CN110327235A - It is a kind of to play close soft cleansing mousse and preparation method thereof - Google Patents
It is a kind of to play close soft cleansing mousse and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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Abstract
Close soft cleansing mousse and preparation method thereof is played the present invention relates to a kind of, the cleansing mousse includes methylglucosamine, fatty acid, surfactant, PEG-75 sher butter glyceride type and water.These above-mentioned substances are combined together by the present invention for the first time, are interacted between component, synergistic, the cleansing mousse foaming abundancy made is careful, can infiltrate into the small pore of deep layer, thoroughly cleaning pore, the removal residual dirt of color make-up, it easily rinses, while also having effects that nourish skin.The preparation method of cleansing mousse of the present invention can guarantee that all materials uniformly mix in the cleansing mousse, form the continuous mixture of stable uniform, it is come into full contact between each component, interaction, it is synergistic, the cleansing mousse foaming abundancy that makes, strong cleaning force, property are mild, soft not tight after washing.In addition, cleansing mousse of the present invention is few using raw material, formula is simple, and easy to operate, high production efficiency can substantially reduce production energy consumption.
Description
Technical field
The present invention relates to daily personal care fields, and in particular to a kind of cleansing mousse and preparation method thereof, more particularly to it is a kind of
Play close soft cleansing mousse and preparation method thereof.
Background technique
Skin care item one of of the face cleaning product as skin basic nursing indispensability, are constantly subjected to consumer and greatly pay close attention to.Mesh
The preceding more popular face cleaning product in the market still face cleaning cream based on soap base system is fine and smooth with foaming abundancy, clean energy
The advantages that power is strong, Yi Chongxi receives the favor of the majority of consumers, but its is inconvenient to use, and the lotion extruded needs first to use hand
Or bubble net gets foam, wastes time a little for the people of present fast pace life.
Cleansing mousse cooperates special vacuum to press pump head, presses lightly on, and moment can extrude foam, and directly upper face is clear
It is clean, it uses conveniently, is more liked by young consumers.Cleansing mousse in the market can substantially be divided into soap base system, amino
Acid surfaces surfactant system.Wherein soap base system pH is higher, and cleaning capacity is strong, slightly has tight feeling after washing.Amino acid surface activity
Agent system is generally weakly acidic, close with skin ph, very mild compared with soap base system, but cleaning capacity is on the weak side, rinses speed
Spend it is slow, after washing slightly have residual feel.
CN105456081A discloses a kind of cleansing mousse and preparation method thereof, the patent formulation with amino acid foaming agent and
The shortcomings that coconut oil foaming agent is principal cleaning ingredients, and system is mild, but there are cleaning capacity is slightly weak and easy residual, makes for a long time
Certain stimulation is generated to skin with meeting.
CN107260579A discloses a kind of mild face cleaning bubble and preparation method thereof, and the patent is living using amino acid surface
The collocation of property agent and soap base, although foaming abundancy is fine and smooth, pH is higher close with Soap-base facial cleanser, and degreasing power is strong, has washed
Tight feeling.
Therefore it provides a kind of foaming abundancy is careful, cleaning capacity is strong, and the mild non-stimulated mousse type face cleaning of Yi Chongxi produces
Product have great importance and vast market prospect in daily cosmetics field.
Summary of the invention
In view of the deficiencies of the prior art, close soft cleansing mousse and its preparation side are played the purpose of the present invention is to provide a kind of
Method, the cleansing mousse include methylglucosamine, fatty acid, surfactant, PEG-75 sher butter glyceride type and water.This
Invention passes through the cooperation of methylglucosamine and other components, and the cleansing mousse foaming abundancy made is careful, can infiltrate into deep layer
In small pore, thoroughly cleaning pore, the residual dirt of color make-up, is easily rinsed, while also having effects that nourish skin.
To achieve this purpose, the present invention adopts the following technical scheme:
In a first aspect, the present invention provides a kind of close soft cleansing mousse of bullet, the cleansing mousse includes methylglucosamine, rouge
Fat acid, surfactant, PEG-75 sher butter glyceride type and water.
The present invention for the first time by methylglucosamine, fatty acid, surfactant, PEG-75 sher butter glyceride type and water this
A little substances are combined together, and are interacted between component, and synergistic, the cleansing mousse foaming abundancy made is careful, can seep
Thoroughly into the small pore of deep layer, thoroughly cleaning pore, the removal residual dirt of color make-up, are easily rinsed, while also having the function for nourishing skin
Effect.
In addition, present invention uses medical grade raw material methylglucosamine (purchase is in Suzhou Jingye Medicine & Chemical Co., Ltd.)
As the neutralizer of the cleansing mousse, the pH value for the cleansing mousse that can make is lower than general soap base system down to 8.3, and
And methylglucosamine is made through glucose reduction amination, source is mild, and can also be with the fatty acid in formula, surface-active
Agent and PEG-75 sher butter glyceride type are synergistic, so that the foam of the cleansing mousse is careful mild, easily rinse,
Skin can also be nourished simultaneously.
In addition to this, the application also uses PEG-75 sher butter glyceride type, the PEG-75 sher butter glycerol
Esters are the water soluble nonionic surfactants in shea butter source, and the stimulation of surfactant in formula can be effectively reduced
Property, and the steady of foaming structure can be improved with fatty acid, surfactant and the methylglucosamine synergy in formula
It is qualitative, keep foam more careful, while also having a Dimethicone Copolyol, washes rear skin softness and do not do.
As the preferred technical solution of the present invention, the cleansing mousse includes the component of following mass percent: methyl Portugal
Osamine 3-16%, fatty acid 2-15%, surfactant 2-18%, PEG-75 sher butter glyceride type 0.1-2% and surplus
Water.
Each component cooperates under above-mentioned extra fine quality ratio, synergy, the cleansing mousse foaming abundancy made,
Strong cleaning force, property are mild and soft not tight after washing, using cleansing mousse of the present invention skin hydration rate after cleaning
1h can reach 78% or more, and 3h can also remain to 40% or more after cleaning.
Methylglucosamine 3-16% in the present invention, for example, can be 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%,
11%, 12%, 13%, 14%, 15% or 16% etc..
Fatty acid 2-15%, for example, can be 2%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%,
13%, 14% or 15% etc..
Surfactant 2-18%, for example, can be 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, 11%,
12%, 13%, 14%, 15%, 16%, 17% or 18% etc..
PEG-75 sher butter glyceride type 0.1-2%, for example, can be 0.1%, 0.3%, 0.4%, 0.5%,
0.8%, 0.9%, 1%, 1.1%, 1.3%, 1.5%, 1.9% or 2% etc..
Preferably, the fatty acid in lauric acid, myristic acid, palmitinic acid or stearic acid any one or at least
Two kinds of combination, preferably lauric acid and/or myristic acid；The combination is typical but non-limiting example has: lauric acid and meat
Myristic acid, lauric acid and palmitinic acid, lauric acid and stearic acid, myristic acid and palmitinic acid, myristic acid and stearic acid, palmitinic acid
With stearic acid etc..
Preferably, the surfactant is selected from cocounut oil acyl glycine potassium, sodium methyl cocoyl taurate, methyl cocoyl
Acyl taurines sodium taurocholate, sodium cocoyl glycinate, sodium lauroyl sarcosine, cocounut oil acyl disodium glutamate, cocounut oil acyl both sexes
Any one in base diethyl acid disodium, lauryl hydroxyl sulfo betaine, Plantacare 818 or Cocoamidopropyl betaine
Or at least two combination, preferably methyl cocoyl taurine sodium taurocholate.
Preferably, the cleansing mousse further includes emollient.
Preferably, mass percentage of the emollient in cleansing mousse is 0.5-3%, such as can be 0.5%,
0.7%, 0.9%, 1%, 1.5%, 1.9%, 2%, 2.2%, 2.5%, 2.9% or 3% etc..
Preferably, the emollient is selected from olive oil PEG-7 esters and/or phytosterol/octyl dodecanol lauroyl paddy
Propylhomoserin ester, preferably olive oil PEG-7 esters.
Wherein, described " phytosterol/octyl dodecanol lauroyl glutamate ester " is a kind of natural origin grease, belongs to day
Right renewable raw materials have good moistening skin-care effect.
Preferably, the cleansing mousse further includes preservative.
Preferably, mass percentage of the preservative in cleansing mousse is 0.7-3.5%, such as be can be
0.7%, 0.8%, 0.9%, 1%, 1.5%, 1.9%, 2%, 2.3%, 2.5%, 2.8%, 3%, 3.2% or 3.5%.
Preferably, the preservative appointing in 1,2- hexylene glycol, parahydroxyacet-ophenone, sodium benzoate, Phenoxyethanol
It anticipates a kind of or at least two combinations, the combination of preferably 1,2- hexylene glycol, sodium benzoate and Phenoxyethanol.
Preferably, the cleansing mousse further includes essence.
Preferably, mass percentage of the essence in cleansing mousse is 0.01-0.2%, such as be can be
0.01%, 0.02%, 0.05%, 0.07%, 0.09%, 0.1%, 0.13%, 0.15%, 0.17%, 0.18% or 0.2%
Deng.
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 3-16%, fatty acid 2-
15%, surfactant 2-18%, PEG-75 sher butter glyceride type class 0.1-2%, emollient 0.5-3%, preservative
0.7-3.5%, essence 0.01-0.2% and excess water.
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 2-9%, lauric acid
2.5-10%, myristic acid 0.5-5%, methyl cocoyl taurine sodium taurocholate 2.0-18%, PEG-75 sher butter are sweet
Grease class 0.1-2%, 1,2- hexylene glycol 0.5-2.5%, sodium benzoate 0.1-0.4%, Phenoxyethanol 0.1-0.5%, olive oil
PEG-7 esters 0.5-3%, essence 0.01-0.2% and excess water.
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 3-8%, lauric acid
2.5-6%, myristic acid 1.5-4%, methyl cocoyl taurine sodium taurocholate 5-10%, PEG-75 sher butter glyceride
Class 0.5-1%, 1,2- hexylene glycol 0.5-1.5%, sodium benzoate 0.2-0.4%, Phenoxyethanol 0.2-0.5%, olive oil PEG-7
Esters 1.5-3%, essence 0.05-0.2% and excess water.
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 7.5%, lauric acid
5%, myristic acid 3%, methyl cocoyl taurine sodium taurocholate 10%, PEG-75 sher butter glyceride type 0.5%, 1,
2- hexylene glycol 1.5%, sodium benzoate 0.25%, Phenoxyethanol 0.3%, olive oil PEG-7 esters 1.5%, essence 0.1% and remaining
Measure water.
Second aspect, the present invention provide a kind of preparation method of close soft cleansing mousse of bullet as described in relation to the first aspect, institute
State preparation method the following steps are included:
(1) methylglucosamine and water are mixed, obtains the first mixed liquor；
(2) it is sweet that fatty acid, surfactant and PEG-75 sher butter are added in the first mixed liquor obtained to step (1)
Grease class, mixing, obtains the second mixed liquor；
(3) optionally preservative, optionally emollient and optionally fragrant are added in the second mixed liquor obtained to step (2)
Essence mixes, and filtering obtains the cleansing mousse.
Preferably, step (1) mixing is to carry out at 75-80 DEG C, such as can be 75 DEG C, 76 DEG C, 77 DEG C, 78
DEG C, 79 DEG C or 80 DEG C etc..
Preferably, step (2) further include: before the mixing, fatty acid is saponified, obtains saponification liquor.
Preferably, the time of the saponification be 20-60min, such as can be 20min, 25min, 30min, 35min,
40min, 45min, 50min, 55min or 60min etc..
Preferably, the temperature of the saponification is 80-85 DEG C, such as can be 80 DEG C, 81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C or 85
DEG C etc..
Preferably, step (2) further include: after the saponification, the saponification liquor is cooled to 60-65 DEG C, such as
It can be 60 DEG C, 61 DEG C, 62 DEG C, 63 DEG C, 64 DEG C or 65 DEG C etc..
Preferably, step (3) further include: the optionally preservative, optionally emollient and optionally essence is being added
Before, the second mixed liquor that step (2) obtains first is cooled to 30-50 DEG C, for example, can be 30 DEG C, 32 DEG C, 35 DEG C, 38 DEG C,
40 DEG C, 42 DEG C, 45 DEG C, 48 DEG C, 49 DEG C or 50 DEG C etc..
Preferably, step (3) further include: before the mixing, will optionally emollient and optionally essence carry out it is pre-
First mix.
Preferably, described be filtered into of step (3) is filtered using 500 mesh filter screens.
Preferably, the preparation method comprises the following steps:
(1) methylglucosamine and water are mixed, is heated to 75-80 DEG C, obtains the first mixed liquor；
(2) fatty acid is added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to 80-85 DEG C, stirs
Mix, be pumped into emulsion pot, be maintained at 75-80 DEG C of saponification 30min, saponification terminates to be cooled to 60-65 DEG C, be added surfactant with
PEG-75 sher butter glyceride type, mixing, obtains the second mixed liquor；
(3) the second mixed liquor that step (2) obtains is cooled to 30-50 DEG C, add optionally preservative and optionally
The mixed liquor of ground emollient and optionally essence mixes, and filtering obtains the cleansing mousse.
Preparation method of the present invention can guarantee that all materials uniformly mix in the cleansing mousse, forms stable uniform and connects
Continuous mixture comes into full contact between each component, interacts, synergistic, the cleansing mousse foaming abundancy that makes, cleaning
Power is strong, property is mild, soft not tight after washing.
Compared with the existing technology, the invention has the following advantages:
(1) present invention uses medical grade raw material methylglucosamines as the neutralizer of the cleansing mousse, can make to obtain
Cleansing mousse pH value down to 8.5 hereinafter, being lower than general soap base system, and methylglucosamine can also be with the fat in formula
Acid, surfactant and PEG-75 sher butter glyceride type are synergistic, the careful temperature of the foam of the cleansing mousse made
With easily rinse, while skin can also be nourished, using the skin hydration rate after 1h up to the skin hydration after 78% or more, 3h
Rate is being maintained at 40% or more, and any skin is suitble to use；
(2) preparation method of the present invention can guarantee that all materials uniformly mix in the cleansing mousse, forms stable uniform and connects
Continuous mixture comes into full contact between each component, interacts, synergistic, the cleansing mousse foaming abundancy that makes, cleaning
Power is strong, property is mild, soft not tight after washing；
(3) cleansing mousse of the present invention is few using raw material, and formula is simple, and easy to operate, high production efficiency can drop significantly
Low production energy consumption.
Detailed description of the invention
Fig. 1 is the initial foam state diagram for the cleansing mousse that embodiment 1 and comparative example 1-5 are prepared.
Fig. 2 is the foam state figure after the cleansing mousse 30min that embodiment 1 and comparative example 1-5 are prepared.
Fig. 3 is that the skin hydration rate curve graph after cleansing mousse use is prepared in embodiment 1-9 and comparative example 1-7.
Specific embodiment
The present invention is described in more detail below.But following examples is only simple example of the invention, not generation
Table or limitation the scope of the present invention, protection scope of the present invention are subject to claims.
Embodiment 1
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is shown in Table 1.
The present embodiment cleansing mousse the preparation method is as follows:
(1) methylglucosamine and water are mixed, is heated to 75 DEG C, obtains the first mixed liquor；
(2) lauric acid and myristic acid are added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to
82 DEG C, stirring is pumped into emulsion pot, is maintained at 80 DEG C of saponification 30min, and saponification terminates to be cooled to 60 DEG C, and methyl cocoyl acyl is added
Base taurine sodium taurocholate and PEG-75 sher butter glyceride type, mixing, obtain the second mixed liquor；
(3) olive oil PEG-7 esters and essence are premixed, obtains premixed liquid, then second that step (2) is obtained mixes
It closes liquid and is cooled to 45 DEG C, 1,2- hexylene glycol, sodium benzoate, Phenoxyethanol and the premixed liquid is added, mixing is filtered using 500 mesh
Net filtration discharging, obtains the cleansing mousse.
Embodiment 2
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is shown in Table 1.
The present embodiment cleansing mousse the preparation method is as follows:
(1) methylglucosamine and water are mixed, is heated to 80 DEG C, obtains the first mixed liquor；
(2) lauric acid and myristic acid are added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to
85 DEG C, stirring is pumped into emulsion pot, is maintained at 75 DEG C of saponification 30min, and saponification terminates to be cooled to 65 DEG C, and methyl cocoyl acyl is added
Base taurine sodium taurocholate and PEG-75 sher butter glyceride type, mixing, obtain the second mixed liquor；
(3) olive oil PEG-7 esters and essence are premixed, obtains premixed liquid, then second that step (2) is obtained mixes
It closes liquid and is cooled to 50 DEG C, 1,2- hexylene glycol, sodium benzoate, Phenoxyethanol and the premixed liquid is added, mixing is filtered using 500 mesh
Net filtration discharging, obtains the cleansing mousse.
Embodiment 3
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is shown in Table 1.
The present embodiment cleansing mousse the preparation method is as follows:
(1) methylglucosamine and water are mixed, is heated to 78 DEG C, obtains the first mixed liquor；
(2) lauric acid and myristic acid are added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to
80 DEG C, stirring is pumped into emulsion pot, is maintained at 77 DEG C of saponification 30min, and saponification terminates to be cooled to 62 DEG C, and methyl cocoyl acyl is added
Base taurine sodium taurocholate and PEG-75 sher butter glyceride type, mixing, obtain the second mixed liquor；
(3) olive oil PEG-7 esters and essence are premixed, obtains premixed liquid, then second that step (2) is obtained mixes
It closes liquid and is cooled to 30 DEG C, 1,2- hexylene glycol, sodium benzoate, Phenoxyethanol and the premixed liquid is added, mixing is filtered using 500 mesh
Net filtration discharging, obtains the cleansing mousse.
Embodiment 4
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is shown in Table 1.
The present embodiment cleansing mousse the preparation method is as follows:
(1) methylglucosamine and water are mixed, is heated to 76 DEG C, obtains the first mixed liquor；
(2) lauric acid and myristic acid are added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to
82 DEG C, stirring is pumped into emulsion pot, is maintained at 76 DEG C of saponification 30min, and saponification terminates to be cooled to 63 DEG C, and methyl cocoyl acyl is added
Base taurine sodium taurocholate and PEG-75 sher butter glyceride type, mixing, obtain the second mixed liquor；
(3) olive oil PEG-7 esters and essence are premixed, obtains premixed liquid, then second that step (2) is obtained mixes
It closes liquid and is cooled to 45 DEG C, 1,2- hexylene glycol, sodium benzoate, Phenoxyethanol and the premixed liquid is added, mixing is filtered using 500 mesh
Net filtration discharging, obtains the cleansing mousse.
The formula of cleansing mousse in embodiment 1-4 is shown in Table 1:
Table 1
Embodiment 5
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is as follows:
A phase: methylglucosamine 3%, excess water；
B phase: palmitinic acid 1.25%, stearic acid 3%；
C phase: cocounut oil acyl glycine potassium 2%, PEG-75 sher butter glyceride type 2%；
D phase: 1,2- hexylene glycol 1%, sodium benzoate 0.25%, Phenoxyethanol 1.3%, 0.5% and of olive oil PEG-7 esters
Essence 0.1%.
The preparation method of the present embodiment is same as Example 1.
Embodiment 6
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is as follows:
A phase: methylglucosamine 5.35%, excess water；
B phase: lauric acid 8%, stearic acid 6.5%；
C phase: sodium methyl cocoyl taurate 18%, PEG-75 sher butter glyceride type 0.1%；
D phase: 1,2- hexylene glycol 1%, sodium benzoate 0.25%, Phenoxyethanol 1.3%, 0.5% and of olive oil PEG-7 esters
Essence 0.1%.
The preparation method of the present embodiment is same as Example 1.
Embodiment 7
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is as follows:
A phase: methylglucosamine 8%, excess water；
B phase: lauric acid 7%, palmitinic acid 1.55%；
C phase: Plantacare 818 10%, PEG-75 sher butter glyceride type 1%；
D phase: 1,2- hexylene glycol 1%, sodium benzoate 0.25%, Phenoxyethanol 1.3%, 0.5% and of olive oil PEG-7 esters
Essence 0.1%.
The preparation method of the present embodiment is same as Example 1.
Embodiment 8
It present embodiments provides and a kind of plays close soft cleansing mousse and preparation method thereof
Wherein, the mass percentage of the cleansing mousse each component is as follows:
A phase: methylglucosamine 10%, excess water；
B phase: lauric acid 5%, palmitinic acid 6.7%；
C phase: Plantacare 818 5%, methyl cocoyl taurine sodium taurocholate 5%, PEG-75 sher butter glyceride
Class 1%；
D phase: 1,2- hexylene glycol 1%, sodium benzoate 0.25%, Phenoxyethanol 1.3%, 0.5% and of olive oil PEG-7 esters
Essence 0.1%.
The preparation method of the present embodiment is same as Example 1.
Embodiment 9
Present embodiments provide it is a kind of play close soft cleansing mousse and preparation method thereof, the difference with embodiment 1 is only that,
Without D phase.
Comparative example 1
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, is not added with
PEG-75 sher butter glyceride type.
Comparative example 2
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, utilizes smart ammonia
Methylglucosamine is substituted in acid.
Comparative example 3
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, utilizes ammonia first
Methylglucosamine is substituted in base propyl alcohol.
Comparative example 4
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, utilizes three second
Methylglucosamine is substituted in hydramine.
Comparative example 5
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, utilizes hydrogen-oxygen
Change potassium and methylglucosamine is substituted.
Comparative example 6
This comparative example provides a kind of cleansing mousse and preparation method thereof, and the difference with embodiment 1 is only that, utilizes cocounut oil
PEG-75 sher butter glyceride type is substituted in amido propyl betaine.
Comparative example 7
This comparative example is the cleansing mousse of certain commercially available famous brand name, and ingredient includes water, propylene glycol, sorb (sugar) alcohol, the moon
Cinnamic acid, myristic acid, Plantacare 818, -6 carboxylic acid of laureth, potassium hydroxide, lauryl hydroxyl sulfo betaine etc..
Performance test and result statistics
1, foam effect compares
The cleansing mousse of embodiment 1 and comparative example 1-5 preparation is respectively adopted, carries out foam effect test experiments.Foam effect
The method of fruit test are as follows: compared using the foam of same press pump packaging material, same dynamics and compression number.Observation just start and
The state of foam, the result is shown in Figure 1 and Fig. 2 are pumped out after 30min.
As seen from Figure 1, the foam of embodiment 1 is the most careful thick and solid, flexible；Comparative example 1, comparative example 2, comparative example
3 and 5 foam of comparative example it is general, careful degree is poorer than embodiment 1, foam loosely without elasticity；4 foam of comparative example is sparse, table
It is existing worst.And comparative example 2 and 3 characteristic odor of comparative example are larger, need to add a large amount of essence and go to cover smell, with essence and
The addition of solubilizer, system irritation further enhance.Figure it is seen that embodiment 1 is also able to maintain good bubble after 30min
Foam state, and the foam of comparative example 1-5 starts to become loose sparse, but the foam state of comparative example 1 should be than comparative example 2-5.
It can be seen that in conjunction with Fig. 1 and Fig. 2 and make the mousse system foam of neutralizer better than other neutralizations with methylglucosamine
Agent, this is because can phase interworking between methylglucosamine, fatty acid, surfactant and PEG-75 sher butter glyceride type
It closes, synergistic, the foam for generating the cleansing mousse being prepared is careful thick and solid flexible, hence it is evident that be better than containing other neutralizations
The formula system of agent.In addition, compared with Example 1, the cleansing mousse of PEG-75 sher butter glyceride type is free of in comparative example 1
Foam state it is obviously poor, this illustrate PEG-75 sher butter glyceride type in system have increase foam, stable foam
Effect.
2, skin moisture content is tested
The preparation of 2.1 samples
The cleansing mousse of embodiment 1-9 and comparative example 1-7 preparation is respectively adopted, carries out test below.
2.2 test equipment
The skin moisture content Corneometer test of German Courage+Khazaka company (German CK company) manufacture
Probe.Using the capacitance of keratoderma before and after the apparatus measures use, the variation of water content of stratum corneum is measured.
2.3 test early-stage preparations
Healthy crowd 320, skin is chosen, the age at 20~45 years old, is divided into 16 groups, every group of 7 males, 13 women, often
A sample in group difference testing example 1-9 and comparative example 1-7.Any product cannot be used (to change within 15 days before recipient site
Cosmetic or topical drug or health care product for oral administration).Before test, it is desirable that subject cleans both hands forearm, wet into 22 ± 1 DEG C of temperature
Sit quietly 30min in the constant temperature and humidity room of degree 50 ± 5%, and keeps relaxation state.Then 3 are marked in tester or so forearm side
×3cm2The square Experimental Area of size, using left arm as the test zone of product, the corresponding symmetrical region of right arm is blank
Control, then the moisture content that probe detects each Test sites is tested with Corneometer, it is repeated 5 times respectively, obtains each survey
The average value of examination records data.Calculation formula are as follows:
Hydration rate (%)=(test value-blank value) × 100/ blank value
2.4 test result
The skin hydration rate of the different time intervals measured the results are shown in Table 2, and skin hydration curve is shown in Fig. 3.
2 different time intervals skin hydration rate (%) of table
As shown in Table 2, after using cleansing mousse 1 hour described in embodiment 1-9, skin hydration rate is higher than 78%, wherein real
The performance of keeping humidity for applying the cleansing mousse of example 1 is most excellent, and skin hydration rate is up to 83.29% after 1 hour, this is because methyl
Amine, fatty acid, methyl cocoyl taurine sodium taurocholate and PEG-75 sher butter glyceride type are assisted under reasonable proportion
Same-action, the cleansing mousse of preparation provide not only effective cleaning power, and have reached nourishing while cleaning skin and protected
The effect of wet.
Compared with Example 1, PEG-75 sher butter glyceride type is free of in the cleansing mousse of comparative example 1, subject makes
After 1 hour, moisture content of skin is on a declining curve, and cocamidopropyl betaine is used in the cleansing mousse of comparative example 6
PEG-75 sher butter glyceride type is substituted, subjects skin's water content is also decreased obviously, it can be seen that PEG-75 butter
Resin glyceride type has good skin-moisturizing, skin effect.
The cleansing mousse of comparative example 2-4 is free of methylglucosamine, is replaced with other neutralizers, and cleansing mousse cleaning capacity becomes
Weak, moistening effect is general, has tight feeling using rear skin；The cleansing mousse of comparative example 5 is free of methylglucosamine potassium hydroxide
Instead of cleaning force is stronger, and skin moisturization is very poor, and it is tight to be easy drying using rear skin.
Using after the cleansing mousse of embodiment 1-9 and comparative example 1-7, skin hydration of the subject in different time intervals point
Rate is as shown in figure 3, using after cleansing mousse 3 hours of embodiment 1-9, and in the case where not smearing other skin care item, skin is still
Water content with higher, skin hydration rate have reached 40% or more, and after using the cleansing mousse of comparative example 1-7, skin water
Conjunction rate is below 35%.
3, erythrocyte hemolysis is tested
3.1 test samples: embodiment 1-9 and comparative example 1-7 is respectively adopted and carries out erythrocyte hemolysis experiment.
3.2 test methods: erythrocyte hemolysis experiment is the alternative of lagophthalmos stimulation test, and basic principle is to pass through measurement
Hemoglobin the amount of dissolution and denaturation degrees carry out damage of the evaluating chemical product to ocular tissue's cell.It is mainly molten by red blood cell in the world
Blood is tested to evaluate cosmetics and its raw material to the irritation of eye.It is real according to the RBC of European alternative authentication center (ECVAM)
Test method for testing and grade scale determine test result, with specific reference to (ECVAM.ECVAM DB-ALM:INVITIONX
Protoco,Red blood cells test system.INVITOX No.37Ispra.Italy:ECVAM,1994.).Knot
Fruit grade scale is as follows:
3 ECVAM cosmetic product RBC of table tests irritation grade scale
| L/D | Classification |
| >100 | It is nonirritant |
| 10 L/D≤100 < | Microstimulation |
| 1 L/D≤10 < | Slight stimulation |
| 0.1 L/D≤10 < | Moderate irritation |
| L/D≤0.1 | Severe irritation |
3.3 test result
The erythrocyte hemolysis experimental result of the embodiment 1-9 and comparative example 1-7 that measure are shown in Table 4.
The erythrocyte hemolysis experimental result of 4 each sample of table
| Sample | pH | HC50(mg/L) | DI (%) | L/D | Evaluation result |
| Embodiment 1 | 8.27 | 9513.54 | 93.43 | 101.83 | It is nonirritant |
| Embodiment 2 | 8.26 | 9227.83 | 92.25 | 100.03 | It is nonirritant |
| Embodiment 3 | 8.26 | 8553 | 84.02 | 99.43 | Microstimulation |
| Embodiment 4 | 8.27 | 8227 | 88.87 | 92.57 | Microstimulation |
| Embodiment 5 | 8.40 | 8335 | 92.35 | 90.25 | Microstimulation |
| Embodiment 6 | 8.31 | 8756 | 98.98 | 88.46 | Microstimulation |
| Embodiment 7 | 8.25 | 8845 | 99.15 | 89.21 | Microstimulation |
| Embodiment 8 | 8.29 | 8231 | 94.00 | 87.56 | Microstimulation |
| Embodiment 9 | 8.26 | 7562 | 98.97 | 76.41 | Microstimulation |
| Comparative example 1 | 8.30 | 4995 | 85.12 | 58.69 | Microstimulation |
| Comparative example 2 | 8.85 | 3980 | 90.09 | 44.18 | Microstimulation |
| Comparative example 3 | 8.70 | 4015 | 90.1 | 44.56 | Microstimulation |
| Comparative example 4 | 8.93 | 3695 | 91.2 | 40.52 | Microstimulation |
| Comparative example 5 | 9.49 | 1560 | 92.59 | 16.85 | Microstimulation |
| Comparative example 6 | 8.29 | 4430 | 96.58 | 45.87 | Microstimulation |
| Comparative example 7 | 9.50 | 854 | 77.62 | 11 | Microstimulation |
Remarks: HC50 is half erythrocyte hemolysis concentration；DI is hemoglobin degenerative index；L/D is the ratio of HC50 and DI
Value.
As shown in Table 4, the pH of embodiment 1 and embodiment 2 is lower and the mildest.The cleansing mousse of comparative example 1 is free of
PEG-75 sher butter glyceride type, it is sweet that using cocamidopropyl betaine PEG-75 sher butter is substituted in comparative example 6
Grease class is in microstimulation.The L/D data of comparative example 1 and comparative example 1 and comparative example 6 can be seen that PEG-75 ox
The addition of oleoresin glyceride type can not only improve foam, nourish skin, can significantly reduce the irritation of sample, be close to or reach
To nonirritant rank.The cleansing mousse of comparative example 2-5 is that other neutralizers replace methylglucosamine, and pH value compares methylglucosamine
System is higher, is in microstimulation, wherein making the mousse irritation maximum of neutralizer of potassium hydroxide.
4, normal individual trial evaluation test
4.1 test populations: healthy 20 people of skin subject of face is selected, the age, men and women was fifty-fifty at 20-45 years old, it is desirable that by
Examination person's health cannot use other any cosmetics or other drugs during test, avoid staying up late, smoke and keeping clear
Light diet, to cosmetics hyperesthesia, can accurately be judged by Normalization rule cosmetics after use.
4.2 test samples: being test sample with embodiment 1 and comparative example 7.
4.3 test methods: every kind of cleansing mousse uses 2 weeks, daily each 1 time of morning and evening, and subject is according in use process
Feel to score, using 5 points of systems, 1 point worst for effect for scoring, and 5 points best for effect, the results are shown in Table 5.It is right in use process
Sample foams richness, cleaning force, easy cleaning degree, is evaluated with rear tight feeling foam sophistication, and wherein highest is divided into 5
Point, it is minimum to be divided into 1 point.
4.4 test result
The practical effect of sample is tracked and recorded, the feedback opinion and finishing analysis of collecting test person, statistics
It the results are shown in Table 5.
5 normal individual trial result average value of table
| Number | Foaming abundancy degree | Foam sophistication | Cleaning force | Easy cleaning degree | With rear tight feeling |
| Embodiment 1 | 4.9 | 4.8 | 4.8 | 4.9 | 4.8 |
| Comparative example 7 | 4.0 | 3.9 | 4.3 | 4.2 | 3.5 |
By 5 result of table as it can be seen that the result of human trial evaluation is poor the effect of significantly contrasting embodiment 1 and comparative example 7
Not.The cleansing mousse foam of embodiment 1 is soft, exquisiteness is abundant, Yi Chongxi, and without dry and astringent tight feeling after use, skin slip moistens；
The higher cleansing mousse pH value of comparative example 7 is 9.50, and long-time service can destroy skin barrier, and it is tight existing to wash rear skin appearance
The case where using moderate stimulation eyes as, some subject feedbacks, use feeling is bad.
In conclusion the close soft cleansing mousse of bullet of the invention, foaming abundancy exquisiteness, strong cleaning force, safety are mild, after washing
Skin softness is not done.Methylglucosamine after neutralization is reasonably being matched with surfactant, PEG-75 sher butter glyceride type
It acts synergistically than lower performance, the cleansing mousse of preparation provides not only effective cleaning power, and has also achieved and nourish moisturizing
The effect of.PEG-75 sher butter glyceride type and olive oil PEG-7 esters can form layer protecting film in skin surface simultaneously,
Have effects that water lock moisturizing, moisturizing, a kind of wash has been prepared and has protected two-in-one cleansing mousse.
The Applicant declares that the present invention is explained by the above embodiments detailed construction feature of the invention, but the present invention is simultaneously
It is not limited to above-mentioned detailed construction feature, that is, does not mean that the present invention must rely on above-mentioned detailed construction feature and could implement.Institute
Belong to those skilled in the art it will be clearly understood that any improvement in the present invention, to the equivalence replacement of component selected by the present invention
And increase, selection of concrete mode of accessory etc., all of which fall within the scope of protection and disclosure of the present invention.
Claims (10)
1. a kind of play close soft cleansing mousse, which is characterized in that the cleansing mousse includes methylglucosamine, fatty acid, surface
Activating agent, PEG-75 sher butter glyceride type and water.
2. cleansing mousse according to claim 1, which is characterized in that the cleansing mousse includes following mass percent
Component: methylglucosamine 3-16%, fatty acid 2-15%, surfactant 2-18%, PEG-75 sher butter glyceride type
0.1-2% and excess water.
3. cleansing mousse according to claim 1 or 2, which is characterized in that the fatty acid is selected from lauric acid, nutmeg
In acid, palmitinic acid or stearic acid any one or at least two combination, preferably lauric acid and/or myristic acid；
Preferably, the surfactant is selected from cocounut oil acyl glycine potassium, sodium methyl cocoyl taurate, methyl cocoyl
Taurine sodium taurocholate, sodium cocoyl glycinate, sodium lauroyl sarcosine, cocounut oil acyl disodium glutamate, cocounut oil acyl both sexes base two
In acetic acid disodium, lauryl hydroxyl sulfo betaine, Plantacare 818 or Cocoamidopropyl betaine any one or extremely
Few two kinds of combination, preferably methyl cocoyl taurine sodium taurocholate.
4. cleansing mousse according to claim 1-3, which is characterized in that the cleansing mousse further includes moisturizing
Agent；
Preferably, mass percentage of the emollient in cleansing mousse is 0.5-3%；
Preferably, the emollient is selected from olive oil PEG-7 esters and/or phytosterol/octyl dodecanol lauroyl glutamate
Ester, preferably olive oil PEG-7 esters.
5. cleansing mousse according to claim 1-4, which is characterized in that the cleansing mousse further includes anti-corrosion
Agent；
Preferably, mass percentage of the preservative in cleansing mousse is 0.7-3.5%；
Preferably, the preservative is any one in 1,2- hexylene glycol, parahydroxyacet-ophenone, sodium benzoate, Phenoxyethanol
Kind or at least two combination, the combination of preferably 1,2- hexylene glycol, sodium benzoate and Phenoxyethanol.
6. cleansing mousse according to claim 1-5, which is characterized in that the cleansing mousse further includes essence；
Preferably, mass percentage of the essence in cleansing mousse is 0.01-0.2%.
7. cleansing mousse according to claim 1-6, which is characterized in that the cleansing mousse includes following quality
The component of percentage: methylglucosamine 3-16%, fatty acid 2-15%, surfactant 2-18%, PEG-75 sher butter are sweet
Grease class class 0.1-2%, emollient 0.5-3%, preservative 0.7-3.5%, essence 0.01-0.2% and excess water；
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 2-9%, lauric acid 2.5-
10%, myristic acid 0.5-5%, methyl cocoyl taurine sodium taurocholate 2-18%, PEG-75 sher butter glyceride type
0.1-2%, 1,2- hexylene glycol 0.5-2.5%, sodium benzoate 0.1-0.4%, Phenoxyethanol 0.1-0.5%, olive oil PEG-7 ester
Class 0.5-3.0%, essence 0.01-0.2% and excess water；
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 3-8%, lauric acid 2.5-
6%, myristic acid 1.5-4%, methyl cocoyl taurine sodium taurocholate 5-10%, PEG-75 sher butter glyceride type
0.5-1%, 1,2- hexylene glycol 0.5-1.5%, sodium benzoate 0.2-0.4%, Phenoxyethanol 0.2-0.5%, olive oil PEG-7 ester
Class 1.5-3.0%, essence 0.05-0.2% and excess water；
Preferably, the cleansing mousse includes the component of following mass percent: methylglucosamine 7.5%, lauric acid 5%, meat
Myristic acid 3%, methyl cocoyl taurine sodium taurocholate 10%, PEG-75 sher butter glyceride type 0.5%, 1,2- oneself two
Alcohol 1.5%, sodium benzoate 0.25%, Phenoxyethanol 0.3%, olive oil PEG-7 esters 1.5%, essence 0.1% and excess water.
8. a kind of any one of -7 preparation method for playing close soft cleansing mousse according to claim 1, which is characterized in that described
Preparation method the following steps are included:
(1) methylglucosamine and water are mixed, obtains the first mixed liquor；
(2) fatty acid saponification is added in the first mixed liquor obtained to step (1), adds surfactant and PEG-75 butter
Resin glyceride type, mixing, obtains the second mixed liquor；
(3) optionally preservative, optionally emollient and optionally essence are added in the second mixed liquor obtained to step (2),
Mixing, filtering, obtains the cleansing mousse.
9. preparation method according to claim 8, which is characterized in that step (1) it is described mixing be at 75-80 DEG C into
Row；
Preferably, step (2) further include: before the mixing, fatty acid is saponified, obtains saponification liquor；
Preferably, the time of the saponification is 20-60min；
Preferably, the temperature of the saponification is 80-85 DEG C；
Preferably, step (2) further include: after the saponification, the saponification liquor is cooled to 60-65 DEG C；
Preferably, step (3) further include: optionally preservative, optionally emollient and optionally before essence is being added, first will
The second mixed liquor that step (2) obtains is cooled to 30-50 DEG C；
Preferably, step (3) further include:, will optionally emollient and optionally essence is mixed in advance before the mixing
It closes；
Preferably, described be filtered into of step (3) is filtered using 500 mesh filter screens.
10. preparation method according to claim 8 or claim 9, which is characterized in that the preparation method comprises the following steps:
(1) methylglucosamine and water are mixed, is heated to 75-80 DEG C, obtains the first mixed liquor；
(2) fatty acid is added in the first mixed liquor obtained to step (1), puts into oily phase pot, is heated to 80-85 DEG C, stir, take out
Enter in emulsion pot, be maintained at 75-80 DEG C of saponification 30min, saponification terminates to be cooled to 60-65 DEG C, and surfactant and PEG- is added
75 sher butter glyceride types, mixing, obtain the second mixed liquor；
(3) the second mixed liquor that step (2) obtains is cooled to 30-50 DEG C, adds optionally preservative and optionally moistened
The mixed liquor of skin agent and optionally essence mixes, and filtering obtains the cleansing mousse.
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