CN113876672A - Amino acid mild tear-free natural plant shampoo and preparation method thereof - Google Patents
Amino acid mild tear-free natural plant shampoo and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses an amino acid mild lachrymatory natural plant shampoo and a preparation method thereof. The amino acid mild tear-free natural plant shampoo disclosed by the invention takes the amino acid surfactant as a foaming cleaning agent, is rich in natural active ingredients, is mild in formula and tear-free, can obviously reduce the occurrence of skin eczema, has no stimulation to hair, skin and eyes, is close to infant washing products, provides hair nutrition, and has the advantages of bright, smooth, elastic, good dry and wet combing property, refreshing and moistening feeling, natural and healthy itching relieving effect and the like.
Description
Technical Field
The invention relates to the technical field of daily chemical industry, in particular to amino acid mild tear-free natural plant shampoo and a preparation method thereof.
Background
The hair is a natural polymer ramie formed by completely keratinized horny cells, the horny cells are filled with keratin consisting of a plurality of amino acids, the content of cysteine is the highest, and the hair also contains a plurality of trace elements and needs nutrition.
Along with the trend of naturalization, nutrition and curative effect of shampoo products, the compound shampoo of natural Chinese herbal medicines, plant extract and natural nutriments which have no side effect and have curative effect and nutritional effect is more and more favored by consumers. At present, the compound shampoo on the market is various in types, is easy to stimulate eyes, and still has no obvious effect on the treatment of the problems of scurf, hair oil, scalp itch, alopecia, moisture retention and the like.
Therefore, the problem to be solved by the technical personnel in the field is urgently needed to provide the amino acid mild tear-free natural plant shampoo which is mild, non-irritating, healthy and environment-friendly.
Disclosure of Invention
In view of the above, the invention provides the amino acid mild lacrimation-free natural plant shampoo, which adopts a mild lacrimation-free formula to gently care the tender eye mask; the cosmetic is characterized in that a parent amino acid component and coconut oil essence are adopted, natural plant extracts such as an aloe extract, a magnolia flower extract, a chamomile extract, a malt extract, a tea tree extract and an olive extract are adopted, no harmful substances such as silicone oil, alcohol and pigment are contained, the cosmetic is rich in natural active ingredients, mild and non-irritant, healthy and environment-friendly, the hair is effectively moistened, the combing performance and scalp antibacterial activity of the hair are improved, and the dandruff is reduced.
In order to achieve the purpose, the invention adopts the following technical scheme:
an amino acid mild tear-free natural plant shampoo comprises the following components in parts by weight: 30-50 parts of amino acid surfactant, 10-15 parts of aloe extract, 10-20 parts of magnolia extract, 10-15 parts of chamomile extract, 15-20 parts of malt extract, 10-15 parts of olive extract, 5-10 parts of carrot extract, 5-10 parts of cocamidopropyl betaine, 5-10 parts of lauramidopropyl amine oxide, 3-5 parts of lactic acid, 5-10 parts of coconut fatty acid monoethanolamide, 5-10 parts of natural betaine, 5-10 parts of salicylic acid, 3-5 parts of alkyl glycoside, 3-5 parts of citric acid and 1-3 parts of plant essential oil.
Preferably, the following components in parts by weight are included: 35-45 parts of amino acid surfactant, 12-14 parts of aloe extract, 13-18 parts of magnolia extract, 12-14 parts of chamomile extract, 17-19 parts of malt extract, 7-8 parts of carrot extract, 7-8 parts of cocamidopropyl betaine, 7-8 parts of lauramidopropyl amine oxide, 3-5 parts of lactic acid, 12-14 parts of olive extract, 7-8 parts of coconut fatty acid monoethanolamide, 7-8 parts of natural betaine, 7-8 parts of salicylic acid, 3-5 parts of alkyl glycoside, 3-5 parts of citric acid and 1-3 parts of plant essential oil.
Preferably, the following components in parts by weight are included: 40 parts of amino acid surfactant, 13 parts of aloe extract, 15 parts of magnolia flower extract, 13 parts of chamomile extract, 18 parts of malt extract, 12 parts of olive extract, 7 parts of carrot extract, 7 parts of cocamidopropyl betaine, 7 parts of lauramidopropyl amine oxide, 4 parts of lactic acid, 7 parts of coconut oil fatty acid monoethanolamide, 7 parts of natural betaine, 8 parts of salicylic acid, 4 parts of alkyl glycoside, 4 parts of citric acid and 2 parts of plant essential oil.
Preferably, the amino acid surfactant is one or a mixture of more of sodium cocoyl glutamate, disodium cocoyl glutamate, potassium cocoyl glutamate, TEA (cocoyl glutamate), sodium lauroyl glutamate, sodium methyl lauroyl taurate, sodium lauroyl sarcosinate and sodium myristoyl sarcosinate.
Preferably, the liquid soap further comprises a conditioning agent, a thickening agent and an emulsifying agent.
Preferably, the conditioning agent is a mixture of propylene glycol, polyquaternium-10, panthenol; the thickening agent is a mixture of guar gum hydroxypropyl trimethyl ammonium chloride and pyridone ethanolamine salt; the emulsifier is water-soluble lanolin.
Preferably, the plant essential oil is one or a mixture of rose essential oil, cherry essential oil and grape essential oil.
Preferably, the alkyl glucoside is one or a mixture of lauryl glucoside, coco glucoside, octyl glucoside and myristyl glucoside.
Preferably, C is also included14-C18Olefin sodium sulfonate, DMDM hydantoin, methyl benzoate, trimethylglycine, propyl acetate, lactic acid, EDTA disodium and phenoxyethanol.
The invention also provides a preparation method of the amino acid mild tear-free natural plant shampoo, which comprises the following steps:
s1, preparation of plant extracts: cleaning the raw materials, and performing ultraviolet sterilization to obtain pretreated raw materials; distilling and extracting aloe, magnolia flower, chamomile, malt, olive and carrot in the pretreated raw materials by a steam distillation method respectively to obtain raw material extracts for later use;
s2, mixing an amino acid surfactant, coconut monoethanolamide, cocamidopropyl betaine, lauramidopropyl amine oxide, lactic acid, natural betaine, salicylic acid and alkyl glycoside with a proper amount of deionized water according to the weight parts, heating to 75-85 ℃, and stirring for 10-30min until the raw materials are completely dissolved;
s3, cooling the system to 40 ℃, adding the raw material extract obtained in the step S1, mixing and stirring uniformly according to the parts by weight, stirring for 10-30min, adding the plant essential oil, stirring and adjusting the viscosity to 7000-9000cP, adding the citric acid to adjust the pH to 5.5-5.8, stirring under the vacuum condition, cooling to 37 ℃, discharging, and filling to obtain the amino acid mild tear-free natural plant shampoo.
The invention also provides application of the amino acid mild tear-free natural plant shampoo in washing and caring products.
In the plant extract, the aloe is rich in vitamins and mineral elements, has the effects of sterilization and inflammation resistance, can balance the pH value of hair, clean pores of the hair, keep the hair moist, stimulate the hair growth cycle and reduce grease secretion; aloe has effects of clearing liver heat, bitter and cold nature, repairing tissue injury, regulating immunity, killing bacteria, cleaning follicular orifice, and protecting hair. The magnolia flower contains various vitamins and alkaloids, has unique volatile oil property, pungent taste and warm property, and has the effects of dispelling wind and cold, dredging orifices, ventilating lung and relieving stuffy nose. The chamomile can moisturize the skin by prolonging the life of stem cells, has the effects of calming, resisting allergy, whitening, resisting inflammation, repairing, relieving itching and the like, and can add bright luster to hair. The malt extract contains abundant vitamins, and can deeply moisten hair roots. The olive extract is purified by a special process and is rich in minerals such as protein, calcium, iron, phosphorus and the like, vitamin A, B, C, D, E and the like, and can promote blood circulation of tiny blood vessels and regulate grease secretion. Has effects of resisting oxidation, scavenging free radicals, and protecting scalp cells, nourishing scalp, and resisting fungi invasion.
According to the technical scheme, compared with the prior art, the amino acid mild tear-free natural plant shampoo disclosed by the invention has the following beneficial effects:
(1) the amino acid mild tear-free natural plant shampoo disclosed by the invention takes the amino acid surfactant as a foaming cleaning agent, is rich in natural active ingredients, is mild in formula and tear-free, can obviously reduce the occurrence of skin eczema, has no stimulation to hair, skin and eyes, is close to infant washing products, provides hair nutrition, and has the advantages of bright, smooth, elastic, dry and wet hair combing property, refreshing and moistening feeling, natural and healthy itching relieving effect.
(2) The surfactant of the invention has the functions of wetting, foaming, defoaming, dispersing, washing, corrosion prevention, antistatic and the like. The thickener can improve and increase the viscosity of shampoo, and make the foam rich and keep the smell. The plant essential oil is an aromatic substance which is specially extracted from plants, contains natural moistening components and can soften the scalp. The olive extract is a natural plant formulation, is easily absorbed, and helps to regulate the pH of the skin. The alkyl glycoside is a highly safe surface active ingredient, and can be used for washing scalp, softening head cradle cap, and removing head dirt.
(3) The amino acid surfactant has the characteristics of good wettability, foamability, antibacterial, corrosion-resistant and antistatic capabilities and the like, is non-toxic and harmless, is mild to skin, has no influence on the environment because degradation products are amino acid and fatty acid, and has good compatibility with other surfactants. The flos Matricariae Chamomillae essence is the concentrated part of the plant essence, and has antiinflammatory, itching relieving, disinfectant, antibacterial, and allergy relieving effects. In addition, the invention selects the alkyl glycoside, which has low surface tension, strong wetting power, rich and fine foam, no toxicity, no harm, no stimulation to skin and broad-spectrum antibacterial activity.
(4) The preparation method of the amino acid mild tear-free natural plant shampoo is simple and efficient, and is suitable for industrial production.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The embodiment discloses an amino acid mild tear-free natural plant shampoo which comprises the following components in parts by weight: 50 parts of amino acid surfactant, 15 parts of aloe extract, 20 parts of magnolia flower extract, 10 parts of chamomile extract, 15 parts of malt extract, 10 parts of olive extract, 10 parts of carrot extract, 10 parts of cocamidopropyl betaine, 10 parts of lauramidopropyl amine oxide, 3 parts of lactic acid, 10 parts of coconut oil fatty acid monoethanolamide, 10 parts of natural betaine, 10 parts of salicylic acid, 5 parts of alkyl glycoside, 3 parts of citric acid and 3 parts of plant essential oil.
Wherein the amino acid surfactant is sodium lauroyl sarcosine, the plant essential oil is rose essential oil, and the alkyl glycoside is lauryl glucoside.
In order to optimize the technical scheme, the raw materials also comprise propylene glycol, polyquaternium-10, panthenol, guar gum hydroxypropyl trimethyl ammonium chloride, pyridone ethanolamine salt and water-soluble lanolin.
In order to optimize the technical scheme, the raw materials also comprise C14-C18Olefin sodium sulfonate, DMDM hydantoin, methyl benzoate, trimethylglycine, propyl acetate, lactic acid, EDTA disodium and phenoxyethanol.
Example 2
The embodiment discloses an amino acid mild tear-free natural plant shampoo which comprises the following components in parts by weight: 30 parts of amino acid surfactant, 10 parts of aloe extract, 10 parts of magnolia flower extract, 15 parts of chamomile extract, 20 parts of malt extract, 15 parts of olive extract, 5 parts of carrot extract, 5 parts of cocamidopropyl betaine, 5 parts of lauramidopropyl amine oxide, 5 parts of lactic acid, 5 parts of coconut oil fatty acid monoethanolamide, 5 parts of natural betaine, 5 parts of salicylic acid, 3 parts of alkyl glycoside, 3 parts of citric acid and 3 parts of plant essential oil.
Wherein the amino acid surfactant is cocoyl glutamic acid TEA salt, the plant essential oil is cherry essential oil, and the alkyl glycoside is cocoyl glucoside.
Example 3
The embodiment discloses an amino acid mild tear-free natural plant shampoo which comprises the following components in parts by weight: 40 parts of amino acid surfactant, 13 parts of aloe extract, 15 parts of magnolia flower extract, 13 parts of chamomile extract, 18 parts of malt extract, 12 parts of olive extract, 7 parts of carrot extract, 7 parts of cocamidopropyl betaine, 7 parts of lauramidopropyl amine oxide, 4 parts of lactic acid, 7 parts of coconut oil fatty acid monoethanolamide, 7 parts of natural betaine, 8 parts of salicylic acid, 4 parts of alkyl glycoside, 4 parts of citric acid and 2 parts of plant essential oil.
Wherein the amino acid surfactant is sodium lauroyl glutamate, the plant essential oil is grape essential oil, and the alkyl glycoside is myristyl glucoside.
Example 4
The embodiment discloses a preparation method of amino acid mild tear-free natural plant shampoo, which comprises the following steps:
s1, preparation of plant extracts: cleaning the raw materials, and performing ultraviolet sterilization to obtain pretreated raw materials; distilling and extracting aloe, magnolia flower, chamomile, malt, olive and carrot in the pretreated raw materials by a steam distillation method respectively to obtain raw material extracts for later use;
s2, mixing an amino acid surfactant, coconut oil fatty acid monoethanolamide, cocamidopropyl betaine, lauramidopropyl amine oxide, lactic acid, natural betaine, salicylic acid and alkyl glycoside with a proper amount of deionized water according to parts by weight, heating to 75-85 ℃, and stirring for 10-30min until the raw materials are completely dissolved, wherein the deionized water accounts for 100-200 parts;
s3, cooling the system to 40 ℃, adding the raw material extract obtained in the step S1, mixing and stirring uniformly according to the parts by weight, stirring for 10-30min, adding the plant essential oil, stirring and adjusting the viscosity to 7000-9000cP, adding the citric acid to adjust the pH to 5.5-5.8, stirring under the vacuum condition, cooling to 37 ℃, discharging, and filling to obtain the amino acid mild tear-free natural plant shampoo.
The technological parameters in the preparation method of the amino acid mild tear-free natural plant shampoo can be selected according to actual needs.
The formula of the hair cream is mild, eyes of infants cannot be stimulated, the head skin can be effectively protected, the occurrence of skin eczema can be obviously reduced, the symptoms of dry and itchy hair can be improved, hair nutrition can be provided, scalp blood circulation can be promoted, and the secretion of scalp grease can be effectively inhibited.
The amino acid mild tear-free natural plant shampoo disclosed by the invention is used for testing the skin irritation.
The skin irritation test was performed as required by the cosmetic hygiene code (2007). The test method comprises the following steps: healthy, adult and skin-damage-free white rabbits are selected for 3 animals, 24 hours before experiment, the two sides of the spine of the back of each rabbit are sheared respectively, the epidermis cannot be damaged, and the hair removing range is respectively 2.5cm multiplied by 2.5 cm. 0.3ml of the shampoo baths of examples 1 to 3 were applied to the hair-removed area of 2.2cm X2.2 cm, respectively. The other side was coated with distilled water as a control. Coating once a day, trimming hair before each coating, removing residual test substance with warm water, and continuously coating for 15 days. The results of the experiment are as follows:
the tested sample points were in the range of 0-0.5 according to skin irritation intensity classification of "cosmetic hygiene standards", which indicates that the sample is not irritating to the skin, and as shown in the above table, the shampoo of the present invention of examples 1-5 is non-irritating to the skin, wherein the shampoo of example 3 has the lowest influence on the skin.
The eye irritation test of the amino acid mild tear-free natural plant shampoo is carried out by adopting a chick embryo chorioallantoic membrane experiment (HET-CAM).
The chick embryo chorioallantoic membrane test (HET-CAM) is an in vitro ocular irritant assessment method, and the chorioallantoic membrane (CAM) is a respiratory membrane that surrounds the chick embryo. The test utilizes the characteristics of complete, obvious and transparent vascular system of chorioallantoic membrane in middle stage of hatched 9-day embryo fertilized chick embryo, a certain amount of test substance is directly contacted with chorioallantoic membrane of chick embryo, the change of chorioallantoic membrane toxicity effect indexes (such as bleeding, blood coagulation and blood vessel melting) is observed after a period of action, and the indexes reflect the change of morphological structure, color and permeability of blood vessels and blood vessel network, reflect the phenomena of chorioallantoic membrane protein denaturation and the damage degree thereof, and then a score is obtained by combination for evaluating the eye irritation of the test substance.
The specific test method is as follows: purchasing 0-day-old chicken embryos, culturing in an incubator at 37.5 +/-0.5 ℃ and with relative humidity of 50-60%, checking the condition of the chicken embryos by using an egg candler when the chicken embryos are incubated for 9 days, and discarding the chicken embryos which are not incubated to live or fertilized.
Selecting 6 alive chick embryos, and taking out the chorioallantoic membranes for use according to a correct operation method. 0.3mL of the amino acid mild lacrimation-free shampoo is directly dripped on the surface of a chorioallantoic membrane, the reaction condition of the chorioallantoic membrane is observed under a microscope, and the time of each toxic effect within 5 minutes of action is recorded. And additionally arranging a negative control group and a positive control group, selecting a sodium chloride solution with the mass concentration of 0.9% as the negative control group, and selecting a 0.1mol/L sodium hydroxide solution as the positive control group.
And (4) evaluating the results: the test was a liquid sample and the irritation was assessed by the reaction time method. The stimulation score (IS) was calculated using the following formula:
in the formula: SecH: (bleeding time, the average time to onset of bleeding observed on the chorioallantoic membrane in seconds/s); SecL: (vascular melting time, the average time to onset of vascular melting observed on the chorioallantoic membrane in seconds/s); SecC: (clotting time, the average time to the onset of clotting observed on the chorioallantoic membrane in seconds/s); note: if no corresponding vascular effect occurs, the time is recorded as 301 seconds.
Classifying the eye irritation of the test object according to the calculated IS value: IS IS less than 1, and has no irritation; IS IS more than or equal to 1 and less than 5, and IS slightly irritant; IS IS more than or equal to 5 and less than 9, and moderate irritation; IS IS more than or equal to 10 and IS strong in irritation.
The results of the experiment are as follows:
as can be seen from the above table, the IS values of the amino acid mild lacrimation-free natural plant shampoo disclosed by the invention in examples 1-3 are 0.01, 0.02 and 0 respectively, which indicates that the amino acid mild lacrimation-free natural plant shampoo has no irritation to human eyes. Therefore, the soft eye mask adopts a mild lacrimation formula, and gently cares the tender eye mask of a user.
The embodiments in the present description are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same and similar parts among the embodiments are referred to each other.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (10)
1. The amino acid mild tear-free natural plant shampoo is characterized by comprising the following components in parts by weight: 30-50 parts of amino acid surfactant, 10-15 parts of aloe extract, 10-20 parts of magnolia extract, 10-15 parts of chamomile extract, 15-20 parts of malt extract, 10-15 parts of olive extract, 5-10 parts of carrot extract, 5-10 parts of cocamidopropyl betaine, 5-10 parts of lauramidopropyl amine oxide, 3-5 parts of lactic acid, 5-10 parts of coconut fatty acid monoethanolamide, 5-10 parts of natural betaine, 5-10 parts of salicylic acid, 3-5 parts of alkyl glycoside, 3-5 parts of citric acid and 1-3 parts of plant essential oil.
2. The amino acid mild tear-free natural plant shampoo as claimed in claim 1, comprising the following components in parts by weight: 35-45 parts of amino acid surfactant, 12-14 parts of aloe extract, 13-18 parts of magnolia extract, 12-14 parts of chamomile extract, 17-19 parts of malt extract, 7-8 parts of carrot extract, 7-8 parts of cocamidopropyl betaine, 7-8 parts of lauramidopropyl amine oxide, 3-5 parts of lactic acid, 12-14 parts of olive extract, 7-8 parts of coconut fatty acid monoethanolamide, 7-8 parts of natural betaine, 7-8 parts of salicylic acid, 3-5 parts of alkyl glycoside, 3-5 parts of citric acid and 1-3 parts of plant essential oil.
3. The amino acid mild tear-free natural plant shampoo as claimed in claim 1, comprising the following components in parts by weight: 40 parts of amino acid surfactant, 13 parts of aloe extract, 15 parts of magnolia flower extract, 13 parts of chamomile extract, 18 parts of malt extract, 12 parts of olive extract, 7 parts of carrot extract, 7 parts of cocamidopropyl betaine, 7 parts of lauramidopropyl amine oxide, 4 parts of lactic acid, 7 parts of coconut oil fatty acid monoethanolamide, 7 parts of natural betaine, 8 parts of salicylic acid, 4 parts of alkyl glycoside, 4 parts of citric acid and 2 parts of plant essential oil.
4. The amino acid mild tear-free natural plant shampoo according to any one of claims 1-3, wherein the amino acid surfactant is one or a mixture of sodium cocoyl glutamate, disodium cocoyl glutamate, potassium cocoyl glutamate, TEA cocoyl glutamate, sodium lauroyl glutamate, sodium methyl lauroyl taurate, sodium lauroyl sarcosinate and sodium myristoyl sarcosinate.
5. The amino acid mild tear-free natural plant shampoo as claimed in any one of claims 1-3, further comprising a conditioner, a thickener, and an emulsifier.
6. The amino acid mild tear-free natural plant shampoo as defined in claim 5, wherein the conditioner is a mixture of propylene glycol, polyquaternium-10, panthenol; the thickening agent is a mixture of guar gum hydroxypropyl trimethyl ammonium chloride and pyridone ethanolamine salt; the emulsifier is water-soluble lanolin.
7. The amino acid mild tear-free natural plant shampoo as claimed in any one of claims 1-3, wherein the plant essential oil is one or a mixture of rose essential oil, cherry essential oil and grape essential oil.
8. The amino acid mild tear-free natural plant shampoo as claimed in any one of claims 1 to 3 wherein the alkyl glycoside is one or a mixture of lauryl glucoside, coco glucoside, octyl glucoside and myristyl glucoside.
9. A method for preparing the amino acid mild tear-free natural plant shampoo as defined in any one of claims 1 to 8, comprising the steps of:
s1, preparation of plant extracts: cleaning the raw materials, and performing ultraviolet sterilization to obtain pretreated raw materials; distilling and extracting aloe, magnolia flower, chamomile, malt, olive and carrot in the pretreated raw materials by a steam distillation method respectively to obtain raw material extracts for later use;
s2, mixing an amino acid surfactant, coconut monoethanolamide, cocamidopropyl betaine, lauramidopropyl amine oxide, lactic acid, natural betaine, salicylic acid and alkyl glycoside with a proper amount of deionized water according to the weight parts, heating to 75-85 ℃, and stirring for 10-30min until the raw materials are completely dissolved;
s3, cooling the system to 40 ℃, adding the raw material extract obtained in the step S1, mixing and stirring uniformly according to the parts by weight, stirring for 10-30min, adding the plant essential oil, stirring and adjusting the viscosity to 7000-9000cP, adding the citric acid to adjust the pH to 5.5-5.8, stirring under the vacuum condition, cooling to 37 ℃, discharging, and filling to obtain the amino acid mild tear-free natural plant shampoo.
10. Use of the amino acid mild tear-free natural plant shampoo according to any one of claims 1-8, wherein the amino acid mild tear-free natural plant shampoo is used in a cleaning product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114569527A (en) * | 2022-03-08 | 2022-06-03 | 杨卓涛 | Multi-effect repairing shampoo |
| CN115778878A (en) * | 2022-12-22 | 2023-03-14 | 广州世航生物科技有限公司 | Hair care composition and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
| CN108096173A (en) * | 2017-12-28 | 2018-06-01 | 广州蜜妆生物科技有限公司 | Mild amino acid shampoo of a kind of green and preparation method thereof |
-
2020
- 2020-07-01 CN CN202010628996.6A patent/CN113876672A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
| CN108096173A (en) * | 2017-12-28 | 2018-06-01 | 广州蜜妆生物科技有限公司 | Mild amino acid shampoo of a kind of green and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 广州市花郡名臣生物科技有限公司: "优丝雨氨基酸鲜姜净爽洗发露", pages 108 - 3 * |
| 张春花 等: "《茶叶综合利用》", vol. 1, 云南大学出版社, pages: 30 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114569527A (en) * | 2022-03-08 | 2022-06-03 | 杨卓涛 | Multi-effect repairing shampoo |
| CN115778878A (en) * | 2022-12-22 | 2023-03-14 | 广州世航生物科技有限公司 | Hair care composition and preparation method and application thereof |
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