid cleansing product its raw material by weight percentage forms are as follows:
Invention also provides a kind of method for preparing amino acid cleansing product described above, comprising the following steps:
1) emulsion pot is cleaned up, is sterilized;
2) deionized water, glycerol, EDETATE SODIUM, surfactant and D-sorbite are sequentially added into water phase pot, are heated to 70-80 DEG C, stirring and dissolving, confirmation is completely dissolved;
3) water phase pot is cooling, stirring is cooled to 40-50 DEG C;
4) citric acid is dissolved in water in advance, main cooker is added, to being completely dissolved, defoaming is extremely clarified for stirring;
5) main cooker is cooled to 35 DEG C, sequentially add dipotassium glycyrrhizinate, panthenol, MG-60,3-O- ethylascorbyl ether, Preservative, PEG-60 rilanit special and essence, stir to clarify transparent;
6) it is qualified to examine, filtering and discharging;
7) inspection of semifinished product, filling.
In some embodiments of the present invention, in the above-mentioned method and step for preparing amino acid, the surfactant is One or more combinations in following substance: cocounut oil acyl both sexes base diethyl acid disodium, Plantacare 818, lauryl weight ratio beet Alkali, sodium methyl cocoyl taurate amino acid, cocounut oil acyl disodium glutamate, sodium cocoyl glutamate amino acid.
Amino acid cleansing product produced by the present invention has the advantages that
(1) face cleaning product of the invention is weakly acidic, very approximate with the pH value of skin itself, and long-time service can promote Skin acid balance, possesses the sebum film of health.
(2) face cleaning product of the invention includes amino acid surfactant, mildly can effectively remove various dirts, and It is not tight to wash rear moisturizing, it is coarse effectively to alleviate pore, the symptoms such as blackhead, acne.
(3) face cleaning product of the invention is by cocounut oil acyl both sexes base diethyl acid disodium, Plantacare 818, methyl cocoyl ox Sodium sulfonate, lauryl hydroxyl sulfo betaine and amino acid surfactant cocounut oil acyl disodium glutamate, sodium cocoyl glutamate Rational proportion, the cleansing mousse foam made is fine and smooth, and plentiful, cleaning capacity is strong;Collocation glycerol, panthenol, D-sorbite, Radix Glycyrrhizae The skin conditioning agents such as sour dipotassium do not stimulate that (common soap base face cleaning produces so as to be finished rear skin wet not tight for the cleansing mousse Product have dry skin after use, tight, part population meeting allergy).
(4) face cleaning product of the invention is added to MG-60, can not only improve the moisture retention of product, while energy and surface Activating agent synergistic effect, enhances the sophistication, generous sense and elasticity of the cleansing mousse foam.Also add in face cleaning product of the invention Add vitamin C derivatives 3-O- ethylascorbyl ether, it is not only highly stable in chemical property, but also be hydrophilic and oleophilic Amphiprotic substance, it is easy to entered skin corium by cuticula, act on the Cu of tyrosinase2+Inhibit its activity, blocks black The formation of element, the effect of playing anti-oxidant and bright color.
Detailed description of the invention
Antioxidant effect figure of Fig. 1 MG-60 in ascorbic acid solution.
Specific embodiment
With reference to embodiments for further describing the present invention, but these embodiments not limit model of the invention It encloses.Test method without specific conditions in the embodiment of the present invention, usually according to normal condition, or according to raw material or commodity system Make condition proposed by manufacturer.MG-60 is purchased from Amada Co., Ltd.'s woods original, and the reagent in specific source is not specified in remaining, is market The conventional reagent of purchase.
Embodiment 1
A kind of healthy and safe effective amino acid cleansing mousse, by weight percentage its raw material form are as follows:
The step of preparing the amino acid cleansing mousse is as follows:
1) emulsion pot is cleaned up, is sterilized;
2) each component is weighed by weight, by deionized water, glycerol, EDETATE SODIUM, cocounut oil acyl both sexes base diethyl acid disodium, the last of the ten Heavenly stems Base glucoside, lauryl hydroxyl sulfo betaine, sodium methyl cocoyl taurate amino acid, cocounut oil acyl disodium glutamate, coconut palm Oleoyl sodium glutamate amino acid and D-sorbite sequentially add emulsion pot, are heated to 75 DEG C, stirring and dissolving, confirmation is completely dissolved;
3) emulsion pot is cooling, stirring is cooled to 45 DEG C;
4) citric acid is dissolved in water in advance, emulsion pot is added, to being completely dissolved, defoaming is extremely clarified for stirring;
5) emulsion pot is cooled to 35 DEG C, sequentially adds dipotassium glycyrrhizinate, panthenol, MG-60,3-O- ethylascorbyl Ether, preservative, PEG-60 rilanit special and essence, stir to clarify transparent;
6) it is qualified to examine, filtering and discharging;
7) inspection of semifinished product, filling.
Embodiment 2
A kind of healthy and safe effective amino acid cleansing mousse, by weight percentage its raw material form are as follows:
The step of preparing the amino acid cleansing mousse is as follows:
1) emulsion pot is cleaned up, is sterilized;
2) each component is weighed by weight, by deionized water, glycerol, EDETATE SODIUM, cocounut oil acyl both sexes base diethyl acid disodium, the last of the ten Heavenly stems Base glucoside, lauryl hydroxyl sulfo betaine, sodium methyl cocoyl taurate amino acid, cocounut oil acyl disodium glutamate, coconut palm Oleoyl sodium glutamate amino acid and D-sorbite sequentially add emulsion pot, are heated to 75 DEG C, stirring and dissolving, confirmation is completely dissolved;
3) emulsion pot is cooling, stirring is cooled to 45 DEG C;
4) citric acid is dissolved in water in advance, emulsion pot is added, to being completely dissolved, defoaming is extremely clarified for stirring;
5) emulsion pot is cooled to 35 DEG C, sequentially adds dipotassium glycyrrhizinate, panthenol, MG-60,3-O- ethylascorbyl Ether, preservative, PEG-60 rilanit special and essence, stir to clarify transparent;
6) it is qualified to examine, filtering and discharging;
7) inspection of semifinished product, filling.
Embodiment 3
A kind of healthy and safe effective amino acid cleansing mousse, by weight percentage its raw material form are as follows:
The step of preparing the amino acid cleansing mousse is as follows:
1) emulsion pot is cleaned up, is sterilized;
2) each component is weighed by weight, by deionized water, glycerol, EDETATE SODIUM, cocounut oil acyl both sexes base diethyl acid disodium, the last of the ten Heavenly stems Base glucoside, lauryl hydroxyl sulfo betaine, sodium methyl cocoyl taurate amino acid, cocounut oil acyl disodium glutamate, coconut palm Oleoyl sodium glutamate amino acid and D-sorbite sequentially add emulsion pot, are heated to 75 DEG C, stirring and dissolving, confirmation is completely dissolved;
3) emulsion pot is cooling, stirring is cooled to 45 DEG C;
4) citric acid is dissolved in water in advance, emulsion pot is added, to being completely dissolved, defoaming is extremely clarified for stirring;
5) emulsion pot is cooled to 35 DEG C, sequentially adds dipotassium glycyrrhizinate, panthenol, MG-60,3-O- ethylascorbyl Ether, preservative, PEG-60 rilanit special and essence, stir to clarify transparent;
6) it is qualified to examine, filtering and discharging;
7) inspection of semifinished product, filling.
Embodiment 4
1, use feeling evaluation experimental
Test method: randomly selecting healthy skin subject 50, and men and women is fifty-fifty, is randomly divided into 5 groups, every group of 10 people.Choosing Subject's inboard arm 5cm × 6cm healthy skin is determined, in uniform smearing lipstick above.The skin wet of lipstick will be coated with water, Product made from Example 1-3, and soft bubble cleansing mousse and the Cetaphil mildy wash of being full of of Nivea cloud bought from the market As a control group 1 and 2, a pump is squeezed out respectively in above-mentioned humidification zones, is massaged and is rinsed with water after 30s clean, records foamy appearance And use feeling, as a result such as table 1.
Table 1
2, skin is improved and is tested
Test method: volunteer 50 with skin problem are screened, men and women is fifty-fifty, is randomly divided into 5 groups, every group of 10 people. Volunteer's screening criteria: pore is coarse, and face has blackhead or acne, easy long acne, easy allergic skin, inflammatory papules, useless fellow etc. There is the patient of scytitis.The volunteer of 1-3 group is once in the morning and once at night washed using product made from embodiment 1-3 respectively Face, the 4th group and the 5th group of volunteer respectively using the product Nivea cloud of control group 1 and 2 it is soft be full of bubble cleansing mousse and Cetaphil it is clean Face cream once in the morning and once at night washes one's face, and continuous observation 2 months, statistical result was shown in Table 2.
Significantly effectively refer to that scytitis or acne are obviously disappeared.
Effectively refer to that scytitis or acne are disappeared.
Refer to that scytitis or acne are serious without any disappearance sign or more in vain.
Improve ratio=(efficiently individual quantity+significant effective)/tested number × 100%.
Table 2
Embodiment 5
The anti-oxidant experiment of MG-60
Test method: taking 1% ascorbic acid solution of 3 groups of equivalent, wherein group 1 is control group, group 2 contains 10% MG-60, group 3 contain glycerol.It is stored 12 under the conditions of being protected from light for 50 DEG C respectively, each group solution decolourization situation is compared, is seen Fig. 1.As seen from Figure 1, added 2 antioxidant effect of group of MG-60 best.

Claims (5)

1. a kind of healthy and safe effective amino acid cleansing product, it is characterised in that its raw material forms by weight percentage are as follows:
Surfactant 3%-45% Moisturizer 1%-15% 3-O- ethylascorbyl ether 0.05%-3% MG-60 0.1%-5% PEG-60 rilanit special 0.02%-1% PH blender 0.05%-2% Chelating agent 0.01%-0.3% Preservative 0.02%-1% Essence 0.02%-1% Deionized water Surplus
Wherein the surfactant is one or more combinations in following substance: cocounut oil acyl both sexes base diethyl acid disodium, decyl Glucoside, lauryl hydroxyl sulfo betaine, cocounut oil acyl disodium glutamate, sodium cocoyl glutamate and methyl cocoyl ox sulphur Sour sodium;The moisturizer is one or more combinations in following substance: glycerol, D-sorbite, dipotassium glycyrrhizinate and panthenol.
2. amino acid cleansing product according to claim 1, it is characterised in that the pH blender is citric acid.
3. amino acid cleansing product according to claim 1, it is characterised in that the chelating agent is EDETATE SODIUM.
4. amino acid cleansing product according to claim 1, it is characterised in that its raw material forms by weight percentage are as follows:
5. a kind of prepare the method such as amino acid cleansing product of any of claims 1-4, it is characterised in that including Following steps:
1) emulsion pot is cleaned up, is sterilized;
2) deionized water, glycerol, EDETATE SODIUM, surfactant and D-sorbite are sequentially added into emulsion pot, is heated to 70-80 DEG C, stirring and dissolving, confirmation is completely dissolved;
3) emulsion pot is cooling, stirring is cooled to 40-50 DEG C;
4) citric acid is dissolved in water in advance, emulsion pot is added, to being completely dissolved, defoaming is extremely clarified for stirring;
5) emulsion pot is cooled to 35 DEG C, sequentially adds dipotassium glycyrrhizinate, panthenol, MG-60,3-O- ethylascorbyl ether, prevents Rotten agent, PEG-60 rilanit special and essence, stir to clarify transparent;
6) it is qualified to examine, filtering and discharging;
7) inspection of semifinished product, filling.
CN201910272497.5A 2019-04-04 2019-04-04 Healthy, safe and effective amino acid cleansing product and preparation method thereof Active CN109966166B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110623855A (en) * 2019-09-17 2019-12-31 配方化妆品科技(广州)有限公司 Amino acid cleansing mousse and preparation method thereof
CN111529420A (en) * 2020-05-07 2020-08-14 泉后(广州)生物科技研究院有限公司 Mild cleansing mousse suitable for sensitive muscles
CN112587420A (en) * 2020-12-24 2021-04-02 珠海美逸生物科技有限公司 Mild anti-allergy cleansing bubble and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104173261A (en) * 2014-08-28 2014-12-03 皖南医学院 Soothing, anti-allergy and skin-regenerating emulsion and preparation method thereof
CN104958242A (en) * 2015-07-31 2015-10-07 桂林市宏旭生物科技有限公司 Anti-ultraviolet mask liquid and preparation method thereof
CN106236690A (en) * 2016-08-31 2016-12-21 福建省梦娇兰日用化学品有限公司 A kind of amino acid cleansing cream containing various plants composition

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104173261A (en) * 2014-08-28 2014-12-03 皖南医学院 Soothing, anti-allergy and skin-regenerating emulsion and preparation method thereof
CN104958242A (en) * 2015-07-31 2015-10-07 桂林市宏旭生物科技有限公司 Anti-ultraviolet mask liquid and preparation method thereof
CN106236690A (en) * 2016-08-31 2016-12-21 福建省梦娇兰日用化学品有限公司 A kind of amino acid cleansing cream containing various plants composition

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110623855A (en) * 2019-09-17 2019-12-31 配方化妆品科技(广州)有限公司 Amino acid cleansing mousse and preparation method thereof
CN111529420A (en) * 2020-05-07 2020-08-14 泉后(广州)生物科技研究院有限公司 Mild cleansing mousse suitable for sensitive muscles
CN112587420A (en) * 2020-12-24 2021-04-02 珠海美逸生物科技有限公司 Mild anti-allergy cleansing bubble and preparation method thereof

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