CN108852945B - Self-foaming amino acid facial cleanser - Google Patents
Self-foaming amino acid facial cleanser Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/69—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing fluorine
- A61K8/70—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing fluorine containing perfluoro groups, e.g. perfluoroethers
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses a self-foaming amino acid facial cleanser, which comprises an amino surfactant and a self-foaming agent, wherein the self-foaming agent comprises perfluorobutyl methyl ether, ethyl perfluorobutyl ether and polydimethylsiloxane; the weight percentage of the perfluorobutyl methyl ether in the facial cleanser is 0.1-15%, and the weight percentage of the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane in the facial cleanser is 0.1-15%. The facial cleanser disclosed by the invention has a self-foaming effect, the self-foaming time is short, the self-foaming amount is large, the foam is very fine and smooth, mild and non-irritant, the facial skin can be deeply cleaned, and the facial cleanser is very interesting.
Description
Technical Field
The invention relates to a face cleanser, in particular to a self-foaming amino acid face cleanser.
Background
With the continuous improvement of living standard of people, people also put forward higher requirements on products used daily, people want to obtain a cleanser which can generate rich and fine foams without being washed all the time, and the tiny bubbles are utilized to go deep into skin textures and pores to thoroughly clean deeply-stored dirt, so that the self-foaming cleanser can be produced.
The self-foaming face cleansing cream is mainly prepared by using a self-foaming agent and a surfactant in a certain proportion, the types of the self-foaming agent and the surfactant are very many, particularly the types of the surfactant, and the self-foaming agent used in the face cleansing cream is mainly ethers. The traditional self-foaming facial cleanser is long in self-foaming time, low in self-foaming foam amount and not fine enough, and most of the traditional self-foaming facial cleansers use surfactants with larger irritation, so that the barrier function of epidermal secretion can be damaged too strongly, the water loss is serious, and cutin is rough and sensitive.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide the self-foaming amino acid facial cleanser.
In order to achieve the purpose, the invention adopts the technical scheme that: a self-foaming amino acid facial cleanser comprising an amino surfactant and a self-foaming agent, the self-foaming agent comprising perfluorobutyl methyl ether, ethyl perfluorobutyl ether and polydimethylsiloxane; the weight percentage of the perfluorobutyl methyl ether in the facial cleanser is 0.1-15%, and the weight percentage of the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane in the facial cleanser is 0.1-15%.
The three self-foaming agents are selected for the facial cleanser, the viscosity of the facial cleanser can be increased through the three self-foaming agents, so that the stability of the formula is effectively improved, more importantly, the self-foaming capacity of the facial cleanser is exerted to the greatest extent, the foaming time is extremely short, rich and fine foams can be generated, and the tiny bubbles are used for penetrating into skin textures and pores to thoroughly clean deeply-stored dirt, so that the facial cleanser can better achieve the effect of cleaning the face, and is mild and non-irritant.
Preferably, the weight ratio of the perfluorobutyl methyl ether to the mixture of ethyl perfluorobutyl ether and polydimethylsiloxane is: perfluorobutyl methyl ether: the mixture of ethyl perfluorobutyl ether and polydimethylsiloxane was 2: 1.
When the mixture of the perfluorobutyl methyl ether, the ethyl perfluorobutyl ether and the polydimethylsiloxane is prepared according to the proportion, the perfluorobutyl methyl ether, the ethyl perfluorobutyl ether and the polydimethylsiloxane can play a complementary role, so that a user can obtain comfortable feeling after washing.
Preferably, the weight ratio of the ethyl perfluorobutyl ether to the polydimethylsiloxane is: ethyl perfluorobutyl ether: polydimethylsiloxane ═ 1: 1. When the ethyl perfluorobutyl ether and the polydimethylsiloxane are mixed according to the proportion, the self-foaming time is shorter, the foam is finer and more abundant.
Preferably, the weight percentage of the perfluorobutyl methyl ether in the facial cleanser is 0.5-5%, and the weight percentage of the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane in the facial cleanser is 0.5-5%.
By adopting the proportion, the prepared facial cleanser does not damage the normal lipid-containing component structures such as water-fat membranes and intercellular lipids and the like kept by the skin and the normal moisturizing function of the skin, and on the contrary, tiny and exquisite small bubbles can be used for deeply penetrating into skin textures and pores, so that deeply-stored dirt is thoroughly cleaned, the normal moisturizing function of the skin is recovered, and the facial cleanser is moist, comfortable, refreshing and free from tightness after washing.
More preferably, the weight percentage of the perfluorobutyl methyl ether in the facial cleanser is 3%, and the weight percentage of the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane in the facial cleanser is 1.5%. Particularly, when the proportion is adopted, the prepared facial cleanser is most stable, the self-foaming time is short, and the foam is fine.
Preferably, the amino surfactants are cocoyl glutamate TEA salt and sodium cocoyl glycinate; in the facial cleanser, the weight percentage of the cocoyl glutamic acid TEA salt is 1-15%, and the weight percentage of the cocoyl sodium glycinate is 1-40%.
The pH values of the two amino surfactants, namely the cocoyl glutamic acid TEA salt and the cocoyl sodium glycinate, are close to those of human skin, and the surfactant is mild and skin-friendly and can be used for sensitive skin at ease.
More preferably, in the facial cleanser, the content of the TEA salt of cocoyl glutamic acid in percentage by weight is 3-7%, and the content of the sodium cocoyl glycinate in percentage by weight is 18-22%.
When the cocoyl glutamic acid TEA salt and the cocoyl sodium glycinate with the addition amounts are adopted, the cleaning effect can be better played together with the self-foaming agent, and the mild cleaning effect of the fine foam generated by the self-foaming agent and the amino acid surfactant can play a role in mild and deep cleaning.
Most preferably, in the facial cleanser, the content of the cocoyl glutamic acid TEA salt is 5% by weight, and the content of the cocoyl sodium glycinate is 20% by weight. The amino surfactant, especially when added in the above amount, can stabilize the prepared facial cleanser for a long time and ensure mild cleansing effect.
Preferably, the facial cleanser further comprises a co-surfactant which is cocamidopropyl betaine, C12-16 alkyl glucoside and cocamide DEA; the auxiliary surfactants comprise the following components in percentage by weight in the facial cleanser: 1-30% of cocamidopropyl betaine, 0.1-12% of C12-16 alkyl glucoside and 0.1-10% of cocamide DEA.
The auxiliary surfactant has very low irritation to skin, does not cause any stinging feeling to eyes during washing, can be matched with the amino surfactant and the self-foaming agent, has a deep cleaning effect, does not cause excessive elution, and is fresh and cool after washing without tightness.
More preferably, the weight percentage of each auxiliary surfactant in the cleansing milk is as follows: 8-12% of cocamidopropyl betaine, 1-3% of C12-16 alkyl glucoside and 0.1-1% of cocamide DEA.
When the auxiliary surfactants are mixed according to the proportion, the functions of the auxiliary surfactants can be fully exerted, the auxiliary surfactants can be better matched with the amino surfactant, tiny and fine foams can penetrate into skin textures and pores, the amino surfactant and the auxiliary surfactants can promote the cleaning effect, and the auxiliary surfactants are mild and non-irritant, and cannot cause serious water loss, coarse cutin and other symptoms after washing.
Most preferably, the weight percentage of each auxiliary surfactant in the cleansing milk is as follows: cocamidopropyl betaine 10%, C12-16 alkyl glucoside 2% and cocamide DEA 0.5%. When the proportion is adopted, the cleansing milk has the most stable character while the cleansing effect is ensured.
Preferably, the facial cleanser further comprises an influenza modifier; the influenza modifier is a mixture of cassava starch and polymethylsilsesquioxane, and the weight percentage of the influenza modifier in the cleansing milk is 0.1-5%. The influenza modifier is preferably purchased from Baihabo Co, Inc. of Guangzhou, and has a product model of
Commercial products of Pure.
More preferably, the weight percentage content of the influenza modifier in the facial cleanser is 1.2%.
Preferably, the facial cleanser further comprises 0.1-5% of a skin conditioning agent; the skin conditioner is a purslane extract.
The purslane extract is of pure plant source, contains safe and reliable anti-irritation, anti-allergy and anti-inflammatory active ingredients, is safer to use, and can fully exert the anti-allergy and anti-inflammatory effects in the facial cleanser disclosed by the invention.
More preferably, the purslane extract is 1% by weight of the cleansing milk. When the additive amount is adopted, the anti-allergy and anti-inflammatory effects can be fully exerted, and the phenomenon that the additive amount is too much to cause the failure of full utilization is avoided.
Preferably, the facial cleanser further comprises an emulsifier, a humectant and a thickener;
the emulsifier is polyglycerol-2 dipolyhydroxystearate; the weight percentage of the polyglycerol-2 dipolyhydroxystearate in the facial cleanser is 0.1-5%;
the moisturizing agent is glycerin and isononyl isononanoate, and in the facial cleanser, the weight percentage of the glycerin is 0.2-10%, and the weight percentage of the isononyl isononanoate is 0.1-5%;
the thickening agent is PEG-150 distearate and acrylic acid (ester) copolymer, and in the facial cleanser, the weight percentage content of the PEG-150 distearate is 0.01-3%; the weight percentage content of the acrylic acid (ester) copolymer is 1-15%.
The emulsifier, the humectant and the thickener are all selected from mild and non-irritating raw materials.
Preferably, in the facial cleanser, the weight percentage of the polyglycerol-2 dipolyhydroxystearate is 0.5 percent, the weight percentage of the glycerol is 2 percent, the weight percentage of the isononyl isononanoate is 0.8 percent, and the weight percentage of the PEG-150 distearate is 0.3 percent; the weight percentage of the acrylic acid (ester) copolymer is 6 percent.
When the emulsifier, the humectant and the thickener are added in the above amount, the current situation of the facial cleanser can be ensured to be stable for a long time.
Preferably, the facial cleanser further comprises a preservative which is the following components in percentage by weight in the facial cleanser: 0.01-0.5% of methyl hydroxybenzoate and 0.01-1% of phenoxyethanol. The preservatives are mild and non-irritant, and can prolong the shelf life of the facial cleanser.
Preferably, the facial cleanser further comprises 0.1-5% of a light-screening agent, and the light-screening agent is a styrene/acrylic acid (ester) copolymer.
In addition to the above-mentioned components, other auxiliary materials such as essence, pigment, etc. can be added or used by those skilled in the art within the scope not impairing the effects of the present invention.
The invention has the beneficial effects that: the self-foaming amino acid facial cleanser provided by the invention has a self-foaming effect, the self-foaming time is short, the self-foaming foam quantity is large, the foam is very fine and smooth, mild and non-irritant, the facial skin can be deeply cleaned, and the self-foaming amino acid facial cleanser is very interesting.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
Examples 1 to 6
The formulations of the self-foaming amino acid facial cleansers described in examples 1-6 are shown in Table 1.
The preparation method of the self-foaming facial cleanser described in the embodiment 1 to 6 comprises the following steps:
(1) adding glycerol and methyl hydroxybenzoate into a mixture of cassava starch and polymethylsilsesquioxane, stirring for 1-2 minutes, adding deionized water, heating to 80-85 ℃, and homogenizing to obtain particles without obvious particles;
(2) adding the cocoyl glutamic acid TEA salt, the cocoyl sodium glycinate, the cocoamidopropyl betaine, the C12-16 alkyl glucoside, the polyglycerol-2 dipolyhydroxystearate, the isononyl isononanoate and the PEG-150 distearate into a beaker, keeping the temperature of the water bath at 85 ℃, and slowly stirring the mixture for 15 to 20 minutes.
(3) Adding the pre-dispersed acrylic acid (ester) copolymer and styrene/acrylic acid (ester) copolymer, and keeping the temperature for 5-10 minutes.
(4) And after the heat preservation is finished, adding a mixture of perfluorobutyl methyl ether, ethyl perfluorobutyl ether and polydimethylsiloxane, benzyl alcohol, methyl chloroisothiazolinone, methyl isothiazolinone, essence and a purslane (Portulaca OLERACEA) extract, and uniformly mixing to obtain the facial cleanser.
Table 1 formula of self-foaming amino acid face washes as described in examples 1-6
Examples 7 to 12
The formula of the self-foaming amino acid facial cleanser described in examples 7-10 is shown in table 2, the formula of the self-foaming amino acid facial cleanser described in examples 11 and 12 is shown in table 3, and the preparation method is the same as that of examples 1-6.
Comparative examples 1 to 6
The formula of the facial cleanser in the comparative examples 1-4 is shown in table 2, the formula of the facial cleanser in the comparative examples 5 and 6 is shown in table 3, and the preparation method is the same as that in the examples 1-6.
TABLE 2 formula of face cleansing cream described in examples 7 to 10 and comparative examples 1 to 4
Table 3 formula of face washes as described in examples 11 and 12, and comparative examples 5 and 6
| Components | Example 11 | Example 12 | Comparative example 5 | Comparative example 6 |
| Perfluorobutyl methyl ether | 3 | 3 | 3 | 3 |
| Ethyl perfluorobutyl ether | 0.75 | 0.75 | 0.75 | 0.75 |
| Polydimethylsiloxane | 0.75 | 0.75 | 0.75 | 0.75 |
| Cocosyl glutamic acid TEA salt | 3 | 7 | 25 | 0 |
| Cocoyl glycine sodium salt | 22 | 18 | 0 | 25 |
| Cocoamidopropyl betaine | 10 | 10 | 10 | 10 |
| C12-16 alkyl glucoside | 2 | 2 | 2 | 2 |
| Cocoamide DEA | 1.5 | 1.5 | 1.5 | 1.5 |
| Purslane extract | 1 | 1 | 1 | 1 |
| Tapioca starch/polymethylsilsesquioxane | 1.2 | 1.2 | 1.2 | 1.2 |
| Polyglycerol-2 bisPolyhydroxy stearate | 0.5 | 0.5 | 0.5 | 0.5 |
| Glycerol | 2 | 2 | 2 | 2 |
| Isononyl isononanoate | 0.8 | 0.8 | 0.8 | 0.8 |
| PEG-150 distearate | 0.3 | 0.3 | 0.3 | 0.3 |
| Acrylic acid (ester) copolymer | 6 | 6 | 6 | 6 |
| Styrene/acrylic acid (ester) copolymer | 1 | 1 | 1 | 1 |
| Hydroxy phenyl methyl ester | 0.15 | 0.15 | 0.15 | 0.15 |
| Phenoxyethanol | 0.15 | 0.15 | 0.15 | 0.15 |
| Essence | 0.15 | 0.15 | 0.15 | 0.15 |
| Water (W) | Balance of | Balance of | Balance of | Balance of |
Example 13
Testing of the Using Effect of face cleaning cream
The method comprises the following steps: 180 female volunteers with healthy skin, 20-40 years old and 30 years old in average are selected and divided into 18 groups, 10 persons in each group are respectively used with the facial cleansers of examples 1-12 and comparative examples 1-6, the time is 8-9 am, the volunteers are subjected to questionnaire, the feeling of evaluation items before and after use is compared, the feeling is preferably 4 minutes, the good is 3 minutes, generally 2 minutes and the difference is 1 minute, wherein the self-foaming time is sequentially recorded as 2-4 seconds (4 minutes), 5-9 seconds (3 minutes), 10-14 seconds (2 minutes) and more than 15 seconds (1 minute) from short to long, the visually almost invisible foam is 4 minutes, the visually visible foam is 3 minutes, the visually visible foam is 2 minutes, and the visually visible foam is 1 minute. Then, the average value of each item is calculated. The statistical results are shown in table 4.
Table 4 evaluation of use effect of face cleanser
As can be seen from the statistical results in Table 4, the facial cleansers of embodiments 1-12 all have good cleaning effect, moisturizing effect, easy rinsing performance and good comfort after washing. Wherein, through comparing examples 1, 7-10, comparative examples 1-4 to discover, the ratio of the volunteers' use weight is: perfluorobutyl methyl ether: the cleanser of example 1 with the mixture of ethyl perfluorobutyl ether and polydimethylsiloxane 2:1 has shorter self-foaming time, finer foam and richer foam, and can bring better cleaning power, and the weight ratio of the ethyl perfluorobutyl ether to the polydimethylsiloxane is as follows: ethyl perfluorobutyl ether: when the polydimethylsiloxane is 1:1, the self-foaming time can be effectively shortened, and the foam is more exquisite and rich. The comparison also shows that under the condition that the addition amount of the self-foaming agent is consistent, compared with the condition that only one or two of the self-foaming agent is used, when the perfluoro butyl methyl ether, the ethyl perfluoro butyl ether and the polydimethylsiloxane are used simultaneously, the self-foaming time is shorter, the foam is finer and smoother, the foam quantity is richer, the cleaning power is stronger, and better comfort can be brought. It was found by comparing examples 1, 11, 12 and comparative examples 5, 6 that, in the case of consistent addition of the amino surfactants, the volunteers evaluated higher cleaning power using both of the cocoyl glutamate TEA salt and sodium cocoyl glycinate of the present invention than using only one of them, especially when the weight ratio of the two amino surfactants was: cocoyl glutamate TEA salt: when the ratio of cocoyl sodium glycinate to cocoyl sodium glycinate is 1:4, the cleaning effect is optimal, and the skin feel is more comfortable after face cleaning.
The self-foaming times of examples 1, 7 to 10 and comparative examples 1 to 4 were measured, and the average of five times of the test time was taken, and the test results are shown in Table 5.
TABLE 5 self-foaming time test results
As can be seen from Table 5, it was found from the results of example 1 and comparative examples 1 to 4 that the addition of three types of self-foaming agents is effective in shortening the foaming time; from a comparison of examples 1, 7 and 8, it was found that, with the same total amount of added self-foaming agent, when the weight ratio of perfluorobutyl methyl ether to the mixture of ethyl perfluorobutyl ether and polydimethylsiloxane: perfluorobutyl methyl ether: the spontaneous bubble time was shorter when the mixture of ethyl perfluorobutyl ether and polydimethylsiloxane was 2:1, and from the comparison of examples 1, 9, 10, it was found that when the weight ratio of ethyl perfluorobutyl ether to polydimethylsiloxane was: ethyl perfluorobutyl ether: when the mixture of polydimethylsiloxanes is 1:1, the self-foaming time is shorter.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. A self-foaming amino acid facial cleanser, which is characterized by comprising an amino surfactant and a self-foaming agent, wherein the self-foaming agent comprises perfluorobutyl methyl ether, ethyl perfluorobutyl ether and polydimethylsiloxane; the weight percentage of the perfluorobutyl methyl ether in the facial cleanser is 0.1-15%, and the weight percentage of the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane in the facial cleanser is 0.1-15%;
the amino surfactant is cocoyl glutamic acid TEA salt and cocoyl sodium glycinate; in the facial cleanser, the weight percentage of the cocoyl glutamic acid TEA salt is 1-15%, and the weight percentage of the cocoyl sodium glycinate is 1-40%;
the weight ratio of the perfluorobutyl methyl ether to the mixture of the ethyl perfluorobutyl ether and the polydimethylsiloxane is as follows: perfluorobutyl methyl ether: mixture of ethyl perfluorobutyl ether and polydimethylsiloxane =2: 1; the weight ratio of the ethyl perfluorobutyl ether to the polydimethylsiloxane is as follows: ethyl perfluorobutyl ether: polydimethylsiloxane =1: 1.
2. The self-foaming amino acid facial cleanser of claim 1, wherein the weight percentage of said perfluorobutyl methyl ether in said facial cleanser is 0.5-5%, and the weight percentage of said mixture of ethyl perfluorobutyl ether and polydimethylsiloxane in said facial cleanser is 0.5-5%.
3. The self-foaming amino acid facial cleanser of claim 1, wherein said perfluorobutyl methyl ether is present in said facial cleanser in an amount of 3% by weight and said mixture of ethyl perfluorobutyl ether and polydimethylsiloxane is present in said facial cleanser in an amount of 1.5% by weight.
4. The self-foaming amino acid facial cleanser of claim 1, wherein the weight percentage of the cocoyl glutamate TEA salt is 3-7% and the weight percentage of the cocoyl sodium glycinate is 18-22%.
5. The self-foaming amino acid facial cleanser of claim 1, further comprising co-surfactants of cocamidopropyl betaine, C12-16 alkyl glucoside, and cocamide DEA; the auxiliary surfactants comprise the following components in percentage by weight in the facial cleanser: 1-30% of cocamidopropyl betaine, 0.1-12% of C12-16 alkyl glucoside and 0.1-10% of cocamide DEA.
6. The self-foaming amino acid facial cleanser of claim 5, wherein each co-surfactant is present in the facial cleanser in an amount by weight: 8-12% of cocamidopropyl betaine, 1-3% of C12-16 alkyl glucoside and 0.1-1% of cocamide DEA.
7. The self-foaming amino acid facial cleanser of claim 1, further comprising an influenza modifier; the influenza modifier is a mixture of cassava starch and polymethylsilsesquioxane, and the weight percentage of the influenza modifier in the cleansing milk is 0.1-5%.
8. The self-foaming amino acid facial cleanser of claim 1, further comprising 0.1-5% of a skin conditioning agent; the skin conditioner is a purslane extract.
9. The self-foaming amino acid facial cleanser of claim 1, further comprising an emulsifier, a humectant, and a thickener;
the emulsifier is polyglycerol-2 dipolyhydroxystearate; the weight percentage of the polyglycerol-2 dipolyhydroxystearate in the facial cleanser is 0.1-5%;
the moisturizing agent is glycerin and isononyl isononanoate, and in the facial cleanser, the weight percentage of the glycerin is 0.2-10%, and the weight percentage of the isononyl isononanoate is 0.1-5%;
the thickening agent is PEG-150 distearate and acrylic acid (ester) copolymer, and in the facial cleanser, the weight percentage content of the PEG-150 distearate is 0.01-3%; the weight percentage content of the acrylic acid (ester) copolymer is 1-15%.
10. The self-foaming amino acid facial cleanser of claim 9, wherein said polyglycerol-2 dipolyhydroxystearate is present in an amount of 0.5% by weight, said glycerol is present in an amount of 2% by weight, said isononyl isononanoate is present in an amount of 0.8% by weight, and said PEG-150 distearate is present in an amount of 0.3% by weight; the weight percentage of the acrylic acid (ester) copolymer is 6 percent.
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| CN109464300B (en) * | 2018-12-28 | 2021-07-09 | 中山市天图精细化工有限公司 | Post-foaming facial cleanser and preparation method thereof |
| CN109646378B (en) * | 2019-01-30 | 2020-12-15 | 佛山市百分之秀化妆品有限公司 | Whitening and moisturizing freckle-removing emulsion and preparation method thereof |
| CN110693748B (en) * | 2019-11-04 | 2023-05-05 | 木芷秋山(广州)化妆品研究开发有限公司 | Amino acid foam facial cleanser and preparation method thereof |
| CN111631965A (en) * | 2020-07-07 | 2020-09-08 | 美丽链接生物科技研究院(广东)有限公司 | Plant-derived facial mask with cleaning and makeup removing functions |
| CN113274316A (en) * | 2021-05-12 | 2021-08-20 | 上海肤徕生物高科技有限公司 | Self-foaming amino acid repairing face wash and preparation process thereof |
| CN114903811A (en) * | 2022-05-20 | 2022-08-16 | 广东博然堂生物科技有限公司 | Face cleansing liquid and face cleansing towel adopting plant surfactant and preparation method |
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