CN110623855A - Amino acid cleansing mousse and preparation method thereof - Google Patents
Amino acid cleansing mousse and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses an amino acid face-cleaning mousse and a preparation method thereof. According to the invention, the zwitterionic surfactant, the nonionic surfactant, the amino acid type surfactant and the anionic surfactant are reasonably proportioned to prepare the cleansing mousse foam which is fine, smooth and full and has strong cleaning capability; the facial cleansing mousse is matched with skin conditioners such as glycerin, panthenol and sorbitol, so that the skin is not tight and does not irritate the skin after the facial cleansing mousse is used; the glycosyl trehalose/hydrogenated starch hydrolysate can improve the moisture retention of the product, and can simultaneously act synergistically with various surfactants to enhance the fineness, fullness and elasticity of the cleansing mousse foam; the vitamin C derivative 3-O-ethyl ascorbic acid has the functions of resisting oxidation and brightening skin, is easy to absorb and can be kept stable in the product for a long time, so that the antioxidant activity of the product is ensured.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to an amino acid face cleaning mousse and a preparation method thereof.
Background
In daily life, various grease and dirt can be left and accumulated on the facial skin, if the facial skin is not cleaned in time, the left glyceride and dirt are easy to be oxidized, and simultaneously, microorganisms are easy to breed to damage the skin health. Facial skin cleansing is the first step in skin care. Most consumers can select the glycerin soap base type face cleaning product with strong cleaning power and rich foam, most face cleaning products in the market belong to the type face cleaning product, but the type face cleaning product has strong glycerin degreasing power, the skin is too dry and tight after being cleaned, and meanwhile, the pH value of the type face cleaning product is generally higher and the irritation is larger.
In recent years, amino acid glycerin cleansing products which take mild amino acid surfactants as main cleansing components appear on the market, and the cleansing products are characterized by high-efficiency cleansing, mild skin-friendly property, low irritation and capability of being used by children and sensitive skin. However, the viscosity of the amino acid surfactant in the amino acid cleansing product changes greatly along with the temperature, and after the amino acid cleansing product is stored for a period of time, the product is difficult to keep the original state, even the defects of coarseness, water discharge and the like can occur, the stability is poor, and the foam is not rich enough.
Disclosure of Invention
The invention aims to provide an amino acid face-cleaning mousse and a preparation method thereof, so as to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
in a first aspect, the amino acid cleansing mousse provided by the invention comprises the following raw materials in parts by weight: 0.5 to 10% of glycerin, 0.01 to 0.3% of chelating agent, 2 to 25% of zwitterionic surfactant, 0.1 to 1% of nonionic surfactant, 0.5 to 15% of amino acid type surfactant, 0.1 to 8.0% of anionic surfactant, 0.5 to 5.0% of sorbitol, 0.05 to 2.0% of pH regulator, 0.05 to 3.0% of dipotassium glycyrrhizinate, 0.05 to 3.0% of D-panthenol, 0.1 to 5.0% of glycosyl trehalose/hydrogenated starch hydrolysate, 0.1 to 3.0% of 3-o-ethyl ascorbic acid, 0.02 to 1.0% of preservative, 0.02 to 1.0% of PEG-60 hydrogenated castor oil, 0.02 to 1.0% of essence and the balance of water.
Preferably, the zwitterionic surfactant is selected from any one or two of disodium cocoyl amphodiacetate and lauryl hydroxy sulfobetaine.
Preferably, the nonionic surfactant is decyl glucoside.
Preferably, the amino acid type surfactant is selected from one or more of sodium methylcocoyltaurate, sodium cocoylglutamate/disodium cocoylglutamate.
Preferably, the chelating agent is disodium edetate.
Preferably, the pH regulator is citric acid.
Preferably, the amino acid cleansing mousse comprises the following raw materials in parts by weight: 2.0 to 5.0% of glycerin, 0.1 to 0.3% of chelating agent, 7.3 to 14.3% of zwitterionic surfactant, 0.1 to 0.5% of nonionic surfactant, 9.0 to 10% of amino acid type surfactant, 2.0 to 6.0% of anionic surfactant, 1.0 to 3.0% of sorbitol, 0.5 to 1.0% of pH regulator, 0.1 to 0.3% of dipotassium glycyrrhizinate, 0.5 to 1.0% of D-panthenol, 1.0 to 2.0% of glycosyl trehalose/hydrogenated starch hydrolysate, 0.1 to 0.5% of 3-o-ethyl ascorbic acid, 0.1 to 0.5% of preservative, 0.5 to 1.0% of PEG-60 hydrogenated castor oil, 0.02 to 0.05% of essence, and the balance of water.
In a second aspect, the present invention provides a method for preparing an amino acid facial mousse according to the first aspect, comprising the following steps:
(1) adding water, glycerol, a chelating agent, a zwitterionic surfactant, a nonionic surfactant, an amino acid surfactant, an anionic surfactant and sorbitol into a stirring pot, heating to 70-80 ℃, and stirring until the mixture is completely dissolved;
(2) stirring to reduce the temperature in the stirring pot to 40-50 ℃, adding citric acid into the stirring pot, stirring until the citric acid is completely dissolved, and defoaming until the citric acid is clear;
(3) and continuously stirring to reduce the temperature of the stirring pot to 35 ℃, adding the glycyrrhizic acid dimethyl, the D-panthenol, the glycosyl trehalose/hydrogenated starch hydrolysate, the 3-o-ethyl ascorbic acid, the preservative, the PEG-60 hydrogenated castor oil and the essence, stirring until the mixture is clear and transparent, and filtering and discharging to obtain the amino acid cleansing mousse.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, the zwitterionic surfactant, the nonionic surfactant, the amino acid type surfactant and the anionic surfactant are reasonably proportioned to prepare the cleansing mousse foam which is fine, smooth and full and has strong cleaning capability; the skin conditioners such as glycerin, panthenol, sorbitol, dipotassium glycyrrhizinate and the like are matched, so that the face cleaning mousse is not tight and does not irritate the skin after being used; the glycosyl trehalose/hydrogenated starch hydrolysate can improve the moisture retention of the product, and can simultaneously act synergistically with various surfactants to enhance the fineness, fullness and elasticity of the cleansing mousse foam; the vitamin C derivative 3-o-ethyl ascorbic acid has the functions of resisting oxidation and brightening skin, and the 3-o-ethyl ascorbic acid is a stable vitamin C derivative, is easy to absorb and can be kept stable in the product for a long time, so that the antioxidant activity of the product is ensured.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
The glycosyl trehalose/hydrogenated starch hydrolysate used in the present invention was glycosyl trehalose/hydrogenated starch hydrolysate MG-60 available from Kabushiki Kaisha.
It should be noted that sodium cocoyl glutamate/disodium cocoyl glutamate used in the present invention is an amisft series CS-22 product available from japanese gourmet.
Example 1
The preparation method of the amino acid cleansing mousse provided by the embodiment comprises the following steps:
(1) weighing the raw materials according to the raw material ratio of example 1 in the table 1;
(2) sequentially adding water, glycerol, disodium ethylene diamine tetraacetate, disodium cocoyl amphodiacetate, decyl glucoside, lauryl hydroxy sulfobetaine, sodium methyl cocoyl taurate, sodium cocoyl glutamate/disodium cocoyl glutamate and sorbitol into a stirring pot, heating to 70-80 ℃, and stirring until the materials are completely dissolved;
(3) stirring to reduce the temperature in the stirring pot to 40-50 ℃, adding citric acid into the stirring pot, stirring until the citric acid is completely dissolved, and defoaming until the citric acid is clear;
(4) and (3) continuously stirring to reduce the temperature of the stirring pot to 35 ℃, sequentially adding the dimethyl glycyrrhizinate, the D-panthenol, the glycosyl trehalose/hydrogenated starch hydrolysate, the 3-o-ethyl ascorbic acid, the preservative, the PEG-60 hydrogenated castor oil and the essence into the stirring pot, stirring until the mixture is clear and transparent, and filtering and discharging to obtain the amino acid face-cleaning mousse.
Examples 2 to 6
In order to further illustrate the beneficial effects of the invention, the amino acid cleansing mousse is prepared by weighing the raw materials according to the mixture ratio shown in the table 1 and then according to the steps (2) to (4) of the example 1.
TABLE 1 statistical tables of the raw materials used in the examples
Comparative example 1
To further illustrate the beneficial effects of the present invention, this comparative example prepared a cleansing product using a similar preparation method to that of example 1, and differed from example 1 only in that: the present comparative example did not use a glycosyl trehalose/hydrogenated starch hydrolysate.
Comparative example 2
To further illustrate the beneficial effects of the present invention, this comparative example prepared a cleansing product using a similar preparation method to that of example 1, and differed from example 1 only in that: the comparative example did not employ sodium cocoyl glutamate/disodium cocoyl glutamate.
Efficacy test 1:
to further illustrate the beneficial effects of the present invention, the appearance, foam and stability of the products obtained in the above examples and comparative examples were tested, wherein the stability test is as follows: the products obtained in the above examples and comparative examples were stored at high temperature (45 ℃) and low temperature (-15 ℃) for 24 hours, and then returned to room temperature, and the morphology of the face-cleaning mousse was observed.
TABLE 2
Efficacy test 2:
the evaluation method comprises the following steps: selecting 80 female volunteers, wherein 40 female volunteers respectively comprise oily skin, neutral skin and dry skin, cleaning the face of the female volunteers by using the products of examples 1-6 and comparative examples 1-2 respectively by the same method, after trial for 7 days, developing questionnaires on the female volunteers, wherein evaluation indexes comprise product cleaning power, water wettability, anti-allergic power and fragrance prolonging time, the final evaluation result adopts arithmetic mean value statistics, the statistical test result is shown in table 3, the test result adopts 5 grades, and the test result is from 5 to 1 grades, and is good, common, poor and very poor in sequence.
TABLE 3 test results
| Product(s) | Cleaning power | Degree of water wettability | Antiallergic effect | Prolonged fragrance |
| Example 1 | 4.3 | 4.5 | 4.5 | 4.3 |
| Example 2 | 4.5 | 4.6 | 4.6 | 4.5 |
| Example 3 | 4.6 | 4.7 | 4.5 | 4.6 |
| Example 4 | 4.2 | 4.3 | 4.4 | 4.3 |
| Example 5 | 3.8 | 3.2 | 3.6 | 3.9 |
| Example 6 | 3.4 | 3.8 | 3.3 | 3.8 |
| Comparative example 1 | 3.3 | 3.3 | 3.4 | 3.1 |
| Comparative example 2 | 3.1 | 3.0 | 3.0 | 3.0 |
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (8)
1. The amino acid cleansing mousse is characterized by comprising the following raw materials in parts by weight: 0.5 to 10% of glycerin, 0.01 to 0.3% of chelating agent, 2 to 25% of zwitterionic surfactant, 0.1 to 1% of nonionic surfactant, 0.5 to 15% of amino acid type surfactant, 0.1 to 8.0% of anionic surfactant, 0.5 to 5.0% of sorbitol, 0.05 to 2.0% of pH regulator, 0.05 to 3.0% of dipotassium glycyrrhizinate, 0.05 to 3.0% of D-panthenol, 0.1 to 5.0% of glycosyl trehalose/hydrogenated starch hydrolysate, 0.1 to 3.0% of 3-o-ethyl ascorbic acid, 0.02 to 1.0% of preservative, 0.02 to 1.0% of PEG-60 hydrogenated castor oil, 0.02 to 1.0% of essence and the balance of water.
2. The amino acid facial mousse according to claim 1, wherein the zwitterionic surfactant is selected from any one or both of disodium cocoamphodiacetate and lauryl hydroxysultaine.
3. The amino acid facial mousse according to claim 1 wherein the non-ionic surfactant is decyl glucoside.
4. The amino acid facial mousse according to claim 1, wherein the amino acid based surfactant is selected from one or both of sodium methylcocoyltaurate, disodium cocoylglutamate/sodium cocoylglutamate.
5. The amino acid facial mousse according to claim 1, wherein the chelating agent is disodium ethylenediaminetetraacetic acid.
6. The amino acid facial mousse according to claim 1, wherein the pH adjusting agent is citric acid.
7. The amino acid cleansing mousse according to claim 1, comprising the following raw materials in parts by weight: 2.0 to 5.0% of glycerin, 0.1 to 0.3% of chelating agent, 7.3 to 14.3% of zwitterionic surfactant, 0.1 to 0.5% of nonionic surfactant, 9 to 10% of amino acid type surfactant, 2.0 to 6.0% of anionic surfactant, 1.0 to 3.0% of sorbitol, 0.5 to 1.0% of pH regulator, 0.1 to 0.3% of dipotassium glycyrrhizinate, 0.5 to 1.0% of D-panthenol, 1.0 to 2.0% of glycosyl trehalose/hydrogenated starch hydrolysate, 0.1 to 0.5% of 3-o-ethyl ascorbic acid, 0.1 to 0.5% of preservative, 0.5 to 1.0% of PEG-60 hydrogenated castor oil, 0.02 to 0.05% of essence, and the balance of water.
8. A method for preparing the amino acid facial mousse according to any one of claims 1-7, comprising the steps of:
(1) adding water, glycerol, a chelating agent, a zwitterionic surfactant, a nonionic surfactant, an amino acid surfactant, an anionic surfactant and sorbitol into a stirring pot, heating to 70-80 ℃, and stirring until the mixture is completely dissolved;
(2) stirring to reduce the temperature in the stirring pot to 40-50 ℃, adding citric acid into the stirring pot, stirring until the citric acid is completely dissolved, and defoaming until the citric acid is clear;
(3) and continuously stirring to reduce the temperature of the stirring pot to 35 ℃, adding the glycyrrhizic acid dimethyl, the D-panthenol, the glycosyl trehalose/hydrogenated starch hydrolysate, the 3-o-ethyl ascorbic acid, the preservative, the PEG-60 hydrogenated castor oil and the essence, stirring until the mixture is clear and transparent, and filtering and discharging to obtain the amino acid cleansing mousse.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910875730.9A CN110623855A (en) | 2019-09-17 | 2019-09-17 | Amino acid cleansing mousse and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111529420A (en) * | 2020-05-07 | 2020-08-14 | 泉后(广州)生物科技研究院有限公司 | Mild cleansing mousse suitable for sensitive muscles |
| CN112294674A (en) * | 2020-10-22 | 2021-02-02 | 广州源美药业科技有限公司 | Pure plant deep cleaning amino acid face cleaning mousse |
| CN112545919A (en) * | 2020-12-14 | 2021-03-26 | 广州市拉凯尔干细胞研究所 | Dual hyaluronic acid face-cleaning mousse |
| CN112587420A (en) * | 2020-12-24 | 2021-04-02 | 珠海美逸生物科技有限公司 | Mild anti-allergy cleansing bubble and preparation method thereof |
| CN115721592A (en) * | 2022-12-12 | 2023-03-03 | 深圳市理然化妆品有限公司 | Soapberry face-cleaning mousse and preparation method thereof |
| CN115813788A (en) * | 2022-12-26 | 2023-03-21 | 福建片仔癀化妆品有限公司 | Mild self-corrosion-resistant and foam-dense cleansing bubble liquid and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111529420A (en) * | 2020-05-07 | 2020-08-14 | 泉后(广州)生物科技研究院有限公司 | Mild cleansing mousse suitable for sensitive muscles |
| CN112294674A (en) * | 2020-10-22 | 2021-02-02 | 广州源美药业科技有限公司 | Pure plant deep cleaning amino acid face cleaning mousse |
| CN112545919A (en) * | 2020-12-14 | 2021-03-26 | 广州市拉凯尔干细胞研究所 | Dual hyaluronic acid face-cleaning mousse |
| CN112587420A (en) * | 2020-12-24 | 2021-04-02 | 珠海美逸生物科技有限公司 | Mild anti-allergy cleansing bubble and preparation method thereof |
| CN115721592A (en) * | 2022-12-12 | 2023-03-03 | 深圳市理然化妆品有限公司 | Soapberry face-cleaning mousse and preparation method thereof |
| CN115813788A (en) * | 2022-12-26 | 2023-03-21 | 福建片仔癀化妆品有限公司 | Mild self-corrosion-resistant and foam-dense cleansing bubble liquid and preparation method thereof |
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Application publication date: 20191231 |
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| RJ01 | Rejection of invention patent application after publication |