CN108066222A - A kind of scalp care hair shampoo of the extract of bran containing tea and preparation method thereof - Google Patents
A kind of scalp care hair shampoo of the extract of bran containing tea and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of scalp care hair shampoos of the extract of bran containing tea and preparation method thereof, the shampoo uses the surfactant system compounded by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract and Cocoamidopropyl betaine, using the coral ginger oil of natural botanical source as main antibacterial anti-dandruff active ingredient, it acts synergistically with the tea bran extract and tea polyphenols of natural botanical source, debris removing significant effect.The formula is mildly non-stimulated, detergency is good, foam is high and stablizes, the wet comb performance of dry comb of hair is good, dandruff can be removed, the scalp problems such as head is itched, hair caused by long-time service chemical small molecule bacteriostatic agent can be avoided to dry up, the situation that dim mute, anti-dandruff effect declines and dandruff aggravates, long-time service can equally realize efficient debris removing, it is anti-dandruff to realize safety and effectivity, is suitble to long-time service.
Description
Technical field
The invention belongs to daily cosmetics fields, and in particular to a kind of preparation and its preparation side for cleaning scalp or hair
Method.
Background technology
With the quickening pace of modern life, the increasing of operating pressure, more and more artificial dandruffs and it is worried, dandruff problem is
Through becoming the second largest hair healthy problem for being only second to alopecia and perplexing consumer.It is reported according to professional investigation, about 67%
There is dandruff puzzlement in people, that is, the people for having 2/3 had dandruff problem, in addition, nearly 95% interviewee has rebound phenomenon,
And the Proportion of patients for occurring dandruff recurrence within 5 days is up to 90%.
Anti-dandruff raw material currently on the market in many anti-dandruff shampoos is common to be mainly made of chemical raw material, such as pyrithione
Zinc, climbazole, pyridone ethanolamine, salicylic acid, ketone health Cuo etc., these raw material fungistatic effects are strong, have when just beginning to use very well
Anti-dandruff effect, but irritation is big, is often present with sedimentation and metachromatism in the application of shampoo formula, to photo-labile and
Degreasing power is too strong, and long-time service can cause hair dry up, is low and deep, there be not the problems such as gloss；And with the extension of usage time,
The situation generation that anti-dandruff effect declines and has dandruff to have exacerbation.Therefore, there is an urgent need for develop healthier, safer go on Vehicles Collected from Market
Shampoo is considered to be worth doing, to meet the demand of the anti-dandruff and health of hair of consumer.
The content of the invention
It is an object of the invention to provide a kind of scalp care hair shampoo of the extract of bran containing tea and preparation method thereof, the shampoos
Using the surfactant body compounded by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract and Cocoamidopropyl betaine
System using the coral ginger oil of natural botanical source as main antibacterial anti-dandruff active ingredient, carries with the tea bran of natural botanical source
Object and tea polyphenols is taken to act synergistically, debris removing significant effect, the formula is mildly non-stimulated, long-term safety can long-time service, solve
The anti-dandruff effect of dandruff control shampoo containing long-time service declines the problem of even aggravating in the market.
To achieve these goals, this invention takes following technical schemes：
A kind of scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, composition bag
It includes：
In preferred technical solution, a kind of scalp care hair shampoo of the extract of bran containing tea accounts for the weight of shampoo with each component
Percentages, composition include：
In preferred technical solution, the pH value of the scalp care hair shampoo is 5.5~6.5.
In preferred technical solution, the tea bran extract is made according to the following steps：3~4mL is corresponded to according to every gram of tea bran
Ethanol solution ratio, will tea bran crush after be added to concentration expressed in percentage by volume be 80% ethanol solution in, after stirring evenly,
20~40min of ultrasonic extraction under conditions of temperature is 40~50 DEG C, supersonic frequency is 20~30kHz, separating and filtering, gained filter
Concentrated dry the tea bran extract of liquid.
In preferred technical solution, the coral ginger oil liposome is temperature sensitive type coral ginger oil nano liposomes.
In preferred technical solution, the temperature sensitive type coral ginger oil nano liposomes are made by following methods：
To be (4~5) by mass ratio：The total phospholipids of 1 dipalmitoylphosphatidylcholine and hydrogenated soy phosphatidyl choline composition
It is placed in reaction vessel, adds in chloroform thereto to being completely dissolved, then rotary evaporation makes chloroform volatilize completely, anti-
It answers and uniform liposome membrane is formed on chamber wall；After coral ginger oil and the abundant mixing of Tween-80,30~35 DEG C are added to
PH value is in 6.5 phosphate buffer solution, again after mixing, is poured into the reaction vessel with the liposome membrane,
40~50 DEG C of thermostatic ultrasonics 20~after forty minutes stand 3~5 it is small when to get coral ginger oil Liposomal suspensions；Wherein, total phospholipids with
The proportioning of phosphate buffer solution is 4~10mg/mL, and the mass ratio of total phospholipids, coral ginger oil and Tween-80 is (5~6)：(1
~2)：(1~2).
In further preferred technical solution, the proportioning of total phospholipids and chloroform is 4~10mg/mL.
In preferred technical solution, the mass ratio of the total phospholipids, coral ginger oil and Tween-80 is 5：1：1.
In the present invention, the dosage of the coral ginger oil liposome is with coral ginger oil liposome in coral ginger oil Liposomal suspensions
Weight calculated.
In preferred technical solution, the coral ginger oil is made by the following method：It is first that dry coral ginger powder is broken, then will
Coral ginger particle supercritical CO2When extraction 1~3 is small in extractor, extraction flow velocity is 15~25L/h, and extracting pressure is
20MPa~30MPa, extraction temperature are 30~50 DEG C；Then decompression separation is carried out, separating pressure is 3MPa~6MPa, and separation is warm
It spends for 30~50 DEG C, when disengaging time is 0.5~1 small.
In preferred technical solution, extraction temperature is 45 DEG C, extraction flow velocity 20L/h, extracting pressure 25MPa.
The present invention also provides the preparation methods of the scalp care hair shampoo of the above-mentioned extract of bran containing tea, comprise the following steps：
Citric acid and water are mixed, 50~70 DEG C are heated to, by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract, coconut oleoyl amine
Propyl betaine, tea polyphenols are added thereto, and stirring is so that be uniformly mixed；Be cooled to 15~35 DEG C, by coral ginger oil liposome,
PEG (polyethylene glycol) and vitamin E are added thereto, and stirring to be uniformly mixed, and is cooled to room temperature, obtains scalp care hair shampoo.
In preferred technical solution, PEG PEG-14M.
In the present invention, the room temperature typically refers to 20~25 DEG C.
In the present invention, using by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract and Cocoamidopropyl betaine
The surfactant system of compounding, synergistic effect is apparent, and detergency is good, and foam is high and stablizes, and is influenced from water hardness, temperature
With it is non-stimulated；Existing chemical small molecule (zinc pyrithione, piroctone second are substituted using the coral ginger oil of natural botanical source
Alcohol amine salt etc.) as main antibacterial anti-dandruff active ingredient, tea bran extract and the tea polyphenols synergistic effect with natural botanical source,
Inhibitory action of the main active terpinene-4-alcohol to chlosma of coral ginger oil is enhanced, and is turned by antioxygen
With the peroxide for influencing dandruff and generating is reduced, so as to which dandruff be blocked to generate, fundamentally the effect of realization anti-dandruff and itching-relieving, dispel
Consider significant effect to be worth doing, mildly non-stimulated to scalp, long-time service will not induce dandruff；Moreover, main anti-dandruff active ingredient coral
Ginger oil is added in the form of temperature sensitive type liposome, and coral ginger oil is wrapped in interior, the liposome in storage at normal temperature by nano liposomes
The active ingredient of coral ginger oil and external environment isolation are come, avoid the main active terpinene -4- of coral ginger oil
The slow oxidation of alcohol is undergone phase transition when in use with liposome during 42 DEG C or more warm water washings, liposome interior it is antibacterial anti-dandruff
Active ingredient releases, and plays the antibacterial effect of debris removing, simultaneously as the structure of liposome and the protoplast phase of cell
Seemingly, liposome can interact (intermembranous transfer, contact release, absorption, fusion, phagocytosis etc.) with cell, what enhancing was wrapped up
Active ingredient enhances antibacterial effect, reduces activity, while reach the mesh suppressed growth of microorganism to the permeability of cell
's；Further, since phosphatide can occur slightly to be bonded with the keratin of cuticula, the crude of hair, the dry comb of hair can be repaired
Wet comb performance improvement；Using PEG and vitamin E, it can not only enhance stability of the liposome in system, but also can be with regulation system
Viscosity and denseness.In other words, surfactant system each component compound synergic, antibacterial anti-dandruff each active ingredient synergistic effect, coral
Coral ginger oil liposome and PEG and vitamin E compound synergic between each system are also synergistic effect in entire shampoo, so as to
Realize good anti-dandruff clean volatility.
Compared with prior art, the present invention has technique effect beneficial below：
Inventive formulation is mildly non-stimulated, and detergency is good, and foam is high and stablizes, and the wet comb performance of dry comb of hair is good, can
Removal dandruff, head such as are itched at the scalp problems, hair caused by long-time service chemical small molecule bacteriostatic agent can be avoided to dry up, it is dim it is mute,
The situation that anti-dandruff effect declines and dandruff aggravates, long-time service can equally realize efficient debris removing, and it is anti-dandruff to realize safety and effectivity,
It is very suitable for long-time service.
Specific embodiment
In order to which the present invention is better described, technical scheme is readily appreciated with reference to specific embodiments to this
Invention is described in further detail.It is to be understood that following embodiments is merely to illustrate the present invention, this hair is not represented or limited
Bright rights protection scope, protection scope of the present invention are subject to claims.
Reagents or instruments used without specified manufacturer in following embodiment is the routine that can be commercially available
Product.For example, tea bran can be bought from end of the bridge oil pressing mill of Yingde City of Guangdong Province, coral ginger comes from Guizhou, biennial, two palmityl phosphorus
Phosphatidylcholine (DPPC) and hydrogenated soy phosphatidyl choline (HSPC) can be bought from Shanghai Advanced viecle Technology Co., Ltd., tea polyphenols
(purity>98%) can be bought from Changsha Xu He bio tech ltd, vitamin E (purity 100%) can be from the large dimension food in Guangzhou
Product Technology Co., Ltd. buys, and PEG-14M (DOW Chemical) can be that Chemical Co., Ltd. buys from Guangzhou U.S.A.
The preparation process of the scalp care hair shampoo of the extract of bran containing tea：
(1) preparation of tea bran extract：The ratio of the ethanol solution of 4mL is corresponded to according to every gram of tea bran, after tea bran is crushed
Be added to concentration expressed in percentage by volume be 80% ethanol solution in, after stirring evenly, temperature be 50 DEG C, supersonic frequency 25kHz
Under conditions of ultrasonic extraction 20min, separating and filtering, gained concentrating filter liquor it is dry tea bran extract.
(2) preparation of coral ginger oil：First by coral ginger when 35 DEG C of dryings 24 are small, grain size is then crushed to as 7mm or so,
By 1kg coral ginger particle supercritical COs2When extraction 2.5 is small in extractor, the pressure controlled in extractor is 25MPa, warm
It spends for 45 DEG C, extraction flow velocity is 20L/h；Then decompression separation is carried out in knockout drum, the pressure controlled in knockout drum is 5MPa,
Temperature is 30 DEG C, and when disengaging time is 0.5 small, separating obtained product is coral ginger oil.
(3) preparation of coral ginger oil liposome：
To be 4 by mass ratio：1 dipalmitoylphosphatidylcholine (DPPC) and hydrogenated soy phosphatidyl choline (HSPC) composition
Total phospholipids is placed in reaction vessel, adds in chloroform (10mg total phospholipidses:1mL chloroforms) to being completely dissolved, then it is placed in Rotary Evaporators
On, under room temperature, with the rotating speed rotary evaporation of 15rpm, chloroform is made to volatilize completely, uniform fat is formed in reactor vessel wall
Plastid film；After coral ginger oil and the abundant mixing of Tween-80,35 DEG C of pH value is added to as 6.5 phosphate buffer solution
In, again after mixing, pour into the reaction vessel with liposome membrane, 45 DEG C of thermostatic ultrasonics stood after 30 minutes 4 it is small when, i.e.,
Obtain temperature sensitive type coral ginger oil Liposomal suspensions；Wherein, the proportioning of total phospholipids and phosphate buffer solution (PBS) is 10mg total phosphorus
Fat：1mLPBS, the mass ratio of total phospholipids, coral ginger oil and Tween-80 is 5：1：1.
(4) preparation of the scalp care hair shampoo of the extract of bran containing tea
Citric acid and water are mixed, 70 DEG C are heated to, by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract, cocounut oil
Amido propyl betaine, tea polyphenols are added thereto, and stirring is so that be uniformly mixed；Be cooled to 30 DEG C, by coral ginger oil liposome,
PEG-14M and vitamin E are added thereto, and stirring to be uniformly mixed, and is cooled to room temperature, obtains scalp care hair shampoo.
Each group distribution ratio reference example 1 below~5, wherein, the dosage of coral ginger oil liposome is with coral ginger oil lipid
The weight of coral ginger oil liposome is calculated in body suspension, i.e., according to the total phospholipids, coral ginger oil and Tween-80 added in
Total weight calculate.For example, in 100 parts of shampoos, coral ginger oil liposome is 5 parts, includes total phospholipids, coral that is, taking
The total weight of coral ginger oil and Tween-80 is 5 parts of coral ginger oil Liposomal suspensions.
Embodiment 1
The scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, and composition includes：
Embodiment 2
The scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, and composition includes：
Embodiment 3
The scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, and composition includes：
Embodiment 4
The scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, and composition includes：
Embodiment 5
The scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, and composition includes：
The pH for measuring above-mentioned scalp care hair shampoo is 5.5~6.5.
And it is tested for the property by following explanation：
The mode of volunteer's sensory evaluation is taken in anti-dandruff and itching-relieving performance and smooth easy Carding Degree detection, and there are heads by volunteer
Bits and scalp itching problem, six groups altogether, every group of 12 volunteers.It is washed in the same manner when volunteer is using shampoo sample
Head, the smooth easy Carding Degree after hair anti-dandruff and itching-relieving effect and use is washed in sensory evaluation shampoo, wherein anti-dandruff effect is according to head
Bits number and size score, antipruritic effect is to itch the time of beginning according to head and degree that head is itched scores, and smoothness is
Required time length is stretched out after artificially knotting according to hair naturally again to give a mark, dried easy Carding Degree is according to drying
The combing difficulty or ease situation of hair is given a mark afterwards.
Evaluation cycle is surrounding, and evaluation is using 5 points of systems, and 5 points are best result, and 1 point is minimum point, and fraction is higher to represent effect
Better.
Zinc pyrithione (ZPT) is current the most widely used small molecule anti-dandruff agent, with commercially available addition zinc pyrithione
(ZPT) shampoo is as a comparison case.The evaluation result of comparative example and Examples 1 to 5 is as shown in table 1.
The different group shampoo Analyses Methods for Sensory Evaluation Results of table 1
| Anti-dandruff and itching-relieving | Dry cardability | Wet cardability | Feel | Comprehensive grading | |
| Embodiment 1 | 4.5 | 4.5 | 4.8 | 4.7 | 18.5 |
| Embodiment 2 | 4.4 | 4.3 | 4.7 | 4.4 | 17.8 |
| Embodiment 3 | 4.2 | 4.5 | 4.6 | 4.5 | 17.8 |
| Embodiment 4 | 4.3 | 4.4 | 4.7 | 4.6 | 18.0 |
| Embodiment 5 | 4.4 | 4.3 | 4.6 | 4.5 | 17.8 |
| Comparative example | 3.6 | 3.2 | 3.6 | 3.6 | 14.0 |
First, to be evaluated according to volunteer, dandruff control shampoo containing cleaning hair provided by the invention is used continuously, hair quality is submissive,
Without visible dandruff, itch phenomenon completely disappears naked eyes, and hair and hair can keep salubrious for a long time clean.
Secondly, dandruff control shampoo containing provided by the invention and the shampoo of commercially available addition zinc pyrithione (ZPT) are carried out pair
Than the results are shown in Table 1.As can be seen from Table 1, compared to comparative example, Examples 1 to 5 show better anti-dandruff and itching-relieving,
Dry, wet carding effect, and dry not short-tempered, the good hand touch of feeling well in hair back is washed, long-time service is anti-dandruff with obvious effects.
It should be understood by those skilled in the art that suitable pearling agent, essence can be also added as needed in inventive formulation
Deng.
It should be understood by those skilled in the art that the foregoing is merely several specific embodiments of the present invention, the present invention
It is not limited to that.It should be pointed out that for those of ordinary skill in the art, many modification and improvement can also be made,
All deformations or improvement without departing from described in claim are regarded as protection scope of the present invention
It should be noted that embodiment described above is only used for explaining the present invention, do not form to any of the present invention
Limitation, by referring to exemplary embodiments, invention has been described, it should be appreciated that word wherein used is descriptive
With explanatory vocabulary rather than limited vocabulary.The present invention can be made within the scope of the claims by regulation
It changes and the present invention is revised from scope and spirit of the present invention not.Although the present invention described in it relates to
And specific method, material and embodiment, it is not intended that the present invention is limited to wherein disclosed particular case, on the contrary, this hair
It is bright to can be extended to other all methods and applications with identical function.
Claims (10)
1. a kind of scalp care hair shampoo of the extract of bran containing tea, is accounted for by each component in terms of the weight percent of shampoo, composition includes：
2. the scalp care hair shampoo of the extract of bran containing tea as described in claim 1 accounts for the weight percent of shampoo with each component
Meter, composition include：
3. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 1 or 2, it is characterised in that：The anti-dandruff shampoo
The pH value of shampoo is 5.5~6.5.
4. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 1 or 2, it is characterised in that：The tea bran extraction
Object is made according to the following steps：The ratio of the ethanol solution of 3~4mL is corresponded to according to every gram of tea bran, body is added to after tea bran is crushed
Product percentage concentration be 80% ethanol solution in, after stirring evenly, temperature be 40~50 DEG C, supersonic frequency is 20~30kHz
Under conditions of 20~40min of ultrasonic extraction, separating and filtering, gained concentrating filter liquor it is dry tea bran extract.
5. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 1 or 2, it is characterised in that：The coral ginger oil
Liposome is temperature sensitive type coral ginger oil nano liposomes.
6. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 5, it is characterised in that：The temperature sensitive type coral ginger
Oily nano liposomes are made by following methods：
To be (4~5) by mass ratio：The total phospholipids of 1 dipalmitoylphosphatidylcholine and hydrogenated soy phosphatidyl choline composition is placed in
In reaction vessel, chloroform is added in thereto to being completely dissolved, then rotary evaporation makes chloroform volatilize completely, holds in reaction
Uniform liposome membrane is formed on wall；After coral ginger oil and the abundant mixing of Tween-80,30~35 DEG C of pH value is added to
In 6.5 phosphate buffer solution, again after mixing, to pour into the reaction vessel with the liposome membrane, 40~
50 DEG C of thermostatic ultrasonics 20~after forty minutes stand 3~5 it is small when to get coral ginger oil Liposomal suspensions；Wherein, total phospholipids and phosphoric acid
The proportioning of salt buffer solution is 4~10mg/mL, and the mass ratio of total phospholipids, coral ginger oil and Tween-80 is (5~6)：(1~2)：
(1~2).
7. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 6, it is characterised in that：The total phospholipids, coral
The mass ratio of ginger oil and Tween-80 is 5：1：1.
8. the scalp care hair shampoo of the extract of bran containing tea as claimed in claims 6 or 7, it is characterised in that：The coral ginger oil
It is made by the following method：First will dry coral ginger powder it is broken, then by coral ginger particle supercritical CO21 is extracted in extractor
~3 it is small when, extraction flow velocity be 15~25L/h, extracting pressure be 20MPa~30MPa, extraction temperature be 30~50 DEG C；Then into
Row decompression separation, separating pressure are 3MPa~6MPa, and separation temperature is 30~50 DEG C, when disengaging time is 0.5~1 small.
9. the scalp care hair shampoo of the extract of bran containing tea as claimed in claim 8, it is characterised in that：Extraction temperature for 45 DEG C,
Extract flow velocity 20L/h, extracting pressure 25MPa.
10. the preparation method of the scalp care hair shampoo such as the extract of bran containing tea according to any one of claims 1 to 9, including
Following steps：Citric acid and water are mixed, are heated to 50~70 DEG C, by ethoxylated dodecyl alcohol ammonium sulfate, tea bran extract,
Cocoamidopropyl betaine, tea polyphenols are added thereto, and stirring is so that be uniformly mixed；15~35 DEG C are cooled to, by coral ginger oil
Liposome, PEG and vitamin E are added thereto, and stirring to be uniformly mixed, and is cooled to room temperature, obtains scalp care hair shampoo.
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| CN201810064988.6A CN108066222B (en) | 2018-01-23 | 2018-01-23 | Dandruff removing shampoo containing tea bran extract and preparation method thereof |
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| CN111759783A (en) * | 2020-08-13 | 2020-10-13 | 湖南省康多利油脂有限公司 | Tea bran essence-containing care shampoo and preparation method thereof |
| CN111840230A (en) * | 2020-08-13 | 2020-10-30 | 蚌埠学院 | Ginger volatile oil liposome and preparation method and application thereof |
| CN111991303A (en) * | 2020-09-27 | 2020-11-27 | 广州德谷个人护理用品有限公司 | Plant extract composition with multi-target scalp oil control and dandruff removal effects, preparation method thereof and scalp care composition |
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