CN112675047B - Double-layer bath foam and preparation method thereof - Google Patents
Double-layer bath foam and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of bath products, and discloses double-layer bath foam and a preparation method thereof. The double-layer bath foam provided by the invention comprises an aqueous phase and an oil phase, wherein the aqueous phase comprises the following components: amino acid surfactant, nonionic surfactant, humectant, pH regulator, antiseptic, essence, and water; the oil phase comprises the following components: synthetic oil and fat, animal oil and fat, and vegetable oil and fat. The bath foam provided by the invention has a double-layer appearance, the upper layer is white and non-transparent, the lower layer is transparent, and under the scientific proportion, the amino acid surfactant and the nonionic surfactant are perfectly matched with excellent moisturizing grease, so that the skin is mildly cleaned, and the bath foam has the effects of moisturizing, oxidation resistance, whitening and the like.
Description
Technical Field
The invention relates to the technical field of bath products, in particular to double-layer bath foam and a preparation method thereof.
Background
The bath foam has the primary function of mainly cleaning the skin of the whole body, along with the development of economy and the improvement of living standard, the quality requirement of people on the bath foam is rapidly improved, and the requirement of consumers cannot be met by pure skin cleaning. In addition to skin cleaning, consumers have higher requirements on skin care effects of the bath foam, such as moistening, oxidation resistance and the like, and meanwhile, consumers also pursue more beautiful appearance and use feeling of the bath foam.
Chinese patent CN201710524659.0 discloses a double-layer bath foam comprising, by weight, an upper layer solution and a lower layer solution; the upper layer solution consists of the following components: 3% of potassium cetyl ether phosphate, 2% of sodium lauroyl glutamate, 1% of cocamide betaine, 1% of sodium lauryl amphoacetate, 0.5% of PEG-7 cocoyl glyceride, 1% of decyl glucoside, 1% of PEG-80 sorbitan laurate, 4% of sweet almond oil, 0.5% of tea seed oil, 0.5% of tocopherol acetate, 0.0005-0.01% of preservative and essence, and the balance of deionized water; the lower layer solution consists of the following components: 8% of potassium cetyl ether phosphate, 6% of sodium lauroyl glutamate, 3% of cocamide betaine, 1% of sodium lauryl amphoacetate, 1% of PEG-7 cocoglyceride, 2% of decyl glucoside, 2% of PEG-80 sorbitan laurate, 4% of glycerol, 0.5% of betaine, 0.0005-0.01% of preservative and essence, and the balance of deionized water. However, the oil disclosed by the patent is sweet almond oil and tea seed oil, the total content of the oil is 4.5%, the content is not high, and the unique skin care effects of moistening, oxidation resistance, whitening and the like of the oil are hardly exerted. However, when the double-layer bath foam has high oil content, the double-layer bath foam is easy to have oily use feel, and the double-layer bath foam is slowly layered again after being shaken uniformly.
Therefore, there is a need for a bilayer bath lotion with high oil content and good use feeling to meet the expanding market demand.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention mainly aims to provide the double-layer bath foam which has white and non-transparent upper layer and transparent lower layer, has high content of functional grease and good use feeling.
The invention also aims to provide a preparation method of the double-layer bath foam.
In order to achieve the purpose, the invention adopts the following technical scheme:
a dual layer body wash comprising an aqueous phase and an oil phase, the aqueous phase comprising the following components: amino acid surfactant, nonionic surfactant, humectant, pH regulator, antiseptic, essence, and water; the oil phase comprises the following components: synthetic oil and fat, animal oil and fat, and vegetable oil and fat.
Preferably, the double-layer bath foam comprises an aqueous phase and an oil phase, wherein the aqueous phase comprises the following components in parts by mass: 3-25 parts of amino acid surfactant, 1-5 parts of nonionic surfactant, 1-5 parts of humectant, 0.01-0.5 part of pH regulator, 0.3-0.8 part of preservative, 0.05-0.5 part of essence and 10-90 parts of water; the oil phase comprises, by mass, 5-15 parts of synthetic oil and fat, 1-5 parts of animal oil and fat and 2-10 parts of vegetable oil and fat.
Preferably, the weight ratio of the water phase to the oil phase in the double-layer bath foam is 4:1-9:1.
preferably, the mass ratio of the amino acid surfactant to the nonionic surfactant is 3:1-5:1.
preferably, the amino acid surfactant comprises at least one of sodium cocoamidopropionate, sodium lauroyl sarcosinate, and sodium cocoyl methyl taurate.
Preferably, the amino acid surfactant is a mixture of sodium cocoamidopropionate, sodium lauroyl sarcosinate and sodium cocoyl methyl taurate; wherein the mass ratio of the sodium cocoamidopropionate to the sodium lauroyl sarcosinate to the sodium cocoyl methyl taurate is (5-10): (5-10): (2-5).
Preferably, the nonionic surfactant comprises PEG-50 shea butter.
Preferably, the humectant comprises glycerin; the pH regulator comprises citric acid; the preservative comprises phenoxyethanol.
Preferably, the animal fat comprises squalane.
Preferably, the vegetable oil comprises grape seed oil and wheat germ oil.
Preferably, the synthetic oil or fat comprises caprylic/capric triglyceride.
The grape seed oil has the characteristics of skin friendliness, good transdermal property, safety and no stimulation, contains the components such as horned turtle alkene and VE, and has the effects of removing free radicals, resisting aging, whitening, astringing and controlling oil; the wheat germ oil is rich in various physiological active substances, such as vitamin E and various unsaturated fatty acids, has the effects of delaying skin aging, increasing skin softness, whitening skin, fading and eliminating striae gravidarum and wrinkles and the like, and is excellent skin conditioning oil; squalane can be rapidly dissolved with moisture and grease in skin to form a natural protective barrier, has excellent stability, can not generate oxidation with air, ultraviolet rays and the like, can effectively protect the skin from being damaged by external substances, has excellent permeability and high-efficiency oxygen carrying performance, can adjust the water-oil balance of the skin, and avoids the rough and dark skin; caprylic/capric triglyceride is a highly refreshing odorless oil, has characteristics compatible with human skin, can be applied to oily skin, and has effects of lubricating and softening skin.
Preferably, the double-layer bath foam comprises an aqueous phase and an oil phase, wherein the aqueous phase comprises the following components in parts by mass: 1-10 parts of sodium cocoamidopropionate, 1-10 parts of sodium lauroyl sarcosinate, 1-5 parts of sodium cocoyl methyl taurate, 1-5 parts of PEG-50 shea butter, 1-5 parts of glycerol, 0.01-0.5 part of citric acid, 0.3-0.8 part of phenoxyethanol, 0.05-0.5 part of essence and 10-90 parts of water; the oil phase comprises the following components in parts by mass: 5-15 parts of caprylic/capric triglyceride, 1-5 parts of squalane, 1-5 parts of grape seed oil and 1-5 parts of wheat germ oil.
Preferably, the mass ratio of the caprylic/capric triglyceride, the squalane, the grape seed oil and the wheat germ oil is (5-8): (2-4): (2-3): (3-5).
Preferably, the mass ratio of the sodium cocoamidopropionate to the sodium lauroyl sarcosinate to the PEG-50 shea butter is (5-10): (5-10): (2-5): (3-5).
The double-layer bath foam provided by the invention can be added with a plurality of proper components such as thickening agent, antioxidant, bioactive substance, skin conditioner and the like on the premise of not influencing the effect of the invention.
The invention also provides a preparation method of the double-layer bath foam, which comprises the following steps:
(1) Preparation of the aqueous phase: at normal temperature, all components of the water phase are uniformly mixed according to a certain proportion to obtain the water-soluble emulsion;
(2) Preparation of an oil phase: at the normal temperature, the reaction kettle is, uniformly mixing the components of the oil phase according to the proportion to obtain the oil phase;
(3) Preparing the double-layer bath foam: and (3) mixing the water phase and the oil phase uniformly at normal temperature, and standing for layering to obtain the double-layer bath foam.
Compared with the prior art, the invention has the following advantages and technical effects:
(1) The double-layer bath foam provided by the invention has double-layer appearance, the upper layer is white and opaque, the lower layer is transparent, and the double-layer bath foam is shaken up before use.
(2) The bath foam provided by the invention has the advantages of high foaming speed, rich and dense foam, moist but not greasy skin after use, improved bath experience of consumers, and capability of recovering double-layer appearance in a short time after shaking uniformly.
(3) The bath foam provided by the invention is fresh and cool in texture, and can be used with a conventional pump head or a mousse pump head.
(4) The double-layer bath foam provided by the invention is prepared without heating, only the water phase and the oil phase are separated and stirred uniformly, then the two phases are mixed and shaken uniformly according to a proportion, and the double-layer bath foam can be obtained by layering after standing.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited thereto. All the raw materials and reagents used in the present invention are commercially available raw materials and reagents, unless otherwise specified. The amount of each component in the examples is g and mL in parts by mass.
EXAMPLE 1 preparation of double-layered bath foam
(1) Preparation of an aqueous phase: stirring 1 part of sodium cocoamido propionate, 1 part of sodium lauroyl sarcosinate, 1 part of sodium cocoacyl methyl taurate, 1 part of PEG-50 shea butter, 3 parts of glycerol, 0.5 part of citric acid, 0.5 part of phenoxyethanol, 0.05 part of essence and 90 parts of water for 30min at the condition of 600r/min by mass at normal temperature to obtain a water phase;
(2) Preparation of oil phase: at normal temperature, 15 parts of caprylic/capric triglyceride, 3 parts of squalane, 3 parts of grape seed oil and 2 parts of wheat germ oil are stirred for 30min under the condition of 600r/min by mass parts to obtain an oil phase.
(3) Preparing the double-layer bath foam: mixing the water phase and the oil phase according to the ratio of 9:1 under the condition of 600r/min, stirring for 30min and mixing to obtain the double-layer bath foam.
EXAMPLE 2 preparation of double-layered bath foam
(1) Preparation of the aqueous phase: stirring 10 parts of sodium cocoamido propionate, 10 parts of sodium lauroyl sarcosinate, 5 parts of sodium cocoyl methyl taurate, 5 parts of PEG-50 shea butter, 3 parts of glycerol, 0.5 part of citric acid, 0.5 part of phenoxyethanol, 0.05 part of essence and 60 parts of water for 1h at the normal temperature in parts by mass under the condition of 300r/min to obtain a water phase;
(2) Preparation of an oil phase: at normal temperature, 10 parts of caprylic/capric triglyceride, 5 parts of squalane, 5 parts of grape seed oil and 5 parts of wheat germ oil are stirred for 1 hour at the condition of 300r/min by mass to obtain an oil phase.
(3) Preparing the double-layer bath foam: mixing the water phase and the oil phase according to the proportion of 4:1 at a mass ratio of 300r/min, stirring for 1h, and mixing to obtain the double-layer bath foam.
EXAMPLE 3 preparation of double-layered bath foam
(1) Preparation of an aqueous phase: stirring 5 parts of sodium cocoamido propionate, 5 parts of sodium lauroyl sarcosinate, 2 parts of sodium cocoyl methyl taurate, 3 parts of PEG-50 shea butter, 5 parts of glycerol, 0.05 part of citric acid, 0.3 part of phenoxyethanol, 0.1 part of essence and 80 parts of water for 1h at the normal temperature under the condition of 300r/min by mass to obtain a water phase;
(2) Preparation of an oil phase: at normal temperature, 5 parts of caprylic/capric triglyceride, 2 parts of squalane, 2 parts of grape seed oil and 3 parts of wheat germ oil are stirred for 1 hour at the condition of 300r/min by mass to obtain an oil phase.
(3) Preparing the double-layer bath foam: mixing the water phase and the oil phase according to the ratio of 6:1 at a mass ratio of 300r/min, stirring for 1h, and mixing to obtain the double-layer bath foam.
EXAMPLE 4 preparation of double-layered bath foam
(1) Preparation of the aqueous phase: stirring 8 parts of sodium cocoamido propionate, 8 parts of sodium lauroyl sarcosinate, 3 parts of sodium cocoyl methyl taurate, 4 parts of PEG-50 shea butter, 2 parts of glycerol, 0.05 part of citric acid, 0.3 part of phenoxyethanol, 0.1 part of essence and 75 parts of water at the condition of 900r/min for 20min by mass at normal temperature to obtain a water phase;
(2) Preparation of an oil phase: at normal temperature, 8 parts of caprylic/capric triglyceride, 4 parts of squalane, 3 parts of grape seed oil and 5 parts of wheat germ oil are stirred for 20min under the condition of 900r/min by mass parts to obtain an oil phase.
(3) Preparing the double-layer bath foam: mixing the water phase and the oil phase according to the proportion of 5:1 at the mass ratio of 900r/min, stirring for 20min, and mixing to obtain the double-layer bath foam.
EXAMPLE 5 preparation of double-layered bath foam
(1) Preparation of an aqueous phase: stirring 8 parts of sodium cocoamido propionate, 8 parts of sodium lauroyl sarcosinate, 3 parts of sodium cocoyl methyl taurate, 5 parts of PEG-50 shea butter, 3 parts of glycerol, 0.01 part of citric acid, 0.8 part of phenoxyethanol, 0.5 part of essence and 70 parts of water for 30min at the condition of 600r/min by mass at normal temperature to obtain a water phase;
(2) Preparation of an oil phase: at normal temperature, 7 parts of caprylic/capric triglyceride, 3 parts of squalane, 3 parts of grape seed oil and 4 parts of wheat germ oil are stirred for 30min under the condition of 600r/min by mass parts to obtain an oil phase.
(3) Preparing the double-layer bath foam: mixing the water phase and the oil phase according to the ratio of 8:1 at a mass ratio of 600r/min, stirring for 30min, and mixing to obtain the double-layer bath foam.
Comparative example 1
The comparative example 1 is different from the example 3 in that the mass ratio of the water phase to the oil phase is 3.
Comparative example 2
Comparative example 2 is different from example 3 in that the mass ratio of the water phase to the oil phase is 20.
Comparative example 3
Comparative example 3 differs from example 3 in that the mass ratio of the amino acid surfactant to the nonionic surfactant is 2.
Comparative example 4
Comparative example 4 differs from example 3 in that the zwitterionic surfactant cocoamidobetaine was used instead of sodium cocoamidopropionate and decyl glucoside was used instead of PEG-50 shea butter.
Delamination test
The samples of examples 1 to 5 and comparative examples 1 to 4 were respectively filled in PET bottles, shaken well and then allowed to stand until complete delamination, the appearance of the samples was observed and the time for delamination was counted, and the specific results are shown in table 1.
TABLE 1 standing layering test results after shaking up each sample
As can be seen from the data in Table 1, the double-layer bath foam prepared in the embodiments 1-5 of the invention can keep the white and opaque upper layer and the colorless and transparent lower layer, and can be delaminated within 5min after shaking; as can be seen from comparative example 1, when the addition amount of the oil is too high, the problems of turbidity of the lower layer solution, wall hanging of the oil and slow layering speed are easily caused; as can be seen from comparative examples 3 and 4, when the proportion of the surface active agent and the formula are changed, the bath foam has poor layering effect and slow layering speed.
Examination of comprehensive effects
45 women of 20-40 years old were selected as trial subjects, and randomly divided into 9 groups, and the arms were washed with the baths prepared in examples 1-5 and comparative examples 1-4, respectively. It is administered twice daily for 4 weeks. The using effects of the ingredients are divided into 5 points: 5 is the highest score, which means better and very satisfactory; 4, the classification is very good; 3 is acceptable; a score of less than 3 is not acceptable. The specific results are shown in Table 2.
Table 2. Comprehensive effect investigation results of various groups of samples
| Group of | Nourishing ability | Refreshing feeling | Foamability | Detergency |
| Example 1 | 4.2 | 4.7 | 5 | 5 |
| Example 2 | 4.8 | 4.5 | 5 | 5 |
| Example 3 | 4.7 | 4.6 | 5 | 5 |
| Example 4 | 4.5 | 4.7 | 5 | 5 |
| Example 5 | 4.3 | 4.6 | 5 | 5 |
| Comparative example 1 | 4.3 | 2.8 | 3.7 | 3.8 |
| Comparative example 2 | 3.5 | 4.6 | 3.2 | 5 |
| Comparative example 3 | 4.2 | 3.8 | 4.2 | 5 |
| Comparative example 4 | 4.2 | 3.8 | 3.5 | 5 |
As can be seen from the results in Table 2, the test subjects of the double-layered bath foam prepared in examples 1-5 of the present invention have high evaluations for nourishing, refreshing, foaming and detergency; comparative example 1 was poor in refreshing feeling, and the evaluation of foaming property and detergency was also general; the moisturizing feeling and foamability of comparative example 2 were more general; the refreshing feeling of comparative example 3 was general; the evaluation on the refreshing feeling and the foamability of the comparative example 4 is general, and the synergistic effect of the components in the double-layer bath foam formula provided by the invention can ensure that consumers enjoy the unique experience of combining cleaning and skin care in the bathing process; meanwhile, the product has soft foam, and the consumer can feel like a cloud when bathing, and the product has a silk-like skin touch.
The above embodiments are the best mode for carrying out the present invention, but the embodiments of the present invention are not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be regarded as equivalent substitutions and are included in the scope of the present invention.
Claims (4)
1. A double-layer bath foam is characterized in that,
the double-layer bath foam comprises a water phase and an oil phase, wherein the mass ratio of the water phase to the oil phase is 4:1-9:1;
the water phase comprises the following components in parts by mass: 1-10 parts of sodium cocoamidopropionate, 1-10 parts of sodium lauroyl sarcosinate, 1-5 parts of sodium cocoyl methyltaurate, 1-5 parts of PEG-50 shea butter, 1-5 parts of glycerol, 0.01-0.5 part of citric acid, 0.3-0.8 part of phenethyl alcohol, 0.05-0.5 part of essence and 60-90 parts of water, wherein the ratio of the total mass of the sodium cocoamidopropionate, the sodium lauroyl sarcosinate and the sodium cocoyl methyltaurate to the mass of the PEG-50 shea butter is 3:1-5:1;
the oil phase comprises the following components in parts by mass: 5-15 parts of caprylic/capric triglyceride, 1-5 parts of squalane, 1-5 parts of grape seed oil and 1-5 parts of wheat germ oil.
2. The dual layer body wash of claim 1, wherein: the mass ratio of the caprylic/capric triglyceride to the squalane to the grape seed oil to the wheat germ oil is (5-8): (2-4): (2-3): (3-5).
3. The double-layered body wash of claim 1, wherein: the mass ratio of the sodium cocoamidopropionate to the sodium lauroyl sarcosinate to the sodium cocoyl methyl taurate to the PEG-50 shea butter is (5-10): (5-10): (2-5): (3-5).
4. The method of preparing a double layer body wash according to any one of claims 1-3, comprising the steps of:
(1) Preparation of the aqueous phase: at normal temperature, uniformly mixing all components of the water phase according to a proportion to obtain the water-soluble polymer;
(2) Preparation of oil phase: at normal temperature, all components of the oil phase are uniformly mixed according to a certain proportion to obtain the oil phase;
(3) Preparation of the double-layer bath foam: and (3) mixing the water phase and the oil phase uniformly at normal temperature, and standing for layering to obtain the double-layer bath foam.
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| CN113749953B (en) * | 2021-08-26 | 2022-08-30 | 广州环亚化妆品科技股份有限公司 | Double-layer shower gel with stable milk cover layer and preparation method thereof |
| CN115813791A (en) * | 2022-12-16 | 2023-03-21 | 湖州嘉亨实业有限公司 | Water-oil bidirectional bath oil and preparation method thereof |
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