CN116135201A - Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof - Google Patents

Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof Download PDF

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Publication number
CN116135201A
CN116135201A CN202310347071.8A CN202310347071A CN116135201A CN 116135201 A CN116135201 A CN 116135201A CN 202310347071 A CN202310347071 A CN 202310347071A CN 116135201 A CN116135201 A CN 116135201A
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hair
washing
product
drying speed
improving
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刘伟
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Guangzhou Meisi Biotechnology Co ltd
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Guangzhou Meisi Biotechnology Co ltd
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Priority to CN202310347071.8A priority Critical patent/CN116135201A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/54Polymers characterized by specific structures/properties
    • A61K2800/542Polymers characterized by specific structures/properties characterized by the charge
    • A61K2800/5426Polymers characterized by specific structures/properties characterized by the charge cationic
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/60Particulates further characterized by their structure or composition
    • A61K2800/61Surface treated
    • A61K2800/614By macromolecular compounds
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention discloses a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials: bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water; according to the invention, by adding the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer and the hydrogenated castor oil/sebacic acid copolymer, and combining the bionic amino acid and the surfactant, the shampoo can adhere the broken hair scales on the hair surface and form a hydrophobic barrier on the hair surface, so that moisture can be blocked by a hydrophobic membrane to stay on the surface during the shampoo, the moisture is prevented from entering the hair core, the drying speed after the shampoo is obviously improved, the adhesion of the hair after the hair is dried can be reduced, and the hair is more fluffy.

Description

Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof
Technical Field
The invention relates to the technical field of daily chemicals, in particular to a washing and caring product for improving the hair drying speed and the fluffiness after washing hair and a preparation method thereof.
Background
With the acceleration of the life rhythm, the great working pressure and the pollution of the living environment, more and more consumers have the problems of excessive secretion of scalp grease, dandruff, scalp sensitivity and the like, so that the efficacy requirements of the consumers on the washing and caring products are gradually increased; especially, women mostly leave long hair, and the hair scales on the surface of the hairline can be damaged due to the fact that the women frequently dye and perming, and grease can be filled into the damaged hair scales, so that the hairline is not easy to clean.
Most of the commercial washing and protecting products at present generally contain silicone oil, and the silicone oil is easy to accumulate after long-time repeated use, so that the problems of sticky hair and the like are caused; meanwhile, although some washing and protecting products without silicone oil are sold on the market, the scalp barrier is damaged due to the fact that the cleaning force is too strong, moisture enters the hair core, the hair drying speed is slow, the hair is sticky and difficult to comb, and therefore the washing and protecting product for improving the hair drying speed and the bulking degree after washing and protecting is provided and a preparation method of the washing and protecting product.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a washing and caring product for improving the hair drying speed and the fluffiness after washing and a preparation method thereof, so as to solve the problems in the prior art.
The invention solves the technical problems by adopting the following technical scheme:
the invention provides a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials:
bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.01-0.5% of bionic amino acid, 0.1-0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 13-25% of surfactant, 0.08-0.15% of hydrogenated castor oil/sebacic acid copolymer, 0.03-0.12% of PCA zinc, 0.05-0.2% of foaming agent, 0.1-0.5% of preservative, 0.5-2.5% of thickener and the balance of deionized water.
Preferably, the washing and caring product for improving the hair drying speed and the bulking degree after washing hair comprises the following raw materials in percentage by weight:
0.25% of bionic amino acid, 0.2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 19% of surfactant, 0.11% of hydrogenated castor oil/sebacic acid copolymer, 0.07% of PCA zinc, 0.12% of foaming agent, 0.3% of preservative, 1.5% of thickener and the balance of deionized water.
Preferably, the bionic amino acid comprises sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1-1.5.
Preferably, the surfactant is one or more of sodium laureth sulfate, cocamidopropyl betaine and cocamide MEA.
Preferably, the foaming agent is sodium cocoyl isethionate.
Preferably, the preservative is one or more of phenoxyethanol, ethylhexyl glycerol and p-hydroxyacetophenone.
Preferably, the thickener is one or more of sodium chloride and laureth-2.
The washing and protecting product is also added with a modified nano silicon dioxide synergistic graphene agent, and the addition amount is 5-10%;
the preparation method of the modified nano-silica synergistic graphene agent comprises the following steps: firstly, putting nano silicon dioxide into a chitosan aqueous solution with the mass fraction of 5% which is 3-5 times that of the nano silicon dioxide, and uniformly stirring;
then adding graphene accounting for 1-5% of the total amount of nano silicon dioxide, silane coupling agent KH560 accounting for 2-5% and sodium oxalate accounting for 1-5%, uniformly stirring, washing with water and drying to obtain a product;
then placing the product into a ball mill for ball milling modification, wherein the ball milling rotating speed is 500-1000r/min, the ball milling time is 20-30min, and the ball grinding agent accounting for 2-5% of the total amount of the product is added in the ball milling; after ball milling, washing and drying to obtain the modified nano-silica synergistic graphene agent;
the ball grinding agent comprises 1-3 parts of cetyl trimethyl ammonium bromide, 2-5 parts of lanthanum sulfate, 1-4 parts of sodium alginate and 10-20 parts of hydrochloric acid solution, wherein the mass fraction of the hydrochloric acid solution is 10-20%.
The invention also provides a preparation method of the washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following steps:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 55-65 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, after the mixed solution B in the step two is cooled to 40-55 ℃, adding a foaming agent, a modified nano silicon dioxide synergistic graphene agent and a preservative, and then starting a stirrer to stir uniformly to obtain a semi-finished product;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.2-7.6, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 30-35 ℃.
Preferably, the temperature is raised during the mixing in the first step, the temperature is raised to 70-80 ℃ at 5-10 ℃/min, the homogenizing time is 5-10min, and the stirring speed of the stirrer in the first to fourth steps is 30-50r/min.
Preferably, the ultrasonic mixing process in the second step is to carry out ultrasonic mixing for 50-80min at the power of 250-350W, and the pH value in the fourth step is adjusted by adding citric acid.
Sarcosine: when used in shampoo, the product is prepared from Quillaja saponaria bark by extracting with hot water or aqueous ethanol, precipitating with diethyl ether or acetone, recrystallizing, and refining.
10-hydroxydecanoic acid: the oil control component 10-hydroxy-decanoic acid contained in the royal jelly is simulated through technical development, the production of grease can be controlled by reducing the number of active sebaceous glands and sebum secretion, and meanwhile, the royal jelly has excellent antibacterial activity.
The acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer has the main functions of antistatic and hair setting agent and film forming agent in cosmetics and skin care products, and through electrostatic adsorption, a small amount of the copolymer is deposited and coated on the surface of hair to promote the bulkiness of hair.
The hydrogenated castor oil/sebacic acid copolymer can condition and deeply repair damaged hair and hair scales, increase hair luster and smoothness, has good compounding property with a surfactant, and has high extraction safety from plants.
PCA zinc: the process of sebum secretion from the sebaceous glands is called seborrhea, and zinc PCA controls the secretion of fats, and zinc PCA is zinc pyrrolidone carboxylate, and shampoo containing the component plays a role in removing dandruff and is obtained by purchase.
Sodium cocoyl isethionate: the natural vegetable oil is derived, can be completely degraded, has better environmental protection, can provide rich and fine foam, and has excellent degreasing capability.
Compared with the prior art, the invention has the following beneficial effects:
according to the invention, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer and hydrogenated castor oil/sebacic acid copolymer are added, bionic amino acid and a surfactant are used together, and the combination of two cationic polymers enables shampoo to adhere to broken hair scales on the hair surface and form a hydrophobic barrier on the hair surface, moisture can be blocked on the surface by a hydrophobic membrane during shampoo, moisture is prevented from entering a hair core, the drying speed after shampoo is obviously improved, adhesion of hair after hair drying can be reduced, hair is enabled to be fluffier, the synergistic effect is achieved by adding the modified nano silicon dioxide to the modified nano silicon dioxide, graphene, silane coupling agent KH560 and sodium oxalate are matched by processing the nano silicon dioxide through chitosan solution, ball milling modification is carried out, and the optimized raw materials can be improved by adding ball grinding agent in ball milling to the optimized raw materials to the synergistic effect with a product system.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The invention provides a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials:
bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.01-0.5% of bionic amino acid, 0.1-0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 13-25% of surfactant, 0.08-0.15% of hydrogenated castor oil/sebacic acid copolymer, 0.03-0.12% of PCA zinc, 0.05-0.2% of foaming agent, 0.1-0.5% of preservative, 0.5-2.5% of thickener and the balance of deionized water.
The washing and caring product for improving the hair drying speed and the fluffiness after washing the hair in the embodiment comprises the following raw materials in percentage by weight:
0.25% of bionic amino acid, 0.2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 19% of surfactant, 0.11% of hydrogenated castor oil/sebacic acid copolymer, 0.07% of PCA zinc, 0.12% of foaming agent, 0.3% of preservative, 1.5% of thickener and the balance of deionized water.
The bionic amino acid of this example includes sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1-1.5.
The surfactant in this embodiment is one or more of sodium laureth sulfate, cocamidopropyl betaine, and cocamide MEA.
The foaming agent of this example is sodium cocoyl isethionate.
The preservative of the embodiment is one or more of phenoxyethanol, ethylhexyl glycerol and p-hydroxyacetophenone.
The thickener of this example is one or more of sodium chloride and laureth-2.
The washing and protecting product is also added with a modified nano silicon dioxide synergistic graphene agent, and the addition amount is 5-10%;
the preparation method of the modified nano-silica synergistic graphene agent comprises the following steps: firstly, putting nano silicon dioxide into a chitosan aqueous solution with the mass fraction of 5% which is 3-5 times that of the nano silicon dioxide, and uniformly stirring;
then adding graphene accounting for 1-5% of the total amount of nano silicon dioxide, silane coupling agent KH560 accounting for 2-5% and sodium oxalate accounting for 1-5%, uniformly stirring, washing with water and drying to obtain a product;
then placing the product into a ball mill for ball milling modification, wherein the ball milling rotating speed is 500-1000r/min, the ball milling time is 20-30min, and the ball grinding agent accounting for 2-5% of the total amount of the product is added in the ball milling; after ball milling, washing and drying to obtain the modified nano-silica synergistic graphene agent;
the ball grinding agent comprises 1-3 parts of cetyl trimethyl ammonium bromide, 2-5 parts of lanthanum sulfate, 1-4 parts of sodium alginate and 10-20 parts of hydrochloric acid solution, wherein the mass fraction of the hydrochloric acid solution is 10-20%.
The preparation method of the washing and caring product for improving the hair drying speed and the fluffiness after washing hair in the embodiment comprises the following steps:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 55-65 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, after the mixed solution B in the step two is cooled to 40-55 ℃, adding a foaming agent, a modified nano silicon dioxide synergistic graphene agent and a preservative, and then starting a stirrer to stir uniformly to obtain a semi-finished product;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.2-7.6, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 30-35 ℃.
In the first step of the embodiment, the temperature is raised during mixing, the temperature is raised to 70-80 ℃ at 5-10 ℃/min, the homogenizing time is 5-10min, and the stirring speed of the stirrer in the first to fourth steps is 30-50r/min.
In the second step of the embodiment, the ultrasonic mixing process is to perform ultrasonic mixing for 50-80min at the power of 250-350W, and in the fourth step, the pH value is adjusted by adding citric acid.
Example 1.
The invention provides a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials:
bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.01% of bionic amino acid, 0.1% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 13% of surfactant, 0.08% of hydrogenated castor oil/sebacic acid copolymer, 0.03% of PCA zinc, 0.05% of foaming agent, 0.1% of preservative, 0.5% of thickener and the balance of deionized water.
The bionic amino acid of this example includes sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1.
the surfactant in this example is sodium laureth sulfate, cocamidopropyl betaine.
The foaming agent of this example is sodium cocoyl isethionate.
The preservative of this example is phenoxyethanol or ethylhexyl glycerol.
The thickener of this example is sodium chloride.
The preparation method of the washing and caring product for improving the hair drying speed and the fluffiness after washing hair in the embodiment comprises the following steps:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 55 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, after the mixed solution B in the step two is cooled to 40 ℃, a foaming agent and a preservative are added, a stirrer is started to stir uniformly, and a semi-finished product is obtained;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.2, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 30 ℃.
In the first embodiment, the temperature is raised during mixing, the temperature is raised to 70 ℃ at 5 ℃/min, the homogenizing time is 5min, and the stirring speed of the stirrer in the first to fourth steps is 30r/min.
In the second step of the present embodiment, the ultrasonic mixing process is to perform ultrasonic mixing for 50min at a power of 250W, and in the fourth step, the PH is adjusted by adding citric acid.
Example 2.
The invention provides a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials:
bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.5% of bionic amino acid, 0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 25% of surfactant, 0.15% of hydrogenated castor oil/sebacic acid copolymer, 0.12% of PCA zinc, 0.2% of foaming agent, 0.5% of preservative, 2.5% of thickener and the balance of deionized water.
The bionic amino acid of this example includes sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1.5.
the surfactant of this example is cocamidopropyl betaine and cocamide MEA.
The foaming agent of this example is sodium cocoyl isethionate.
The preservative of this example is ethylhexyl glycerol, p-hydroxyacetophenone.
The thickener of this example was laureth-2.
The preparation method of the washing and caring product for improving the hair drying speed and the fluffiness after washing hair in the embodiment comprises the following steps:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 65 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, cooling the mixed solution B in the step two to 55 ℃, adding a foaming agent and a preservative, and then starting a stirrer to stir uniformly to obtain a semi-finished product;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.6, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 35 ℃.
In the first step of this example, the temperature is raised by heating to 80℃at 10℃per minute, the homogenization time is 10 minutes, and the stirring speed of the stirrer in the first to fourth steps is 50r/min.
In the second step of the present embodiment, the ultrasonic mixing process is to perform ultrasonic mixing for 80 minutes at a power of 350W, and in the fourth step, the PH is adjusted by adding citric acid.
Example 3.
The invention provides a washing and caring product for improving the hair drying speed and the fluffiness after washing hair, which comprises the following raw materials:
bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.25% of bionic amino acid, 0.2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 19% of surfactant, 0.11% of hydrogenated castor oil/sebacic acid copolymer, 0.07% of PCA zinc, 0.12% of foaming agent, 0.3% of preservative, 1.5% of thickener and the balance of deionized water.
The bionic amino acid of this example includes sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1.3.
the surfactant in this example is sodium laureth sulfate, cocoamide MEA.
The foaming agent of this example is sodium cocoyl isethionate.
The preservative of this example is phenoxyethanol and p-hydroxyacetophenone.
The thickeners of this example are sodium chloride and laureth-2.
The preparation method of the washing and caring product for improving the hair drying speed and the fluffiness after washing hair in the embodiment comprises the following steps:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 60 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, after the mixed solution B in the step two is cooled to 50 ℃, a foaming agent and a preservative are added, a stirrer is started to stir uniformly, and a semi-finished product is obtained;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.4, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 32 ℃.
In the first step of this example, the temperature is raised during mixing, the temperature is raised to 75 ℃ at 7.5 ℃/min, the homogenization time is 8min, and the stirring speed of the stirrer in the first to fourth steps is 40r/min.
In the second step of the present embodiment, the ultrasonic mixing process is to perform ultrasonic mixing for 65min with a power of 300W, and in the fourth step, the PH is adjusted by adding citric acid.
Comparative example 1.
The difference from example 3 is that no acrylamide propyltrimethylammonium chloride/acrylamide copolymer is added.
Comparative example 2.
The difference from example 3 is that no hydrogenated castor oil/sebacic acid copolymer is added.
Comparative example 3.
Unlike example 3, no biomimetic amino acid was added.
Performance testing was performed on shampoos made from the products of examples 1-3 and comparative examples 1-3;
1. tester condition
60 female testers were selected, with an age distribution of 25-45 years, wherein the testers were non-gestational, non-lactating, non-menstrual beginner and non-menopausal.
2. Test method
Wherein 60 testers are randomly divided into 6 groups of 10 testers, and shampoo prepared in examples 1-3 and comparative examples 1-3 is sequentially used in the A/B/C/D/E/F test group, and when the shampoo is used, the shampoo is used for washing hair once every two days and 30 days; the tester scores the samples according to his own use experience. The scoring criteria used a 10 point scale, with higher scores representing better results. Finally, the average value was calculated for each shampoo score, and the results are shown in the following table.
Figure SMS_1
As can be seen from examples 1-3; the shampoo prepared by the invention has better oil control effect and dryness after being used, simultaneously prevents excessive sebum from being generated, keeps hair fluffy and improves hair comb property.
As can be seen from comparative example 1 and example 3, the effect evaluation after the use of the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer is obviously inferior to that of example 3, the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer has the advantages of setting after the hair washing, resisting static electricity, avoiding the disheveled hair after the hair is dried and improving the combing property of the hair;
furthermore, it was found from comparative examples 2 to 3 that the shampoo to which the hydrogenated castor oil/sebacic acid copolymer and the biomimetic amino acid were not added had an effect slightly better than that of comparative example 2, but the effects of both were significantly inferior to that of the present invention, as seen from the evaluation of the tester after 30 use.
The innovation point of the invention is that:
according to the invention, by adding the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer and the hydrogenated castor oil/sebacic acid copolymer, and combining the bionic amino acid and the surfactant, the shampoo can adhere the broken hair scales on the hair surface and form a hydrophobic barrier on the hair surface, so that moisture can be blocked by a hydrophobic membrane to stay on the surface during the shampoo, the moisture is prevented from entering the hair core, the drying speed after the shampoo is obviously improved, the adhesion of the hair after the hair is dried can be reduced, and the hair is more fluffy.
Optimized embodiment
The addition amount of the modified nano silicon dioxide synergistic graphene agent is 7%;
the preparation method of the modified nano-silica synergistic graphene agent comprises the following steps: firstly, putting nano silicon dioxide into a chitosan aqueous solution with the mass fraction of 5% which is 4 times of that of the nano silicon dioxide, and uniformly stirring;
then adding graphene accounting for 4 percent of the total amount of nano silicon dioxide, 4.5 percent of silane coupling agent KH560 and 3 percent of sodium oxalate, uniformly stirring, washing with water and drying to obtain a product;
putting the product into a ball mill for ball milling modification, wherein the ball milling rotating speed is 750r/min, the ball milling time is 25min, and a ball milling agent accounting for 3.5% of the total amount of the product is added into the ball mill; after ball milling, washing and drying to obtain the modified nano-silica synergistic graphene agent;
the ball grinding agent comprises 2 parts of cetyl trimethyl ammonium bromide, 3.5 parts of lanthanum sulfate, 2 parts of sodium alginate and 15 parts of hydrochloric acid solution, wherein the mass fraction of the hydrochloric acid solution is 15%.
Figure SMS_2
After testing, the performance of the product was further improved and optimized relative to the examples.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Equivalent similar components may be substituted by those skilled in the art based on the teachings of this invention, but such substituted components are still within the scope of this invention.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.

Claims (10)

1. A washing and caring product for improving the hair drying speed and the fluffiness after washing hair is characterized by comprising the following raw materials: bionic amino acid, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant, hydrogenated castor oil/sebacic acid copolymer, PCA zinc, foaming agent, preservative, thickener and deionized water;
the specific formula comprises the following raw materials in percentage by weight: 0.01-0.5% of bionic amino acid, 0.1-0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 13-25% of surfactant, 0.08-0.15% of hydrogenated castor oil/sebacic acid copolymer, 0.03-0.12% of PCA zinc, 0.05-0.2% of foaming agent, 0.1-0.5% of preservative, 0.5-2.5% of thickener and the balance of deionized water.
2. A hair care product for improving the post-shampoo hair drying speed and the bulk according to claim 1, which is characterized by comprising the following raw materials in percentage by weight:
0.25% of bionic amino acid, 0.2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 19% of surfactant, 0.11% of hydrogenated castor oil/sebacic acid copolymer, 0.07% of PCA zinc, 0.12% of foaming agent, 0.3% of preservative, 1.5% of thickener and the balance of deionized water.
3. The washing and caring product for improving the drying speed and the bulk after washing hair according to claim 1, wherein the bionic amino acid comprises sarcosine and 10-hydroxydecanoic acid, and the mass ratio of the sarcosine to the 10-hydroxydecanoic acid is 1:1-1.5.
4. A hair care product for improving post-shampoo hair drying speed and bulk according to claim 1 wherein said surfactant is one or more of sodium laureth sulfate, cocamidopropyl betaine, cocamide MEA.
5. A hair care product for improving post-shampoo hair drying speed and bulk according to claim 1 wherein said foaming agent is sodium cocoyl isethionate.
6. The washing and caring product for improving the hair drying speed and the bulk after washing hair according to claim 1, wherein the preservative is one or more of phenoxyethanol, ethylhexyl glycerol and p-hydroxyacetophenone; the thickener is one or more of sodium chloride and laureth-2.
7. The washing and caring product for improving the hair drying speed and the bulk after washing hair according to claim 1, wherein the washing and caring product is further added with a modified nano-silica synergistic graphene agent, and the addition amount is 5-10%;
the preparation method of the modified nano-silica synergistic graphene agent comprises the following steps: firstly, putting nano silicon dioxide into a chitosan aqueous solution with the mass fraction of 5% which is 3-5 times that of the nano silicon dioxide, and uniformly stirring;
then adding graphene accounting for 1-5% of the total amount of nano silicon dioxide, silane coupling agent KH560 accounting for 2-5% and sodium oxalate accounting for 1-5%, uniformly stirring, washing with water and drying to obtain a product;
then placing the product into a ball mill for ball milling modification, wherein the ball milling rotating speed is 500-1000r/min, the ball milling time is 20-30min, and the ball grinding agent accounting for 2-5% of the total amount of the product is added in the ball milling; after ball milling, washing and drying to obtain the modified nano-silica synergistic graphene agent;
the ball grinding agent comprises 1-3 parts of cetyl trimethyl ammonium bromide, 2-5 parts of lanthanum sulfate, 1-4 parts of sodium alginate and 10-20 parts of hydrochloric acid solution, wherein the mass fraction of the hydrochloric acid solution is 10-20%.
8. A method of preparing a hair care product for enhancing post-shampoo hair drying speed and bulk according to any one of claims 1 to 7, comprising the steps of:
firstly, mixing acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, surfactant and hydrogenated castor oil/sebacic acid copolymer with deionized water, homogenizing, and starting a stirrer to stir until the mixture is completely dissolved to obtain a mixed solution A;
step two, cooling the mixed solution A in the step one to 55-65 ℃, adding the bionic amino acid, PCA zinc and a thickening agent, stirring by a stirrer, and simultaneously carrying out ultrasonic mixing to obtain a mixed solution B;
step three, after the mixed solution B in the step two is cooled to 40-55 ℃, adding a foaming agent, a modified nano silicon dioxide synergistic graphene agent and a preservative, and then starting a stirrer to stir uniformly to obtain a semi-finished product;
and fourthly, regulating the pH value of the semi-finished product in the third step to 7.2-7.6, continuously stirring uniformly by a stirrer, and discharging after the temperature of the semi-finished product is reduced to 30-35 ℃.
9. The method for preparing a washing and caring product for improving the post-shampoo hair drying speed and the bulk according to claim 8, wherein the temperature is raised during the mixing in the first step, the temperature is raised to 70-80 ℃ at 5-10 ℃/min, the homogenizing time is 5-10min, and the stirring speed of the stirrer in the first to fourth steps is 30-50r/min.
10. The method for preparing a washing and caring product for improving the hair drying speed and the bulk after washing hair according to claim 8, wherein the ultrasonic mixing process in the second step is to carry out ultrasonic mixing for 50-80min at the power of 250-350W, and the pH value in the fourth step is adjusted by adding citric acid.
CN202310347071.8A 2023-04-04 2023-04-04 Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof Pending CN116135201A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116449029A (en) * 2023-06-15 2023-07-18 广州市丰华生物股份有限公司 Kit for quantitatively detecting inhibin A and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114432168A (en) * 2022-03-13 2022-05-06 浙江浩迈科技有限公司 Formula and preparation method of oil-control fluffy liquid
CN115068401A (en) * 2022-06-30 2022-09-20 广州美思生物技术有限公司 Long-acting oil-control plump and fluffy bionic amino acid shampoo and preparation method thereof
CN115160877A (en) * 2022-08-11 2022-10-11 君子兰涂料(天津)有限公司 UV (ultraviolet) film-coated finish paint and preparation method thereof
CN115645306A (en) * 2022-11-15 2023-01-31 广州美思生物技术有限公司 Hair care product for enlarging, softening, fluffing and improving glossiness of hair and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114432168A (en) * 2022-03-13 2022-05-06 浙江浩迈科技有限公司 Formula and preparation method of oil-control fluffy liquid
CN115068401A (en) * 2022-06-30 2022-09-20 广州美思生物技术有限公司 Long-acting oil-control plump and fluffy bionic amino acid shampoo and preparation method thereof
CN115160877A (en) * 2022-08-11 2022-10-11 君子兰涂料(天津)有限公司 UV (ultraviolet) film-coated finish paint and preparation method thereof
CN115645306A (en) * 2022-11-15 2023-01-31 广州美思生物技术有限公司 Hair care product for enlarging, softening, fluffing and improving glossiness of hair and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
亚什兰: "让受损发丝重获新生的奥秘", pages 2, Retrieved from the Internet <URL:《https://www.sohu.com/a/156132943_722795》> *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116449029A (en) * 2023-06-15 2023-07-18 广州市丰华生物股份有限公司 Kit for quantitatively detecting inhibin A and preparation method thereof
CN116449029B (en) * 2023-06-15 2023-09-01 广州市丰华生物股份有限公司 Kit for quantitatively detecting inhibin A and preparation method thereof

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