CN110025552A - A kind of increase hair tensile strength and the amino acid shampoo of elongation percentage and preparation method thereof - Google Patents
A kind of increase hair tensile strength and the amino acid shampoo of elongation percentage and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of shampoos for increasing hair tensile strength and elongation percentage, it is made of the raw material of following weight percent: dodecyl ether sulfate ammonium 1~3%, coco betaine 1~4%, coco alkyl glucoside 1~5%, sodium N-lauroyl sarcosinate 2~10%, composite vegetables extractive 3 ~ 5%, PEG-7 olive grease 1~2%, Polyquaternium-10 0.1~0.5%, coconut oleoyl amine monoethanolamine 0.2~1%, PEG-120 methyl dioleate 0.2~1%, benzoic acid 0.01~0.05%, salicylic acid 0.01~0.05%, glycerol 1~5%, essence 0.3~0.8%, surplus is water.Composite vegetables extractive used by shampoo of the present invention is ginger, slender acanthopanax ginseng, India is blue and granatum is according to mass ratio (1 ~ 4): (1 ~ 4): (1 ~ 4): the extract that (1 ~ 4) obtains achieves unexpected technical effect in terms of increasing hair tensile strength and elongation percentage；The composite vegetables extractive that specific extracting method obtains makes shampoo of the present invention have excellent tensile strength and fracture elongation.
Description
Technical field
The present invention relates to daily cosmetics fields, are specifically related to a kind of hair washing for increasing hair tensile strength and elongation percentage
Water and preparation method thereof.
Background technique
Hair be it is a kind of be made of the horn cell of angling, complicated natural polymer subbundle.In horn cell
Primary structure is fusiform keratinous fibers, there is matrix in varying numbers, residual cells core and melanin granule therebetween.Angle
Matter chemical fibre dimension is successively made of complicated keratin network.Keratin in hair fiber there is crystal region and amorphous region,
The ratio that crystalline portion accounts for whole fiber is known as crystallinity.The parallel degree of macromolecular chain main shaft and fiber axis inside hair fiber
The referred to as degree of orientation.Crystallinity and the degree of orientation can characterize the height of the quantity of regular regional and order degree in hair fiber.It is high
Many properties (such as mechanical property) of molecular fiber depend greatly on high molecular coherent condition and strand each
Connection type between structural unit.
Several factors can adversely affect hair, such as (hair dyeing is scalded for environment (light, heat etc.), chemical substance
Hair etc.) etc. can all influence the health of hair.The damage of hair can be roughly divided into according to the extraneous factor difference for causing it to change
Following several types:
(1) physical damnification refers to that apply external force damages to hair bring.Causing one of hair damage external force is combing
Frictional force caused by comb bring drawing force and comb teeth during hair.When being not easy to comb when hair surface is coarse, this
Kind damages outstanding Yi Fasheng.Close stripping fork, metal and plastic comb may also increase the chance of combing damage.Against the scale of hair cuticle
When coverage direction is inversely combed, the tilting of hair cuticle is easiest to occur so that peeling off.In addition there are also get a haircut when scissors and
Power is cut in cutting for blunt, the extraneous various frictional force to hair.
(2) chemical damage refer to cause hair structure composition substance-keratin structure change and caused by damage,
Mainly caused by the various chemical reactions in hair.These chemical reaction include life in various agent for permanent hair waving, hair dye,
Bleaching agent and straight hair agent destroy the keratin structure of hair.They are all to penetrate into cortical layer structure from hair cuticle and send out
Raw various effects.Hair-waving and straight hair process are that reducing substances first destroys the disulfide bond in keratin, then passes through oxidant again
It is combined in new position.Hair dyeing is that oxidation polymerization occurs inside hair by oxidation dye to act on forming macromolecule pigment
To complete dyeing course.Decoloration is then to realize the decoloration drift of hair come the melanin substance in oxidation hair using bleaching agent
It is white.These chemical actions destroy the inside composed structure of hair without exception, and inevitable damage is caused to hair.
(3) thermal damage refers to that temperature is excessively high and causes the damage of hair during using hair dryer or hair-waving.High temperature can be with
Make the moisture evaporation in hair, cause the withered fragility of hair fiber, along with external force stretching or rubbing action and easily make hair
Fracture.
(4) the ultraviolet light irradiation accumulation in daylight reaches some strength, can cause variation and the protein of hair structure
Light degradation phenomenon.Melanin in hair fiber is oxidizable by dayligth effect and discolouration phenomena occurs, and keratin structure
In tryptophan, cystine and tyrosine light degradation can also occur.In addition, hair is exposed in external environment all day, various gas
Wait phenomenon all can cause to damage to hair, accelerate the aging of hair.
Hair damage is mainly shown as that feel is poor, and hair surface is coarse, jaundice and lackluster, elasticity variation, stretching
Easily broken hair etc., especially hair shows apparent difference after impaired in tensile strength and extensibility.
Although there is the formula diversified shampoo product of type in currently available technology, the effect of different product
Difference is also larger.For example, prior art discloses entitled " a kind of mild amino acid shampoo and preparation method thereof "
Chinese patent application, Publication No. CN 106176270A, the invention provide amino acid shampoo include following component: rouge
Fat alcohol polyoxyethylene amine, coco betaine, alkyl glycosides, amino acid surfactant, water-soluble grease, Polyquaternium-10,
Coconut oleoyl amine monoethanolamine, PEG-120 methyl dioleate, benzoic acid, salicylic acid, glycerol, essence and water.The amino acid
Shampoo has good blistering, foam stability, and appropriateness cleans washability, and moisturizing effect is good；Hair after washing is bright, soft
It is suitable, flexible, cardability is good；It is milder to skin, nontoxic non-stimulated and comfortable soft and moist.But the effect of shampoo, is limited,
It is not obvious in terms of increasing hair tensile strength and elongation percentage effect.Therefore, develop a kind of increase hair tensile strength and
The shampoo product of elongation percentage has good market prospects.
Summary of the invention
In view of the deficienciess of the prior art, the object of the present invention is to provide a kind of increase hair tensile strength and elongation percentage
Shampoo.The present invention is realized particular by following technical scheme:
A kind of shampoo increasing hair tensile strength and elongation percentage, is made: dodecyl of the raw material of following weight percent
Ether sulfate ammonium 1~3%, coco betaine 1~4%, coco alkyl glucoside 1~5%, sodium N-lauroyl sarcosinate 2
~10%, composite vegetables extractive 3 ~ 5%, PEG-7 olive grease 1~2%, Polyquaternium-10 0.1~0.5%, cocounut oil acyl
Amine monoethanolamine 0.2~1%, PEG-120 methyl dioleate 0.2~1%, benzoic acid 0.01~0.05%, salicylic acid
0.01~0.05%, glycerol 1~5%, essence 0.3~0.8%, surplus are water.
Preferably, a kind of shampoo increasing hair tensile strength and elongation percentage, by the raw material system of following weight percent
At: dodecyl ether sulfate ammonium 2%, coco betaine 3%, coco alkyl glucoside 2%, sodium N-lauroyl sarcosinate
5%, composite vegetables extractive 4%, PEG-7 olive grease 2%, Polyquaternium-10 0.25%, coconut oleoyl amine monoethanolamine
0.5%, PEG-120 methyl dioleate 0.5%, benzoic acid 0.03%, salicylic acid 0.03%, glycerol 3%, essence
0.5%, surplus is water.
Preferably, the composite vegetables extractive is ginger, slender acanthopanax ginseng, India is blue and granatum is according to mass ratio (1 ~ 4):
(1 ~ 4): (1 ~ 4): the extract that (1 ~ 4) obtains.
Preferably, the composite vegetables extractive preparation method the following steps are included:
(1) ginger, slender acanthopanax ginseng, India orchid and granatum are weighed according to the mass ratio, is crushed after drying, is by solid-to-liquid ratio g/mL
75% ethanol solution of volumetric concentration is added in 1:30, and ultrasonic wave assisted extraction 50 minutes, filtering, filter residue repeated to extract 1 time, filtrate
Merge, is concentrated under reduced pressure；
(2) concentrate is extracted twice with isometric ethyl acetate, and extract liquor merges, recycling ethyl acetate to half volume, after with
Isometric 4% sodium hydroxide solution of mass concentration extraction；
(3) extract liquor is added the gelatin solution that mass concentration is 5%, stood overnight, filtered with dilute hydrochloric acid tune pH value to 4；It collects
Precipitating filters out insoluble matter with the dissolution of 60% acetone soln, and filtrate recycles acetone；
(4) after filtrate recycling acetone, it is splined on the polyamide chromatographic column pre-processed, successively with the volume of 3-6 times of column volume
Concentration 20%, 40%, 60% and anhydrous ethanol elution, and anhydrous ethanol elution liquid is collected, it is concentrated under reduced pressure, freeze-drying must answer
Close plant extracts.
The present invention increases the preparation method of the shampoo of hair tensile strength and elongation percentage, comprising the following steps:
(1) it adds water in reaction cylinder, dodecyl ether sulfate ammonium is added, is heated to 75~80 DEG C while stirring, completely
Dissolution, obtains solution A；
(2) coco betaine and coco alkyl glucoside are added in Xiang Shangshu solution A, stirs evenly, is cooled to 70~75
DEG C, it is completely dissolved, obtains solution B；
(3) sodium N-lauroyl sarcosinate, composite vegetables extractive and Polyquaternium-10 are added in Xiang Shangshu solution B, stirring is equal
It is even, 55~65 DEG C are cooled to, glycerol is added, is stirred evenly, is completely dissolved, solution C is obtained；
(4) above-mentioned solution C is cooled to 35~45 DEG C, PEG-7 olive grease, benzoic acid, salicylic acid and essence is added, finally plus
Enter coconut oleoyl amine monoethanolamine and PEG-120 methyl dioleate, be uniformly mixed, discharging to get.
Compared with prior art, the beneficial effect of cosmetics of the present invention is: (1) compound plant used by shampoo of the present invention
Object extract is ginger, slender acanthopanax ginseng, India is blue and granatum is according to mass ratio (1 ~ 4): (1 ~ 4): (1 ~ 4): what (1 ~ 4) obtained mentions
Object is taken, achieves unexpected technical effect in terms of increasing hair tensile strength and elongation percentage；(2) specific to extract
The composite vegetables extractive that method obtains makes shampoo of the present invention have excellent tensile strength and fracture elongation.
Specific embodiment
The present invention is described in further detail below with reference to embodiment.
Embodiment 1:
A kind of shampoo increasing hair tensile strength and elongation percentage, is made: dodecyl of the raw material of following weight percent
Ether sulfate ammonium 2%, coco betaine 3%, coco alkyl glucoside 2%, sodium N-lauroyl sarcosinate 5%, compound plant
Object extract 4%, PEG-7 olive grease 2%, Polyquaternium-10 0.25%, coconut oleoyl amine monoethanolamine 0.5%, PEG-120
Methyl dioleate 0.5%, benzoic acid 0.03%, salicylic acid 0.03%, glycerol 3%, essence 0.5%, surplus are water.
Preferably, the composite vegetables extractive is ginger, slender acanthopanax ginseng, India is blue and granatum is according to mass ratio 1:1:1:
1 obtained extract, preparation method the following steps are included:
(1) ginger, slender acanthopanax ginseng, India orchid and granatum are weighed according to the mass ratio, is crushed after drying, is by solid-to-liquid ratio g/mL
75% ethanol solution of volumetric concentration is added in 1:30, and ultrasonic wave assisted extraction 50 minutes, filtering, filter residue repeated to extract 1 time, filtrate
Merge, is concentrated under reduced pressure；
(2) concentrate is extracted twice with isometric ethyl acetate, and extract liquor merges, recycling ethyl acetate to half volume, after with
Isometric 4% sodium hydroxide solution of mass concentration extraction；
(3) extract liquor is added the gelatin solution that mass concentration is 5%, stood overnight, filtered with dilute hydrochloric acid tune pH value to 4；It collects
Precipitating filters out insoluble matter with the dissolution of 60% acetone soln, and filtrate recycles acetone；
(4) after filtrate recycling acetone, it is splined on the polyamide chromatographic column pre-processed, successively with the volume of 3-6 times of column volume
Concentration 20%, 40%, 60% and anhydrous ethanol elution, and anhydrous ethanol elution liquid is collected, it is concentrated under reduced pressure, freeze-drying must answer
Close plant extracts.
The preparation method of the shampoo for increasing hair tensile strength and elongation percentage, comprising the following steps:
(1) it adds water in reaction cylinder, dodecyl ether sulfate ammonium is added, is heated to 80 DEG C while stirring, is completely dissolved,
Obtain solution A；
(2) coco betaine and coco alkyl glucoside are added in Xiang Shangshu solution A, stirs evenly, is cooled to 70 DEG C, it is complete
Fully dissolved obtains solution B；
(3) sodium N-lauroyl sarcosinate, composite vegetables extractive and Polyquaternium-10 are added in Xiang Shangshu solution B, stirring is equal
It is even, 55 DEG C are cooled to, glycerol is added, is stirred evenly, is completely dissolved, solution C is obtained；
(4) above-mentioned solution C is cooled to 45 DEG C, PEG-7 olive grease, benzoic acid, salicylic acid and essence is added, is eventually adding coconut palm
Oleamide monoethanolamine and PEG-120 methyl dioleate, be uniformly mixed, discharging to get.
Embodiment 2-3, comparative example 1-8 shampoo the preparation method is the same as that of Example 1, the difference is that composite plant mentions
Take the mass ratio of each plant material in object different, referring specifically to table 1.
Table 1
Comparative example 9:
The preparation method is the same as that of Example 1 for shampoo, the difference is that in the step of preparation method of composite vegetables extractive (4)
" collect 40% ethanol eluate, be concentrated under reduced pressure, freeze-drying obtains composite vegetables extractive ".
One, influence of the measurement composition to hair tensile strength
After the hair of same source is cleaned with 5% NaLS, with 5% soaking with sodium hydroxide 30 minutes, pure water was clear
It after washing, is impregnated 15 hours with the shampoo solution of the shampoo formulation 1g/L of embodiment 1-3, comparative example 1-8, after pure water cleaning
Naturally dry.
It measures tension reduced rate (%).Tension reduced rate (%) is with rheometer (Model 200-2J, Fudo Kogyo
Co, Japan) measured in the case where 20 DEG C ± 2 DEG C and relative humidity are 60 ± 4%.The original length of hair is 50 millis
Rice, extension rate is 5 cm per minutes and full scale is 200gf.
Tension is calculated according to the following formula reduces percentage:
Tension reduces (%)=(Fo-F1)/(Fo) × 100
Wherein F0 is original power needed for making elongate fiber 20%；F1 is strength needed for making same fiber uphold 20% again.
(referring to .Gupta: The use of multiple test methods in the of N .B .Fair and B .S
analysis of the effect of cosmetic treatment on the surface properties of
Human hair, XIVth IFSCC Congress, Barcelona, Vol II, p113-1124(1986)).
The tension reduced rate (%) of five hair samples of every group of test, is then averaged.Test result see the table below 2.
Table 2
From test result as can be seen that the shampoo of 1-3 of the embodiment of the present invention has excellent raising hair tensile property, wherein
Embodiment 1 is optimal technical solution.By the experimental test data of comparative example 1-4 it can be concluded that the present invention is by ginger, five
The plant extracts extracted after adding ginseng, India blue and granatum Four Plants raw material compounding, is added in shampoo, is opening
Unexpected synergy is achieved in terms of power reduced rate.Meanwhile it can be with by the experimental test data of comparative example 5-8
Conclude that the mass ratio of ginger, slender acanthopanax ginseng, India orchid and granatum Four Plants raw material not in (1 ~ 4) of the invention: (1 ~ 4):
(1 ~ 4): in the numberical range of (1 ~ 4), then hair tension reduced rate will be greatly reduced.Pass through the test of comparative example 9 and embodiment 1
Test data is it can be concluded that the composite vegetables extractive that specific extracting method obtains makes shampoo of the present invention with excellent
Different tensile strength.
Two, hair draws high performance test
Under 20 DEG C, 45% relative humidities, tested using INSTRON-4466 type strength experimental machine, drawing high speed is
15mm·min-1, force value resolution ratio is 0.01N, then the elongation at break (%) of 5 hair samples of every group of test is averaged
Value.
Test result see the table below 3.
Table 3
From test result as can be seen that the shampoo of 1-3 of the embodiment of the present invention has excellent raising hairs break extension forthright
Can, wherein embodiment 1 is optimal technical solution.By the experimental test data of comparative example 1-4 it can be concluded that the present invention will
The plant extracts extracted after ginger, slender acanthopanax ginseng, India orchid and granatum Four Plants raw material compounding, is added to shampoo
In, unexpected synergy is achieved in terms of improving hairs break elongation percentage.Meanwhile passing through comparative example 5-8's
Experimental test data are it can be concluded that ginger, slender acanthopanax are joined, India is blue and the mass ratio of granatum Four Plants raw material is not at this
Invent (1 ~ 4): (1 ~ 4): (1 ~ 4): in the numberical range of (1 ~ 4), then hairs break elongation percentage will be greatly reduced.Pass through comparative example
9 with the experimental test data of embodiment 1 it can be concluded that the composite vegetables extractive that specific extracting method obtains makes this
Invention shampoo has excellent fracture elongation.
Claims (5)
1. a kind of shampoo for increasing hair tensile strength and elongation percentage, which is characterized in that by the raw material of following weight percent
It is made: dodecyl ether sulfate ammonium 1~3%, coco betaine 1~4%, coco alkyl glucoside 1~5%, laurel
Sarcosinate 2~10%, composite vegetables extractive 3 ~ 5%, PEG-7 olive grease 1~2%, Polyquaternium-10 0.1~
0.5%, coconut oleoyl amine monoethanolamine 0.2~1%, PEG-120 methyl dioleate 0.2~1%, benzoic acid 0.01~
0.05%, salicylic acid 0.01~0.05%, glycerol 1~5%, essence 0.3~0.8%, surplus are water.
2. a kind of shampoo for increasing hair tensile strength and elongation percentage according to claim 1, which is characterized in that by such as
The raw material of lower weight percent is made: dodecyl ether sulfate ammonium 2%, coco betaine 3%, coco alkyl glucoside
2%, sodium N-lauroyl sarcosinate 5%, composite vegetables extractive 4%, PEG-7 olive grease 2%, Polyquaternium-10
0.25%, coconut oleoyl amine monoethanolamine 0.5%, PEG-120 methyl dioleate 0.5%, benzoic acid 0.03%, salicylic acid
0.03%, glycerol 3%, essence 0.5%, surplus are water.
3. a kind of shampoo for increasing hair tensile strength and elongation percentage according to claim 1 or 2, which is characterized in that
The composite vegetables extractive is ginger, slender acanthopanax ginseng, India is blue and granatum is according to mass ratio (1 ~ 4): (1 ~ 4): (1 ~ 4): (1 ~
4) extract obtained.
4. a kind of shampoo for increasing hair tensile strength and elongation percentage according to claim 3, which is characterized in that described
The preparation method of composite vegetables extractive the following steps are included:
(1) ginger, slender acanthopanax ginseng, India orchid and granatum are weighed according to the mass ratio, is crushed after drying, is by solid-to-liquid ratio g/mL
75% ethanol solution of volumetric concentration is added in 1:30, and ultrasonic wave assisted extraction 50 minutes, filtering, filter residue repeated to extract 1 time, filtrate
Merge, is concentrated under reduced pressure；
(2) concentrate is extracted twice with isometric ethyl acetate, and extract liquor merges, recycling ethyl acetate to half volume, after with
Isometric 4% sodium hydroxide solution of mass concentration extraction；
(3) extract liquor is added the gelatin solution that mass concentration is 5%, stood overnight, filtered with dilute hydrochloric acid tune pH value to 4；It collects
Precipitating filters out insoluble matter with the dissolution of 60% acetone soln, and filtrate recycles acetone；
(4) after filtrate recycling acetone, it is splined on the polyamide chromatographic column pre-processed, successively with the volume of 3-6 times of column volume
Concentration 20%, 40%, 60% and anhydrous ethanol elution, and anhydrous ethanol elution liquid is collected, it is concentrated under reduced pressure, freeze-drying must answer
Close plant extracts.
5. a kind of preparation method of shampoo for increasing hair tensile strength and elongation percentage according to claim 1 or 2,
It is characterized in that, comprising the following steps:
(1) it adds water in reaction cylinder, dodecyl ether sulfate ammonium is added, is heated to 75~80 DEG C while stirring, completely
Dissolution, obtains solution A；
(2) coco betaine and coco alkyl glucoside are added in Xiang Shangshu solution A, stirs evenly, is cooled to 70~75
DEG C, it is completely dissolved, obtains solution B；
(3) sodium N-lauroyl sarcosinate, composite vegetables extractive and Polyquaternium-10 are added in Xiang Shangshu solution B, stirring is equal
It is even, 55~65 DEG C are cooled to, glycerol is added, is stirred evenly, is completely dissolved, solution C is obtained；
(4) above-mentioned solution C is cooled to 35~45 DEG C, PEG-7 olive grease, benzoic acid, salicylic acid and essence is added, finally plus
Enter coconut oleoyl amine monoethanolamine and PEG-120 methyl dioleate, be uniformly mixed, discharging to get.
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| CN201910367260.5A CN110025552B (en) | 2019-05-05 | 2019-05-05 | Amino acid shampoo capable of increasing tensile strength and elongation of hair and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287338A (en) * | 2015-11-12 | 2016-02-03 | 施庚伟 | Oil-removing and hair-loss-preventing shampoo and preparation method thereof |
| CN105581917A (en) * | 2016-02-23 | 2016-05-18 | 广州市高姿化妆品有限公司 | Cosmetic composition for enhancing tensile strength and extensibility of keratin fiber, and especially hair |
| CN105662946A (en) * | 2016-01-19 | 2016-06-15 | 上海清轩生物科技有限公司 | Pomegranate peel extract preparation method and application of pomegranate peel extract to cosmetics |
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
-
2019
- 2019-05-05 CN CN201910367260.5A patent/CN110025552B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287338A (en) * | 2015-11-12 | 2016-02-03 | 施庚伟 | Oil-removing and hair-loss-preventing shampoo and preparation method thereof |
| CN105662946A (en) * | 2016-01-19 | 2016-06-15 | 上海清轩生物科技有限公司 | Pomegranate peel extract preparation method and application of pomegranate peel extract to cosmetics |
| CN105581917A (en) * | 2016-02-23 | 2016-05-18 | 广州市高姿化妆品有限公司 | Cosmetic composition for enhancing tensile strength and extensibility of keratin fiber, and especially hair |
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
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Denomination of invention: An amino acid shampoo for increasing the tensile strength and elongation of hair and its preparation method Effective date of registration: 20221102 Granted publication date: 20220408 Pledgee: Zengcheng sub branch of Guangzhou Rural Commercial Bank Co.,Ltd. Pledgor: Guangzhou Meisi Biotechnology Co.,Ltd. Registration number: Y2022980020581 |