CN106236613A - Clear bubble facial milk cleanser of a kind of clean profit and preparation method thereof - Google Patents
Clear bubble facial milk cleanser of a kind of clean profit and preparation method thereof Download PDFInfo
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- CN106236613A CN106236613A CN201610799182.2A CN201610799182A CN106236613A CN 106236613 A CN106236613 A CN 106236613A CN 201610799182 A CN201610799182 A CN 201610799182A CN 106236613 A CN106236613 A CN 106236613A
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/10—Washing or bathing preparations
Abstract
The invention belongs to cosmetic technical field, be specifically related to clear bubble facial milk cleanser of a kind of clean profit and preparation method thereof.This bubble facial milk cleanser includes each component of following percentage by weight: mustard seed oil 0.1% 5% is saved at deep-sea two, emulsifying agent 0.04% 2.4%, foaming agent 1% 30%, two phase stratification regulator 0 4%, pH adjusting agent regulation pH to 5.5 7.0, chelating agen 0.01% 0.1%, preservative 0.08% 1%, oil phase 2% 30%, deionized water surplus.The facial milk cleanser novel appearance that the application provides, with front in upper and lower two-layer, all can produce rapidly a large amount of uniform, fine and smooth, abundant foam after the shake several seconds；There is obvious cleaning effect, have obvious moisture feeling with rear without obvious sticky sense, skin, moist tight；To no skin irritation；And damaged skin is had significantly repair improvement result.
Description
Technical field
The invention belongs to cosmetic technical field, be specifically related to clear bubble facial milk cleanser of a kind of clean profit and preparation method thereof.
Background technology
Face cleaning, is that the mode using washing removes the skins such as the sebum of skin of face surface attachment, horny layer chip, perspiration
Physiological metabolism product and dust, microorganism, cosmetics residue etc., be the first step of skin protection, and select face cleaning to produce mistakenly
Product are the roots causing a lot of people skin problem occur.
What common face cleaning product was focused on is all high-efficiency cleaning, pore cleanser, deoils, and but have ignored product itself to skin
Stimulation, in order to improve decontamination, oil removing ability, add the compositions such as the extremely strong surfactant of alkalescence, foaming agent, soap base, and
Our skin is but weakly acidic, and life-time service will be injured；More seriously, the sebum layer of skin also can be destroyed,
Once losing sebum layer, skin is highly susceptible to external injury, and particularly with sensitive skin, this injury is more difficult to the imagination.
Showing through investigation, the women of 51.4% and the male of 38.2% think it oneself is sensitive skin.Further, since various from
So (microorganism, dust, light, heat etc.) and anthropic factor (as life-time service can damage skin containing fruit acid, salicylic acid, tretinoin
And other functional skin care item, also having some in the case of unclear, life-time service adds the product of hormone, causes
Skin collagen degeneration, blood capillary elasticity reduces and fragility increases, and finally results in telangiectasis and atrophoderma, also
There are excessive cleaning skin, repeated multiple times use cleaning product also can damage keratodermatitis.), our skin also becomes more to come
The most sensitive, and then various skin problem occurs: such as corse sweat pore, blackhead, easy long pox, easy allergy etc..
The face cleaning product category provided on existing market is varied, and pH is that the face cleaning product of alkalescence can preferably remove
The dirt of skin surface, but this also destroys the sebum layer of skin simultaneously, makes skin lose the natural cover for defense；PH is weakly acidic
Product is less to the injury of skin, but cleaning dynamics is more weak.The amino acids face cleaning product occurred recently delays to a certain extent
With above-mentioned contradiction, such as amino acid cleansing mousse, this series products while high-efficiency cleaning, stimulation gentle, low, it is adaptable to various
The skin of type.But this series products is mainly provided by part foreign brand name, expensive, ordinary consumer is embarrassed to be accepted.
Through retrieval, it has been disclosed that the Chinese patent application document about face cleaning product more, but these products all exist one
Determine problem, it is impossible to meet the needs of real life, be exemplified below:
1) in Chinese invention patent ZL200710044428.6, a kind of Subacidity skin-moistening synthesis facial soap is disclosed, should
The pH value of faintly acid facial soap is between 4.5-6.5, close to the weak acid environment of human body skin, goes fat power low, and performance is gentle, energy
Enough avoid the stimulation to skin in washing process.But, there is facial soap and easily stick with paste rotten shortcoming in water in this formula, and has sand
Grain sense.
2) Chinese patent application 201510255532.4 discloses a kind of still facial milk cleanser, its by Aloe, Fructus Chaenomelis, Fructus Lycii,
Fructus Gleditsia, Oleum sesami and lecithin are made.This facial milk cleanser use natural material make, safe without toxic side effect, to facial skin without
Stimulation, does not produce foam during use, the crowd being suitable for all kinds of skin quality uses.But oily skin and deep skin are cleaned
Cleaning dynamics poor.
3) Chinese patent application 201410372117.2 discloses a kind of fizzy cleansing cream, emulsifying silicon, PEG-40,
Stearic acid, cetyl alcohol, glycerol, Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, citric acid, propylene glycol, deionized water, gluconic acid chlorine
Oneself is fixed and potassium sorbate prepares.Although this application claims that its cleansing cream provided can produce abundant bubble, have the most clear
Clean performance, but the most do not produce bubble, its clean-up performance is how, is also unknown.
In a word, there are the following problems for the face cleaning product provided in prior art: (1) clean-up performance is poor, it is impossible to effectively go
Dirt except skin surface；(2) there is stronger zest to skin in the fractions in product；(3) skin can effectively be removed
Skin surface, but the natural containment of skin surface is damaged, it is unsuitable for life-time service. simultaneously；(4) cleannes height, character temperature
With, but price is higher, embarrasses ordinary consumer to accept.
Summary of the invention
In order to solve the problems referred to above that in prior art, face cleaning product exists, the application aims to provide one can high-efficient cleaning
Clean, character is gentle, low cost, it is adaptable to the facial milk cleanser of all kinds skin, it is possible not only to effective cleaning skin, for a long time
During use, it is also possible to Glycerin, carry out damaged skin repairing and improve.
In order to realize foregoing invention purpose, it is clean that one of them technical scheme of the application provides the clear bubble of a kind of clean profit
Face breast, it includes each component of following percentage by weight:
Wherein, described deep-sea two save mustard seed oil have another name called Crambe abyssinica seed oil, its rich in skin essential fatty acid omega 3,
Omega 6, omega 9 and docosenoic acid C22:1.
Result of the test shows, deep-sea two is saved mustard seed oil and had the sliding application skinfeel of stronger oxidation stability, silk and preferably
Ground permeability.Functionally Omega-3 can make skin equilibrium moisturizing and keep fit, and strengthens soft and slender cell membrane, makes cell obtain
Sufficient nourishing, is got rid of intracellular refuse effectively；Skin corium is made to secret out of collagen and the elastic fiber of more strength, side
Help and smooth away wrinkles and microgroove, and sturdy gradually in lax skin；The common skin that can alleviate for want of Omega-3 and cause is asked
Topic, including pachylosis, intensive stain, heel be full of cracks, eczema, psoriasis, acne, blackhead and hoary hair etc.；Omega 6 is permissible
Help to reduce percutaneous water loss, maintain the barrier function of skin；Omega 9 can strengthen skin barrier function.So, changing
In cosmetic, addition deep-sea two is saved mustard seed oil and can be formed natural moisture barrier at skin surface, prevent water loss；Make skin soft
Profit is elastic and dynamic.
Preferably, the weight ratio of mustard seed oil and oil phase, foaming agent is saved at described deep-sea two is (1-5): (20-30): (20-
30).The facial milk cleanser prepared in this proportion can effectively remove the horny layer chip of skin surface, cosmetics residue etc.
Dirt, can play moist protective effect to the sebum layer of skin surface again simultaneously.
It is further preferred that it is (1-3) that the weight ratio of mustard seed oil and oil phase, foaming agent is saved at described deep-sea two: (22-26):
(22-26), such as, 1:21:22；3:25:25；2:24:22 or 1:22:26.The facial milk cleanser prepared in this proportion is not only
There is above-mentioned functions, during life-time service, also skin surface is had obvious repair function.
Preferably, described emulsifying agent be HLB value be the nonionic surfactant of 8-18, as being selected from inulin lauryl base ammonia
Carbamate, anhydrous sorbitol laurate, polyoxyethylene sorbitol lanolin derivative, polyoxyethylene sorbitol Cera Flava are derivative
One or more in thing and polyoxyethylene laurel ether；
More preferably inulin lauryl carbamate.
Preferably, also including the emulsion adjuvant of 0.1%-5% in described bubble facial milk cleanser, wherein, described emulsion adjuvant is
Sucrose lauric acid, self emulsifying monoglyceride, tristerin, PEG-100 stearate, the smooth laurate of Pyrusussuriensis, Natrulon H-10
One or more in laurate and Natrulon H-10 stearate；
It is further preferred that described emulsion adjuvant is sucrose lauric acid.
It is further preferred that the weight ratio of described emulsifying agent, emulsion adjuvant and foaming agent is (0.4-2.4): (1-5):
(20-30).The facial milk cleanser foaming abundancy provided in this proportion is little to skin irritation.
Preferably, described foaming agent is the surfactant under faintly acid or neutrallty condition with foaming function, optional
From trideceth sodium sulfate, PEG-80 anhydrous sorbitol laurate, sodium laureth sulfate, laureth-
13 carboxylic acid sodium, C12-16 alkyl androstanediol, C8-14 alkyl androstanediol, lauryl hydroxyl sulfo betaine, lauryl alcohol sulfuric ester
Ammonium, sodium lauroyl sarcosine, lauroyl Herba bromi japonici amino acid sodium, cocamido propyl betaine, Coco-Glucoside, cocoyl hydroxyl
In ethyl imidazol(e) quinoline, cocoyl isethionate and cocos nucifera oil acyl both sexes base oxalic acid disodium and sodium cocoamphoacetate
One or more.
Preferably, described pH adjusting agent is citric acid or its aqueous solution.
Preferably, described chelating agen is EDETATE SODIUM.
Preferably, described preservative is benzoic acid and salt thereof or ester, benzyl alcohol, chlorphenesin, dehydroacetic acid or its salt, double
(methylol) imidazolidinyl urea, diformazan hydroxyl dimethyl hydantoin, phenoxyethanol, sorbic acid and salt, methylisothiozoline
One or more in ketone and hydroxylphenyl ester；
It is further preferred that described hydroxylphenyl ester is in methyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate and butyl hydroxybenzoate
Plant or multiple.
Preferably, described oil phase is Jojoba oil, Fructus oleae europaeae fruit oil, Oleum Vitis viniferae, vaseline, Dormant oils, tetramethylolmethane four
Different monooctyl ester, polydimethylsiloxane, lecithin, octyl dodecanol, Parleam, neopentyl glycol two heptanoate, lavandula angustifolia
One or more in Limnanthes Alba Seed Oil oily, white, caprylic/capric triglyceride and isopropyl myristate.
Herein described two phase stratification regulator, contributes to the balance that regulation is oily, water is biphase, stablizing of promotion system；Excellent
Selection of land, described two phase stratification regulator is Polyethylene Glycol-90M and/or sodium chloride.
Preferably, described bubble facial milk cleanser also includes wetting agent 0.0001%-10%, and/or skin effect agent
0.0001%-30%, wherein, described skin effect agent, can improve the new old generation of cell by stimulating skin key cells
Thank speed and defending performance or suppress the activity of key enzyme, and then playing the new cell ratio of raising, improve skin elasticity, elimination
Wrinkle or promote the function that impaired skin recovers.
It is further preferred that described wetting agent is glycerol, propylene glycol, butanediol, methyl propanediol, dipropylene glycol, poly-sweet
One or more in oil, glycerin polyether and erythritol；
Described skin effect agent be Flos Nelumbinis extract, glucosan, hamamelis extract, camomile extract, trehalose,
One or more in biological polyoses glue, Narcissus Tazetta L. Var extract, glycosphingolipids and Herba portulacae extract.
In one embodiment, described clean profit clear bubble facial milk cleanser, it includes each component of following percentage by weight:
Preferably, in the above-described embodiments, propyl hydroxybenzoate, the weight ratio of Methylisothiazolinone are 1:(1-5), further
It is preferably 1:(2-5), more preferably 1:3.6；
The weight ratio of Dormant oils, caprylic/capric triglyceride and isopropyl myristate is 1:(1-5): (1-5)；Further
It is preferably 1:(1-3): (1-3)；More preferably 1:1:1.
In another embodiment, described clean profit clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The another one technical scheme of the application provides a kind of preparation method preparing above-mentioned bubble facial milk cleanser, and it is concrete
Comprise the steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85-90 DEG C in aqueous phase pot, continues at stirring shape
Add two phase modifiers under state, be sequentially added into oil removing phase after being completely dissolved, each component that deep-sea two is saved outside mustard seed oil, preservative,
After stirring, after being cooled to 45 DEG C, add preservative；
3) oil phase, deep-sea two are saved after mustard seed oil is mixed and stirred for uniformly and be transferred in emulsifying pot, adjust after stirring 5-8 minute
Joint pH to 5.5-7.0；
4) with the speed stirring bottom discharge of 10～15 revs/min.
Preferably, in said method, during stirring, in emulsifying pot, the rotational frequency of stirring motor is 30-50Hz.
Wherein, the preservative with preferable hydrothermal stability also can be in step 2) in be cooled to 45 DEG C before add.
Compared with prior art, the bubble facial milk cleanser that the application provides has a following beneficial effect:
(1) facial milk cleanser that the application provides adds deep-sea two and saves mustard seed oil, due to deep-sea two save in mustard seed oil rich in
Skin essential fatty acid omega 3, omega 6, omega 9 and docosenoic acid C22:1, have stronger oxidation-stabilized
Property, the sliding application skinfeel of silk and preferably permeability so that product is while removing dirt, can be in skin surface shape
Become natural moisture barrier, prevent water loss；Make the soft and moist elasticity of skin and dynamic.
(2) the facial milk cleanser novel appearance that the application provides, with front in upper and lower two-layer, all can produce rapidly big after the shake several seconds
The foam that amount is uniform, fine and smooth, abundant, and foam can stable existence several minutes；Result of the test shows, embodiment 1,2,4 provide
Facial milk cleanser with rear without obvious sticky sense, a punching is the cleanest, has obvious cleaning effect, and the cosmetics that can remove skin surface are residual
Stay the dirts such as thing, and the product that embodiment 1-4 provides has obvious moisture feeling with rear skin, moist tight.
(3) the facial milk cleanser nonirritant that the application provides.Animal test results shows, the embodiment of the present application 1-4 provides
Facial milk cleanser does not all show any skin wound repair.
(4) damaged skin is also had and significantly repairs improvement result by the facial milk cleanser that the application provides.Result of the test shows, by
The facial milk cleanser that the embodiment of the present application 1-4 provides is to the improvement ratio of inflammatory skin all more than 70%, and it is clean that embodiment 3 provides
Face breast effect is the most obvious, the improvement rate of skin be can reach 90%, and commercially available common facial milk cleanser is (as after Korea Spro, lactalbumin is washed one's face
Breast) to inflammatory skin substantially without reparation improvement result.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further elaborated.These embodiments are only in order at purpose of explanation,
And do not limit the scope of the invention and essence.
Embodiment 1
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The method preparing this bubble facial milk cleanser, specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85 DEG C in aqueous phase pot, continues under stirring
Add Polyethylene Glycol-90M, after being completely dissolved, be sequentially added into anhydrous sorbitol laurate, sucrose lauric acid, cocamidopropyl propyl amide
Glycine betaine, sodium chloride and EDETATE SODIUM, stir, and adds chlorphenesin after being cooled to 45 DEG C；
3) Dormant oils, caprylic/capric triglyceride, isopropyl myristate and deep-sea two are saved mustard seed oil to be mixed and stirred for all
It is transferred to after even in emulsifying pot, with citric acid regulation to 6-6.2 after stirring 6 minutes；
4) with the speed stirring bottom discharge of 10 revs/min.
Embodiment 2
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The method preparing this bubble facial milk cleanser, specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85 DEG C in aqueous phase pot, continues under stirring
It is sequentially added into anhydrous sorbitol laurate, sucrose lauric acid, cocamido propyl betaine, sodium chloride and EDETATE SODIUM, stirs
Mix uniformly, after being cooled to 45 DEG C, add phenoxyethanol；
3) it is transferred in emulsifying pot, after stirring 6 minutes after Dormant oils and caprylic/capric triglyceride being mixed and stirred for uniformly
With citric acid regulation to 6-6.2；
4) with the speed stirring bottom discharge of 12 revs/min.
Embodiment 3
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The method preparing this bubble facial milk cleanser, specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 90 DEG C in aqueous phase pot, regulation emulsifying pot stirs
The rotational frequency of motor is 30Hz, adds Polyethylene Glycol-90M, be sequentially added into inulin lauryl after being completely dissolved under stirring
The acid of aminocarbamic acid ester, sucrose lauric, cocamido propyl betaine, sodium lauroyl sarcosine, trideceth sodium sulfate,
Sodium chloride, EDETATE SODIUM, glycerol, Flos Nelumbinis extract, Methylisothiazolinone and Dormant oils, be down to room temperature after stirring；
3) Dormant oils, caprylic/capric triglyceride, isopropyl myristate and deep-sea two are saved mustard seed oil to be mixed and stirred for all
Being transferred to after even in emulsifying pot, regulate to 6.8-7.0 with citric acid after stirring 6 minutes, wherein, the rotational frequency of stirring motor is
50Hz；
4) with the rotational frequency of stirring motor as 30Hz, rotating speed is the speed stirring bottom discharge of 15 revs/min.
Embodiment 4
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The method preparing this bubble facial milk cleanser, specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85 DEG C in aqueous phase pot, regulation emulsifying pot stirs
The rotational frequency of motor is 50Hz, is sequentially added into inulin lauryl carbamate, sucrose lauric acid, self emulsifying monoglyceride, coconut palm
Oleamide CAB, sodium cocoamphoacetate, lauryl hydroxyl sulfo betaine, EDETATE SODIUM, glycerol, fourth two
Alcohol, camomile extract and Bis(hydroxymethyl)imidazolidinyl urea, stir, and adds dehydroacetic acid after being cooled to 45 DEG C；
3) Fructus oleae europaeae fruit oil, Oleum Vitis viniferae and deep-sea two are saved after mustard seed oil is mixed and stirred for uniformly and be transferred to emulsifying pot
In, regulate to 6.8-7.0 with citric acid after stirring 8 minutes, wherein, the rotational frequency of stirring motor is 50Hz；
4) with the rotational frequency of stirring motor as 50Hz, rotating speed is the speed stirring bottom discharge of 15 revs/min.
Comparative example 1
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
The method preparing this bubble facial milk cleanser, specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85 DEG C in aqueous phase pot, regulation emulsifying pot stirs
The rotational frequency of motor is 50Hz, adds Polyethylene Glycol-90M, be sequentially added into polyoxyethylene after being completely dissolved under stirring
Sorbitol lanolin derivative, Natrulon H-10 stearate, cocamido propyl betaine, sodium lauroyl sarcosine, tridecane
Alcohol polyethers sodium sulfate, sodium chloride and EDETATE SODIUM, stir, and adds methyl hydroxybenzoate, methylisothiozoline after being cooled to 45 DEG C
Ketone；
3) it is transferred to emulsifying after Dormant oils, caprylic/capric triglyceride and isopropyl myristate being mixed and stirred for uniformly
In Guo, regulating to 6.8-7.0 with citric acid after stirring 8 minutes, wherein, the rotational frequency of stirring motor is 50Hz；
4) with the rotational frequency of stirring motor as 50Hz, rotating speed is the speed stirring bottom discharge of 15 revs/min.
Comparative example 2
A kind of clean moistening clear bubble facial milk cleanser, it includes each component of following percentage by weight:
Prepare the method for this bubble facial milk cleanser with embodiment 3.
Embodiment 5
1, sensory evaluation test
Method of testing: randomly select healthy skin experimenter 120, the age be 18-40 year, man, female half and half, be randomly divided into
6 groups, often organize 20 people.In the range of selected experimenter's inboard arm 5cm × 6cm healthy skin, in this range above uniform application
Amass the eyebrow pencil for 3cm × 1cm and lipstick.
With water, inboard arm is scribbled the bottle that the skin moisturizing of eyebrow pencil and lipstick, Example 1-4 and comparative example 1,2 prepare
Dress product (specification: 100mL), observe after the 10-15 second that fluctuates foam situation and extrude the foam of a diameter of 0.5-0.8cm in
Above-mentioned wetting zones, gently rubs massage 30s, rinses well with flowing water afterwards with hands.The outward appearance of foam and clear before record foam extrusion
Wash effect, wash rear skinfeel.Result such as table 1 below.
Table 1 the application provide facial milk cleanser outward appearance and cleaning effect, wash rear skinfeel
Result of the test shows, the facial milk cleanser that the embodiment of the present application 1,2,4 provides with front in upper and lower two-layer, equal after the shake several seconds
A large amount of uniform, fine and smooth, abundant foam can be produced rapidly, and foam can stably stand 5-10 minute；With rear without obvious sticky sense,
One punching is i.e. clean, has obvious cleaning effect, can remove the dirt such as cosmetics residue of skin surface, and embodiment 1-4 carries
For the rear skin of product have obvious moisture feeling, moist tight.
2, chmice acute irritation test
Take 120 healthy white mouse, male and female half and half, be randomly divided into 6 groups, often group 20.Test all uses own control.Test
Before, defeathering to be implemented in white mouse ridge back of the body both sides, notes not injuring skin, defeathering scope is 3cm × 5cm, left and right each.Use respectively
The bubble 0.1mL produced after the facial milk cleanser shake that embodiment 1-4 and comparative example 1,2 prepare is applied directly to animal subject side and is good for
On health skin, smear 30s.After use oleic acid paper that this side skin is covered, then be fixed with adhesive plaster and binder.Separately
Side uses same method to process, and changing facial milk cleanser is distilled water.1,24,48 hours the most after experiment, use distilled water cleaning
Tested skin is also observed, and scoring.Standards of grading are with reference to GB 7919-87 safety evaluation of cosmetics program and method.
Wherein, skin wound repair standards of grading reference such as table 2 below, skin irritation emphasizes standards of grading such as table 3 below.Experimental result is as follows
Table 4.
Table 2 skin wound repair standards of grading
Table 3 skin irritation intensity ratings standard
| Intensity | Score value |
| Nonirritant | 0-0.4 |
| Subexcite | 0.5-1.9 |
| Medium zest | 2.0-5.9 |
| Strong and stimulating | 6.0-8.0 |
The facial milk cleanser zest test result that table 4 the embodiment of the present application 1-4 and comparative example 1,2 prepare
Result of the test shows, after tested white mouse skin surface smears the facial milk cleanser that the embodiment of the present application 1-4 provides, does not all go out
What skin wound repair incumbent, between stimulus intensity scoring is for 0-0.4, is nonirritant.But add substantial amounts of in component
During surfactant (such as comparative example 1), facial milk cleanser can cause obvious irritant reaction, and white mouse skin surface produces obvious erythema；
Additionally change other component, such as emulsifying agent, co-emulsifier etc. (comparative example 2), also can cause skin that redness occurs, show certain
Zest.
3, the reparation to skin improves test
Select the female volunteers 160 in 18-40 year and be randomly divided into 8 groups, often organizing 20 people.It is followed successively by tested group of 1-4；Right
According to group 1,2；Control group A, B.The product prepared with embodiment 1-4 and comparative example 1,2 as test products, the happy poem bought from market
After wind cry of certain animals Jizhou Island moisturizing thermal water cleansing mousse (120mL) and Korea Spro, lactalbumin Cleansing Foam (120mL) is respectively reference product
A, B, subject washes one's face with tested products and reference substance respectively, and every day is the most each once, and continuous observation 3 months is added up and remembers
Record result of the test.Result such as table 5 below.
Wherein, the screening criteria of volunteer: corse sweat pore, face have blackhead or acne, easy long pox, easy allergic skin, inflammation
Disease property pimple, pustule etc. have the patient of scytitis.
Effective refer to above-mentioned scytitis be improved significantly；
Effectively refer to that above-mentioned scytitis has been alleviated；
Invalid refer to that above-mentioned scytitis is without any improvement or has increased the weight of.
Improve ratio=(efficiently individual quantity+effective number)/tested number × 100%.
The reparation of skin is improved situation statistics by the facial milk cleanser that table 5 the application provides
By above-mentioned result of the test it can be seen that inflammatory skin is changed by the facial milk cleanser provided by the embodiment of the present application 1-4
Kind ratio is all more than 70%, and the facial milk cleanser effect that embodiment 3 provides is the most obvious, and the improvement rate of skin can reach 90%, and
Commercially available common facial milk cleanser (such as lactalbumin Cleansing Foam after Korea Spro) to inflammatory skin substantially without repair improvement result.
Above-mentioned example is only used as descriptive purpose, and the scope of the present invention is not limited thereto.To those skilled in the art
For modify and be apparent from, the present invention is only limited by scope.
Claims (10)
1. a clean profit clear bubble facial milk cleanser, it includes each component of following percentage by weight:
Facial milk cleanser the most according to claim 1, it is (1-that the weight ratio of mustard seed oil and oil phase, foaming agent is saved at described deep-sea two
5):(20-30):(20-30)；It is preferably (1-3): (22-26): (22-26).
Facial milk cleanser the most according to claim 1, described emulsifying agent be HLB value be the nonionic surfactant of 8-18, choosing
From inulin lauryl carbamate, anhydrous sorbitol laurate, polyoxyethylene sorbitol lanolin derivative, polyoxyethylene
One or more in sorbitol beeswax derivatives and polyoxyethylene laurel ether；It is preferably inulin lauryl carbamate.
Facial milk cleanser the most according to claim 1, also includes the emulsion adjuvant of 0.1%-5%, institute in described bubble facial milk cleanser
Stating emulsion adjuvant is sucrose lauric acid, self emulsifying monoglyceride, tristerin, PEG-100 stearate, the smooth lauric acid of Pyrusussuriensis
One or more in ester, Natrulon H-10 laurate and Natrulon H-10 stearate；It is preferably sucrose lauric acid.
Facial milk cleanser the most according to claim 4, the weight ratio of described emulsifying agent, emulsion adjuvant and foaming agent is (0.4-
2.4):(1-5):(20-30)。
Facial milk cleanser the most according to claim 1, described foaming agent is selected from trideceth sodium sulfate, PEG-80 dehydration mountain
Pears alcohol laurate, sodium laureth sulfate, laureth-13 carboxylic acid sodium, C12-16 alkyl androstanediol, C8-14 alkane
Base glucoside, lauryl hydroxyl sulfo betaine, lauryl alcohol sulfuric ester ammonium, sodium lauroyl sarcosine, lauroyl Herba bromi japonici aminoacid
Sodium, cocamido propyl betaine, Coco-Glucoside, cocoyl hydroxyethyl imidazole quinoline, cocoyl isethionate and coconut palm
One or more in oleoyl both sexes base oxalic acid disodium and sodium cocoamphoacetate；
Described pH adjusting agent is citric acid or its aqueous solution；
Described chelating agen is EDETATE SODIUM；
Described preservative is benzoic acid and salt thereof or ester, benzyl alcohol, chlorphenesin, dehydroacetic acid or its salt, double (methylol) miaow
Oxazolidinyl urea, diformazan hydroxyl dimethyl hydantoin, phenoxyethanol, sorbic acid and salt, Methylisothiazolinone and hydroxy benzenes
One or more in ester；
Described oil phase be Jojoba oil, Fructus oleae europaeae fruit oil, Oleum Vitis viniferae, vaseline, Dormant oils, the different monooctyl ester of tetramethylolmethane four, poly-two
Methylsiloxane, lecithin, octyl dodecanol, Parleam, neopentyl glycol two heptanoate, Oleum lavandula angustifolia, Bai Chihua seed
One or more in oil, caprylic/capric triglyceride and isopropyl myristate；
Described two phase stratification regulator is Polyethylene Glycol-90M and/or sodium chloride.
Facial milk cleanser the most according to claim 6, described hydroxylphenyl ester is methyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate and hydroxyl
One or more in butyl benzenesulfonamide.
8., according to the facial milk cleanser according to any one of claim 1-7, described facial milk cleanser also includes wetting agent 0.0001%-
10%, and/or skin effect agent 0.0001%-30%, described wetting agent be glycerol, propylene glycol, butanediol, methyl propanediol,
One or more in dipropylene glycol, polyglycereol, glycerin polyether and erythritol；
Described skin effect agent is Flos Nelumbinis extract, glucosan, hamamelis extract, camomile extract, trehalose, biology
One or more in polysaccharide gum, Narcissus Tazetta L. Var extract, glycosphingolipids and Herba portulacae extract.
Facial milk cleanser the most according to claim 1, it includes each component of following percentage by weight:
Described propyl hydroxybenzoate, the weight ratio of Methylisothiazolinone are 1:(1-5), preferably 1:(2-5), more preferably 1:
3.6；
The weight ratio of described Dormant oils, caprylic/capric triglyceride and isopropyl myristate is 1:(1-5): (1-5)；It is preferably
1:(1-3):(1-3)；More preferably 1:1:1.
10. the method preparing facial milk cleanser as claimed in any one of claims 1-9 wherein, it specifically includes following steps:
1) each component is weighed by weight；
2) it is transferred in emulsifying pot insulation after deionized water being heated to 85-90 DEG C in aqueous phase pot, continues under stirring
Add two phase modifiers, be sequentially added into oil removing phase after being completely dissolved, each component that deep-sea two is saved outside mustard seed oil, preservative, stirring
After Jun Yun, after being cooled to 45 DEG C, add preservative；
3) oil phase, deep-sea two are saved after mustard seed oil is mixed and stirred for uniformly and be transferred in emulsifying pot, after stirring 5-8 minute, regulate pH
To 5.5-7.0；
4) with the speed stirring bottom discharge of 10-15 rev/min；
Preferably, in said method, during stirring, in emulsifying pot, the rotational frequency of stirring motor is 30-50Hz.
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Effective date of registration: 20190711 Address after: 516000 Yingguang Village Industrial Park, Lilin Town, Zhongkai High-tech Zone, Huizhou City, Guangdong Province Patentee after: Peng Shi (Huizhou) Industrial Development Co., Ltd. Address before: 518103 8-11 Huafa Industrial Park, Fuyuan Road, Fuyong Town, Baoan District, Shenzhen City, Guangdong Province Co-patentee before: Yang Dahai Patentee before: Peng Yanhui Co-patentee before: Gu Kui |