CN110638717A - Softening composition and shampoo thereof - Google Patents

Abstract

The invention provides a softening composition and shampoo thereof, wherein the softening composition contains almond extract, wheat bran extract, ginger root extract and basil extract. The four plant extracts can effectively revive scalp and nourish hair follicles, so that damaged hair is repaired, and the hair is recovered to be healthy and smooth. The composition greatly improves the moisturizing ability of the hair care product, enhances the smooth feeling of the hair, and can be combined with other functional reagents to form a hair washing product with excellent hair care effect. Further, the shampoo is developed based on the softening composition, has the effects of refreshing, moisturizing, moistening and nourishing hair, and is strong in moisturizing ability and soft and smooth in hair.

Description

Softening composition and shampoo thereof

Technical Field

The invention relates to the field of washing and care products, in particular to a softening composition and shampoo thereof.

Background

The hair washing and caring product is an important class of cosmetics and becomes a necessity for people's life. As consumers' economic purchasing power increases and their awareness changes, their needs also change. "washing" is the most basic requirement, and "nursing" is a higher level of personal psychological satisfaction pursued on the basis of washing.

At present, shampoo on the market mainly depends on silicone oil to improve smoothness of hair after washing, but the use of silicone oil components always has a certain controversial. One of the characteristics of the silicone oil is that the silicone oil is insoluble in water and is difficult to wash when the hair is washed, so the silicone oil can be adsorbed on the hair to improve the smoothness of the hair, and the silicone oil can also remain in scalp pores to cause the blockage of hair follicles, the occurrence of red swelling, acne and even alopecia.

In recent years, no silicone oil shampoo is started, but the problems of poor smoothness of hair after washing and the like exist. Therefore, the softening composition is developed to replace silicone oil, so that smoothness of the shampoo without silicone oil is improved, and the softening composition has very important practical significance and wide market value.

Disclosure of Invention

The invention aims to solve the technical problems that the existing shampoo product without silicone oil is poor in smoothness and easy to cause hair dryness and the like, and provides a softening composition. The composition greatly improves the moisturizing ability of hair washing and caring products and enhances the smooth feeling of hair.

The invention also provides a hair care composition containing the softening composition, and the composition combines the softening composition with other functional agents to form a hair washing product with excellent hair care effect.

The invention is realized by the following technical scheme:

the invention aims to provide a softening composition which comprises an almond extract, a wheat bran extract, a ginger root extract and a basil extract. The almond extract has the effects of moistening, nourishing and repairing injury; the wheat bran extract has the effects of moistening and balancing and reviving scalp; the ginger root extract has the effects of mildness, nourishing, freshness and comfort; the basil extract has the effects of dispelling wind and removing heat and refreshing hair roots. The four plant extracts can effectively revive scalp and nourish hair follicles, so that damaged hair is repaired, and the hair is recovered to be healthy and smooth.

Alternatively, the almond extract: wheat bran extract: ginger root extract: basil extract (1-10): (1-10): (1-10): (1-10).

Alternatively, the almond extract: wheat bran extract: ginger root extract: basil extract (5-10): (5-10): (1-5): (1-5).

Optionally, hydrolyzed keratin, collagen, and D-panthenol.

The structure composition of the hydrolyzed keratin is similar to that of hair, and the hydrolyzed keratin can form a transparent film on the surface of the hair, effectively repair the damaged hair, make the damaged hair smooth and elastic, and achieve the repairing and nursing effects. Collagen is also called collagen, and is important protein for hair, and the hair has high content of collagen, so that the hair has certain structure and mechanical properties, such as tensile strength, tensile force, elastic force and the like, and the properties can support and protect the hair. The D-panthenol can keep moisture of hair for a long time, improve hair combing property, reduce hair bifurcation formation, improve hair injury condition, thicken hair, and make hair bright. The composite use of the hydrolyzed keratin, the collagen and the D-panthenol and the softening composition can play a role in immediately repairing damaged hair, enhance the moisturizing capability, keep the hair healthy and not dry, and improve the softness.

Alternatively, (almond extract + wheat bran extract + ginger root extract + basil extract) by weight: hydrolysis of keratin: collagen: d-panthenol ═ (0.01 to 0.1): (0.01-0.2): (0.05-0.5): (0.03-0.3).

The invention also provides shampoo containing the softening composition.

Optionally, the shampoo further comprises hair conditioning agent, foaming agent, and skin conditioning agent.

Optionally, the shampoo further comprises thickener, chelating agent, aromatic, emulsifier, antiseptic, pH regulator, and solvent.

Optionally, the shampoo contains the following components by weight: 0.1-1 part of softening composition, 2-3 parts of hair care conditioner, 20-35 parts of foaming agent, 0.5-1.0 part of skin conditioner, 0.05-0.2 part of thickening agent, 0.05-0.1 part of chelating agent, 0.5-1 part of aromatic, 1-3 parts of emulsifier, 0.2-0.6 part of preservative, 0.1-0.2 part of pH regulator and 50-70 parts of solvent.

Optionally, the hair care conditioner is selected from at least one of polyquaternium-10, polyquaternium-22, polyquaternium-6, schizophyllan, oleyl alcohol.

Optionally, the foaming agent is selected from at least one of sodium fatty alcohol-polyoxyethylene ether sulfate, cocamidopropyl betaine, sodium lauroyl sarcosine, disodium cocoamphodiacetate, decyl glucoside, and sodium cocoamidopropionate.

Optionally, the skin conditioning agent is selected from at least one of peony seed oil, crabapple seed oil, camellia seed oil, sodium pyrrolidone carboxylate, lanolin, notoginseng radix extract, polygonum multiflorum extract, and astragalus platyphylla extract.

Optionally, the thickener is selected from hydroxypropyl guar hydroxypropyl trimonium chloride.

Optionally, the chelating agent is selected from disodium edetate.

Optionally, the fragrance is selected from perfumes.

Optionally, the emulsifier is selected from at least one of PEG-7 glyceryl cocoate, PPG-5-ceteth-20, glyceryl cocoate, cocamide MEA, hydrogenated lecithin.

Optionally, the preservative is selected from at least one of phenoxyethanol, DMDM hydantoin, and sodium benzoate.

Optionally, the pH adjusting agent is selected from citric acid.

Optionally, the solvent is selected from water.

The invention also provides a preparation method of the shampoo, which comprises the following steps:

when preparing shampoo, the formula is divided into A, B1, B2 and C, D phases;

phase A contains the following raw materials: water, polyquaternium-10, hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, ethylene diamine tetraacetic acid disodium, hydrolyzed keratin, schizophyllan and sodium laureth sulfate;

b1 phase: cocamidopropyl betaine, polyquaternium-6, polyquaternium-22;

b2 phase: decyl glucoside, peony seed oil, Indian fruit seed oil, camellia seed oil, polygonum multiflorum extract, astragalus platyphylla extract, sodium pyrrolidone carboxylate, D-panthenol and essence;

and C phase: sodium lauroyl sarcosinate, disodium cocoyl amphodiacetate, PEG-7 glyceryl cocoate, oleyl alcohol, collagen, lanolin, phenoxyethanol, DMDM hydantoin, a suitable amount of citric acid, sodium cocoamidopropionate, a pseudo-ginseng extract, an almond extract, a wheat bran extract, a ginger root extract, and a basil extract;

phase D: and the balance of citric acid.

The preparation method comprises the following steps:

(1) adding the phase A raw material into a container, uniformly stirring, and heating to 75-80 ℃ to obtain a phase A mixture;

(2) cooling the phase A mixture to below 50 ℃, adding the pre-dissolved phase B1 raw material and the pre-dissolved phase B2 raw material into a container, and uniformly stirring;

(3) and (3) adding the C-phase raw material into the feed liquid obtained in the step (2), uniformly stirring, adding the D-phase raw material, and uniformly stirring to obtain the shampoo.

Optionally, in the step (1), the temperature of the feed liquid is increased to 75-80 ℃ within 0.5-2 min.

Optionally, in the step (1), after heating to 75-80 ℃, the temperature is kept for 3-7 min.

Optionally, in the step (3), the viscosity is adjusted to 1000-3000mpa · s.

The invention has the following beneficial effects:

the invention provides a softening composition for a hair washing and protecting product, which consists of an almond extract, a wheat bran extract, a ginger root extract and a basil extract.

Further, the shampoo is developed based on the softening composition, has the effects of refreshing, moisturizing, moistening and nourishing hair, and is strong in moisturizing ability and soft and smooth in hair.

Detailed Description

The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.

Unless otherwise indicated, reagents and materials used in the following examples are commercially available.

The water in the following examples is deionized water.

Example 1

The formulation of this example is shown in Table 1.

TABLE 1

According to weight, in the hair-moistening traditional Chinese medicine composition, an almond extract: wheat bran extract: ginger extract: basil extract 7:6:4: 3.

When preparing shampoo, the formula is divided into A, B1, B2 and C, D phases;

phase A contains the following raw materials: water, polyquaternium-10, hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, ethylene diamine tetraacetic acid disodium, hydrolyzed keratin, schizophyllan and sodium laureth sulfate;

b1 phase: cocamidopropyl betaine, polyquaternium-6, polyquaternium-22;

b2 phase: decyl glucoside, peony seed oil, Indian fruit seed oil, camellia seed oil, polygonum multiflorum extract, astragalus platyphylla extract, sodium pyrrolidone carboxylate, D-panthenol and essence;

and C phase: sodium lauroyl sarcosinate, disodium cocoyl amphodiacetate, PEG-7 glyceryl cocoate, oleyl alcohol, collagen, lanolin, phenoxyethanol, DMDM hydantoin, a suitable amount of citric acid, sodium cocoamidopropionate, a pseudo-ginseng extract, an almond extract, a wheat bran extract, a ginger root extract, and a basil extract;

phase D: and the balance of citric acid.

The preparation process flow is as follows:

1. adding the phase A raw material into an emulsifying container, starting stirring, heating to 75-80 ℃ after 1 minute, stirring until the phase A raw material is completely dissolved, sampling and checking whether particles are absent, and preserving heat for 5 minutes and then cooling.

2. When the temperature of the phase A is reduced to below 50 ℃, adding the pre-dissolved phase B1 and the pre-dissolved phase B2 into an emulsification container, and uniformly stirring at 20-25 rpm.

3. Adding the phase C raw materials in sequence, stirring at 20-30rpm, and dissolving uniformly.

4. Adding the phase D raw material, and adjusting the viscosity to 1000-.

The product prepared in this example is shampoo.

Example 2

In this embodiment, in the hair-moistening traditional Chinese medicine composition, the almond extract: wheat bran extract: ginger extract: basil extract is 1:1:1:1, the other ingredients and the preparation method are the same as example 1.

Example 3

In this embodiment, in the hair-moistening traditional Chinese medicine composition, the almond extract: wheat bran extract: ginger extract: basil extract was 7:10:7:9, other ingredients and preparation method were the same as example 1.

Example 4

In this example, the raw materials are shown in table 2. The preparation method is the same as example 1.

TABLE 2

Example 5

In this example, the raw materials are shown in table 3. The preparation method is the same as example 1.

TABLE 3

Example 6

In this example, the raw materials are shown in table 4. The preparation method is the same as example 1.

TABLE 4

Example 7

In this example, the raw materials are shown in table 5. The preparation method is the same as example 1.

TABLE 5

Example 8

In this example, the raw materials are shown in table 6. The preparation method is the same as example 1.

TABLE 6

Comparative example 1

The formulation and preparation method of the shampoo of the comparative example are basically the same as those of example 1, except that the hair-moistening traditional Chinese medicine composition does not contain almond extract and wheat bran extract.

Comparative example 2

The formulation and preparation method of the shampoo of the comparative example are basically the same as those of example 1, except that the hair-moistening traditional Chinese medicine composition does not contain ginger root extract and basil extract.

Comparative example 3

The formulation and preparation method of the shampoo of this comparative example are substantially the same as example 1, except that the hair-moisturizing traditional Chinese medicine composition is not contained in the softening composition.

Comparative example 4

The formulation and preparation of the shampoo of this comparative example is essentially the same as in example 1, except that the softening composition does not contain hydrolyzed keratin, collagen, D-panthenol.

Comparative example 5

The formulation and preparation of the shampoo of this comparative example is substantially the same as in example 1, except that, by weight, in the softening composition, the almond extract: wheat bran extract: ginger root extract: basil extract 20: 20: 20: 0.5.

comparative example 6

The formulation and preparation of the shampoo of this comparative example is substantially the same as in example 1, except that, by weight, in the softening composition, the almond extract: wheat bran extract: ginger root extract: basil extract 0.5: 0.5: 0.5: 20.

comparative example 7

The formulation and preparation of the shampoo of this comparative example is substantially the same as in example 1, except that, by weight, in the softening composition, the almond extract: wheat bran extract: ginger root extract: basil extract 0.5: 20: 20: 0.5.

and (3) performance testing:

the shampoos prepared in examples 1-8 and comparative examples 1-7 were tested for their effect on hair combing and smoothness performance.

Experimental grouping: the 20-50-year-old population is selected as a test object, the test object is randomly divided into 15 groups, 20 groups are selected, and the groups have no significant difference in age, hair breakage, hair loss, alopecia, thin, soft and thin hair degree and the like and have comparability.

(II) the use method of the shampoo:

after hair is wetted, a proper amount of shampoo is taken to rub out foams, the foams are uniformly smeared on the hair, the finger abdomen is used for drawing a circle for massage, the hair is gently rubbed from the hair root to the hair tip for 5min, and then the hair is washed clean by clear water.

(III) a friction work test method:

treating the hair bundle with a product amount of 0.1ml/g, kneading and foaming for 30s, allowing the foam to stay on the hair bundle for 1min, rinsing with water at 37 deg.C and flow rate of 45 litters/minute for 30s, and pressing the water on the hair every 5 s; the above operation was repeated to perform the second washing. The tresses were then combed with a comb and rinsed under a tap for 1-2 seconds. Subsequently, the hair strands were suspended in a 20. + -. 1 ℃ RH 50. + -. 5% constant temperature and humidity environment, allowed to dry, allowed to equilibrate for 24 hours, and then tested.

1. The test apparatus and materials were as follows:

hair tester, model specification: MTT 175; electronic balance, Yingweigi.

2. The hair tester parameters were set as follows:

Test Mode：Compression；Rate:150mm/min；Displacement:30mm；Cycles:1。

3. testing the hair bundle:

selecting 10 hair bundles, wherein the specification is as follows: asian hair, weight of 2.5g, length of 15cm, virgin hair.

4. The testing process comprises the following steps:

10 tresses of hair were selected and randomly divided into 7 groups of 5 tresses each. The sample set hair strand product was tested for frictional properties after treatment and the comparative example for frictional properties.

5. The test analysis method comprises the following steps:

using the SPSS software analysis, 7 hair tresses (5 tresses per group) were treated with test and control samples and subjected to a hair tress friction test, the test data was subjected to an independent sample t test, the test level α was 0.05, the difference in friction between the test sample and the control sample was analyzed, and the percent difference from the control was calculated.

TABLE 7

As can be seen from table 7, after the hair shampoo in each example has been shampooed, the hair friction work is significantly less than that in each comparative example, comparative examples 1 and 2, the hair-moisturizing traditional Chinese medicine composition is reduced by two components, the hair-moisturizing traditional Chinese medicine composition is not used in comparative example 3, and hydrolyzed keratin, collagen and D-panthenol are not contained in comparative example 4, which all cause significant reduction in the smoothing effect of the hair shampoo, and comparative examples 5 to 7, when the amount of the individual components in the hair-moisturizing traditional Chinese medicine composition is too large, the amount of the other components is too small, which also causes significant reduction in the smoothing effect of the hair shampoo.

The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims (10)

1. A softening composition comprising an almond extract, a wheat bran extract, a ginger root extract, and a basil extract.

2. The softening composition of claim 1, wherein the almond extract: wheat bran extract: ginger root extract: basil extract (1-10): (1-10): (1-10): (1-10), preferably, the almond extract: wheat bran extract: ginger root extract: basil extract (5-10): (5-10): (1-5): (1-5).

3. The softening composition of any one of claims 1-2, further comprising hydrolyzed keratin, collagen, and D-panthenol.

4. Softening composition according to claim 3, characterized in that (almond extract + wheat bran extract + ginger root extract + basil extract) by weight: hydrolysis of keratin: collagen: d-panthenol ═ (0.01 to 0.1): (0.01-0.2): (0.05-0.5): (0.03-0.3).

5. A shampoo comprising the softening composition of any one of claims 1-4.

6. The shampoo of claim 5 further comprising a hair conditioning agent, a foaming agent, and a skin conditioning agent.

7. The shampoo according to claim 6, further comprising a thickener, a chelating agent, a fragrance, an emulsifier, a preservative, a pH adjuster, and a solvent.

8. The shampoo according to claim 7, characterized by comprising the following components by weight: the softening composition of any one of claims 1-4, 0.1-1 part of hair conditioner, 2-3 parts of hair care conditioner, 20-35 parts of foaming agent, 0.5-1.0 part of skin conditioner, 0.05-0.2 part of thickener, 0.05-0.1 part of chelating agent, 0.5-1 part of aromatic, 1-3 parts of emulsifier, 0.2-0.6 part of preservative, 0.1-0.2 part of pH regulator and 50-70 parts of solvent.

9. The shampoo according to claim 8, wherein the hair conditioning agent is at least one selected from polyquaternium-10, polyquaternium-22, polyquaternium-6, schizophyllan, and oleyl alcohol, the foaming agent is at least one selected from sodium fatty alcohol polyoxyethylene ether sulfate, cocamidopropyl betaine, sodium lauroyl sarcosinate, disodium cocoamphodiacetate, decyl glucoside, and sodium cocoamidopropionate, the skin conditioning agent is at least one selected from peony seed oil, crataegus seed oil, camellia seed oil, sodium pyrrolidone carboxylate, lanolin, panax notoginseng extract, polygonum multiflorum extract, and astragalus platyphylla extract, the thickening agent is selected from hydroxypropyl guar hydroxypropyl trimonium chloride, the chelating agent is disodium edetate, the fragrance is selected from essence, the emulsifying agent is PEG-7 glyceryl cocoate oleate, At least one of PPG-5-cetyl polyether-20, glycerol cocoate, cocamide MEA and hydrogenated lecithin, wherein the preservative is selected from at least one of phenoxyethanol, DMDM hydantoin and sodium benzoate, the pH regulator is selected from citric acid, and the solvent is selected from water.

10. The method for preparing the shampoo as claimed in claim 9, wherein the method comprises the following steps:

when preparing shampoo, the formula is divided into A, B1, B2 and C, D phases;

phase A contains the following raw materials: water, polyquaternium-10, hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, ethylene diamine tetraacetic acid disodium, hydrolyzed keratin, schizophyllan and sodium laureth sulfate;

the B1 phase contains the following raw materials: cocamidopropyl betaine, polyquaternium-6, polyquaternium-22;

the B2 phase contains the following raw materials: decyl glucoside, peony seed oil, Indian fruit seed oil, camellia seed oil, polygonum multiflorum extract, astragalus platyphylla extract, sodium pyrrolidone carboxylate, D-panthenol and essence;

phase C contains the following raw materials: sodium lauroyl sarcosinate, disodium cocoyl amphodiacetate, PEG-7 glyceryl cocoate, oleyl alcohol, collagen, lanolin, phenoxyethanol, DMDM hydantoin, a suitable amount of citric acid, sodium cocoamidopropionate, a pseudo-ginseng extract, an almond extract, a wheat bran extract, a ginger root extract, and a basil extract;

phase D contains the following raw materials: the balance of citric acid;

the preparation method comprises the following steps:

(1) adding the phase A raw material into a container, uniformly stirring, and heating to 75-80 ℃ to obtain a phase A mixture;

(2) cooling the phase A mixture to below 50 ℃, adding the pre-dissolved phase B1 raw material and the pre-dissolved phase B2 raw material into a container, and uniformly stirring;

(3) and (3) adding the C-phase raw material into the feed liquid obtained in the step (2), uniformly stirring, adding the D-phase raw material, and uniformly stirring to obtain the shampoo.