CN107095807B - Double-layer bath foam and preparation method thereof - Google Patents

Double-layer bath foam and preparation method thereof Download PDF

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CN107095807B
CN107095807B CN201710524659.0A CN201710524659A CN107095807B CN 107095807 B CN107095807 B CN 107095807B CN 201710524659 A CN201710524659 A CN 201710524659A CN 107095807 B CN107095807 B CN 107095807B
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bath foam
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double
foam
layer solution
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CN107095807A (en
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孟宪云
李雪竹
陈晓朋
李汉玲
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Guangzhou Ousia Industrial Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/463Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/604Alkylpolyglycosides; Derivatives thereof, e.g. esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
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  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses double-layer bath foam and a preparation method thereof. The double-layer bath foam comprises an upper layer solution: 5-10% of anionic surfactant, 3-5% of zwitterionic surfactant, 2-4% of nonionic surfactant, 3-8% of grease and a proper amount of preservative and essence; the lower layer solution contained: 5-20% of anionic surfactant, 3-6% of zwitterionic surfactant, 2-6% of nonionic surfactant and 20-80% of water. Also comprises humectant, active compound, pigment, antiseptic, and essence. The bath foam provided by the invention is divided into two layers in a static state, and the bath foam needs to be used after being shaken up. After the foam pump head is matched for use, not only can uniform and fine foam be generated, but also the skin can be moistened and not dried by the grease and the humectant in the formula.

Description

Double-layer bath foam and preparation method thereof
Technical Field
The invention relates to a mixture for cleaning bodies, belongs to the technical field of daily washing products, and particularly relates to double-layer bath foam and a preparation method thereof.
Background
The bath foam is a cleaning agent for human body, and is mainly used for cleaning the skin of the whole body. The bath foam on the market at present has the defects of dry and tight skin, little foam, difficult washing and the like; and the single appearance is generally a viscous liquid or paste product.
Along with the improvement of living standard, people have higher and higher requirements on bath foam, and the bath foam is not only required to be safe, not irritate skin, have dense and rich foam, moisten after use, nourish and care skin, but also have attractive appearance. In order to meet the needs of the consumer,
the double-layer bath foam is invented aiming at the defects of most of the existing bath foam, has rich foam, is safe and not irritant, and is moistened and not dry after use.
The product of the invention differs from the patented product 201410516485:
1) the invention 201410516485 provides a bath foam formula which has nutrition protection effect on human skin; the bath foam formula has the advantages that the skin is moistened, the skin is prevented from being dried and cracked, and the skin is repaired through the grease and the active ingredients;
2) the appearance is different, the product of the invention is divided into two layers of water-like liquid, and the patent product 201410516485 is viscous uniform liquid with certain fluidity.
The product of the invention differs from the patented product 201410435702.2:
1) the appearance is different, the product of the invention is divided into two layers of water-like liquid, and the patent product is viscous uniform liquid with certain fluidity.
2) The bath foam has different efficacy approaches, and the formula of the bath foam can achieve the effects of moistening skin, preventing skin chap and repairing skin through certain grease and active ingredients. The invention 201410435702.2 is a bath lotion for softening skin, keeping moisture and relieving fatigue.
Disclosure of Invention
The invention aims to provide a double-layer bath foam which is a bath foam for moistening skin, preventing skin chap and repairing skin through certain grease and active ingredients, has rich foam, is moist and not dry after use and nourishes skin.
In order to realize the technical points, the invention is implemented by the following scheme:
a double-layer bath foam comprising, in weight percent, an upper layer solution and a lower layer solution, the upper layer mixture comprising: 5-10% of anionic surfactant, 3-4% of zwitterionic surfactant, 2-5% of nonionic surfactant and 3-6% of grease;
the lower layer mixture comprises: 5-20% of anionic surfactant, 3-6% of zwitterionic surfactant, 2-6% of nonionic surfactant and 20-80% of water. The rest humectant, active compound, pigment, antiseptic, and essence in appropriate amount.
The anionic surfactant comprises fatty alcohol-polyoxyethylene ether phosphate which mainly refers to potassium cetyl ether phosphate, and alkyl polyoxyethylene ether sulfate which mainly refers to one or a combination of more of sodium lauryl ether sulfate, sodium lauryl sulfosuccinate and sodium lauroyl glutamate;
the zwitterionic surfactant comprises one or a combination of two of cocamide betaine and sodium lauryl amphoacetate;
the nonionic surfactant comprises one or more of PEG-7 coco glyceride, lauryl amine oxide, decyl glucoside, and PEG-80 sorbitan laurate.
The oil comprises one or more of mineral oil, vegetable oil and tocopherol acetate.
The double-layer bath foam also comprises 0.2 to 1 percent of active compound according to the weight percentage; and 1-6% of humectant, wherein the active compound is one or more of honey extract, aloe extract and horse chestnut extract; the humectant contains one or more of glycerol, butanediol and betaine.
The double-layer bath foam further comprises 0.0005-0.01 wt% of other components, wherein the other components comprise pigments, preservatives, essences and the like.
The preparation method of the double-layer bath foam comprises the following steps:
adding deionized water into an emulsifying pot, respectively adding raw materials of potassium cetyl ether phosphate, sodium lauryl ether sulfate, sodium lauryl amphoacetate, PEG-7 cocoyl glyceride, decyl glucoside, PEG-80 sorbitan laurate, sweet almond oil, tea seed oil, tocopherol acetate and glycerol into the emulsifying pot in sequence, heating to 75-80 ℃, and uniformly stirring; cooling to 40 + -5 deg.C, adding betaine, antiseptic and essence, stirring, and making.
By means of the technical scheme, the invention has the following advantages and beneficial effects:
1) the double-layer bath foam has the upper layer which is a mixture of grease and a surfactant, and the lower layer which is a mixture of the surfactant, water, a humectant, an active ingredient, a pigment, essence and the like.
2) The appearance of the invention is a two-layer bath foam, which is the bath foam for moistening skin, preventing skin chap and repairing skin through some grease and active ingredients, and has the characteristics of abundant foam, moistening without dryness after use and nourishing skin.
Detailed Description
The present invention will be described in further detail with reference to the following preferred examples and effect test examples, but the present invention is not limited to the following examples. The following percentages are all weight percentages.
Example 1
A double-layer bath foam is divided into two layers in appearance, namely an upper layer solution and a lower layer solution, and comprises the following components:
the upper layer solution comprises the following components: 2% of potassium cetyl ether phosphate, 3% of sodium lauryl ether sulfate, 1% of sodium lauryl amphoacetate, 0.5% of PEG-7 cocoglyceride, 1% of decyl glucoside, 1% of PEG-80 sorbitan laurate, 4% of sweet almond oil, 0.5% of tea seed oil, 0.5% of tocopherol acetate, and a proper amount of preservative and essence.
The lower layer solution comprises the following components: 3% of potassium cetyl ether phosphate, 6% of sodium lauryl ether sulfate, 3% of sodium lauryl amphoacetate, 1% of PEG-7 cocoyl glyceride, 2% of decyl glucoside, 2% of PEG-80 sorbitan laurate, 4% of glycerol, 0.5% of betaine, a proper amount of preservative and essence, and the balance of deionized water.
The preparation method of the double-layer bath foam comprises the following steps:
1) adding deionized water into an emulsifying pot, respectively adding raw materials of potassium cetyl ether phosphate, sodium lauryl ether sulfate, sodium lauryl amphoacetate, PEG-7 cocoyl glyceride, decyl glucoside, PEG-80 sorbitan laurate, sweet almond oil, tea seed oil, tocopherol acetate and glycerol into the emulsifying pot in sequence, heating to 75-80 ℃, and uniformly stirring;
2) cooling to 40 + -5 deg.C, adding betaine, antiseptic and essence, stirring, and making.
Example 2
A double-layer bath foam is divided into two layers in appearance, namely an upper layer solution and a lower layer solution, and comprises the following components:
the upper layer solution comprises the following components: 3% of potassium cetyl ether phosphate, 2% of sodium lauroyl glutamate, 1% of cocoamidobetaine, 1% of sodium lauryl amphoacetate, 0.5% of PEG-7 cocoglyceride, 1% of decyl glucoside, 1% of PEG-80 sorbitan laurate, 4% of sweet almond oil, 0.5% of tea seed oil, 0.5% of tocopherol acetate, and proper amounts of preservatives and essences.
The lower layer solution comprises the following components: 8% of potassium cetyl ether phosphate, 6% of sodium lauroyl glutamate, 3% of cocoamidobetaine, 1% of sodium lauryl amphoacetate, 1% of PEG-7 cocoglyceride, 2% of decyl glucoside, 2% of PEG-80 sorbitan laurate, 4% of glycerol, 0.5% of betaine, a proper amount of preservative and essence, and the balance of deionized water.
The preparation method of the double-layer bath foam comprises the following steps:
1) adding deionized water into an emulsifying pot, respectively adding raw materials of potassium cetyl ether phosphate, sodium lauroyl glutamate, cocamidopropyl betaine, sodium lauryl amphoacetate, PEG-7 cocoyl glyceride, decyl glucoside, PEG-80 sorbitan laurate, sweet almond oil, tea seed oil, tocopherol acetate and glycerol into the emulsifying pot in sequence, heating to 75-80 ℃, and uniformly stirring.
2) Cooling to 40 + -5 deg.C, adding betaine, antiseptic and essence, stirring, and making.
Example 3
A double-layer bath foam is divided into two layers in appearance, namely an upper layer solution and a lower layer solution, and comprises the following components:
the upper layer solution comprises the following components: 4% of potassium cetyl ether phosphate, 2% of sodium lauroyl glutamate, 1% of cocamidobetaine, 2% of sodium lauryl amphoacetate, 0.5% of PEG-7 cocoglyceride, 1% of decyl glucoside, 1% of PEG-80 sorbitan laurate, 4% of sweet almond oil, 0.5% of tea seed oil, 0.5% of tocopherol acetate, and proper amounts of preservatives and essences.
The lower layer solution comprises the following components: 8% of potassium cetyl ether phosphate, 4% of sodium lauroyl glutamate, 2% of cocoamidobetaine, 3% of sodium lauryl amphoacetate, 1% of PEG-7 cocoglyceride, 2% of decyl glucoside, 2% of PEG-80 sorbitan laurate, 4% of glycerol, 0.5% of betaine, a proper amount of preservative and essence, and the balance of deionized water.
The preparation method of the double-layer bath foam comprises the following steps:
1) adding deionized water into an emulsifying pot, respectively adding raw materials of potassium cetyl ether phosphate, sodium lauroyl glutamate, cocamidopropyl betaine, sodium lauryl amphoacetate, PEG-7 cocoyl glyceride, decyl glucoside, PEG-80 sorbitan laurate, sweet almond oil, tea seed oil, tocopherol acetate and glycerol into the emulsifying pot in sequence, heating to 75-80 ℃, and uniformly stirring.
2) Cooling to 40 + -5 deg.C, adding betaine, antiseptic and essence, stirring, and making.
The following are the test examples of the effect application:
the comparison of the using effects of the examples 1, 2 and 3 with the comparative examples 1 (common surface-active bath cream) and 2 (common bath cream containing grease) is shown in the following table 1:
40 test persons (12 persons with dry skin, 16 persons with neutral skin and 12 persons with oily skin; the higher the score is, the easier the water flushing is, the full score is 5).
TABLE 1 test results (unit: min) of examples 1 to 3 and comparative examples 1 to 2
Figure BDA0001338288160000041
Figure BDA0001338288160000051
The results in Table 1 show that examples 1-3 tested with the control: the foam, water flushing, moistening feeling and skin comfort level are obviously better than those of a contrast sample.
Therefore, the double-layer bath foam composition provided by the invention not only has abundant foams, but also has good moistening and comfortable feeling on the skin.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.

Claims (1)

1. A double-layer bath foam, which is characterized by comprising an upper layer solution and a lower layer solution in percentage by weight; the upper layer solution consists of the following components: 3% of potassium cetyl ether phosphate, 2% of sodium lauroyl glutamate, 1% of cocamide betaine, 1% of sodium lauryl amphoacetate, 0.5% of PEG-7 cocoyl glyceride, 1% of decyl glucoside, 1% of PEG-80 sorbitan laurate, 4% of sweet almond oil, 0.5% of tea seed oil, 0.5% of tocopherol acetate, 0.0005-0.01% of preservative and essence, and the balance of deionized water;
the lower layer solution consists of the following components: 8% of potassium cetyl ether phosphate, 6% of sodium lauroyl glutamate, 3% of cocamide betaine, 1% of sodium lauryl amphoacetate, 1% of PEG-7 cocoglyceride, 2% of decyl glucoside, 2% of PEG-80 sorbitan laurate, 4% of glycerol, 0.5% of betaine, 0.0005-0.01% of preservative and essence, and the balance of deionized water.
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CN107982088A (en) * 2017-11-24 2018-05-04 广州市梦采生物科技有限公司 A kind of bilayer cleansing mousse and preparation method thereof
CN111388360A (en) * 2020-03-31 2020-07-10 深圳市美福源日用品有限公司 Bathing essential oil and preparation method thereof
CN112137917A (en) * 2020-11-02 2020-12-29 浙江有北化妆品有限公司 Double-layer bath essence composition
CN112675047B (en) * 2020-12-31 2023-02-10 彭氏(惠州)实业发展有限公司 Double-layer bath foam and preparation method thereof
CN113749953B (en) * 2021-08-26 2022-08-30 广州环亚化妆品科技股份有限公司 Double-layer shower gel with stable milk cover layer and preparation method thereof
CN114259435B (en) * 2021-11-29 2023-09-05 澳宝化妆品(惠州)有限公司 Sulfate-free double-layer cleaning composition
CN114259436B (en) * 2021-11-29 2023-11-17 澳宝化妆品(惠州)有限公司 Double-layer cleaning composition and preparation method thereof

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JPH10101529A (en) * 1996-09-24 1998-04-21 Shiseido Co Ltd Multiphase separation type cleaning agent
CN1275907A (en) * 1996-09-24 2000-12-06 尤尼利弗公司 Liquid compositions comprising stability enhancing surfactants and method of enhancing low temperature stability thereof
JP4129388B2 (en) * 2002-12-24 2008-08-06 株式会社ファンケル Multi-layer cosmetic
JP2011213682A (en) * 2010-03-31 2011-10-27 Naris Cosmetics Co Ltd Foaming cleansing cosmetic
CN103505381A (en) * 2013-09-17 2014-01-15 广州环亚化妆品科技有限公司 Double-layer makeup removal emulsion and preparation method thereof
CN106236613A (en) * 2016-08-31 2016-12-21 彭燕辉 Clear bubble facial milk cleanser of a kind of clean profit and preparation method thereof

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