CN106176270A - A kind of amino acid shampoo of gentleness and preparation method thereof - Google Patents
A kind of amino acid shampoo of gentleness and preparation method thereof Download PDFInfo
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- CN106176270A CN106176270A CN201610784031.XA CN201610784031A CN106176270A CN 106176270 A CN106176270 A CN 106176270A CN 201610784031 A CN201610784031 A CN 201610784031A CN 106176270 A CN106176270 A CN 106176270A
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- amino acid
- shampoo
- gentleness
- water
- amine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention belongs to cosmetics of everyday use field, be specifically related to amino acid shampoo of a kind of gentleness and preparation method thereof.The amino acid shampoo that the present invention provides includes following component: aliphatic alcohol polyethenoxy amine, coco betaine, alkyl polyglucoside, amino acid surfactant, water-soluble grease, polyquaternary ammonium salt 10, coconut oleoyl amine monoethanolamine, PEG 120 methyl dioleate, benzoic acid, salicylic acid, glycerol, essence and water.The amino acid shampoo that the present invention provides has good foaming, foam stability, and appropriateness cleaning washability, moisturizing effect is good；Hair after washing is bright, submissive, flexible, cardability is good；Gentleer to skin, nontoxic non-stimulated and comfortable soft and moist.
Description
Technical field
The invention belongs to cosmetics of everyday use field, be specifically related to amino acid shampoo of a kind of gentleness and preparation method thereof.
Background technology
Market of Chinese Shampoo is that personal care market develops the earliest, one of the fastest market.Market competition, factory
Business faces more pressure, needs constantly to release new product and promotion method to increase the market competitiveness.Because being development
Market faster, so consumer relative has more ripe consumption habit, consumption demand more becomes sectionalization.The most on the market
Shampoo generally has that foam performance is poor, degreasing power is too strong and causes that hair is dry and astringent, cardability is poor, hair is low and deep unglazed etc. asks
Topic.
Chinese patent application 201610046179.3 discloses a kind of amino acid bio shampoo, belongs to chemical field, its
Component (percentage by weight) including: amino acid bio surfactant 13-30%, coconut oil methyl cholamine 2.00-5.00%, has natural
Preservative 0.10-1.00%, conditioner 2.00-3.500%, residue water is supplied.The shampoo that this invention provides, foam is rich
Rich, fine and closely woven, soft, wash rear hair a softer and smoother touch, combing is light, does not deposits, can use safely, but its cleaning washability is too
By force, and moisturizing effect is general.
Chinese patent application 201410680573.3 discloses a kind of fizzy shampoo, including 10～25% surface
Activating agent, 1～10% conditioner, 1～5% thickening agent and 1～5% functional aid, described surfactant be AES,
One or more in AESA, aminoacid, the shampoo that this invention is provided can also add essence, preservative and pigment.This
Shampoo has more foam, and durable lather, can protect hair from hair washing time frictionally damage, but its cleaning washing energy
Power is the strongest.
Summary of the invention
For solving problems of the prior art, it is an object of the invention to provide the amino acid shampoo of a kind of gentleness
And preparation method thereof, the gentle rational compatibility of amino acid shampoo that the present invention provides, have and preferably clean washability,
Hair elasticity and cardability can be improved, and non-stimulated to skin gentleness.
The invention provides the amino acid shampoo of a kind of gentleness, including following component and percentage by weight thereof:
Fat aliphatic alcohol polyethenoxy amine 1～3%, coco betaine 1～4%, alkyl polyglucoside 1～5%, amino acid surface
Activating agent 2～10%, water-soluble grease 1～2%, Polyquaternium-10 0.1～0.5%, coconut oleoyl amine monoethanolamine 0.2～
1%, PEG-120 methyl dioleate 0.2～1%, benzoic acid 0.1～0.5%, salicylic acid 0.1～0.5%, glycerol 1～
5%, essence 0.3～0.8% and water 67～92%.
The amino acid shampoo that the present invention provides use amino acid surfactant and coco betaine, alkyl polyglucoside,
The surfactants such as coconut oleoyl amine monoethanolamine are collaborative compounding, significantly alleviate or eliminate use coconut oleoyl amine monoethanolamine and cause
The side effect of skin burn feeling, twinge or scratchiness, and on decontamination, foaming, steady bubble, there is synergism.
Further, described amino acid shampoo is made up of following component and percentage by weight thereof:
Aliphatic alcohol polyethenoxy amine 2%, coco betaine 3%, alkyl polyglucoside 2%, amino acid surfactant 5%,
Water-soluble grease 1.5%, Polyquaternium-10 0.25%, coconut oleoyl amine monoethanolamine 0.5%, PEG-120 methyl two oleic acid
Ester 0.5%, benzoic acid 0.25%, salicylic acid 0.25%, glycerol 3%, essence 0.5% and water 81.25%.
The composition of amino acid shampoo has been carried out preferably by the present invention, preferably after composition synergism is maximized,
Significantly improve foaming power, reduce system zest, increase skin moisture-keeping, the cardability strengthening hair and plentiful degree, and
Improve the bactericidal antiphlogistic of system.
Further, described aliphatic alcohol polyethenoxy amine is dodecyl ether sulfate ammonium.
Further, described alkyl polyglucoside is coco alkyl glucoside.
Further, described water-soluble grease is PEG-7 Fructus Canarii albi oils and fats.
Further, described amino acid surfactant is pressed weight by sodium N-lauroyl sarcosinate and sodium cocoyl glutamate
Measure and form than 3:1.
In the amino acid shampoo that the present invention provides, amino acid surfactant is sodium N-lauroyl sarcosinate and cocos nucifera oil acyl
The complex of base sodium glutamate.Sodium lauroyl sarcosine is a kind of surfactant as mild as a dove, superior foaminess, and bubble
Foam is fine and smooth, lasting, has antibiotic and sterilizing, and biological degradability is good simultaneously, environmentally safe；Sodium cocoyl glutamate foam
Suitably, washing force strong, to hard water strong adaptability, can effectively repair damaged hair, and the softest to skin or eyes, and can
Quickly to be decomposed by biology.Under cas fortuit, being compounded by above two aminoacid, obtain after compounding is compound
Thing is non-stimulated to human body skin, nontoxic, and it is soft and moist to feel comfortably cool, and this complex has stronger sterilization and antistatic is made simultaneously
With, the cardability of hair can be improved, quickly repair damaged hair.
Meanwhile, present invention also offers the preparation method of the amino acid shampoo of a kind of gentleness, comprise the following steps:
S1 adds water in reaction cylinder, adds aliphatic alcohol polyethenoxy amine, is heated to 75～80 DEG C while stirring, completely
Dissolve, obtain solution A；
S2 adds coco betaine and alkyl polyglucoside in above-mentioned solution A, stirs, and is cooled to 70～75 DEG C, complete
CL, obtains solution B；
S3 adds amino acid surfactant and Polyquaternium-10 in above-mentioned solution B, stirs, be cooled to 55～
65 DEG C, add glycerol, stir, be completely dissolved, obtain solution C；
Above-mentioned solution C is cooled to 35～45 DEG C by S4, adds water-soluble grease, benzoic acid, salicylic acid and essence, adjusts simultaneously
Joint pH value, is eventually adding coconut oleoyl amine monoethanolamine and PEG-120 methyl dioleate regulation viscosity, mix homogeneously, goes out
Material, to obtain final product.
Further, in described step S1, the temperature of heating is 78 DEG C, and in S2, the temperature of cooling is 72 DEG C.
Further, described regulation pH value is for using Fructus Citri Limoniae acid for adjusting pH value to 5.5～6.5.
Further, described viscosity is 2000～4000.
The amino acid shampoo that the present invention provides not only improves foaming power, reduces system zest, adds skin
Moisture retention, enhances the cardability of hair and plentiful degree, also improves the bactericidal antiphlogistic of system.
Compared with prior art, the amino acid shampoo that the present invention provides has good foaming, foam stability, appropriateness cleaning
Washability, moisturizing effect is good；Hair after washing is bright, submissive, flexible, cardability is good；Gentleer to skin, nontoxic nothing
Stimulate, and comfortable soft and moist.
Detailed description of the invention
Being described in further details the present invention below by specific embodiment, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.
Embodiment 1-3, comparative example 1-2
In table 1, list 3 specific embodiments and the group of 2 comparative examples of amino acid shampoo provided by the present invention
Divide and percentage by weight.
Table 1 embodiment and comparative example component and percentage by weight thereof
Comparative example 1 is with the difference of embodiment 2, by sodium N-lauroyl sarcosinate and sodium cocoyl glutamate weight ratio
3:1 replaces with 1:1.
Comparative example 2 is with the difference of embodiment 2, and sodium cocoyl glutamate replaces with sodium lauroyl glutamate and meat
Fructus Amomi Rotundus acyl group propylhomoserin sodium.
The preparation method of the amino acid shampoo of embodiment 1 is:
S1 adds water in reaction cylinder, adds aliphatic alcohol polyethenoxy amine, is heated to 78 DEG C while stirring, the most molten
Solve, obtain solution A；
S2 adds coco betaine and alkyl polyglucoside in above-mentioned solution A, stirs, and is cooled to 72 DEG C, the most molten
Solve, obtain solution B；
S3 adds amino acid surfactant and Polyquaternium-10 in above-mentioned solution B, stirs, is cooled to 60 DEG C,
Add glycerol, stir, be completely dissolved, obtain solution C；
Above-mentioned solution C is cooled to 40 DEG C by S4, adds water-soluble grease, benzoic acid, salicylic acid and essence, is simultaneously introduced lemon
Lemon acid for adjusting pH value, to 6.0, is eventually adding coconut oleoyl amine monoethanolamine and PEG-120 glucose oleate regulation viscosity is
2500, mix homogeneously, discharging, to obtain final product.
The preparation method of the amino acid shampoo of embodiment 2-3 and comparative example 1-2 is similar to Example 1.
Test example one, shampoo initial foam high measure are tested
Measuring according to GB13173-2008, method is as follows: Example 1, embodiment 2, embodiment 3, comparative example 1 and contrast
The each 2.5g of shampoo prepared by example 2, dissolves with 150mg/kg hard water respectively, transfers in 1000mL volumetric flask, and be diluted to
Scale, shakes up, then solution is placed in (40 ± 0.5) DEG C water bath with thermostatic control ageing, starts total time 30min from adding water-soluble sample, with
Measure foam height with Roche foam meter afterwards, record initial foam height, be shown in Table 2.
Table 2 shampoo initial foam height
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | |
| Initial foam height/mm | 120 | 130 | 125 | 100 | 105 |
Being known by table 2, the initial foam height of amino acid shampoo prepared by the present invention is 120-130mm, and comparative example 1 He
The weak effect of the amino acid shampoo that the foaming characteristic of comparative example 2 is prepared than embodiment of the present invention 1-3, illustrates the coconut palm that the present invention provides
Oleoyl sodium glutamate and sodium N-lauroyl sarcosinate are mutually collaborative strengthens foaming characteristic, and optimal when weight ratio is 3:1.
Test example two, irritation test/toxicology test
1. test material: embodiment 1, embodiment 2 and the amino acid shampoo of embodiment 3 preparation
2. subjects: choose healthy rabbit 60, body weight 180-220g, male and female half and half.Send outer inspection to Guangdong quality inspection institute
Detection.
3. content of the test:
24h before test, cuts off the hair of experiment spinal column both sides, white rabbit back, does not damage epidermis, be respectively 3cm about unhairing scope
×3cm.Take tested material (i.e. embodiment 1-3) each 0.5g to be added on 4 layers of gauze of 2.5cm × 2.5cm, be affixed on side skin, use
After one layer of oilpaper covers, with immobilization with adhesive tape, opposite side is blank.Remove tested material after closing 4h, and wash away with clear water residual
Stay tested material, in removing after tested material 1,24,48h observe the reaction of recipient site local skin, by " cosmetics health specification "
(version in 2007) skin irritation/corrosion test carries out dermoreaction scoring, combines with the meansigma methods of animal subject integration
Close and evaluate, and observe other side effect effects in addition to zest.
4. result of the test:
In test, each observing time puts top average ＜ 0.5, belongs to nonirritant.That is, irritation test result
For: nonirritant.Acute ocular irritation test result is: nonirritant.Therefore the amino acid shampoo that the present invention provides is to skin
Gentleer, nontoxic non-stimulated.
Claims (10)
1. a gentle amino acid shampoo, it is characterised in that include following component and percentage by weight thereof:
Aliphatic alcohol polyethenoxy amine 1～3%, coco betaine 1～4%, alkyl polyglucoside 1～5%, amino acid surfactant
2～10%, water-soluble grease 1～2%, Polyquaternium-10 0.1～0.5%, coconut oleoyl amine monoethanolamine 0.2～1%, PEG-
120 methyl dioleates 0.2～1%, benzoic acid 0.1～0.5%, salicylic acid 0.1～0.5%, glycerol 1～5%, essence
0.3～0.8% and water 67～92%.
The amino acid shampoo of gentleness the most according to claim 1, it is characterised in that by following component and weight percent thereof
Than composition:
Aliphatic alcohol polyethenoxy amine 2%, coco betaine 3%, alkyl polyglucoside 2%, amino acid surfactant 5%, water-soluble
Property oils and fats 1.5%, Polyquaternium-10 0.25%, coconut oleoyl amine monoethanolamine 0.5%, PEG-120 methyl dioleate
0.5%, benzoic acid 0.25%, salicylic acid 0.25%, glycerol 3%, essence 0.5% and water 81.25%.
The amino acid shampoo of gentleness the most according to claim 1 and 2, it is characterised in that: described aliphatic alcohol polyethenoxy
Amine is dodecyl ether sulfate ammonium.
The amino acid shampoo of gentleness the most according to claim 1 and 2, it is characterised in that: described alkyl polyglucoside is cocos nucifera oil
Base alkyl androstanediol.
The amino acid shampoo of gentleness the most according to claim 1 and 2, it is characterised in that: described water-soluble grease is
PEG-7 Fructus Canarii albi oils and fats.
The amino acid shampoo of gentleness the most according to claim 1 and 2, it is characterised in that: described amino acid surface activity
Agent is made up of by weight 3:1 sodium N-lauroyl sarcosinate and sodium cocoyl glutamate.
The preparation method of the amino acid shampoo of gentleness the most according to claim 1 and 2, it is characterised in that include following
Step:
S1 adds water in reaction cylinder, adds aliphatic alcohol polyethenoxy amine, is heated to 75～80 DEG C while stirring, the most molten
Solve, obtain solution A；
S2 adds coco betaine and alkyl polyglucoside in above-mentioned solution A, stirs, and is cooled to 70～75 DEG C, the most molten
Solve, obtain solution B；
S3 adds amino acid surfactant and Polyquaternium-10 in above-mentioned solution B, stirs, is cooled to 55～65 DEG C,
Add glycerol, stir, be completely dissolved, obtain solution C；
Above-mentioned solution C is cooled to 35～45 DEG C by S4, adds water-soluble grease, benzoic acid, salicylic acid and essence, regulates pH simultaneously
Value, be eventually adding coconut oleoyl amine monoethanolamine and PEG-120 methyl dioleate regulation viscosity, mix homogeneously, discharging, i.e.
?.
The preparation method of the amino acid shampoo of gentleness the most according to claim 7, it is characterised in that: in described step S1
The temperature of heating is 78 DEG C, and in step S2, the temperature of cooling is 72 DEG C.
The preparation method of the amino acid shampoo of gentleness the most according to claim 7, it is characterised in that: described regulation pH
Value is for using Fructus Citri Limoniae acid for adjusting pH value to 5.5～6.5.
The preparation method of the amino acid shampoo of gentleness the most according to claim 7, it is characterised in that: described viscosity
It is 2000～4000.
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511139A (en) * | 2016-12-24 | 2017-03-22 | 江西宜信堂医疗科技有限公司 | Cream shampoo liquid and preparing method thereof |
| CN106726704A (en) * | 2016-12-25 | 2017-05-31 | 江西宜信堂医疗科技有限公司 | A kind of sterilization shampoo and preparation method thereof |
| CN107308041A (en) * | 2017-06-15 | 2017-11-03 | 广州暨南生物医药研究开发基地有限公司 | A kind of gentle nourishing type shampoo and preparation method thereof |
| CN107898662A (en) * | 2017-12-29 | 2018-04-13 | 广州慈康生物科技有限公司 | A kind of shampoo of scalp care |
| CN107970132A (en) * | 2017-10-24 | 2018-05-01 | 东莞星美新新材料科技有限公司 | The shampoo of anti-dandruff and itching-relieving |
| CN108685760A (en) * | 2018-08-01 | 2018-10-23 | 湘南学院 | A kind of composition for soap base product |
| CN109864898A (en) * | 2019-04-11 | 2019-06-11 | 河南工业大学 | A kind of fermentation wheat germ peptide shampoo and preparation method thereof |
| CN109908061A (en) * | 2019-04-30 | 2019-06-21 | 郭玲玲 | A kind of fizzy dandruff control shampoo containing and preparation method thereof |
| CN110025552A (en) * | 2019-05-05 | 2019-07-19 | 郭玲玲 | A kind of increase hair tensile strength and the amino acid shampoo of elongation percentage and preparation method thereof |
| CN111388365A (en) * | 2020-03-17 | 2020-07-10 | 广州市加中榕科技有限公司 | Silicon-free smoothing and anti-dandruff shampoo and preparation method thereof |
| CN113876672A (en) * | 2020-07-01 | 2022-01-04 | 广州楚颜化妆品有限公司 | Amino acid mild tear-free natural plant shampoo and preparation method thereof |
| CN114288209A (en) * | 2021-10-25 | 2022-04-08 | 纳爱斯丽水日化有限公司 | Double-layer shampoo composition and preparation method thereof |
| CN116637047A (en) * | 2023-05-30 | 2023-08-25 | 广州美思生物技术有限公司 | Tear-free shampoo and preparation method thereof |
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511139A (en) * | 2016-12-24 | 2017-03-22 | 江西宜信堂医疗科技有限公司 | Cream shampoo liquid and preparing method thereof |
| CN106726704A (en) * | 2016-12-25 | 2017-05-31 | 江西宜信堂医疗科技有限公司 | A kind of sterilization shampoo and preparation method thereof |
| CN107308041A (en) * | 2017-06-15 | 2017-11-03 | 广州暨南生物医药研究开发基地有限公司 | A kind of gentle nourishing type shampoo and preparation method thereof |
| CN107970132A (en) * | 2017-10-24 | 2018-05-01 | 东莞星美新新材料科技有限公司 | The shampoo of anti-dandruff and itching-relieving |
| CN107898662A (en) * | 2017-12-29 | 2018-04-13 | 广州慈康生物科技有限公司 | A kind of shampoo of scalp care |
| CN108685760A (en) * | 2018-08-01 | 2018-10-23 | 湘南学院 | A kind of composition for soap base product |
| CN109864898A (en) * | 2019-04-11 | 2019-06-11 | 河南工业大学 | A kind of fermentation wheat germ peptide shampoo and preparation method thereof |
| CN109908061B (en) * | 2019-04-30 | 2022-01-07 | 胡小龙 | Anti-dandruff shampoo rich in foam and preparation method thereof |
| CN109908061A (en) * | 2019-04-30 | 2019-06-21 | 郭玲玲 | A kind of fizzy dandruff control shampoo containing and preparation method thereof |
| CN110025552A (en) * | 2019-05-05 | 2019-07-19 | 郭玲玲 | A kind of increase hair tensile strength and the amino acid shampoo of elongation percentage and preparation method thereof |
| CN110025552B (en) * | 2019-05-05 | 2022-04-08 | 广州美思生物技术有限公司 | Amino acid shampoo capable of increasing tensile strength and elongation of hair and preparation method thereof |
| CN111388365A (en) * | 2020-03-17 | 2020-07-10 | 广州市加中榕科技有限公司 | Silicon-free smoothing and anti-dandruff shampoo and preparation method thereof |
| CN113876672A (en) * | 2020-07-01 | 2022-01-04 | 广州楚颜化妆品有限公司 | Amino acid mild tear-free natural plant shampoo and preparation method thereof |
| CN114288209A (en) * | 2021-10-25 | 2022-04-08 | 纳爱斯丽水日化有限公司 | Double-layer shampoo composition and preparation method thereof |
| CN114288209B (en) * | 2021-10-25 | 2023-11-24 | 纳爱斯丽水日化有限公司 | Double-layer shampoo composition and preparation method thereof |
| CN116637047A (en) * | 2023-05-30 | 2023-08-25 | 广州美思生物技术有限公司 | Tear-free shampoo and preparation method thereof |
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| CN106176270B (en) | 2017-10-24 |
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