CN111759783A - Tea bran essence-containing care shampoo and preparation method thereof - Google Patents
Tea bran essence-containing care shampoo and preparation method thereof Download PDFInfo
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- CN111759783A CN111759783A CN202010811610.5A CN202010811610A CN111759783A CN 111759783 A CN111759783 A CN 111759783A CN 202010811610 A CN202010811610 A CN 202010811610A CN 111759783 A CN111759783 A CN 111759783A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/14—Drugs for dermatological disorders for baldness or alopecia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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Abstract
The invention relates to the technical field of shampoo, and particularly relates to a maintenance shampoo containing tea bran essence and a preparation method thereof. The feed comprises the following raw materials: the tea bran essence-containing hand sanitizer has a good scale removal effect by adding the tea bran essence, can keep hair black and bright, repair damaged hair, supplement nutrients for the hair, has the effects of removing dandruff and relieving itching, can prevent alopecia and hair loss, has a hair growth effect, belongs to natural raw materials, is non-toxic and harmless, and not only has the effects of removing dandruff and relieving itching, but also has the effects of bacteriostasis and sterilization by mixing salt and borax.
Description
Technical Field
The invention relates to the technical field of shampoo, and particularly relates to a maintenance shampoo containing tea bran essence and a preparation method thereof.
Background
Shampoo, also called shampoo, shampoo or shampoo cream, is a shampoo product which is most widely applied, is one of the most commonly used hair cosmetics, is used for cleaning grease, sweat stain, cells which are shed from the scalp, foreign dust, microorganisms, residues and bad smell of a setting product and the like which are secreted by a human body and are attached to the scalp and hair, and keeping the scalp and the hair clean and attractive, and the modern society has more and more rapid pace of life, brings a plurality of problems of irregular work and rest, high mental stress, frequent insomnia and the like, and the hair health problem, especially the problem of more dandruff and scalp itching, which are difficult to solve by people for a long time, so that in order to facilitate the use of people with different hair qualities, various types of shampoo are produced;
with the increasing variety of shampoos, people have continuous requirements on the performances of the shampoos. However, the shampoo in the current market has the following problems:
1. the effect of relieving itching and removing dandruff after use is poor;
2. it has no sterilizing ability.
Disclosure of Invention
The invention aims to provide a care shampoo containing tea bran essence and a preparation method thereof, and aims to solve the problems in the background art.
In order to achieve the above purpose, in one aspect, the invention provides a care shampoo containing tea bran essence, which comprises the following raw materials: 15-30% of tea bran essence, 10-35% of surfactant, 0.3-0.5% of conditioner, 0.5-1.5% of pearling agent, 0.1-0.5% of thickening agent, 0.1-0.5% of preservative, 0.3-0.7% of essence, 0.1-0.5% of neutralizer and the balance of deionized water.
The tea bran contains tea saponin in the liquid juice directly mashed with the tea bran and soaked with water, has good scale removal effect, is commonly used for washing hair and clothes, can keep the hair black and bright, repair damaged hair and supplement nutrients for the hair when being used for washing the hair, does not have dandruff when being used for washing the hair, relieves itching, can prevent alopecia and hair loss, has hair growth effect, does not contain any chemical raw material, is nontoxic and safe, and is the best choice for the pregnant woman to wash the hair.
As a further improvement of the present technical solution, the surfactant includes a primary surfactant and a secondary surfactant;
the main surface active agent is one or more of K12, AES, AESA, K12A and AESS, the main surface active agent is K12 and AESS, the dosage is 10-25%, and the main surface active agent mainly plays roles of foaming, cleaning hair and the like;
the auxiliary surfactant is one or more of CAB, SHD, APG, coconut oil fatty acid diethanolamide, imidazoline and amino acid, the auxiliary surfactant is CAB and coconut oil fatty acid diethanolamide, the dosage is 1-10%, and the auxiliary surfactant mainly plays a role in auxiliary foaming, thickening, foam stabilization and reduction of stimulation of the main surfactant.
As a further improvement of the technical scheme, the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property and antistatic property, damaged hair quality is repaired, the hair is soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the hair to be adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses on improving the combing property during the wet hair.
As a further improvement of the technical scheme, the thickening agent is salt and borax, the thickening principle is that after electrolyte is added, micelle on the surface swells, the movement resistance is increased, the viscosity on the surface is increased, the borax is weak alkali and has weak bacteriostasis effect like boric acid, a culture medium contains 10% of borax by using a flat plate method, and the borax has inhibition effect on escherichia coli, pseudomonas aeruginosa, bacillus anthracis, shigella flexneri, shigella, typhoid bacillus, paratyphoid bacillus, proteus, staphylococcus and candida albicans, and has good effects on eliminating scalp itching and reducing scurf after salt is added into a small amount of borax and put into a basin and a proper amount of clear water is added to dissolve the borax and wash the hair.
As a further improvement of the technical scheme, the preservative is DMDM hydantoin, has a preservative effect on the shampoo, and prolongs the shelf life of the shampoo.
As a further improvement of this solution, the neutralizing agent is citric acid, which is required for some of the highly alkaline ingredients used in shampoo.
On the other hand, the invention provides a preparation method of a care shampoo containing tea bran essence, which comprises any one of the above care shampoos containing tea bran essence, and the operation steps are as follows:
s1, adding a main surfactant into a stirring kettle, adding a proper amount of deionized water, and heating;
s2, adding the auxiliary surfactant into a stirring kettle, and uniformly stirring to completely dissolve the surfactant;
s3, adding the thickening agent into the solution, and uniformly stirring to form a consistency;
s4, reducing the temperature, adding a conditioner and a pearling agent, and uniformly stirring to completely dissolve;
s5, adding the tea bran essence, and uniformly stirring to completely dissolve the tea bran essence;
s6, reducing the temperature, adding the preservative and the essence, and stirring uniformly;
s7, adding a neutralizer to adjust the pH value of the solution, and stirring at a low speed;
s8, standing overnight for defoaming, and finishing the preparation.
The preparation method of the invention has the advantages of simple process, convenient operation, low cost and easy industrial production, and the prepared ginseng effervescent tablet has uniform components and stable quality.
Preferably, in the S1-S3, the heating temperature of the stirring kettle is 70-80 ℃, the stirring time is 1-2 hours, the raw materials are completely dissolved, and the phenomenon of insoluble particles or agglomeration of the product is avoided.
Preferably, in the S4-S5, the temperature is reduced to 55-65 ℃, and the stirring time is 1-2 hours, so that the raw materials are fully dispersed, and transparent particles with different sizes are avoided.
Preferably, in S6-S7, the temperature is reduced to 40-50 ℃, the stirring time is 0.5-1.5h, the pH value of the solution is adjusted to 5.0-6.0, and the low-speed stirring time is 0.5-1h, so that the solution is fully mixed, and the pH value is more suitable for human bodies to use.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the tea bran essence-containing care shampoo and the preparation method thereof, the tea bran essence is added, so that the care shampoo has a good scale removal effect, can keep hair black and bright, repair damaged hair, supplement nutrients for the hair, has the effects of removing dandruff and relieving itching, can prevent alopecia and hair loss, has a hair growth effect, belongs to natural raw materials, and is non-toxic and harmless.
2. In the maintenance shampoo containing the tea bran essence and the preparation method thereof, through the mixing of the salt and the borax, the effects of removing dandruff and relieving itching are achieved, and the effects of bacteriostasis and sterilization are achieved.
Drawings
FIG. 1 is an overall flow diagram of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1 a nourishing shampoo containing tea bran essence and a method for preparing the same, includes:
firstly, mixing and preparing raw materials
Adding 10% of main surfactant into a stirring kettle, adding a proper amount of deionized water, heating to 70-80 ℃, adding 1% of auxiliary surfactant into the stirring kettle, uniformly stirring, stirring until the surfactant is completely dissolved, adding 0.1% of thickening agent into the solution, and stirring for 1-2 hours to generate consistency;
the main surface active agents are K12 and AESS, which mainly play roles of foaming, hair cleaning and the like, and the auxiliary surface active agents are CAB and coconut oil fatty acid diethanolamide, which mainly play roles of auxiliary foaming, thickening, foam stabilizing and main surface active agent stimulation reduction;
the thickening agent is salt and borax, the thickening principle is that after electrolyte is added, micelle on the surface swells, movement resistance is increased, viscosity on the surface is increased, borax is weak base and has weak bacteriostatic action like boric acid, a small amount of borax is added into salt and is placed into a basin, and a proper amount of clear water is added to dissolve the borax and wash the hair, so that the hair shampoo has good effects on eliminating scalp itching and reducing dandruff.
Secondly, adding functional auxiliary agent to prepare
Reducing the temperature to 55-65 deg.C, adding 0.3% of conditioner and 0.5% of pearling agent into the solution, stirring for 1 hr to dissolve completely, adding 15% of tea bran essence into the solution, and stirring well to dissolve completely;
reducing the temperature to 40-50 deg.C, adding antiseptic 0.1% and essence 0.3% into the solution, stirring for 0.5-1.5 hr to dissolve completely;
the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property and is antistatic, damaged hair quality is repaired, the hair is soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the conditioner adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses more on improving the combing property during wet hair;
the tea bran contains tea saponin in the liquid juice directly pounding the tea bran and extracted by water, and has good scale removal effect, hair can be kept black and bright by washing the hair, damaged hair quality is repaired, and nutrients are supplemented for the hair.
Preparation of shampoo containing tea bran essence
Adding 0.1% of neutralizing agent into the solution, adjusting the pH value of the solution to 5.0, and stirring at low speed for 0.5 h; standing overnight to defoam the solution, thus finishing the preparation of the shampoo.
Example 2a nourishing shampoo containing tea bran essence and a preparation method thereof, includes:
firstly, mixing and preparing raw materials
Adding 25% of main surfactant into a stirring kettle, adding a proper amount of deionized water, heating to 70-80 ℃, adding 10% of auxiliary surfactant into the stirring kettle, uniformly stirring, stirring until the surfactant is completely dissolved, adding 0.5% of thickening agent into the solution, and stirring for 1-2 hours to generate consistency;
the main surface active agents are K12 and AESS, which mainly play roles of foaming, hair cleaning and the like, and the auxiliary surface active agents are CAB and coconut oil fatty acid diethanolamide, which mainly play roles of auxiliary foaming, thickening, foam stabilizing and main surface active agent stimulation reduction;
the thickening agent is salt and borax, the thickening principle is that after electrolyte is added, micelle on the surface swells, movement resistance is increased, viscosity on the surface is increased, borax is weak base and has weak bacteriostatic action like boric acid, a small amount of borax is added into salt and is placed into a basin, and a proper amount of clear water is added to dissolve the borax and wash the hair, so that the hair shampoo has good effects on eliminating scalp itching and reducing dandruff.
Secondly, adding functional auxiliary agent to prepare
Reducing the temperature to 55-65 deg.C, adding 0.5% of conditioner and 1.5% of pearling agent into the solution, stirring for 1-2 hr to dissolve completely, adding 30% of tea bran essence into the solution, and stirring uniformly to dissolve completely;
reducing the temperature to 40-50 deg.C, adding antiseptic 0.5% and essence 0.7% into the solution, stirring for 0.5-1.5 hr to dissolve completely;
the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property and is antistatic, damaged hair quality is repaired, the hair is soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the conditioner adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses more on improving the combing property during wet hair;
the tea bran contains tea saponin in the liquid juice directly pounding the tea bran and extracted by water, and has good scale removal effect, hair can be kept black and bright by washing the hair, damaged hair quality is repaired, and nutrients are supplemented for the hair.
Preparation of shampoo containing tea bran essence
Adding 0.5% of neutralizing agent into the solution, adjusting the pH value of the solution to 6.0, and stirring at low speed for 0.5-1 h; standing overnight to defoam the solution, thus finishing the preparation of the shampoo.
Example 3 a conditioning shampoo containing tea bran essence and a preparation method thereof, includes:
firstly, mixing and preparing raw materials
Adding 22.5% of main surfactant into a stirring kettle, adding a proper amount of deionized water, heating to 70-80 ℃, adding 5.5% of auxiliary surfactant into the stirring kettle, stirring uniformly until the surfactant is completely dissolved, adding 0.3% of thickening agent into the solution, and stirring for 1-2h to generate consistency;
the main surface active agents are K12 and AESS, which mainly play roles of foaming, hair cleaning and the like, and the auxiliary surface active agents are CAB and coconut oil fatty acid diethanolamide, which mainly play roles of auxiliary foaming, thickening, foam stabilizing and main surface active agent stimulation reduction;
the thickening agent is salt and borax, the thickening principle is that after electrolyte is added, micelle on the surface swells, movement resistance is increased, viscosity on the surface is increased, borax is weak base and has weak bacteriostatic action like boric acid, a small amount of borax is added into salt and is placed into a basin, and a proper amount of clear water is added to dissolve the borax and wash the hair, so that the hair shampoo has good effects on eliminating scalp itching and reducing dandruff.
Secondly, adding functional auxiliary agent to prepare
Reducing the temperature to 55-65 deg.C, adding 0.4% of conditioner and 1% of pearling agent into the solution, stirring for 1-2 hr to dissolve completely, adding 22.5% of tea bran essence into the solution, and stirring well to dissolve completely;
reducing the temperature to 40-50 deg.C, adding antiseptic 0.3% and essence 0.5% into the solution, stirring for 0.5-1.5 hr to dissolve completely;
the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property and is antistatic, damaged hair quality is repaired, the hair is soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the conditioner adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses more on improving the combing property during wet hair;
the tea bran contains tea saponin in the liquid juice directly pounding the tea bran and extracted by water, and has good scale removal effect, hair can be kept black and bright by washing the hair, damaged hair quality is repaired, and nutrients are supplemented for the hair.
Preparation of shampoo containing tea bran essence
Adding 0.3% of neutralizing agent into the solution, adjusting the pH value of the solution to 5.5, and stirring at low speed for 0.5-1 h; standing overnight to defoam the solution, thus finishing the preparation of the shampoo.
The shampoo containing the tea bran essence prepared by the invention has good antibacterial property, and the detection indexes of the shampoo containing the tea bran essence prepared by the invention are shown in table 1:
TABLE 1
As shown in table 1, in the shampoo containing tea bran essence prepared by the invention, the antibacterial ability of the shampoo is strongest in example 3, and although the antibacterial effect is not much different from that of example 2, the excessively added thickener easily causes the shampoo to be too thick, so that the antibacterial effect and the consistency of the shampoo are best when the thickener is 0.3%.
Comparative example 1 a conditioning shampoo containing tea bran essence and a preparation method thereof, comprising:
firstly, mixing and preparing raw materials
Adding 22.5% of main surfactant into a stirring kettle, adding a proper amount of deionized water, heating to 70-80 ℃, adding 5.5% of auxiliary surfactant into the stirring kettle, stirring uniformly until the surfactant is completely dissolved, adding 0.3% of thickening agent into the solution, and stirring for 1-2h to generate consistency;
the main surface active agents are K12 and AESS, which mainly play roles of foaming, hair cleaning and the like, and the auxiliary surface active agents are CAB and coconut oil fatty acid diethanolamide, which mainly play roles of auxiliary foaming, thickening, foam stabilizing and main surface active agent stimulation reduction;
the thickening agent is salt, and the thickening principle is that after electrolyte is added, micelles on the surface swell, the movement resistance is increased, and the viscosity on the surface is increased.
Secondly, adding functional auxiliary agent to prepare
Reducing the temperature to 55-65 deg.C, adding 0.4% of conditioner and 1% of pearling agent into the solution, stirring for 1-2 hr to dissolve completely, adding 22.5% of tea bran essence into the solution, and stirring well to dissolve completely;
reducing the temperature to 40-50 deg.C, adding antiseptic 0.3% and essence 0.5% into the solution, stirring for 0.5-1.5 hr to dissolve completely;
the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property and is antistatic, damaged hair quality is repaired, the hair is soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the conditioner adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses more on improving the combing property during wet hair;
the tea bran contains tea saponin in the liquid juice directly pounding the tea bran and extracted by water, and has good scale removal effect, hair can be kept black and bright by washing the hair, damaged hair quality is repaired, and nutrients are supplemented for the hair.
Preparation of shampoo containing tea bran essence
Adding 0.3% of neutralizing agent into the solution, adjusting the pH value of the solution to 5.5, and stirring at low speed for 0.5-1 h; standing overnight to defoam the solution, thus finishing the preparation of the shampoo.
Comparative example 2a shampoo and a process for the preparation thereof comprising:
firstly, mixing and preparing raw materials
Adding 22.5% of main surfactant into a stirring kettle, adding a proper amount of deionized water, heating to 70-80 ℃, adding 5.5% of auxiliary surfactant into the stirring kettle, stirring uniformly until the surfactant is completely dissolved, adding 0.3% of thickening agent into the solution, and stirring for 1-2h to generate consistency;
the main surface active agents are K12 and AESS, which mainly play roles of foaming, hair cleaning and the like, and the auxiliary surface active agents are CAB and coconut oil fatty acid diethanolamide, which mainly play roles of auxiliary foaming, thickening, foam stabilizing and main surface active agent stimulation reduction;
the thickening agent is salt and borax, the thickening principle is that after electrolyte is added, micelle on the surface swells, movement resistance is increased, viscosity on the surface is increased, borax is weak base and has weak bacteriostatic action like boric acid, a small amount of borax is added into salt and is placed into a basin, and a proper amount of clear water is added to dissolve the borax and wash the hair, so that the hair shampoo has good effects on eliminating scalp itching and reducing dandruff.
Secondly, adding functional auxiliary agent to prepare
Reducing the temperature to 55-65 ℃, adding 0.4% of conditioner and 1% of pearling agent into the solution, and stirring for 1-2h to completely dissolve the conditioner and the pearling agent;
reducing the temperature to 40-50 deg.C, adding antiseptic 0.3% and essence 0.5% into the solution, stirring for 0.5-1.5 hr to dissolve completely;
the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil, the cationic guar gum can show excellent antistatic property and conditioning effect after being adsorbed on hair, the wet combing property of the hair is improved, the hair can keep luster, softness and elasticity for a long time, the softness is extremely mild to skin and eyes, the irritation of a surfactant in a formula product can be relieved, the cationic hydroxyethyl cellulose has excellent conditioning property, is antistatic, repairs damaged hair quality, enables the hair to be soft, smooth and elastic, in addition, the irritation of a detergent to the skin can be relieved, the cationic effect enables the conditioner adsorbed on the hair to improve the conditioning property after the hair is dried, and the emulsified silicone oil focuses more on improving the combing property during the wet hair.
Preparation of shampoo containing tea bran essence
Adding 0.3% of neutralizing agent into the solution, adjusting the pH value of the solution to 5.5, and stirring at low speed for 0.5-1 h; standing overnight to defoam the solution, thus finishing the preparation of the shampoo.
The shampoo containing the tea bran essence has good antibacterial property, the antibacterial property of the shampoo is greatly related to the added borax, and in order to verify the related technical scheme, the applicant performs the following tests:
comparative example 1: the prepared wormwood essential oil was tested for its relevant index using the method of examples 1-3 with only the sandblasting removed, as shown in table 2:
TABLE 2
According to the table 1, the inhibition effect of the prepared shampoo on pathogenic bacteria is obviously reduced under the condition of only removing the borax, and the comparative example 1 can show that the inhibition rate on each pathogenic bacteria is 20.2%, 21.0%, 19.6% and 18.9% respectively when the borax is removed, so that the borax is an important part for influencing the antibacterial rate of the shampoo.
Comparative example 3
The comparative example provides a preparation of a hand sanitizer containing tea bran essence, which comprises the following components in percentage by weight: 13% of tea bran essence, 22.5% of surfactant, 0.4% of conditioner, 1% of pearling agent, 0.09% of thickening agent, 0.3% of preservative, 0.5% of essence, 0.3% of neutralizer and the balance of deionized water;
the range was different compared to examples 1-3.
Comparative example 4
The comparative example provides a preparation of a hand sanitizer containing tea bran essence, which comprises the following components in percentage by weight: 10% of tea bran essence, 22.5% of surfactant, 0.4% of conditioner, 1% of pearling agent, 0.08% of thickening agent, 0.3% of preservative, 0.5% of essence, 0.3% of neutralizer and the balance of deionized water;
the range was different compared to examples 1-3.
Comparative example 5
The comparative example provides a preparation of a hand sanitizer containing tea bran essence, which comprises the following components in percentage by weight: 10% of tea bran essence, 22.5% of surfactant, 0.4% of conditioner, 1% of pearling agent, 0.05% of thickening agent, 0.3% of preservative, 0.2% of essence, 0.8% of neutralizer and the balance of deionized water;
the range was different compared to examples 1-3.
Comparative example 6
The comparative example provides a preparation of a hand sanitizer containing tea bran essence, which comprises the following components in percentage by weight: 8% of tea bran essence, 22.5% of surfactant, 0.4% of conditioner, 0.5-1.5% of pearling agent, 0.05% of thickening agent, 0.3% of preservative, 0.1% of essence, 0.09% of neutralizer and the balance of deionized water;
the range was different compared to examples 1-3.
Comparative example 7
The comparative example provides a preparation of a hand sanitizer containing tea bran essence, which comprises the following components in percentage by weight: 8% of tea bran essence, 33% of surfactant, 0.5% of conditioner, 1.5% of pearling agent, 0.3% of preservative, 0.5% of essence, 0.3% of neutralizer and the balance of deionized water;
the range was different compared to examples 1-3.
The preparation method of the hand sanitizer containing camellia oil essence provided by the comparative examples 3-7 is the same as that of the examples 1-3, wherein the missing substances are not added directly, and other steps are not changed, so that the description is omitted.
Test example 1
The shampoos provided in examples 1-3 and comparative examples 1-7 were subjected to sensory tests, a trial group consisting of 50 persons was randomly invited to observe and use the shampoo, the invitations were performed in batches and evaluated separately, in the test process, one shampoo was tried every two weeks, and then the trials were continued, and the sensory evaluation criteria are shown in table 3:
TABLE 3
| Appearance (fen) | Fragrance (fen) | Consistency (fen) | Relieving itching (fen) | Dandruff removing (fen) | Comfort (fen) |
| Clarification (5) | Pure (5) | Suitably (5) | Preferably (5) | Preferably (5) | Comfort (5) |
| Turbid (4) | In general (4) | Thick (4) | In general (4) | In general (4) | In general (4) |
| With foreign matter (2) | Peculiar smell (2) | Book of excess (2) | No sense (3) | No effect (2) | Stimulus (2) |
The statistical panel scored examples 1-3, with the average of 50 scores for each hand cleanser containing camellia oil extract as the final score, and the results are shown in table 4:
TABLE 4
| Example 1 | Example 2 | Example 3 | |
| Average score (point) | 4.78 | 4.86 | 4.95 |
The statistical test panel scored on controls 1-6, and the average of 50 scores for each hand sanitizer containing camellia oil extract was taken as the final score, with the results shown in table 5:
TABLE 5
As can be seen from tables 3 to 5, compared with comparative examples 1 to 7, the shampoos provided in examples 1 to 3 of the present invention have good appearance and consistency, pure and positive odor, significant antipruritic and anti-dandruff effects, and high comfort during use, which indicates that the shampoo containing tea bran essence provided by the present invention has more reasonable components and matching ratio, and the quality of the prepared shampoos is better due to the synergistic cooperation of the raw materials.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (10)
1. A care shampoo containing tea bran essence comprises the following raw materials: 15-30% of tea bran essence, 10-35% of surfactant, 0.3-0.5% of conditioner, 0.5-1.5% of pearling agent, 0.1-0.5% of thickening agent, 0.1-0.5% of preservative, 0.3-0.7% of essence, 0.1-0.5% of neutralizer and the balance of deionized water.
2. The maintenance shampoo containing tea bran essence and the preparation method thereof as claimed in claim 1, wherein the maintenance shampoo comprises: the surfactant comprises a primary surfactant and a secondary surfactant;
the main surface active agent is one or more of K12, AES, AESA, K12A and AESS, the main surface active agent is K12 and AESS, and the using amount is 10-25%;
the auxiliary surfactant is one or more of CAB, SHD, APG, coconut oil fatty acid diethanolamide, imidazoline and amino acid, and the auxiliary surfactant is CAB and coconut oil fatty acid diethanolamide.
3. The maintenance shampoo containing tea bran essence and the preparation method thereof as claimed in claim 1, wherein the maintenance shampoo comprises: the conditioner is cationic guar gum, cationic hydroxyethyl cellulose and emulsified silicone oil.
4. The maintenance shampoo containing tea bran essence and the preparation method thereof as claimed in claim 1, wherein the maintenance shampoo comprises: the thickening agent is salt and borax.
5. The maintenance shampoo containing tea bran essence and the preparation method thereof as claimed in claim 1, wherein the maintenance shampoo comprises: the preservative is DMDM hydantoin.
6. The maintenance shampoo containing tea bran essence and the preparation method thereof as claimed in claim 1, wherein the maintenance shampoo comprises: the neutralizing agent is citric acid.
7. A method for preparing a care shampoo containing tea bran essence, which comprises the care shampoo containing tea bran essence of any one of claims 1 to 6, and comprises the following steps:
s1, adding a main surfactant into a stirring kettle, adding a proper amount of deionized water, and heating;
s2, adding the auxiliary surfactant into a stirring kettle, and uniformly stirring to completely dissolve the surfactant;
s3, adding the thickening agent into the solution, and uniformly stirring to form a consistency;
s4, reducing the temperature, adding a conditioner and a pearling agent, and uniformly stirring to completely dissolve;
s5, adding the tea bran essence, and uniformly stirring to completely dissolve the tea bran essence;
s6, reducing the temperature, adding the preservative and the essence, and stirring uniformly;
s7, adding a neutralizer to adjust the pH value of the solution, and stirring at a low speed;
s8, standing overnight for defoaming, and finishing the preparation.
8. The method for preparing a conditioning shampoo containing tea bran essence as claimed in claim 7, wherein the method comprises the following steps: in the S1-S3, the heating temperature of the stirring kettle is 70-80 ℃, and the stirring time is 1-2 h.
9. The method for preparing a conditioning shampoo containing tea bran essence as claimed in claim 7, wherein the method comprises the following steps: in the steps S4-S5, the temperature is reduced to 55-65 ℃, and the stirring time is 1-2 h.
10. The method for preparing a conditioning shampoo containing tea bran essence as claimed in claim 7, wherein the method comprises the following steps: in the steps S6-S7, the temperature is reduced to 40-50 ℃, the stirring time is 0.5-1.5h, the pH value of the solution is adjusted to 5.0-6.0, and the low-speed stirring time is 0.5-1 h.
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