CN110897988B - Hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and preparation method thereof - Google Patents
Hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and a preparation method thereof. The amino acid shampoo comprises the following components in parts by weight: 10-40 parts of a surfactant A; 1-30 parts of a surfactant B; 1-30 parts of a surfactant C; 0.01-5 parts of sturgeon roe extract liposome; 0.1 part of EDTA-2 NA; 0.5-5 parts of squalane; 0.01-2 parts of citric acid; 0.1-1 part of guar hydroxypropyl trimethyl ammonium chloride; 0.3 part of daily essence; 0.5 part of preservative; 100 parts of deionized water To. The invention aims to provide the shampoo which has good foaming capacity and cleaning capacity, is rich in foam and easy to wash, nourishes scalp and strengthens hair roots.
Description
Technical Field
The invention belongs to the technical field of extraction and processing of daily chemicals, and particularly relates to a hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and a preparation method thereof.
Background
The sturgeon roe has high nutritive value, is crystal-clear and transparent, is rich in protein, and has a content of 29 percent. And contains a plurality of trace elements and a plurality of microorganisms, and belongs to luxury goods with great value in the skin care field and the food field. Therefore, sturgeon roe is named as black gold.
Sturgeon roe is rich in rare nutrients such as essential fatty acid omega3, vitamins A, B and D, protein, amino acids and trace elements, and is a natural source of skin tissue structure and components required for survival. When applied to the skin, the active substances can greatly improve the vitality of the skin. The sturgeon roe extract is a powerful moisturizing and nourishing material, and can supplement water deeply and supply nutrition and moisture to stratum corneum deeply. It also can promote cell proliferation, differentiation, and cell structure renewal, and restore skin to young state. In addition, the omega3 has anti-inflammatory effect and has inhibitory effect on inflammatory factors.
In recent years, due to environmental pollution and increasing pressure of life, health problems of consumers are becoming more and more significant, and scalp health is also becoming a major concern. These problems are mainly: itching scalp, allergic redness, dandruff breeding, easy hair loss, easy hair cavity breakage and the like. The shampoo product for developing hair tonic and hair nourishing needs to solve the problems of good scalp health and easy breakage of hair cavities.
Researches prove that the sturgeon roe extract is rich in vitamins, proteins, amino acids and other nutrient substances, is easy to absorb and has a very good effect on maintaining the healthy state of the scalp. Meanwhile, the sturgeon roe extract has a good effect on repairing hair cavities, and can improve damaged hair quality and restore the hair quality to a healthy state after long-term continuous use.
Cosmetic and food homology has been well applied in the cosmetic field, and represents both the safety and the effectiveness of the raw materials.
With the demand of consumers for high-end washing and caring, sturgeon roe extract shampoo rich in nutrition is popular, and at present, no washing and caring product taking sturgeon roe extract as a raw material exists.
Disclosure of Invention
In view of the above, the invention aims to provide the hair-strengthening and hair-nourishing amino acid shampoo containing the sturgeon roe extract liposome, which has good foaming performance, good cleaning and washing capacity, and is capable of nourishing scalp and strengthening hair roots.
The invention also aims to provide a preparation method of the hair-strengthening and hair-nourishing amino acid shampoo containing the sturgeon roe extract liposome.
In order to solve the above-described problems, the present invention is achieved by the following means.
A hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome comprises the following components in parts by weight:
10-40 parts of surfactant A, 1-30 parts of surfactant B, 1-30 parts of surfactant C, 0.01-5 parts of sturgeon seed extract liposome, 0.1 part of EDTA-2NA, 0.5-5 parts of squalane, 0.01-2 parts of citric acid, 0.1-1 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 0-0.3 part of daily essence, 0-0.5 part of preservative and 100 parts of deionized water To.
Furthermore, the surfactant A is one or more of sodium cocoyl isethionate, sodium methyl cocoyl taurate, sodium lauroyl sarcosinate and sodium cocoyl sarcosinate, and the content of the surfactant A is 25 to 35 parts.
Furthermore, in the hair-strengthening and hair-restoring amino acid shampoo containing the sturgeon roe extract liposome, the surfactant B is one or more of cocamidopropyl betaine, lauramidopropyl betaine and hydroxysulfobetaine, and the content of the surfactant B is 10-25 parts.
Furthermore, the hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome comprises 15-25 parts of surfactant C, wherein the surfactant C is one or more of disodium lauryl sulfosuccinate, sodium myristoyl sarcosinate, sodium lauroyl methylaminopropionate, sodium lauroyl glutamate and sodium cocoyl glutamate.
Furthermore, the hair-strengthening and hair-nourishing amino acid shampoo containing the sturgeon roe extract liposome is characterized in that the preservative is one or more of phenoxyethanol, sodium benzoate, jasmonic acid and ethylhexyl glycerin, and the content of the preservative is 0.3-0.5.
The invention also discloses a preparation method of the hair-strengthening and hair-nourishing amino acid shampoo containing the sturgeon roe extract liposome, which comprises the following steps:
1) preparing sturgeon roe extract liposome;
2) stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature to disperse completely;
3) after the solution is stable, adding EDTA-2NA, and stirring and dispersing the solution completely;
4) after the solution is stabilized, heating the main tank to 65-75 ℃, adding the surfactant A, and stirring and dispersing completely;
5) after the solution is stable, adding the surfactants B and C, and stirring and dispersing completely;
6) cooling to below 50 ℃;
7) after the solution is stable, adding a preservative, and stirring and dispersing the preservative until the preservative is completely dissolved;
8) adding squalane and daily essence during stirring, and completely stirring and dispersing;
9) adding sturgeon roe extract liposome, stirring and dispersing completely;
10) adding a proper amount of citric acid according to the pH result, and stirring and completely dispersing;
11) stirring, cooling to 30 ℃, and bottling to obtain the sturgeon roe extract liposome hair-strengthening and hair-nourishing amino acid shampoo.
Further, the sturgeon roe extract liposome comprises the following formula components in percentage by total weight of the liposome:
60-85% of glycerol; 5 to 15 percent of water; 1-10% of caprylic capric triglyceride; 1-10% of lecithin; 0.2 to 5 percent of sturgeon roe extract.
Further, the preparation method of the sturgeon roe extract liposome comprises the following specific steps:
dispersing the lecithin in caprylic/capric triglyceride and glycerol, heating to 60-70 deg.C to form transparent yellow liquid, slowly adding deionized water at the same temperature under stirring to form slightly transparent yellowish liquid, slowly cooling to below 45 deg.C under stirring, adding sturgeon seed extract, stirring, cooling to 30 deg.C, filtering with 200 mesh sieve, and discharging to obtain sturgeon seed liposome.
Compared with the prior art, the invention has the following beneficial effects:
1) according to the invention, the sturgeon roe extract is wrapped by the liposome, and due to the double-layer wrapping effect of the liposome, the active ingredients of the sturgeon roe extract are more stable and more effective continuously;
2) according to the invention, the stable and uniform form of the sturgeon roe extract liposome hair-nourishing amino acid shampoo is realized by screening out a proper surfactant and a proper cationic polymer;
3) according to the invention, different sturgeon roe extract liposome quantities are adjusted, so that different products for nourishing scalp and strengthening and toughening hair roots can be obtained.
Drawings
FIG. 1 shows the results of the foaming force test in examples 1 to 3 of the present invention and the comparative example.
Detailed Description
The following detailed description of the embodiments of the present invention will be provided in conjunction with the embodiments, so that how to implement the technical solutions to solve the technical problems and achieve the technical effects of the present invention can be fully understood and implemented.
The invention discloses a hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and a preparation method thereof. The amino acid shampoo comprises the following components in parts by weight:
10-40 parts of a surfactant A; 1-30 parts of surfactant B; 1-30 parts of surfactant C; 0.01-5 parts of sturgeon roe extract liposome; 0.1 part of EDTA-2 NA; 0.5-5 parts of squalane; 0.01-2 parts of citric acid; 0.1-1 part of guar hydroxypropyl trimethyl ammonium chloride; 0-0.3 part of daily essence; 0-0.5 part of preservative; 100 parts of deionized water To.
The sources and the effect and the action principles of the raw material components of the invention are respectively introduced as follows:
1. surface active agent
The surfactants selected by the invention are respectively as follows: the main surfactants are surfactants A and C, which have main cleaning efficacy; the auxiliary surfactant is a surfactant B which mainly plays a role in thickening an amino acid system and enriching foams.
2. Sturgeon roe extract liposome
The sturgeon roe extract liposome is prepared from 60-85% of glycerin; 5-15% of deionized water; 1-10% of caprylic capric triglyceride; 1-10% of lecithin; 0.2-5% of sturgeon roe extract.
The glycerol is a carrier and a solvent for liposome formation and also has a certain humectant effect in a final product; caprylic capric triglyceride is an oil phase, lecithin is an important component for forming a bilayer structure, and the sturgeon roe extract forms a closed protection space by forming the bilayer structure, so that the protective activity is achieved and a certain slow release effect is achieved. The sturgeon roe extract is an active substance which effectively improves the health state of the scalp, and can make the scalp more healthy after long-term use, so that the hair is strong, tough, elastic and glossy.
Wherein the glycerol is selected from Neisseria malayi; the caprylic capric triglyceride is selected from Pasteur; the lecithin is selected from Japanese solar chemical S-10 (lecithin activity content 25% -30%); the sturgeon roe extract is selected from Shanghai Yi Cuminum biological technology Company and The Innovation Company, preferably Shanghai Yi Cuminum biological technology Company.
3. Other components
Wherein EDTA-2NA is a commercially available chelating agent; the squalane is a conditioner and is matched with the cationic polymer to provide good experience for the hair washing process; citric acid is a commercially available pH modifier; guar hydroxypropyl trimonium chloride is a cationic polymer, is selected from Nippon chemical, forms a flocculation structure through interaction with anionic surfactant and other conditioners, and can play a role in smoothing in a wet hair stage and smoothing in a dry hair process; the daily-use fragrance is selected from Qiwashington, the main fragrance source and is synergistically conditioned.
The invention aims to provide the shampoo which has good foaming capacity and cleaning capacity, is rich in foam and easy to wash, nourishes scalp and strengthens hair roots.
The following parts by weight may be in units of g or kg.
Example 1
A hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome comprises the following raw material components in parts by weight: 25 parts of cocoyl sarcosine sodium; 20 parts of lauramidopropyl betaine; 15 parts of sodium lauroyl glutamate, 0.3 part of sturgeon roe extract liposome, 0.1 part of EDTA-2NA, 1 part of squalane, 0.5 part of citric acid, 0.3 part of guar gum hydroxypropyl trimethyl ammonium chloride, 0.3 part of daily essence, 0.5 part of preservative and 100 parts of deionized water To.
Wherein, the sturgeon roe extract liposome is prepared from 65% of glycerin; 15% of water; caprylic capric triglyceride 10%; 5% of lecithin; 5 percent of sturgeon roe extract.
The preparation method comprises the following steps of:
1) preparing a sturgeon roe extract: dispersing lecithin in caprylic/capric triglyceride and glycerol, heating to 60-70 deg.C to form transparent yellow liquid, slowly adding deionized water at the same temperature under stirring to form slightly transparent yellowish liquid, slowly cooling to below 45 deg.C under stirring, adding sturgeon roe extract, stirring, cooling to 30 deg.C, filtering with 200 mesh sieve, and discharging to obtain sturgeon roe extract liposome;
2) stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature to disperse completely;
3) after the solution is stable, adding EDTA-2NA, and stirring and dispersing the solution completely;
4) after the solution is stabilized, heating the main tank to 65-75 ℃, adding sodium cocoyl sarcosinate, and stirring and dispersing completely;
5) after the solution is stable, adding lauramidopropyl betaine and sodium lauroyl glutamate, and stirring and dispersing completely;
6) cooling to below 50 ℃;
7) after the solution is stable, adding preservatives phenoxyethanol and ethylhexyl glycerol, and stirring and dispersing the mixture until the mixture is complete;
8) adding squalane and daily essence during stirring, and completely stirring and dispersing;
9) adding sturgeon roe extract, and stirring and dispersing completely;
10) adding a proper amount of citric acid according to the pH result, and stirring and completely dispersing;
11) stirring, cooling to 30 ℃, and bottling to obtain the sturgeon roe extract liposome hair-strengthening and hair-nourishing amino acid shampoo.
Example 2
The amino acid shampoo containing sturgeon roe extract liposome for strengthening and restoring hair comprises the following raw material components in parts by weight:
30 parts of sodium methyl cocoyl taurate; 20 parts of hydroxysulfobetaine; 15 parts of sodium myristoyl sarcosinate, 0.6 part of sturgeon seed extract liposome, 0.1 part of EDTA-2NA, 4 parts of squalane, 0.5 part of citric acid, 0.3 part of guar gum hydroxypropyl trimethyl ammonium chloride, 0.3 part of daily essence, 0.5 part of preservative and 100 parts of deionized water To.
Wherein, the sturgeon roe extract liposome is prepared from 85% of glycerin; 5% of water; caprylic capric triglyceride 5%; 9.8% of lecithin; 0.2 percent of sturgeon roe extract.
The preparation method comprises the following steps of:
1) preparing sturgeon roe extract liposome: dispersing lecithin in caprylic/capric triglyceride and glycerol, heating to 60-70 deg.C to form transparent yellow liquid, slowly adding deionized water at the same temperature under stirring to form slightly transparent yellowish liquid, slowly cooling to below 45 deg.C under stirring, adding sturgeon roe extract, stirring, cooling to 30 deg.C, filtering with 200 mesh sieve, and discharging to obtain sturgeon roe extract liposome.
2) Stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature to disperse completely;
3) after the solution is stable, adding EDTA-2NA, and stirring and dispersing the solution completely;
4) after the solution is stabilized, heating the main tank to 65-75 ℃, adding sodium methyl cocoyl taurate, and stirring and dispersing completely;
5) after the solution is stable, adding hydroxysulfobetaine and myristoyl sarcosine sodium, and stirring and dispersing completely;
6) cooling to below 50 ℃;
7) after the solution is stable, adding preservatives pentanediol and sodium benzoate, and stirring and dispersing the mixture till the mixture is complete;
8) adding squalane and daily essence during stirring, and completely stirring and dispersing;
9) adding sturgeon roe extract liposome, stirring and dispersing completely;
10) adding a proper amount of citric acid according to the pH result, and stirring and completely dispersing;
11) stirring, cooling to 30 ℃, and bottling to obtain the sturgeon roe extract hair-strengthening and hair-nourishing amino acid shampoo.
Example 3
The amino acid shampoo containing sturgeon roe extract liposome for strengthening and restoring hair comprises the following raw material components in parts by weight:
28 parts of sodium lauroyl sarcosinate; 20 parts of cocamidopropyl betaine; 17 parts of disodium laureth sulfosuccinate, 0.6 part of salmon roe extract liposome, 0.1 part of EDTA-2NA, 4 parts of squalane, 0.5 part of citric acid, 0.4 part of guar gum hydroxypropyl trimethyl ammonium chloride, 0.3 part of daily essence, 0.5 part of preservative and 100 parts of deionized water To.
Wherein, the sturgeon roe extract liposome is 75% of glycerol calculated according to the total amount of the liposome; 10% of water; 1% of caprylic capric triglyceride; 9% of lecithin; 5 percent of sturgeon roe extract.
The preparation method comprises the following steps of:
1) preparing sturgeon roe extract liposome: dispersing lecithin in caprylic/capric triglyceride and glycerol, heating to 60-70 deg.C to form transparent yellow liquid, slowly adding deionized water at the same temperature under stirring to form slightly transparent yellowish liquid, slowly cooling to below 45 deg.C under stirring, adding sturgeon roe extract, stirring, cooling to 30 deg.C, filtering with 200 mesh sieve, and discharging to obtain sturgeon roe extract liposome;
2) stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature to disperse completely;
3) after the solution is stable, adding EDTA-2NA, and stirring and dispersing the solution completely;
4) after the solution is stabilized, heating the main tank to 65-75 ℃, adding sodium lauroyl sarcosine, and stirring and dispersing completely;
5) after the solution is stable, adding the cocamidopropyl betaine and disodium laureth sulfosuccinate, and stirring and dispersing completely;
6) cooling to below 50 ℃;
7) after the solution is stable, adding preservatives, namely the jasmonic acid and the caprylyl glycol, and stirring and dispersing the mixture till the mixture is complete;
8) adding squalane and daily essence during stirring, and completely stirring and dispersing;
9) adding sturgeon roe extract liposome, stirring and dispersing completely;
10) adding a proper amount of citric acid according to the pH result, and stirring and completely dispersing;
11) stirring, cooling to 30 ℃, and bottling to obtain the sturgeon roe extract liposome hair-strengthening and hair-nourishing amino acid shampoo.
The following are contents of the effect test examples.
In addition, to better evaluate the efficacy of each example, the following experiments were performed:
effect test example 1(Performance test)
1.1 Dry Wet combing Performance
Preparing six hair strands damaged to the same extent, soaking in 5% sodium lauryl sulfate aqueous solution for 2 hr, washing with corresponding shampoo, and testing wet comb;
after being naturally dried for 24 hours, the dry combing was tested, and wet combing performance and dry combing performance were tested using a multifunctional hair tester (model: british DIA-strong MTT 175), each set of test data being an average value after 10 parallel tests, and the dry and wet combing performance test results are shown in table 1 below:
TABLE 1 Dry and Wet combing Performance test results
Note: comparative example 1 is a product prepared by removing the liposome content of the sturgeon roe extract of example 1; comparative example 2 is a product prepared by removing the liposome content of the sturgeon roe extract of example 2; comparative example 3 is a product prepared by removing the liposome content of the sturgeon roe extract of example 3; the control was a commercial shampoo.
According to the results in the table 1, the dry-wet combing property of the hair is obviously improved after the sturgeon roe extract liposome is added, and compared with a control group (commercially available shampoo), the dry-wet combing property of the hair is improved by the shampoo prepared by the formula provided by the invention, so that the sturgeon roe extract liposome hair-strengthening and hair-nourishing amino acid shampoo provided by the invention has the effect of repairing and lubricating the hair.
1.2 testing of foaming Properties
The foaming power of the shampoo was measured by a Roche foamer (model: GB-T74621994), each set of data was an average value of 10 parallel tests, and the results of the measurement of the foaming power performance of the amino acid shampoo for strengthening and nourishing hair using the fish roe extract liposome prepared in the above examples 1 to 3 are shown in FIG. 1.
The results according to fig. 1 show that the foaming effect of the example group is significantly better than that of the control group.
Effect test example 2(clinical test)
2.1 testing of toughness, scalp itching and gloss
Subject: 400 volunteers with damaged hair aged 30-50 years.
The experimental method comprises the following steps: the volunteers were divided into 4 groups of 100 persons, and the 1 st to 4 th groups were treated with the inventive examples 1, 2, 3 and control, respectively, once a day, and 2.5g of the inventive liquid shampoo was administered each time. The effect was observed on day 7, respectively, and the results were measured, as shown in table 2.
TABLE 2 tenacity, scalp itch and gloss tests
According to the experimental data in the table 2, the shampoo prepared in the embodiments 1 to 3 can obviously enhance the toughness and glossiness of the hair and reduce the itching degree of the scalp.
2.2 Effect of sturgeon roe extract liposome addition on product Performance
Taking example 1 as an example, the influence of the amount of the sturgeon roe on the product performance is explored by regulating and controlling the amount of the sturgeon roe, and the specific experimental test results are shown in the following table 3.
TABLE 3 Effect of the added amount of liposomes in Acipenser sinensis roe extract on the product Properties
| Performance of | 0％ | 0.3％ | 0.6％ | 0.9％ | 1.2％ | 1.5％ | 1.8％ |
| Hair strength and toughness | 8.5 | 9.0 | 9.3 | 9.3 | 9.4 | 9.5 | 9.5 |
| Degree of scalp itching | 8.8 | 9.2 | 9.3 | 9.3 | 9.4 | 9.3 | 9.4 |
| Degree of gloss | 6.6 | 7.5 | 7.8 | 8.0 | 8.0 | 8.0 | 8.1 |
Note: the score was 10 points.
Note: the quality is obviously improved; preferably, there is a slight improvement; the ineffectiveness was no improvement.
From the content in the table 3, it can be seen that increasing the addition amount of the sturgeon roe extract liposome has significant effects on hair toughness and scalp itching resistance, but the effect is not increased obviously after excessive addition, the cost is increased more, and the addition amount of 0.6% is ideal. In addition, the glossiness of the shampoo can be well improved by adding the sturgeon roe extract liposome.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (9)
1. The hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome is characterized by being prepared from the following components in parts by weight:
10-40 parts of a surfactant A;
the surfactant A is one or more of sodium cocoyl isethionate, sodium methyl cocoyl taurate, sodium lauroyl sarcosinate and sodium cocoyl sarcosinate;
1-30 parts of a surfactant B;
the surfactant B is one or more of cocamidopropyl betaine, lauramidopropyl betaine and hydroxysulfobetaine;
1-30 parts of a surfactant C;
the surfactant C is one or more of disodium lauryl sulfosuccinate, sodium myristoyl sarcosinate, sodium lauroyl methylaminopropionate, sodium lauroyl glutamate and sodium cocoyl glutamate;
0.01-5 parts of sturgeon roe extract liposome;
according to the total amount of the liposome, the sturgeon roe extract liposome comprises the following components in percentage by weight:
60-85% of glycerol; 5 to 15 percent of water; 1-10% of caprylic capric triglyceride; 1-10% of lecithin; 0.2-5% of sturgeon roe extract;
dispersing the lecithin in caprylic/capric triglyceride and glycerol, heating to 60-70 ℃ to form transparent yellow liquid, slowly adding deionized water at the same temperature under stirring to form slightly transparent yellowish liquid, slowly cooling to below 45 ℃ under stirring, adding the sturgeon roe extract, stirring, cooling to 30 ℃, filtering with 200 meshes, and discharging to obtain the sturgeon roe liposome;
2. the hair-strengthening amino acid shampoo containing sturgeon roe extract liposome according to claim 1, which is characterized in that: the content of the surfactant A is 25-35 parts.
3. The hair-strengthening amino acid shampoo containing sturgeon roe extract liposome according to claim 1, which is characterized in that: the content of the surfactant B is 10-25 parts.
4. The hair-strengthening amino acid shampoo containing sturgeon roe extract liposome according to claim 1, which is characterized in that: the content of the surfactant C is 15-25 parts.
5. The hair-strengthening amino acid shampoo containing sturgeon roe extract liposome according to claim 1, which is characterized in that:
the preservative is one or more of phenoxyethanol, sodium benzoate, jasmonic acid, ethylhexyl glycerol, pentanediol and caprylyl glycol.
6. The hair-strengthening amino acid shampoo containing sturgeon roe extract liposome according to claim 1, which is characterized in that: the content of the sturgeon roe extract liposome is 0.6 part.
7. The preparation method of the hair-strengthening and hair-nourishing amino acid shampoo containing the sturgeon roe extract liposome is characterized by comprising the following steps of:
1) preparing sturgeon roe extract liposome;
2) stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature to disperse completely;
3) after the solution is stable, adding EDTA-2NA, and stirring and dispersing the solution completely;
4) after the solution is stabilized, heating the main tank to 65-75 ℃, adding the surfactant A, and stirring and dispersing completely;
5) after the solution is stable, adding the surfactants C and B, and stirring and dispersing completely;
6) cooling to below 50 ℃;
7) after the solution is stable, adding a preservative, and stirring and dispersing the preservative until the preservative is completely dissolved;
8) adding squalane and daily essence during stirring, and completely stirring and dispersing;
9) adding sturgeon roe extract liposome, stirring and dispersing completely;
10) adding a proper amount of citric acid according to the pH result, and stirring and completely dispersing;
11) stirring, cooling to 30 ℃, and bottling to obtain the sturgeon roe extract liposome hair-strengthening and hair-nourishing amino acid shampoo.
8. The method of claim 7, wherein: stirring guar hydroxypropyl trimethyl ammonium chloride in deionized water at normal temperature for completely dispersing for 15-25 minutes at the speed of 100-500 r/min.
9. The method of claim 7, wherein: in the step 4), the heating temperature is between 65 and 75 ℃; the stirring speed for stirring and dispersing completely is 100-300 r/min.
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| CN113509429B (en) * | 2021-07-19 | 2023-11-03 | 加来(济南)生活科技有限公司 | Liposome anti-wrinkle composition containing sturgeon caviar extract, and preparation method and application thereof |
| KR102519730B1 (en) * | 2022-10-13 | 2023-04-10 | 이용광 | Functional composition for hair loss relief and hair growth containing sturgeon extract |
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