CN114246812B - Skin cleaning composition and preparation method and application thereof - Google Patents
Skin cleaning composition and preparation method and application thereof Download PDFInfo
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- CN114246812B CN114246812B CN202111610371.8A CN202111610371A CN114246812B CN 114246812 B CN114246812 B CN 114246812B CN 202111610371 A CN202111610371 A CN 202111610371A CN 114246812 B CN114246812 B CN 114246812B
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a skin cleaning composition, a preparation method and application thereof, wherein the skin cleaning composition comprises the following components in parts by weight: 10-30 parts of natural grease, 10-80 parts of synthetic ester, 10-80 parts of polyol and 0.5-5 parts of emulsifier. The skin cleaning composition provided by the invention can realize the advantages of warm makeup removal, freshness, no stimulation, strong makeup removal capability, convenience in use and moisturizing property after washing, and meanwhile, the skin cleaning composition has no bitter taste similar to EO series surfactants in commercial makeup removal products, is soft in taste, and can be safely applied to faces, eyes and lips. The skin cleaning composition disclosed by the invention has the advantages that when the skin cleaning composition is smeared, the skin is gently massaged, so that pores are opened, the skin attaching effect is good, the color cosmetics are quickly dissolved and dirt in the pores is thoroughly removed by utilizing the rolling effect of gel, the skin cleaning composition can be quickly emulsified when being wetted by adding water, is extremely easy to wash, and the dirt and the color cosmetics residues are quickly taken away by water flow, so that the skin cleaning composition is clean.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a skin cleaning composition, and a preparation method and application thereof.
Background
In recent years, with the improvement of national income and consumption capability, chinese cosmetics have been greatly developed, which are not available, and consumers actively select various cosmetics to protect and modify skin. Daily-use make-up (including BB creams, lipsticks, lip colors, eyebrow pencils, eye shadows, blushers, etc.) and sun-protection products all contain a large amount of grease, wax grease, silicone oil or oil-dispersion components, and are strong in skin adhesion and difficult to clean with conventional cleansing products on the market, for example: the protective film formed on the skin surface by the sun cream, the pollution particles attached to the barrier cream, the color makeup attached to the mucous membrane of the eyes, blackhead dirt caused by sebum oxidation at the root of eyelashes and deep in pores, dirt attached to the old and waste cutin and the like are difficult to clean, and the following skin problems are easily caused: meibomian gland blockage, dry eye, pigmentation, skin aging, pore blockage, comedones, etc., and even causes an impaired skin barrier. Therefore, the cleansing products are continuously expanded in the market as transition products for connecting the makeup and the skin care products.
The cleansing products commonly used in the market at present comprise cleansing cream, cleansing milk, cleansing gel, cleansing oil, cleansing water, cleansing wet tissue and the like; more makeup removers and makeup removers are used. The cleansing water mainly uses the principle of surfactant micelle to remove makeup, has fresh texture, but has relatively poor makeup removing capability, the commonly used surfactant contains PEG, has large using amount and potential irritation, has bitter taste when used for lips, and is easy to damage skin by repeatedly wiping with cleansing cotton when the cleansing water is used. The cleansing oil is prepared by dissolving cleansing oil by using oil and fat according to a similar compatibility principle, has strong cleansing capability, but is greasy in skin feel after washing, easy to be acne-closed and needs to be further cleaned by using facial cleanser. The two types of common cleansing products have low viscosity, are easy to run off when being smeared, are inconvenient to use and have waste of products. In addition, the existing commercial cleansing products often contain mineral oil, polyethylene wax and the like, and skin allergy is easy to cause when the purity of the components is insufficient, so that along with rapid permeation of color makeup habits, fine and upgrade of skin care requirements and acceleration of life rhythm, the development of a mild cleansing product which does not damage sebum membranes, protects skin barriers and is easy to use is particularly important.
Disclosure of Invention
In order to overcome the problems of the prior art, one of the purposes of the present invention is to provide a skin cleansing composition which uses natural oils and synthetic esters as main makeup removing components, and uses natural source emulsifying agent to prepare gel-like skin cleansing composition.
The second object of the present invention is to provide a method for preparing a skin cleansing composition.
It is a further object of the present invention to provide a use of a skin cleansing composition in cosmetics.
In order to achieve the aim of the invention, the technical scheme adopted by the invention is as follows:
the first aspect of the invention provides a skin cleaning composition, which comprises the following components in parts by weight: 10-30 parts of natural grease, 10-80 parts of synthetic ester, 10-80 parts of polyol and 0.5-5 parts of emulsifier.
Preferably, the emulsifier is a naturally derived emulsifier.
In the skin cleaning composition, 0.5-5 parts of emulsifying agent; preferably, the emulsifier is 0.5-5 parts; further preferably, the emulsifier is 1 to 3 parts.
Preferably, the emulsifier is at least one selected from sodium surfactin, hydrogenated lecithin, sucrose stearate, polyglyceryl-10 oleate, polyglyceryl-2 triisostearate, caprylic/capric glyceride polyglyceryl-10 ester; further preferably, the emulsifier is at least one selected from the group consisting of sodium surfactin, hydrogenated lecithin, polyglyceryl-2 oleate, polyglyceryl-2 triisostearate, caprylic/capric glyceride polyglyceryl-10; still more preferably, the emulsifier is at least one selected from sodium surfactin and hydrogenated lecithin.
In the skin cleansing composition of the present invention, 10-80 parts of polyhydric alcohol; preferably, the polyol is 15-60 parts; further preferably, the polyol is 30 to 40 parts.
Preferably, the polyol is selected from at least one of C2-C12 polyols; further preferably, the polyol is at least one selected from the group consisting of C3-C5 triols and C2-C6 diols; still more preferably, the polyol is at least one of glycerol, dipropylene glycol, 1, 3-propanediol, 1, 3-butanediol, 2, 3-butanediol, 1, 2-pentanediol, 1, 2-hexanediol; more preferably, the polyol is glycerol.
Preferably, the natural oil is a natural vegetable oil.
In the skin cleaning composition, the natural oil is 10-30 parts; preferably, the natural oil is 15-30 parts; still more preferably, the natural oil is 15-25 parts.
Preferably, the natural oil is selected from at least one of wheat germ oil, rice bran oil, corn oil, soybean oil, coconut oil, camellia seed oil, white pool seed oil, sea buckthorn seed oil, sweet almond oil, grape seed oil, macadamia nut seed oil, berhard walnut seed oil, jojoba seed oil, saffron oil, sucrose squalane, jatropha seed oil, dog rose fruit oil and avocado oil; further preferably, the natural oil is at least one selected from rice bran oil, jojoba seed oil, sea buckthorn seed oil, sweet almond oil, ber hard walnut seed oil, white pond flower seed oil, sucrose squalane, saffron oil and wheat germ oil.
In the skin cleaning composition, the synthetic ester is 10-80 parts; preferably, the synthetic ester is 20-60 parts; further preferably, the synthetic ester is 30 to 40 parts.
Preferably, the synthetic ester is selected from at least one of glycerol tri (ethylhexanoate), caprylic/capric acid glyceride, isopropyl myristate, isononyl isononanoate, isononoyl isononanoate, ethylhexyl palmitate, coco caprylic/capric acid ester, cetyl ethyl hexanoate, diisostearyl malate, pentaerythritol tetra (ethylhexanoate), isopropyl lauroyl sarcosinate; further preferably, the synthetic ester is selected from at least one of cetyl ethyl hexanoate, diisostearyl malate, isotridecyl isononanoate, coco caprylic/capric acid ester, caprylic/capric acid glyceride.
Preferably, the skin cleansing composition further comprises at least one of essential oils, additives, thickeners, preservatives, water.
Preferably, the skin cleansing composition further comprises the following components in parts by weight: 0-2 parts of essential oil, 0-5 parts of additive, 0-5 parts of thickener and 0-1 part of preservative.
Preferably, the skin cleansing composition is gel-like.
In the skin cleaning composition, the essential oil is 0 to 2 parts; preferably, the essential oil is 0 to 2 parts, but the essential oil is not 0; further preferably, the essential oil is 0.5 to 1.5 parts.
Preferably, the essential oil is at least one selected from rosemary essential oil, sage essential oil, lavender essential oil, orange peel essential oil, ylang essential oil, tea tree essential oil, geranium essential oil, and chamomile essential oil; further preferably, the essential oil is at least one selected from lavender essential oil, orange peel essential oil, ylang-ylang essential oil, geranium essential oil, chamomile essential oil, rosemary essential oil.
In the skin cleaning composition, 0 to 5 parts of additive is added; preferably, the additive is 0 to 5 parts, but the additive is not 0; further preferably, the additive is 0.5 to 2.5 parts.
Preferably, the additive is at least one selected from rhamnolipid, hyaluronic acid, sodium hyaluronate, sodium polyglutamate, stearoyl polyglucosamine, tremella extract, green orange extract, tea polyphenol, polyaspartic acid, amino acid humectant, pullulanase polysaccharide, erythritol, rhamnose and stachyose.
In the skin cleaning composition, 0 to 5 parts of thickener; preferably, the thickener is 0 to 4 parts; further preferably, the thickener is 0 to 2.5 parts.
Preferably, the thickener comprises an aqueous phase thickener and an oil phase thickener.
Preferably, the aqueous phase thickener comprises at least one of dibutyl ethyl hexanoyl glutamine, dibutyl lauroyl glutamate, polyglycerol-10 behenate/eicosanedioate, xanthan gum, carrageenan.
Preferably, the oil phase thickener comprises at least one of glyceryl behenate/eicosadioate, pentaerythritol behenate, and glyceryl tri-hydroxystearate.
In the skin cleaning composition, 0 to 1 part of preservative is used; preferably, the preservative is 0 to 1 part, but the preservative is not 0; further preferably, the preservative is 0.5 to 1.5 parts.
Preferably, the preservative is at least one selected from phenoxyethanol, ethylhexyl glycerol, octanoyl hydroxamic acid, sodium citrate, and p-hydroxyacetophenone.
The second aspect of the present invention also provides a method for preparing the skin cleansing composition according to the first aspect of the present invention, wherein the method uses a D-phase emulsification method.
Preferably, the D-phase emulsification method comprises the steps of:
s1: mixing polyol, additive, preservative and water to obtain phase A; mixing natural oil, synthetic ester and essential oil to obtain phase B; the phase A or the phase B further comprises the step of adding an emulsifier;
s2: mixing the phase A with the phase B to obtain the skin cleaning composition.
Preferably, the step S1 further includes a step of adding a thickener.
Preferably, the thickener comprises an aqueous phase thickener and an oil phase thickener.
Preferably, in the step S1, the preparation of the phase a further includes a step of adding an aqueous phase thickener; and/or, the preparation of the phase B further comprises the step of adding an oil phase thickener.
Preferably, the mixing step is by means of heated mixing.
Preferably, the heating temperature is 40-100 ℃; further preferably, the heating temperature is 60 to 90 ℃.
Preferably, the mixing step in step S1 uses at least one of stirring, ultrasound, and shaking.
Preferably, the phase a is a clear solution.
Preferably, in the step S2, the mixing step is performed by at least one of stirring, ultrasonic and shaking.
Preferably, in the step S2, the mixing step is performed by stirring.
Preferably, in the step S2, the stirring speed is 400 to 2000rpm.
Preferably, in the step S2, the stirring step uses two-stage stirring.
Preferably, the first section of the two-section stirring adopts a first stirring speed, and the second section adopts a second stirring speed.
Preferably, the first agitation speed is less than the second agitation speed.
Preferably, the first stirring speed is 400-600rpm; further preferably, the first stirring speed is 450-550rpm; still more preferably, the first stirring speed is 500-550rpm
Preferably, the second stirring speed is 800-2000rpm; further preferably, the second stirring speed is 900-1800rpm; still more preferably, the second stirring speed is 1000-1500rpm.
Preferably, the stirring is performed at a first stirring speed before the phase a and the phase B are mixed to form a thick gel, and at a second stirring speed after the mixing to form a thick gel.
Preferably, the edge scraping treatment is performed during the stirring.
Preferably, stirring is continued for 3-10min after the phase A and phase B are fully mixed.
Preferably, stirring is continued for 5min after the phase a and phase B are fully mixed.
Preferably, step S2 further comprises a step of homogenizing the skin cleansing composition as prepared.
Preferably, the homogenization time is 1 to 2 minutes.
Preferably, step S2 further comprises a step of vacuum deaerating the skin cleansing composition obtained.
Preferably, the temperature of the skin cleansing composition in step S2 is reduced before discharging.
Preferably, the temperature of the skin cleansing composition is reduced to no more than 45 ℃.
The third aspect of the present invention also provides the use of the skin cleansing composition provided in the first aspect of the present invention in cosmetics.
Preferably, the above-described skin cleansing composition is applied in a skin cleansing product.
Preferably, the above-described skin cleansing composition is applied in a facial wash product.
Preferably, the facial wash product is a facial cleanser or a facial cleanser.
Preferably, the above-described skin cleansing composition is applied in a make-up removal product.
Preferably, the makeup removing product is makeup removing gel, makeup removing emulsion, makeup removing water, makeup removing oil or makeup removing gel.
The beneficial effects of the invention are as follows: the skin cleaning composition provided by the invention can realize the advantages of warm makeup removal, freshness, no stimulation, strong makeup removal capability, convenience in use and moisturizing property after washing, and meanwhile, the skin cleaning composition has no bitter taste similar to EO series surfactants in commercial makeup removal products, is soft in taste, and can be safely applied to faces, eyes and lips.
The skin cleaning composition disclosed by the invention has the advantages that when the skin cleaning composition is smeared, the skin is gently massaged, so that pores are opened, the skin attaching effect is good, the color cosmetics are quickly dissolved and dirt in the pores is thoroughly removed by utilizing the rolling action of gel, the skin cleaning composition can be quickly emulsified when being wetted by adding water, is extremely easy to rinse, and dirt and color cosmetics residues are quickly taken away by water flow, so that the skin cleaning composition is clean; meanwhile, the components are matched in a synergistic way, so that after the skin is washed off by water, the skin is moist and smooth, and the skin has lasting moisture retention.
The preparation method of the skin cleaning composition has simple process, easy operation, no requirement on equipment and good reproducibility. Different natural oils are wrapped by emulsifying agent and polyalcohol, and D phase emulsification technique is utilized, thereby forming transparent gel-like product.
Drawings
Fig. 1 is an electron micrograph of the skin cleansing composition of example 1.
Fig. 2 is an electron micrograph of the skin cleansing composition of example 2.
Fig. 3 is an electron micrograph of the skin cleansing composition of example 3.
Fig. 4 is an electron micrograph of the skin cleansing composition of example 4.
Fig. 5 is a graph of shear rheology test results of the skin cleansing compositions of examples 1 to 4.
Detailed Description
The conception and the technical effects produced by the present invention will be clearly and completely described below with reference to the drawings and the embodiments so as to fully understand the objects, features and effects of the present invention. It is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments, and that other embodiments obtained by those skilled in the art without inventive effort are within the scope of the present invention based on the embodiments of the present invention.
The raw materials used in examples 1 to 4 and comparative example 1 below were artificially divided into a component a and a component B. The content of each raw material in the component A and the component B is based on the content of the whole skin cleaning composition. The sum of the weight fractions of all the components in examples 1 to 4 is 100%, and if the sum of the components A and B in examples 1 to 4 and comparative example 1 is less than 100%, the balance is water.
Example 1:
the skin cleaning composition in this example comprises a component A and a component B, wherein the component A comprises the following components in percentage by weight: 0.6% of sodium surfactin, 5% of rhamnolipid (content of effective matters is 10%), 0.5% of phenoxyethanol and 27.5% of glycerol; the component B comprises the following components in percentage by weight: 15% of rice bran oil, 3.0% of jojoba seed oil, 1.0% of sea buckthorn seed oil, 1.0% of sweet almond oil, 0.2% of lavender essential oil, 0.2% of orange peel essential oil, 0.2% of ylang essential oil, 18% of glycerol tri (ethylhexanoate), 10% of isotridecyl isononanoate, 10% of cetyl ethyl hexanoate, 2.8% of isopropyl lauroyl sarcosinate and 5% of isostearyl malate.
The skin cleansing composition in this example was prepared using the following steps:
(1) Uniformly mixing rhamnolipid, phenoxyethanol and glycerol according to the formula, dispersing sodium surfactin in the mixture, heating to 50 ℃ until the sodium surfactin is completely dissolved, and uniformly stirring to obtain a component A; uniformly dispersing the component B in the formula amount in advance to obtain the component B;
(2) Stirring at 500rpm, slowly adding the component B into the component A in batches, and when the viscosity of the formed gel is high, increasing the stirring speed to 1000rpm, and continuously stirring to enable the gel to be uniform and smooth; adding water according to transparency, defoaming, discharging, and preparing the skin cleaning composition in the example.
Example 2
The skin cleansing composition in this example comprises a component a and a component B, wherein: the A component comprises the following components in percentage by weight: 1, 3-propanediol 1%, glycerol 12%, stearoyl polyglucosamine 0.1%, water 4%, sodium citrate 0.01%; the component B comprises the following components in percentage by weight: hydrogenated lecithin 1.5%, polyglycerin-10 oleate 4.25%, polyglycerin-2 oleate 0.75%, polyglycerin-2 triisostearate 5%, bull's hard walnut seed oil 10%, white pool seed oil 3.0%, sucrose squalane 5.0%, geranium essential oil 0.2%, rosemary essential oil 0.2%, chamomile essential oil 0.1%, isononyl isononanoate 10%, cetyl ethyl hexanoate 15%, coco caprylic/capric acid 5%, caprylic/capric triglyceride 22.89%.
The skin cleansing composition in this example was prepared using the following steps:
(1) Heating and dissolving the component A and the component B respectively at 80 ℃ and uniformly mixing;
(2) Slowly adding the component A into the component B at a stirring speed of 500rpm, and when the viscosity of the formed gel is high, increasing the stirring speed to 1000rpm, and continuously stirring to enable the gel to be uniform and smooth; the gel-like skin cleansing composition thus obtained was cooled to 25℃and discharged after deaeration, to thereby obtain a skin cleansing composition in this example.
Example 3
The skin cleansing composition in this example comprises a component a and a component B, wherein: the A component comprises the following components in percentage by weight: 3.0% of polyglycerol-10 behenate/eicosanedioate, 1.5% of polyglycerol-10 stearate, 1.2% of sucrose stearate, 60% of glycerol, 1.0% of dipropylene glycol, 0.2% of sodium hyaluronate, 0.3% of phenoxyethanol, 0.2% of ethylhexyl glycerol and 1.6% of water; the component B comprises the following components in percentage by weight: saffron oil 5%, sweet orange oil 1%, isononyl isononanoate 8%, cetyl alcohol (ethyl hexanoate) 15%, glyceryl behenate/eicosanedioate 2%.
The skin cleansing composition in this example was prepared using the following steps:
(1) Under the stirring speed of 500rpm at 80 ℃, the component A and the component B are respectively heated and dissolved independently and are evenly mixed;
(2) Slowly adding the component A into the component B at a stirring speed of 500rpm, and when the viscosity of the formed gel is high, increasing the stirring speed to 1500rpm, and continuously stirring to enable the gel to be uniform and smooth; cooling the gel-like skin cleaning composition to 60deg.C, and stopping stirring; cooling to room temperature, and discharging to obtain the skin cleaning composition.
Example 4
The skin cleansing composition in this example comprises a component a and a component B, wherein: the A component comprises the following components in percentage by weight: pullulanase polysaccharide 0.2%, rhamnose 0.2%, stachyose 0.1%, dibutyl ethyl hexanoyl glutamine 1.39%, dibutyl lauroyl glutamate 0.61%, 1, 2-pentanediol 5%, glycerol 10%, p-hydroxyacetophenone 0.5%, water 1.5%; the component B comprises the following components in percentage by weight: wheat germ oil 25%, cetyl ethyl hexanoate 20%, polyglycerol-10 dioleate 18%, caprylic/capric triglyceride 15.0%, polyglycerol-2 oleate 2.5%.
The specific preparation steps of the skin cleansing composition in this example are as follows:
(1) Heating and dissolving the component A and the component B respectively and uniformly mixing at 90 ℃ and at a stirring speed of 500rpm;
(2) Slowly adding the component A into the component B at the stirring speed of 500rpm at the temperature of 90-100 ℃, increasing the stirring speed to 1000rpm when the viscosity of the formed gel is high, continuously stirring to fully mix, stopping stirring, cooling to room temperature, and bottling to obtain the skin cleaning composition in the example.
Comparative example 1
The skin cleaning composition in this example comprises a component A and a component B, wherein the component A comprises the following components in percentage by weight: rhamnolipid (content of effective matter 10%) 5%, phenoxyethanol 0.5%, glycerol 26.2%; the component B comprises the following components in percentage by weight: 2% of glyceryl monostearate, 15% of rice bran oil, 3.0% of jojoba seed oil, 1.0% of sea buckthorn seed oil, 1.0% of sweet almond oil, 0.2% of lavender essential oil, 0.2% of orange peel essential oil, 0.1% of ylang-ylang essential oil, 18% of glycerol tri (ethylhexanoate), 10% of isotridecyl isononanoate, 10% of cetyl ethyl hexanoate, 2.8% of isopropyl lauroyl sarcosinate and 5% of isostearyl malate.
The skin cleansing composition in this example was prepared using the following phase inversion emulsification procedure:
(1) Uniformly mixing the rhamnolipid, phenoxyethanol and glycerin according to the formula amount to prepare a component A; heating the component B in the formula amount to 50 ℃ until the component B is completely dissolved, and dispersing the component B uniformly in advance to obtain the component B;
(2) Stirring at a stirring speed of 500rpm, slowly adding the component A into the component B in batches, and when the viscosity of the formed emulsion is high, increasing the stirring speed to 1500rpm, and continuously stirring to enable the emulsion to be uniform and smooth; after defoaming, discharging to prepare the skin cleansing composition in this example.
Comparative example 2
The skin cleansing composition in this example comprises the following components in percentage by weight: 9.5% of PEG-20 glycerol tristearate, 9.5% of sorbitol polyether-30 tetraisostearate, 20.0% of cetyl ethyl hexanoate, 51% of ethylhexyl palmitate, 5.0% of isononyl isononanoate and 5.0% of glycerol tris (ethyl hexanoate).
The skin cleansing composition in this example was prepared using the following mixing procedure:
all the raw materials in the formula amount are mixed and stirred at the stirring speed of 1000rpm, heated to 85 ℃, kept for 10 minutes, stirred and cooled to room temperature, and discharged to prepare the skin cleaning composition in the example.
Performance test:
(1) Storage stability test
The skin cleansing composition samples of examples 1 to 4 and comparative examples 1 to 2 were tested for storage stability under the following individual test conditions: (1) storing for 1 month at a temperature of 50 ℃; (2) storing for 1 month at a temperature of 5 ℃; (3) storing for 1 month at a temperature of-20 ℃; (4) The preparation method comprises the steps of storing for 24 hours at 50 ℃, storing for 24 hours at-20 ℃ and circulating for three times. After the test is completed, the appearance of the skin cleansing composition sample is observed to change. The specific test results are shown in table 1.
TABLE 1 storage stability
As is clear from Table 1, the skin cleansing compositions of examples 1 to 4 each have excellent storage stability and are less likely to deteriorate during storage.
(2) And (3) observing by a microscope:
samples of the skin cleansing compositions of examples 1 to 4 were smeared onto glass slides, respectively, and observed and recorded using an Olympus electron microscope, and specific results are shown in fig. 1 to 4. From fig. 1, it can be seen that the skin cleansing composition of example 1 has a layered structure; from fig. 2, it can be seen that the skin cleansing composition of example 2 has a vesicle structure; it can be seen from fig. 3 and 4 that the skin cleansing compositions of example 3 and example 4 are both of a common emulsion structure.
(3) Shear rheology test:
the viscosity profile of the skin cleansing compositions of examples 1 to 4 was measured at 25℃ using a Haake Mars Modular Advanced Rheometer System rheometer using a frequency sweep mode, rotor P35/Ti, and the results are shown in FIG. 5. As can be seen from FIG. 5, the viscosity of the skin cleansing compositions of examples 1 to 4 decreased rapidly as the shear rate increased. From this, it is apparent that the skin cleansing compositions of examples 1 to 4 have excellent spreadability, and the viscosity of the skin cleansing composition decreases during the spreading process.
(4) Particle size testing:
the particle size of the skin cleansing composition samples in examples 1 to 4 and comparative examples 1 to 2 was measured using a malvern nanoparticle size analyzer, and the specific test method was: firstly, preparing a sample into a 0.1% aqueous solution, uniformly dispersing, taking 1mL of the solution, placing the solution into a sample cell of a particle size analyzer, and measuring the particle size of the sample at 25 ℃. The results are shown in Table 2. As can be seen from table 2: the skin cleansing compositions of examples 1 to 4 had particle diameters between 0.1 and 1 μm, and had smaller particle diameters than those of comparative examples 1 to 2.
(5) Safety evaluation:
human skin patch test:
number of human subjects: 5 people;
age: between 25 and 45 years old;
gender: female;
the patch method comprises the following steps: the normal skin on the curved side of the forearm of the subject was cleaned and wiped dry, the protective paper of the plaque test tape was removed, 0.1g of the test substances in examples 1 to 4 and comparative examples 1 to 2 were dropped into the plaque tester, the plaque test tape was firmly stuck from bottom to top, stuck flat and air was discharged with a palm light pressure. After 24 hours, the test substance was removed, and skin reactions were observed at 0.5 hours, 6 hours, 12 hours, 24 hours, and 48 hours after the removal, and the results were recorded according to the skin reaction classification standard in the cosmetic hygiene Specification, and the specific results are shown in Table 2 below.
Eye and lip irritation test:
the subjects applied make-up products to the skin at the corners of the eyes and lips, and after 10 minutes, applied and removed make-up using the skin cleansing compositions prepared in examples 1 to 4 and comparative examples 1 to 2. In use, the skin cleansing composition is first applied uniformly to the eyes and lips, gently massaged, and after about 1 minute the eye and lip irritation is evaluated. The results are shown in Table 2.
Table 2 skin cleansing composition particle size and irritation
-indicating no stimulus
As can be seen from Table 2, the skin cleansing composition prepared by the present invention has a small particle size and no irritation to skin, eyes and lips.
(6) And (3) testing the cleansing effect:
number of human subjects: 5 people;
age: between 25 and 45 years old;
gender: female;
the testing method comprises the following steps: the normal skin on the curved side of the forearm of the subject was cleaned and wiped dry, and a waterproof eyeliner, lipstick, BB cream was applied to the forearm, dried for 10min, and 0.1g of the skin cleansing composition test sample of examples 1 to 4 and comparative example 2 was added dropwise, and the skin cleansing composition was subjected to circling massage, then to a small amount of water massage, and finally to rinsing with water and wiping off water. The average score was calculated from 5 scale comparisons of skin cling, spreadability, cleaning power, rinse-out, and moisturization. Scoring criteria: the skin cleansing compositions of examples 1 to 4 were tested for skin temperature change before and after application, skin keratinous moisture content before application, and after 30 minutes of removal of the skin cleansing composition, with a score of 1 to 5, 5 being the best and 1 being the worst. The specific test results are shown in tables 3, 4 and 5.
Table 3 cleaning force
| Sample to be tested | BB cream | Waterproof eyeliner | Lipstick |
| Example 1 | 4.5 | 4 | 4.5 |
| Example 2 | 4.5 | 4 | 4.5 |
| Example 3 | 4.5 | 3.5 | 4.5 |
| Example 4 | 4.5 | 4 | 4.5 |
| Comparative example 2 | 4 | 3 | 4 |
TABLE 4 cleansing effect
TABLE 5 skin temperature and moisture variation of keratinous materials
As can be seen from tables 3 to 5, the skin cleansing compositions of examples 1 to 4 of the present invention have a slightly increased skin temperature during use, and have good cleansing power, skin-sticking property, spreadability and rinsing property, without secondary cleansing with a facial cleanser; after application, the skin is smooth, and high horny moisture content is maintained. The invention adopts the emulsifying agent of natural source, solves the problem that the existing emulsifying agent can cause irritation and dehydration when being used on sensitive skin.
As can be seen from tables 1 to 5, the skin cleansing compositions prepared in examples 1 to 4 all have excellent storage stability, smaller particle size, good cleansing power, skin adhesion, spreadability and rinsing performance, and are not irritating to the skin, and compared with examples 3 and 4, examples 1 and 2 have more excellent performance, example 1 uses sodium surfactin as an emulsifier, example 2 uses hydrogenated lecithin as an emulsifier, both can obtain higher viscosity gel without adding a polymer, and the lamellar structure formed in example 1 and the vesicle structure formed in example 2 can effectively wrap up high-content oily components, are opened during application to enable the active components to be rapidly adhered to the skin, are rapidly emulsified in water, are combined with water after washing and discharging, and are smooth and water-locking, and have optimal comprehensive performance.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.
Claims (7)
1. A skin cleansing composition characterized by: the skin cleaning composition comprises the following components in parts by weight: 10-30 parts of natural oil, 10-80 parts of synthetic ester, 10-80 parts of polyalcohol and 0.5-5 parts of emulsifier; the emulsifier is at least one of sodium surfactin, hydrogenated lecithin, sucrose stearate, polyglycerol-10 oleate, polyglycerol-2 triisostearate and caprylic/capric glyceride polyglycerol-10 ester;
the preparation method of the skin cleaning composition adopts a D-phase emulsification method;
the D-phase emulsification method comprises the following steps:
s1: mixing polyol, additive, preservative and water to obtain phase A; mixing natural oil, synthetic ester and essential oil to obtain phase B; the preparation of the phase A or the phase B further comprises the step of adding an emulsifying agent;
s2: mixing the phase A with the phase B to prepare the skin cleaning composition;
the mixing step adopts a heating mixing mode;
the heating temperature is 40-100 ℃;
in the step S2, the stirring step adopts two-section stirring;
the first section of the two-section stirring adopts a first stirring speed, and the second section adopts a second stirring speed;
the first stirring speed is 500-550rpm;
the second stirring speed is 1000-1500rpm;
stirring at a first stirring speed before the phase A and the phase B are mixed to form thick gel, and stirring at a second stirring speed after the phase A and the phase B are mixed to form thick gel;
step S2 further comprises the step of vacuum deaerating the skin cleansing composition obtained.
2. The skin cleansing composition of claim 1, wherein: the natural oil is selected from at least one of wheat germ oil, rice bran oil, corn oil, soybean oil, coconut oil, camellia seed oil, white pool flower seed oil, sea buckthorn seed oil, sweet almond oil, grape seed oil, macadamia nut seed oil, berr hard walnut seed oil, jojoba seed oil, saffron oil, sucrose squalane, siberian rose seed oil, dog tooth rose fruit oil and avocado oil.
3. The skin cleansing composition of claim 1, wherein: the synthetic ester is at least one of glycerol tri (ethylhexanoate), caprylic/capric glyceride, isopropyl myristate, isononyl isononanoate, isononoyl isononanoate, ethylhexyl palmitate, coco caprylic/capric ester, cetyl ethylhexanoate, diisostearyl malate, pentaerythritol tetra (ethylhexanoate) and isopropyl lauroyl sarcosinate.
4. A skin cleansing composition according to any one of claims 1 to 3, characterized in that: the skin cleaning composition further comprises at least one of essential oil, additive, thickener, preservative and water; the thickener comprises an aqueous phase thickener and an oil phase thickener.
5. The skin cleansing composition of claim 1, wherein: the skin cleaning composition also comprises the following components in parts by weight: 0-2 parts of essential oil, 0-5 parts of additive, 0-5 parts of thickener and 0-1 part of preservative.
6. The skin cleansing composition of claim 4, wherein: the skin cleansing composition is gel-like.
7. Use of a skin cleansing composition according to any one of claims 1 to 6 in the preparation of a cosmetic.
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